The tribological behaviors of carbon block sliding against copper ring with and without electric current applied were investigated by using an advanced multifunctional friction and wear tester, and the electric-arc be...The tribological behaviors of carbon block sliding against copper ring with and without electric current applied were investigated by using an advanced multifunctional friction and wear tester, and the electric-arc behaviors were analyzed in detail. The results show that the normal load is one of the main controlling factors for generation of electric arc during friction process with electric current applied. The strength of electric arc is enhanced with the decrease of normal loads and the increase of electric currents. The unstable friction process and the fluctuated dynamic friction coefficients are strongly dependent upon the electric arc. The wear volumes and the wear mechanism of carbon brush were affected by the electric arc obviously. As no electric arc occurs, no clear discrepancy of the wear volumes of the carbon samples with and without electric current applied could be detected. While the wear mechanisms are mainly mechanical wear. However, under the condition of the electric arc appearance, the wear volume of carbon with electric current applied increases much more rapidly than that without electric current applied and also increases obviously with the increase of electric current strengths and the decrease of normal loads. The wear mechanisms of carbon block are mainly electric arc ablation accompanying with adhesive wear and material transferring.展开更多
Multi-pass friction stir processing(M-FSP)was performed to repair the interface defects of AA5083/T2 copper explosive composite plates.The interface morphology and its bonding mechanism were explored.The results show ...Multi-pass friction stir processing(M-FSP)was performed to repair the interface defects of AA5083/T2 copper explosive composite plates.The interface morphology and its bonding mechanism were explored.The results show that higher rotation speed and lower transverse speed produce more heat generated during FSP.The defect-free and good mechanical properties of the AA5083/T2 copper composite plate can be obtained under the condition of the rotation speed of 1200 r/min,the transverse speed of 30 mm/min and the overlap of 2/24.Moreover,M-FSP changes the interface bonding mechanism from metallurgical bonding to vortex connection,improving the bonding strength of composite plate,which can guarantee the repairing quality of composite plates.展开更多
In this study,AA 1050 aluminum alloy and commercially pure copper in annealed and severely plastic deformed conditions were used.The technique used for imposing the severe strain to the sheets was constrained groove p...In this study,AA 1050 aluminum alloy and commercially pure copper in annealed and severely plastic deformed conditions were used.The technique used for imposing the severe strain to the sheets was constrained groove pressing（CGP） process.The annealed and severely plastic deformed sheets were subjected to friction stir welding（FSW） at different rotation and traverse speeds.Cu was placed in advancing side.Constant offset of approximately 1 mm was used toward Al side for all welds.A range of welding parameters which can lead to acceptable welds with appropriate mechanical properties was found.For the FSWed CGPed samples,it was observed that the welding heat input caused grain growth and decrease in hardness value at Al side of the stir zone.It was found that,generally the weakest parts of weld joints of annealed and CGPed samples were Al base metal and stir zone,respectively.Further investigations showed that several forms of intermetallic compounds were produced.展开更多
The basic principle of friction welding is intermetallic bonding at the stage of super plasticity attained with self-generating heat due to friction and finishing at upset pressure. Now the dissimilar metal joints are...The basic principle of friction welding is intermetallic bonding at the stage of super plasticity attained with self-generating heat due to friction and finishing at upset pressure. Now the dissimilar metal joints are especially popular in defense, aerospace, automobile, bio-medical,refinery and nuclear engineerings. In friction welding, some special alloys with dual phase are not joined successfully due to poor bonding strength. The alloy surfaces after bonding also have metallurgical changes in the line of interfacing. The reported research work in this area is scanty. Although the sound weld zone of direct bonding between Tie6Ale4 V and SS304 L was obtained though many trials, the joint was not successful. In this paper, the friction welding characteristics between Tie6Ale4 V and SS304 L into which pure oxygen free copper(OFC) was introduced as interlayer were investigated. Boxe Behnken design was used to minimize the number of experiments to be performed. The weld joint was analyzed for its mechanical strength. The highest tensile strength between Tie6Ale4 V and SS304 L between which pure copper was used as insert metal was acquired. Micro-structural analysis and elemental analysis were carried out by EDS, and the formation of intermetallic compound at the interface was identified by XRD analysis.展开更多
By employing a quasi in situ method, we investigated the dynamic evolution of the grain structure con-sidering the material flow, strain, and strain rate in the friction stir welding of pure copper. The tool' stop...By employing a quasi in situ method, we investigated the dynamic evolution of the grain structure con-sidering the material flow, strain, and strain rate in the friction stir welding of pure copper. The tool' stop action' and rapid cooling were employed and a brass foil was used as a marker to show the material flow path. The grain structure along the material flow path was characterised using electron backscatter diffraction. Static recrystallization occurs for the work-hardened base material in the preheating stage in front of the tool In the acceleration flow stage, grains are significantly refined by plastic deforma-tion, discontinuous dynamic recrystallization, annealing twinning during the strain-induced boundary migration and slight continuous dynamic recrystallization. In the deceleration flow stage, due to a strain reversal, the grain first coarsens, and is thereafter refined again. Finally, the hot-deformed material in the shoulder-affected zone is ‘frozen’ directly whereas that in the probe-affected zone undergoes signif-icant annealing;thus, the recrystallized microstructure and 45°-rotated cube texture are obtained in the probe-affected zone.展开更多
Dissimilar joints comprised of copper–nickel and steel alloys are a challenge for manufacturers in modern industries, as these metals are not thermomechanically or chemically well matched. The present study investiga...Dissimilar joints comprised of copper–nickel and steel alloys are a challenge for manufacturers in modern industries, as these metals are not thermomechanically or chemically well matched. The present study investigated the effects of tool rotational speed and linear speed on the microstructure and mechanical properties of friction stir-welded C71000 copper–nickel and 340 stainless steel alloys using a tungsten carbide tool with a cylindrical pin. The results indicated that a rotational-to-linear speed ratio of 12.5 r/mm did not cause any macro defects, whereas some tunneling defects and longitudinal cracks were found at other ratios that were lower and higher. Furthermore, chromium carbide was formed on the grain boundaries of the 304 stainless steel near the shoulder zone and inside the joint zone, directing carbon and chromium penetration toward the grain boundaries. Tensile strength and elongation percentages were 84% and 65% of the corresponding values in the copper–nickel base metal, respectively.展开更多
Components made by joining different materials are required in various engineering applications.Fabrication of suchcomponents is a challenging task due to the vast difference in mechanical,thermal and electrical prope...Components made by joining different materials are required in various engineering applications.Fabrication of suchcomponents is a challenging task due to the vast difference in mechanical,thermal and electrical properties of the materials beingused.Friction stir welding(FSW)is capable of joining dissimilar materials such as aluminum(Al)and copper(Cu)and thereforeresearchers have used this novel process for dissimilar joining.Consequently,several works pertaining to dissimilar joining,specifically Al?Cu,are available in the literature but they are scattered in different sources,which makes the task of gatheringinformation about dissimilar FSW of Al?Cu cumbersome.This work has been written with an aim to provide all pertinentinformation related to dissimilar FSW of Al?Cu at one place to ease the problems of researchers.It comprehensively covers andsummarizes the topics such as the effect of tool design and geometry,FSW process parameters,FSW strategies on mechanicalproperties,microstructure and formation of defects during dissimilar FSW of Al?Cu.In addition,it also presents and discussesseveral variants of dissimilar FSW of Al?Cu.Finally,this work not only puts forth major findings of the previous researchers but alsosuggests future recommendations for dissimilar FSW of Al?Cu.展开更多
This paper mainly concentrated on the feasibility of friction stir welding of dissimilar metal of aluminum alloy to copper （I2） and a preliminary analysis of welding parameters influencing on the microstructures and...This paper mainly concentrated on the feasibility of friction stir welding of dissimilar metal of aluminum alloy to copper （I2） and a preliminary analysis of welding parameters influencing on the microstructures and properties of joint was carried out. The results indicated that the thickness of workpiece played an important role in the welding parameters which could succeed in the friction stir welding of dissimilar metal of copper to aluminum alloy, and the parameters were proved to be a narrow choice. The interfacial region between copper and aluminum in the dissimilar joint was not uniformly mixed, constituted with part of incomplete mixing zone, complete mixing zone, dispersion zone and the most region＇ s boundary was obvious. Meantime a kind banded structure with inhomogeneous width was formed. The intermetallic compounds generated during friction stir welding in the interfacial region were mainly CugAl4, Al2Cu etc, and their hardness was higher than oihers.展开更多
In this study, the dissimilar friction stir welding （FSW） butt joints between aluminum alloy 5754-H114 and commerciallypure copper were investigated. The thickness of welded plates was 4 mm and the aluminum plate wa...In this study, the dissimilar friction stir welding （FSW） butt joints between aluminum alloy 5754-H114 and commerciallypure copper were investigated. The thickness of welded plates was 4 mm and the aluminum plate was placed on theadvancing side. In order to obtain a suitable flow and a better material mixing, a 1-mm offset was considered for thealuminum plate, toward the butt centerline. For investigating the microstructure and mechanical properties of FSWedjoints, optical microscopy and mechanical tests （i.e., uniaxial tensile test and microhardness） were used, respectively.Furthermore, the analysis of intermetallic compounds and fracture surface was examined by scanning electron microscopyand X-ray diffraction. The effect of heat generation on the mechanical properties and microstructure of the FSWed jointswas investigated. The results showed that there is an optimum amount of heat input. The intermetallic compounds formedin FSWed joints were A14Cu9 and AI2Cu. The best results were found in joints with 1000 rpm rotational speed and100 mm/min travel speed. The tensile strength was found as 219 MPa, which reached 84% of the aluminum base strength.Moreover, maximum value of the microhardness of the stir zone （SZ） was attained as about 120 HV, which was greatlydepended on the grain size, intermetallic compounds and copper pieces in SZ.展开更多
Carbon nanotubes （CNTs） were coated by tungsten layer using metal organic chemical vapor deposition process with tungsten hexacarbonyl as a precursor. The W-coated CNTs （W-CNTs） were dispersed into Cu powders by m...Carbon nanotubes （CNTs） were coated by tungsten layer using metal organic chemical vapor deposition process with tungsten hexacarbonyl as a precursor. The W-coated CNTs （W-CNTs） were dispersed into Cu powders by magnetic stirring process and then the mixed powders were consolidated by spark plasma sintering to fabricate W-CNTs/Cu composites. The CNTs/Cu composites were fabricated using the similafprocesses. The friction coefficient and mass wear loss of W-CNTs/Cu and CNTs/Cu composites were studied. The results showed that the W-CNT content, interfacial bonding situation, and applied load could influence the friction coefficient and wear loss of W-CNTs/Cu com- posites. When the W-CNT content was 1.0 wt.%, the W-CNTs/Cu composites got the minimum friction coefficient and wear loss, which were decreased by 72.1% and 47.6%, respectively, compared with pure Cu specimen. The friction coefficient and wear loss of W-CNTs/Cu composites were lower than those of CNTs/Cu composites, which was due to that the interracial bonding at （W-CNTs）-Cu interface was better than that at CNTs-Cu interface. The friction coefficient of composites did not vary obviously with increasing applied load, while the wear loss of composites increased significantly with the increase of applied load.展开更多
Friction stir spot welding technique was employed to join pure copper （C11000） and pure aluminium （AA1060） sheets. The evolving properties of the welds produced were characterized. The spot welds were produced by ...Friction stir spot welding technique was employed to join pure copper （C11000） and pure aluminium （AA1060） sheets. The evolving properties of the welds produced were characterized. The spot welds were produced by varying the rotational speed, shoulder plunge depth using different tool geometries. The presence of a copper ring of different lengths was observed on both sides of the welds indicating that Cu extruded upward into the Al sheet which contributed to obtaining strong welds. The microstructure showed the presence of copper particles in the aluminium matrix which led to the presence of various intermetallics observed by the energy dispersive spectroscopy and X-ray diffraction. The maximum tensile failure load increases with an increase in the shoulder plunge depth, except for the weld produced at 800 r/min using a conical pin and a concave shoulder. A nugget pull-out failure mode occurred in all the friction stir spot welds under the lap-shear loading conditions. High peaks of Vickers microhardness values were obtained in the vicinity of the keyhole of most of the samples which correlated to the presence of intermetallics in the stir zone of the welds.展开更多
Underwater friction stir processing was performed on commercially pure copper with a purity of 99.8% and a copper-zinc alloy(brass). The tool was made of tungsten carbide in the threaded cone form. Friction stir proce...Underwater friction stir processing was performed on commercially pure copper with a purity of 99.8% and a copper-zinc alloy(brass). The tool was made of tungsten carbide in the threaded cone form. Friction stir processing was performed at a tool rotational speed of 1800 r/min and a tool transverse speed of 4 mm/min while the samples were immersed in a water tank with a water circulation system. In order to evaluate the effect of the number of process passes on the microstructure and mechanical properties of the samples, this process was continued for up to 6 passes. Microscopic studies using light microscopy on commercially pure copper samples show significant decrease in grain size. Likewise, the hardness of the cross-sectional area shows an increase more than the base metal. The X-ray diffraction pattern of the underwater friction stir processed samples in comparison to that of the base metal exhibits shorter and wider peaks, while the background of the pattern is increased. The sum of these factors represents the formation of an amorphous/ultrafine grained structure. Also, the wear behavior of the samples was investigated by means of pin-on-disk method and the results show that the friction coefficient of processed samples is decreased compared to that of the base metal. The results of wear and hardness tests show that the underwater friction stir processing can significantly improve the wear resistance and hardness of commercially pure copper and brass.展开更多
The influence of friction stir welding processing parameters on dissimilar joints conducted between aluminium alloy （AA5754） and commercially pure copper （C11000） was studied. The welds were produced by varying th...The influence of friction stir welding processing parameters on dissimilar joints conducted between aluminium alloy （AA5754） and commercially pure copper （C11000） was studied. The welds were produced by varying the rotational speed from 600 to 1200 r/min and the feed rate from 50 to 300 mm/min. The resulting microstructure and the corrosion properties of the welds produced were studied. It was found that the joint interfacial regions of the welds were characterized by interlayers of aluminium and copper. The corrosion tests revealed that the corrosion resistance of the welds was improved as the rotational speed was increased. The corrosion rates of the welds compared to the base metals were improved compared with Cu and decreased slightly compared with the aluminium alloy. The lowest corrosion rate was obtained at welds produced at rotational speed of 950 r/min and feed rate of 300 mm/min which corresponds to a weld produced at a low heat input.展开更多
An attempt was made to optimize friction welding parameters to attain a minimum hardness at the interface and a maximum tensile strength of the dissimilar joints of AISI 304 austenitic stainless steel （ASS） and copp...An attempt was made to optimize friction welding parameters to attain a minimum hardness at the interface and a maximum tensile strength of the dissimilar joints of AISI 304 austenitic stainless steel （ASS） and copper （Cu） alloy using response surface methodology （RSM）. Three-factor, five-level central composite design matrix was used to specify experimental conditions. Twenty joints were fabricated using ASS and Cu alloy. Tensile strength and interface hardness were measured experimentally. Analysis of variance （ANOVA） method was used to find out significant main and interaction parameters and empirical relationships were developed using regression analysis. The friction welding parameters were optimized by constructing response graphs and contour plots using design expert software. The developed empirical relationships can be effectively used to predict tensile strength and interface hardness of friction welded ASS-Cu joints at 95% confidence level. The developed contour plots can be used to attain required level of optimum conditions to join ASS-Cu alloy by friction welding process.展开更多
In this work,the influence of the Zener-Hollomon(Z)parameter on the microstructure and mechanical properties of copper subjected to friction stir welding(FSW)was investigated.Liquid N2 cooling was conducted to control...In this work,the influence of the Zener-Hollomon(Z)parameter on the microstructure and mechanical properties of copper subjected to friction stir welding(FSW)was investigated.Liquid N2 cooling was conducted to control the cooling rate after the FSW.The obtained results demonstrate that the Z parameter was dependent on the tool rotation rate during the FSW,i.e.,a higher tool rotating rate resulted in a lower Z parameter.The grain size in the stir zone decreased with the increase in the Z parameter.The relationship between the yield strength and the Z parameter is established asσ0.2=σ0+kZn.This relationship exhibited two different plots under the conditions of air cooling and liquid N2 cooling.Even at a similar Z parameter,a significant yield strength difference occurred because massive dislocations,which were caused by the prevention of the post-annealing effect,were maintained in the stir zone.This study suggests that the influence of the post-annealing effect should not be neglected when analyzing the relationship between the Z parameter,micro structure,and mechanical properties.展开更多
The current investigation of refill friction stir spot welding(refill FSSW)Al alloy to copper primarily involved plunging the tool into bottom copper sheet to achieve both metallurgical and mechanical interfacial bond...The current investigation of refill friction stir spot welding(refill FSSW)Al alloy to copper primarily involved plunging the tool into bottom copper sheet to achieve both metallurgical and mechanical interfacial bonding.Compared to conventional FSSW and pinless FSSW,weld strength can be significantly improved by using this method.Nevertheless,tool wear is a critical issue during refill FSSW.In this study,defect-free Al/copper dissimilar welds were successfully fabricated using refill FSSW by only plunging the tool into top Al alloy sheet.Overall,two types of continuous and ultra-thin intermetallic compounds(IMCs)layers were identified at the whole Al/copper interface.Also,strong evidence of melting and resolidification was observed in the localized region.The peak temperature obtained at the center of Al/copper interface was 591℃,and the heating rate reached up to 916℃/s during the sleeve penetration phase.A softened weld region was produced via refill FSSW process,the hardness profile exhibited a W-shaped appearance along middle thickness of top Al alloy.The weld lap shear load was insensitive to the welding condition,whose scatter was rather small.The fracture path exclusively propagated along the IMCs layer of Cu_(9)Al_(4) under the external lap shear loadings,both CuAl_(2) and Cu_(9)Al_(4) were detected on the fractured surface on the copper side.This research indicated that acceptable weld strength can be achieved via pure metallurgical joining mechanism,which has significant potential for the industrial applications.展开更多
Joining of dissimilar aluminium-copper is an emerging area of interest for both research and industry due to its complex nature.Friction stir welding was attempted to evaluate the joint strength without offset at the ...Joining of dissimilar aluminium-copper is an emerging area of interest for both research and industry due to its complex nature.Friction stir welding was attempted to evaluate the joint strength without offset at the butt line between AA6063 to HCP copper sheet under different combination of rotational speed of 800 and 1000 r/min and travel speed of 20 and 40 mm/min.Material flow was studied in detail for different combinations of parameters with optical microscopy and elemental mapping by energy dispersive X-ray spectroscopy（EDS）.The results were correlated with the microstructural characteristics and formation of intermetallics at the bond interface using microhardness test and X-ray diffraction（XRD） technique.Material flow clearly suggests that energy input at 800 r/min and 20 mm/min is sufficient to plasticize both the materials with formation of higher amount of thermodynamically stable and hard intermetallic phases Al4Cu9 and Al Cu4（slower cooling rate of 88 K/s） than that at 800 r/min and 40 mm/min（faster cooling rate of 154 K/s）,attributed maximum joint strength（~78.6% of aluminium base metal）.展开更多
This study was done to evaluate the nugget zone(NZ)corrosion behavior of dissimilar copper/brass joints welded by friction stir lap welding(FSLW)in a solution of 0.015 mol/L borax(pH 9.3).To this end,dissimilar copper...This study was done to evaluate the nugget zone(NZ)corrosion behavior of dissimilar copper/brass joints welded by friction stir lap welding(FSLW)in a solution of 0.015 mol/L borax(pH 9.3).To this end,dissimilar copper/brass plates were welded with two dissimilar heat inputs(low and high)during the welding procedure.The high and low heat inputs were conducted with 710 r/min,16 mm/min and 450 r/min,25 mm/min,respectively.Using open circuit potential(OCP)measurements,electrochemical impedance spectroscopy(EIS)and Tafel polarization tests,the electrochemical behavior of the specimens in borate buffer solution was assessed.With the help of scanning electron microscope(SEM),the morphology of welded specimen surfaces was examined after immersion in the test solution.According to the results,the NZ grain size and resistance improvement reduced due to the nugget zone corrosion with a decreased heat input.The results obtained from Tafel polarization and EIS indicated the improved corrosion behavior of the welded specimen NZ with a decrease in the heat input during the welding process unlike the copper and brass metals.Furthermore,an increased heat input during the welding process shows a reduction in the conditions for forming the passive films with higher protection behavior.展开更多
Copper base alloy was overlaid onto 35CrMnSiA steel plate by tungsten inert gas （TIG） welding method. The heat transfer process was simulated, the microstructures of the copper base overlay were analyzed by scanning...Copper base alloy was overlaid onto 35CrMnSiA steel plate by tungsten inert gas （TIG） welding method. The heat transfer process was simulated, the microstructures of the copper base overlay were analyzed by scanning electron microscopy （SEM） and energy dispersive spectrometer （EDS）, and the friction and abrasion properties of the overlay were measured. The results show that the Fe content increases in the overlay with increasing the welding current. And with the increase of Fe content in the overlay, the friction coefficient increases and the wear mechanism changes from oxidation wear to abrasive wear and plough wear, which is related to the size and quantity of Fe grains in the overlay. While with the increase of Fe content in the overlay, the protection of oxidation layer against the oxidation wear on the melted metal decreases.展开更多
Friction stir spot welding technique was used to join dissimilar combinations of aluminium alloy(Al5052)with copperalloy(C27200)and friction stir spot welding windows such as tool rotational speed–dwell time and tool...Friction stir spot welding technique was used to join dissimilar combinations of aluminium alloy(Al5052)with copperalloy(C27200)and friction stir spot welding windows such as tool rotational speed–dwell time and tool rotational speed?plungedepth diagrams for effective joining of these materials were developed.Using a central composite design model,empirical relationswere developed to predict the changes in tensile shear failure load values and interface hardness of the joints with three processparameters such as tool rotational speed,plunge depth and dwell time.The adequacy of the developed model was verified usingANOVA analysis at95%confidence level.Response surface methodology was used to optimize the developed model to maximizetensile strength and minimize interface hardness.A high tensile shear failure load value of3850N and low interface hardness valueof HV81was observed for joints made under optimum conditions,and validation experiments confirmed the high predictability ofthe developed model with error less than2%.The operating windows developed shall act as reference maps for future designengineers in choosing appropriate friction stir spot welding process parameter values to obtain good joints.展开更多
基金Project (2007CB714703) supported by the National Basic Research Program of ChinaProject (50521503) supported by the National Natural Science Foundation of ChinaProject (20050613015) supported by Research Fund for Doctoral Program of Higher Education of China
文摘The tribological behaviors of carbon block sliding against copper ring with and without electric current applied were investigated by using an advanced multifunctional friction and wear tester, and the electric-arc behaviors were analyzed in detail. The results show that the normal load is one of the main controlling factors for generation of electric arc during friction process with electric current applied. The strength of electric arc is enhanced with the decrease of normal loads and the increase of electric currents. The unstable friction process and the fluctuated dynamic friction coefficients are strongly dependent upon the electric arc. The wear volumes and the wear mechanism of carbon brush were affected by the electric arc obviously. As no electric arc occurs, no clear discrepancy of the wear volumes of the carbon samples with and without electric current applied could be detected. While the wear mechanisms are mainly mechanical wear. However, under the condition of the electric arc appearance, the wear volume of carbon with electric current applied increases much more rapidly than that without electric current applied and also increases obviously with the increase of electric current strengths and the decrease of normal loads. The wear mechanisms of carbon block are mainly electric arc ablation accompanying with adhesive wear and material transferring.
基金The authors are grateful for the financial supports from the National Natural Science Foundation of China(No.51505293)the Natural Science Foundation of Jiangsu Province,China(No.BK20190684)+1 种基金the Natural Science Research of the Jiangsu Higher Education Institutions of China(No.18KJB460016)the Key Laboratory of Lightweight Materials,Nanjing Tech University,as well as by a fellowship from the International Postdoctoral Exchange Followship Program(2020096 to Jian WANG).
文摘Multi-pass friction stir processing(M-FSP)was performed to repair the interface defects of AA5083/T2 copper explosive composite plates.The interface morphology and its bonding mechanism were explored.The results show that higher rotation speed and lower transverse speed produce more heat generated during FSP.The defect-free and good mechanical properties of the AA5083/T2 copper composite plate can be obtained under the condition of the rotation speed of 1200 r/min,the transverse speed of 30 mm/min and the overlap of 2/24.Moreover,M-FSP changes the interface bonding mechanism from metallurgical bonding to vortex connection,improving the bonding strength of composite plate,which can guarantee the repairing quality of composite plates.
基金the Research Board of Sharif University of Technology and Tamkar Industrial Company for the financial support
文摘In this study,AA 1050 aluminum alloy and commercially pure copper in annealed and severely plastic deformed conditions were used.The technique used for imposing the severe strain to the sheets was constrained groove pressing（CGP） process.The annealed and severely plastic deformed sheets were subjected to friction stir welding（FSW） at different rotation and traverse speeds.Cu was placed in advancing side.Constant offset of approximately 1 mm was used toward Al side for all welds.A range of welding parameters which can lead to acceptable welds with appropriate mechanical properties was found.For the FSWed CGPed samples,it was observed that the welding heat input caused grain growth and decrease in hardness value at Al side of the stir zone.It was found that,generally the weakest parts of weld joints of annealed and CGPed samples were Al base metal and stir zone,respectively.Further investigations showed that several forms of intermetallic compounds were produced.
文摘The basic principle of friction welding is intermetallic bonding at the stage of super plasticity attained with self-generating heat due to friction and finishing at upset pressure. Now the dissimilar metal joints are especially popular in defense, aerospace, automobile, bio-medical,refinery and nuclear engineerings. In friction welding, some special alloys with dual phase are not joined successfully due to poor bonding strength. The alloy surfaces after bonding also have metallurgical changes in the line of interfacing. The reported research work in this area is scanty. Although the sound weld zone of direct bonding between Tie6Ale4 V and SS304 L was obtained though many trials, the joint was not successful. In this paper, the friction welding characteristics between Tie6Ale4 V and SS304 L into which pure oxygen free copper(OFC) was introduced as interlayer were investigated. Boxe Behnken design was used to minimize the number of experiments to be performed. The weld joint was analyzed for its mechanical strength. The highest tensile strength between Tie6Ale4 V and SS304 L between which pure copper was used as insert metal was acquired. Micro-structural analysis and elemental analysis were carried out by EDS, and the formation of intermetallic compound at the interface was identified by XRD analysis.
基金partly supported by the New Energy and Industrial Technology Development Organization (NEDO) under the “Innovation Structural Materials Project (Future Pioneering Projects)”a Grant-in-Aid for Science Research from the Japan Society for the Promotion of Science
文摘By employing a quasi in situ method, we investigated the dynamic evolution of the grain structure con-sidering the material flow, strain, and strain rate in the friction stir welding of pure copper. The tool' stop action' and rapid cooling were employed and a brass foil was used as a marker to show the material flow path. The grain structure along the material flow path was characterised using electron backscatter diffraction. Static recrystallization occurs for the work-hardened base material in the preheating stage in front of the tool In the acceleration flow stage, grains are significantly refined by plastic deforma-tion, discontinuous dynamic recrystallization, annealing twinning during the strain-induced boundary migration and slight continuous dynamic recrystallization. In the deceleration flow stage, due to a strain reversal, the grain first coarsens, and is thereafter refined again. Finally, the hot-deformed material in the shoulder-affected zone is ‘frozen’ directly whereas that in the probe-affected zone undergoes signif-icant annealing;thus, the recrystallized microstructure and 45°-rotated cube texture are obtained in the probe-affected zone.
基金the funding support of Babol Noshirvani University of Technology (No. BNUT/370167/97)
文摘Dissimilar joints comprised of copper–nickel and steel alloys are a challenge for manufacturers in modern industries, as these metals are not thermomechanically or chemically well matched. The present study investigated the effects of tool rotational speed and linear speed on the microstructure and mechanical properties of friction stir-welded C71000 copper–nickel and 340 stainless steel alloys using a tungsten carbide tool with a cylindrical pin. The results indicated that a rotational-to-linear speed ratio of 12.5 r/mm did not cause any macro defects, whereas some tunneling defects and longitudinal cracks were found at other ratios that were lower and higher. Furthermore, chromium carbide was formed on the grain boundaries of the 304 stainless steel near the shoulder zone and inside the joint zone, directing carbon and chromium penetration toward the grain boundaries. Tensile strength and elongation percentages were 84% and 65% of the corresponding values in the copper–nickel base metal, respectively.
文摘Components made by joining different materials are required in various engineering applications.Fabrication of suchcomponents is a challenging task due to the vast difference in mechanical,thermal and electrical properties of the materials beingused.Friction stir welding(FSW)is capable of joining dissimilar materials such as aluminum(Al)and copper(Cu)and thereforeresearchers have used this novel process for dissimilar joining.Consequently,several works pertaining to dissimilar joining,specifically Al?Cu,are available in the literature but they are scattered in different sources,which makes the task of gatheringinformation about dissimilar FSW of Al?Cu cumbersome.This work has been written with an aim to provide all pertinentinformation related to dissimilar FSW of Al?Cu at one place to ease the problems of researchers.It comprehensively covers andsummarizes the topics such as the effect of tool design and geometry,FSW process parameters,FSW strategies on mechanicalproperties,microstructure and formation of defects during dissimilar FSW of Al?Cu.In addition,it also presents and discussesseveral variants of dissimilar FSW of Al?Cu.Finally,this work not only puts forth major findings of the previous researchers but alsosuggests future recommendations for dissimilar FSW of Al?Cu.
基金This project is supported by National Natural Science Foundation of China ( NSFC)(10577010)
文摘This paper mainly concentrated on the feasibility of friction stir welding of dissimilar metal of aluminum alloy to copper （I2） and a preliminary analysis of welding parameters influencing on the microstructures and properties of joint was carried out. The results indicated that the thickness of workpiece played an important role in the welding parameters which could succeed in the friction stir welding of dissimilar metal of copper to aluminum alloy, and the parameters were proved to be a narrow choice. The interfacial region between copper and aluminum in the dissimilar joint was not uniformly mixed, constituted with part of incomplete mixing zone, complete mixing zone, dispersion zone and the most region＇ s boundary was obvious. Meantime a kind banded structure with inhomogeneous width was formed. The intermetallic compounds generated during friction stir welding in the interfacial region were mainly CugAl4, Al2Cu etc, and their hardness was higher than oihers.
文摘In this study, the dissimilar friction stir welding （FSW） butt joints between aluminum alloy 5754-H114 and commerciallypure copper were investigated. The thickness of welded plates was 4 mm and the aluminum plate was placed on theadvancing side. In order to obtain a suitable flow and a better material mixing, a 1-mm offset was considered for thealuminum plate, toward the butt centerline. For investigating the microstructure and mechanical properties of FSWedjoints, optical microscopy and mechanical tests （i.e., uniaxial tensile test and microhardness） were used, respectively.Furthermore, the analysis of intermetallic compounds and fracture surface was examined by scanning electron microscopyand X-ray diffraction. The effect of heat generation on the mechanical properties and microstructure of the FSWed jointswas investigated. The results showed that there is an optimum amount of heat input. The intermetallic compounds formedin FSWed joints were A14Cu9 and AI2Cu. The best results were found in joints with 1000 rpm rotational speed and100 mm/min travel speed. The tensile strength was found as 219 MPa, which reached 84% of the aluminum base strength.Moreover, maximum value of the microhardness of the stir zone （SZ） was attained as about 120 HV, which was greatlydepended on the grain size, intermetallic compounds and copper pieces in SZ.
基金financially supported by the National Natural Science Foundation of China (No.50971020)National HighTech Research and Development Program of China (No.2009AA03Z116)
文摘Carbon nanotubes （CNTs） were coated by tungsten layer using metal organic chemical vapor deposition process with tungsten hexacarbonyl as a precursor. The W-coated CNTs （W-CNTs） were dispersed into Cu powders by magnetic stirring process and then the mixed powders were consolidated by spark plasma sintering to fabricate W-CNTs/Cu composites. The CNTs/Cu composites were fabricated using the similafprocesses. The friction coefficient and mass wear loss of W-CNTs/Cu and CNTs/Cu composites were studied. The results showed that the W-CNT content, interfacial bonding situation, and applied load could influence the friction coefficient and wear loss of W-CNTs/Cu com- posites. When the W-CNT content was 1.0 wt.%, the W-CNTs/Cu composites got the minimum friction coefficient and wear loss, which were decreased by 72.1% and 47.6%, respectively, compared with pure Cu specimen. The friction coefficient and wear loss of W-CNTs/Cu composites were lower than those of CNTs/Cu composites, which was due to that the interracial bonding at （W-CNTs）-Cu interface was better than that at CNTs-Cu interface. The friction coefficient of composites did not vary obviously with increasing applied load, while the wear loss of composites increased significantly with the increase of applied load.
基金financial support of the University of Johannesburg and the assistance from Mr Riaan Brown (Nelson Mandela Metropolitan University) for operating the MTS PDS I-Stir machine are acknowledged
文摘Friction stir spot welding technique was employed to join pure copper （C11000） and pure aluminium （AA1060） sheets. The evolving properties of the welds produced were characterized. The spot welds were produced by varying the rotational speed, shoulder plunge depth using different tool geometries. The presence of a copper ring of different lengths was observed on both sides of the welds indicating that Cu extruded upward into the Al sheet which contributed to obtaining strong welds. The microstructure showed the presence of copper particles in the aluminium matrix which led to the presence of various intermetallics observed by the energy dispersive spectroscopy and X-ray diffraction. The maximum tensile failure load increases with an increase in the shoulder plunge depth, except for the weld produced at 800 r/min using a conical pin and a concave shoulder. A nugget pull-out failure mode occurred in all the friction stir spot welds under the lap-shear loading conditions. High peaks of Vickers microhardness values were obtained in the vicinity of the keyhole of most of the samples which correlated to the presence of intermetallics in the stir zone of the welds.
文摘Underwater friction stir processing was performed on commercially pure copper with a purity of 99.8% and a copper-zinc alloy(brass). The tool was made of tungsten carbide in the threaded cone form. Friction stir processing was performed at a tool rotational speed of 1800 r/min and a tool transverse speed of 4 mm/min while the samples were immersed in a water tank with a water circulation system. In order to evaluate the effect of the number of process passes on the microstructure and mechanical properties of the samples, this process was continued for up to 6 passes. Microscopic studies using light microscopy on commercially pure copper samples show significant decrease in grain size. Likewise, the hardness of the cross-sectional area shows an increase more than the base metal. The X-ray diffraction pattern of the underwater friction stir processed samples in comparison to that of the base metal exhibits shorter and wider peaks, while the background of the pattern is increased. The sum of these factors represents the formation of an amorphous/ultrafine grained structure. Also, the wear behavior of the samples was investigated by means of pin-on-disk method and the results show that the friction coefficient of processed samples is decreased compared to that of the base metal. The results of wear and hardness tests show that the underwater friction stir processing can significantly improve the wear resistance and hardness of commercially pure copper and brass.
基金the Tertiary Education Support Program (TESP) of ESKOM for financial support
文摘The influence of friction stir welding processing parameters on dissimilar joints conducted between aluminium alloy （AA5754） and commercially pure copper （C11000） was studied. The welds were produced by varying the rotational speed from 600 to 1200 r/min and the feed rate from 50 to 300 mm/min. The resulting microstructure and the corrosion properties of the welds produced were studied. It was found that the joint interfacial regions of the welds were characterized by interlayers of aluminium and copper. The corrosion tests revealed that the corrosion resistance of the welds was improved as the rotational speed was increased. The corrosion rates of the welds compared to the base metals were improved compared with Cu and decreased slightly compared with the aluminium alloy. The lowest corrosion rate was obtained at welds produced at rotational speed of 950 r/min and feed rate of 300 mm/min which corresponds to a weld produced at a low heat input.
文摘An attempt was made to optimize friction welding parameters to attain a minimum hardness at the interface and a maximum tensile strength of the dissimilar joints of AISI 304 austenitic stainless steel （ASS） and copper （Cu） alloy using response surface methodology （RSM）. Three-factor, five-level central composite design matrix was used to specify experimental conditions. Twenty joints were fabricated using ASS and Cu alloy. Tensile strength and interface hardness were measured experimentally. Analysis of variance （ANOVA） method was used to find out significant main and interaction parameters and empirical relationships were developed using regression analysis. The friction welding parameters were optimized by constructing response graphs and contour plots using design expert software. The developed empirical relationships can be effectively used to predict tensile strength and interface hardness of friction welded ASS-Cu joints at 95% confidence level. The developed contour plots can be used to attain required level of optimum conditions to join ASS-Cu alloy by friction welding process.
基金financial supported by the National Natural Science Foundation of China(No.51805145)the Fundamental Research Funds for the Central Universities of China(No.2018B22514)the Natural Science Foundation of Jiangsu Province(No.BK20160284).
文摘In this work,the influence of the Zener-Hollomon(Z)parameter on the microstructure and mechanical properties of copper subjected to friction stir welding(FSW)was investigated.Liquid N2 cooling was conducted to control the cooling rate after the FSW.The obtained results demonstrate that the Z parameter was dependent on the tool rotation rate during the FSW,i.e.,a higher tool rotating rate resulted in a lower Z parameter.The grain size in the stir zone decreased with the increase in the Z parameter.The relationship between the yield strength and the Z parameter is established asσ0.2=σ0+kZn.This relationship exhibited two different plots under the conditions of air cooling and liquid N2 cooling.Even at a similar Z parameter,a significant yield strength difference occurred because massive dislocations,which were caused by the prevention of the post-annealing effect,were maintained in the stir zone.This study suggests that the influence of the post-annealing effect should not be neglected when analyzing the relationship between the Z parameter,micro structure,and mechanical properties.
基金Supported by National Natural Science Foundation of China(Grant Nos.51975479,51905437)Fundamental Research Funds for the Central Universities(Grant No.3102019QD0404)+1 种基金Science and Technology Bureau of Yulin(Grant No.2019-86-1)High-Level Talent Project of Yulin University,China(Grant No.20GK06).
文摘The current investigation of refill friction stir spot welding(refill FSSW)Al alloy to copper primarily involved plunging the tool into bottom copper sheet to achieve both metallurgical and mechanical interfacial bonding.Compared to conventional FSSW and pinless FSSW,weld strength can be significantly improved by using this method.Nevertheless,tool wear is a critical issue during refill FSSW.In this study,defect-free Al/copper dissimilar welds were successfully fabricated using refill FSSW by only plunging the tool into top Al alloy sheet.Overall,two types of continuous and ultra-thin intermetallic compounds(IMCs)layers were identified at the whole Al/copper interface.Also,strong evidence of melting and resolidification was observed in the localized region.The peak temperature obtained at the center of Al/copper interface was 591℃,and the heating rate reached up to 916℃/s during the sleeve penetration phase.A softened weld region was produced via refill FSSW process,the hardness profile exhibited a W-shaped appearance along middle thickness of top Al alloy.The weld lap shear load was insensitive to the welding condition,whose scatter was rather small.The fracture path exclusively propagated along the IMCs layer of Cu_(9)Al_(4) under the external lap shear loadings,both CuAl_(2) and Cu_(9)Al_(4) were detected on the fractured surface on the copper side.This research indicated that acceptable weld strength can be achieved via pure metallurgical joining mechanism,which has significant potential for the industrial applications.
文摘Joining of dissimilar aluminium-copper is an emerging area of interest for both research and industry due to its complex nature.Friction stir welding was attempted to evaluate the joint strength without offset at the butt line between AA6063 to HCP copper sheet under different combination of rotational speed of 800 and 1000 r/min and travel speed of 20 and 40 mm/min.Material flow was studied in detail for different combinations of parameters with optical microscopy and elemental mapping by energy dispersive X-ray spectroscopy（EDS）.The results were correlated with the microstructural characteristics and formation of intermetallics at the bond interface using microhardness test and X-ray diffraction（XRD） technique.Material flow clearly suggests that energy input at 800 r/min and 20 mm/min is sufficient to plasticize both the materials with formation of higher amount of thermodynamically stable and hard intermetallic phases Al4Cu9 and Al Cu4（slower cooling rate of 88 K/s） than that at 800 r/min and 40 mm/min（faster cooling rate of 154 K/s）,attributed maximum joint strength（~78.6% of aluminium base metal）.
文摘This study was done to evaluate the nugget zone(NZ)corrosion behavior of dissimilar copper/brass joints welded by friction stir lap welding(FSLW)in a solution of 0.015 mol/L borax(pH 9.3).To this end,dissimilar copper/brass plates were welded with two dissimilar heat inputs(low and high)during the welding procedure.The high and low heat inputs were conducted with 710 r/min,16 mm/min and 450 r/min,25 mm/min,respectively.Using open circuit potential(OCP)measurements,electrochemical impedance spectroscopy(EIS)and Tafel polarization tests,the electrochemical behavior of the specimens in borate buffer solution was assessed.With the help of scanning electron microscope(SEM),the morphology of welded specimen surfaces was examined after immersion in the test solution.According to the results,the NZ grain size and resistance improvement reduced due to the nugget zone corrosion with a decreased heat input.The results obtained from Tafel polarization and EIS indicated the improved corrosion behavior of the welded specimen NZ with a decrease in the heat input during the welding process unlike the copper and brass metals.Furthermore,an increased heat input during the welding process shows a reduction in the conditions for forming the passive films with higher protection behavior.
文摘Copper base alloy was overlaid onto 35CrMnSiA steel plate by tungsten inert gas （TIG） welding method. The heat transfer process was simulated, the microstructures of the copper base overlay were analyzed by scanning electron microscopy （SEM） and energy dispersive spectrometer （EDS）, and the friction and abrasion properties of the overlay were measured. The results show that the Fe content increases in the overlay with increasing the welding current. And with the increase of Fe content in the overlay, the friction coefficient increases and the wear mechanism changes from oxidation wear to abrasive wear and plough wear, which is related to the size and quantity of Fe grains in the overlay. While with the increase of Fe content in the overlay, the protection of oxidation layer against the oxidation wear on the melted metal decreases.
文摘Friction stir spot welding technique was used to join dissimilar combinations of aluminium alloy(Al5052)with copperalloy(C27200)and friction stir spot welding windows such as tool rotational speed–dwell time and tool rotational speed?plungedepth diagrams for effective joining of these materials were developed.Using a central composite design model,empirical relationswere developed to predict the changes in tensile shear failure load values and interface hardness of the joints with three processparameters such as tool rotational speed,plunge depth and dwell time.The adequacy of the developed model was verified usingANOVA analysis at95%confidence level.Response surface methodology was used to optimize the developed model to maximizetensile strength and minimize interface hardness.A high tensile shear failure load value of3850N and low interface hardness valueof HV81was observed for joints made under optimum conditions,and validation experiments confirmed the high predictability ofthe developed model with error less than2%.The operating windows developed shall act as reference maps for future designengineers in choosing appropriate friction stir spot welding process parameter values to obtain good joints.
