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Texture Evolution of Columnar Grains in Electrical Steel During Hot Rolling 被引量:3
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作者 SHAO Yuan-yuan YANG Ping +1 位作者 FU Yong-jun MAO Wei-min 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2013年第10期99-106,共8页
Columnar grains in cast slabs of electrical steel show strong anisotropy in grain orientation and morphology and thus influence the subsequent microstructure and texture after hot rolling significantly. The texture ev... Columnar grains in cast slabs of electrical steel show strong anisotropy in grain orientation and morphology and thus influence the subsequent microstructure and texture after hot rolling significantly. The texture evolution of hot rolled sheets containing initial columnar grains with their 〈100〉 directions approximately parallel to the rolling direction (RD), transverse direction (TD) and normal direction (ND) of the hot rolled sheets was investigated by using EBSD technique. The results indicated that, whatever the initial texture of the columnar grains was, typical Goss, brass-type and copper-type shear texture component could develop in shear-deformed surface region. The copper-type texture formed under the maximum shearing force with the fine, sheared or dynamically recrystallized grains, and Goss grains were mainly elongated and deformed grains, while brass grains behaved between them. Ad- ditionally, the rotating relationship of the three types of shear textures was different due to the restriction of grain boundaries. In homogenously deformed center region, the RD sample contained more {112}〈110^-〉 grains, and TD sample was covered by {100} textures such as {100}〈011〉 and {100}〈021〉 with coarse grains, while the ND sample developed many {100}〈001〉 grains which were attributed to more {100} grains in the initial sample. Re- markable texture transition occurred on both sides of grain boundaries when {110} grains were adjacent to mfiber texture grains. It was found that significant texture gradient and preferred distribution of rotating axis existed in the soft orientation grains on the α- fiber when the grains neighbored hard grains on γ-fiber. 展开更多
关键词 electrical steel columnar grain hot rolling TEXTURE ORIENTATION
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Significant influence of sharp grain boundary corner on tensile elongation of copper bars with columnar grains and its mechanism 被引量:2
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作者 Zhang-zhi SHI Hai-peng WANG Xue-feng LIU 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2018年第7期1329-1333,共5页
The reason why elongation of copper bars with columnar grains drops significantly after small cold-drawing was explored. The copper bars were prepared by warm-mould continuous casting. Tensile test was interrupted at ... The reason why elongation of copper bars with columnar grains drops significantly after small cold-drawing was explored. The copper bars were prepared by warm-mould continuous casting. Tensile test was interrupted at various tensile strains in order to detect crack origin. Electron backscattered diffraction(EBSD) was used to analyze dislocation slip bands. It is found that the as-cast microstructure contains sharp grain boundary(GB) corners nearly parallel to the solidification direction(SD). Elongation of the copper bars drops significantly from 68.8% in as-cast state to 18.8% in as-drawn state. It is revealed that plastic deformation becomes severer in the vicinity of sharp GB corners. Locally accumulated internal stress even activates a slip system with very low Schmid factor of 0.17. The localized plastic deformation near sharp grain boundary corner promotes crack initiation and propagation, which eventually leads to the significant drop of elongation. 展开更多
关键词 copper FRACTURE grain boundary corner ELONGATION columnar grain
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Hot deformation characteristics of as-cast high-Cr ultra-super-critical rotor steel with columnar grains 被引量:4
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作者 Zong-ye Ding Qiao-dan Hu +1 位作者 Long Zeng Jian-guo Li 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2016年第11期1275-1285,共11页
Isothermal hot compression tests of as-cast high-Cr ultra-super-critical(USC) rotor steel with columnar grains perpendicular to the compression direction were carried out in the temperature range from 950 to 1250... Isothermal hot compression tests of as-cast high-Cr ultra-super-critical(USC) rotor steel with columnar grains perpendicular to the compression direction were carried out in the temperature range from 950 to 1250°C at strain rates ranging from 0.001 to 1 s^(-1). The softening mechanism was dynamic recovery(DRV) at 950°C and the strain rate of 1 s^(-1), whereas it was dynamic recrystallization(DRX) under the other conditions. A modified constitutive equation based on the Arrhenius model with strain compensation reasonably predicted the flow stress under various deformation conditions, and the activation energy was calculated to be 643.92 kJ ×mol^(-1). The critical stresses of dynamic recrystallization under different conditions were determined from the work-hardening rate(θ)–flow stress(σ) and-θ/σ–σ curves. The optimum processing parameters via analysis of the processing map and the softening mechanism were determined to be a deformation temperature range from 1100 to 1200°C and a strain-rate range from 0.001 to 0.08 s^(-1), with a power dissipation efficiency η greater than 31%. 展开更多
关键词 rotor steel columnar grains dynamic recrystallization constitutive models critical conditions processing maps
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The anisotropic grain size effect on the mechanical response of polycrystals:The role of columnar grain morphology in additively manufactured metals 被引量:1
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作者 S.Amir H.Motaman Dilay Kibaroglu 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2024年第14期240-256,共17页
Additively manufactured(AM)metals exhibit highly complex microstructures,particularly in terms of grain morphology which typically features heterogeneous grain size distribution,irregular and anisotropic grain shapes,... Additively manufactured(AM)metals exhibit highly complex microstructures,particularly in terms of grain morphology which typically features heterogeneous grain size distribution,irregular and anisotropic grain shapes,and the so-called columnar grains.The conventional morphological descriptors based on grain shape idealization are generally inadequate for representing complex and anisotropic grain mor-phology of AM microstructures.The primary aspect of microstructural grain morphology is the state of grain boundary spacing or grain size whose effect on the mechanical response is known to be cru-cial.In this paper,we formally introduce the notion of axial grain size from which we derive mean axial grain size,effective grain size,and grain size anisotropy as robust morphological descriptors ca-pable of effectively representing highly complex grain morphologies.We instantiated a discrete sample of polycrystalline aggregate as a representative volume element(RVE)featuring random crystallographic orientation and misorientation distributions.However,the instantiated RVE incorporates the typical mor-phological features of AM microstructures including distinctive grain size heterogeneity and anisotropic grain size owing to its pronounced columnar grain morphology.We ensured that any anisotropy ob-served in the macroscopic mechanical response of the instantiated sample primarily originates from its underlying anisotropic grain size.The RVE was then employed for mesoscale full-field crystal plasticity simulations corresponding to uniaxial tensile deformation along various axes via a spectral solver and a physics-based crystal plasticity constitutive model which was developed,calibrated,and validated in ear-lier studies.Through the numerical analyses,we isolated the contribution of anisotropic grain size to the anisotropy in the mechanical response of polycrystalline aggregates,particularly those with the charac-teristic complex grain morphology of AM metals.This contribution can be described by an inverse square relation. 展开更多
关键词 Axial grain size grain size anisotropy Strain hardening anisotropy grain morphology Morphological texture columnar grains Additive manufacturing
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Constitutive analysis and optimization on hot working parameters of as-cast high Cr ultra-super-critical rotor steel with columnar grains 被引量:1
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作者 Zong-ye Ding Di Zhang +2 位作者 Qiao-dan Hu Long Zeng Jian-guo Li 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2017年第9期916-924,共9页
Isothermal hot compression tests on the as-cast high-Cr ultra-super-critical rotor steel with columnar grains were carried out in the temperature range from 1223 to 1523Kand at strain rates from 0.001 to 1s^(-1).The... Isothermal hot compression tests on the as-cast high-Cr ultra-super-critical rotor steel with columnar grains were carried out in the temperature range from 1223 to 1523Kand at strain rates from 0.001 to 1s^(-1).The compression direction was parallel to the longitudinal direction of columnar grains.The constitutive equation based on Arrhenius model was presented,and the processing maps based on the dynamic material model were developed,correlating with microstructure observation.The main softening mechanism was dynamic recovery at 1223 Kunder strain rates from 0.1to 1s^(-1),whereas it was dynamic recrystallization under other deformation conditions.The constitutive equation modified by strain compensation reasonably predicted the flow stresses.The processing maps and microstructure evolution mechanism schematic indicated that the optimum hot working parameters lay in the zone defined by the temperature range from 1423 to 1473Kand the strain rate range from 0.001 to 1s^(-1). 展开更多
关键词 As-cast ultra-super-critical rotor steel columnar grain Dynamic recrystallization Modified constitutive equation Processing map
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Effect of titanium content on the refinement of coarse columnar austenite grains during the solidification of peritectic steel 被引量:3
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作者 Jiazhi An Zhaozhen Cai Miaoyong Zhu 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2022年第12期2172-2180,共9页
The effect of titanium content on the refinement of austenite grain size in as-cast peritectic carbon steel was investigated by fast directional solidification experiments with simulating the solidification and growth... The effect of titanium content on the refinement of austenite grain size in as-cast peritectic carbon steel was investigated by fast directional solidification experiments with simulating the solidification and growth of surface and subsurface austenite in continuously cast slabs.Transmission electron microscope(TEM)and scanning electron microscope(SEM)were used to analyze the size and distribution of Ti(C,N)precipitates during solidification.Based on these results,the pinning pressure of Ti(C,N)precipitates on the growth of coarse columnar grains(CCGs)was studied.The results show that the austenite microstructure of as-cast peritectic carbon steel is mainly composed of the regions of CCGs and fine columnar grains(FCGs).Increasing the content of titanium reduces the region and the short axis of the CCGs.When the content of titanium is 0.09wt%,there is no CCG region.Dispersed microscale particles will firstly form in the liquid,which will decrease the transition temperature from FCGs to CCGs.The chain-like nanoscale Ti(C,N)will precipitate with the decrease of the transition temperature.Furthermore,calculations shows that the refinement of the CCGs is caused by the pinning effect of Ti(C,N)precipitates. 展开更多
关键词 peritectic steel grain refinement coarse columnar grain titanium carbonitride pinning pressure
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Effect of compression direction on the dynamic recrystallization behavior of continuous columnar-grained CuNi10Fe1Mn alloy 被引量:1
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作者 Yong-kang Liu Hai-you Huang Jian-xin Xie 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2015年第8期851-859,共9页
The dynamic recrystallization(DRX) behavior of continuous columnar-grained(CCG) Cu Ni10Fe1 Mn alloy was investigated by hot compression along the solidification direction(SD) and perpendicular to the solidificat... The dynamic recrystallization(DRX) behavior of continuous columnar-grained(CCG) Cu Ni10Fe1 Mn alloy was investigated by hot compression along the solidification direction(SD) and perpendicular to the solidification direction(PD). Specimens were compressed to a true strain of 0.8 at temperatures ranging from 25°C to 900°C and strain rates ranging from 0.01 to 10 s-1. The results indicate that DRX nucleation at grain boundaries(GBs) and DRX nucleation at slip bands(SBs) are the two main nucleation modes. For SD specimens, C-shaped bending and zig-zagging of the GBs occurred during hot compression, which made DRX nucleation at the GBs easier than that at the SBs. When ln Z ≤ 37.4(Z is the Zener–Hollomon parameter), DRX can occur in SD specimens with a critical temperature for the DRX onset of;50°C and a thermal activated energy(Q) of 313.5 k J·mol-1. In contrast, in PD specimens, the GBs remained straight, and DRX nucleation occurred preferentially at the SBs. For PD specimens, the critical temperature is about 700°C, Q is 351.7 k J·mol-1, and the occurrence condition of DRX is ln Z ≤ 40.1. The zig-zagging of GB morphology can significantly reduce the nucleation energy at the GBs; as a result, DRX nucleation occurs more easily in SD specimens than in PD specimens. 展开更多
关键词 copper–nickel alloys columnar grains compressive d
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Effects of aging treatment on the microstructure and superelasticity of columnar-grained Cu71Al18Mn11 shape memory alloy 被引量:3
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作者 Ji-li Liu Hai-you Huang Jian-xin Xie 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2016年第10期1157-1166,共10页
The effect of aging treatment on the superelasticity and martensitic transformation critical stress in columnar-grained Cu_(71)Al_(18)Mn_(11) shape memory alloy(SMA) at the temperature ranging from 250°C ... The effect of aging treatment on the superelasticity and martensitic transformation critical stress in columnar-grained Cu_(71)Al_(18)Mn_(11) shape memory alloy(SMA) at the temperature ranging from 250°C to 400°C was investigated. The microstructure evolution during the aging treatment was characterized by optical microscopy, scanning electron microscopy, transmission electron microscopy, and X-ray diffraction. The results show that the plate-like bainite precipitates distribute homogeneously within austenitic grains and at grain boundaries. The volume fraction of bainite increases with the increase in aging temperature and aging time, which substantially improves the martensitic transformation critical stress of the alloy, whereas the bainite only slightly affects the superelasticity. This behavior is attributed to a coherent relationship between the bainite and the austenite, as well as to the bainite and the martensite exhibiting the same crystal structure. The variations of the martensitic transformation critical stress and the superelasticity of columnar-grained Cu_(71)Al_(18)Mn_(11) SMA with aging-temperature and aging time are described by the Austin-Rickett equation, where the activation energy of bainite precipitation is 77.2 kJ ·mol1. Finally, a columnar-grained Cu_(71)Al_(18)Mn_(11) SMA with both excellent superelasticity(5%-9%) and high martensitic transformation critical stress(443-677 MPa) is obtained through the application of the appropriate aging treatments. 展开更多
关键词 copper aluminum manganese alloys shape memory effect columnar grains aging bainite superelasticity
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Enhancement of ductility and improvement of abnormal Goss grain growth of magnetostrictive Fe–Ga rolled alloys
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作者 Ji-heng Li Chao Yuan +2 位作者 Xing Mu Xiao-qian Bao Xue-xu Gao 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2018年第4期444-452,共9页
The influences of initial microstructures on the mechanical properties and the recrystallization texture of magnetostrictive 0.1 at% Nb C-doped Fe83 Ga17 alloys were investigated. The directionally solidified columnar... The influences of initial microstructures on the mechanical properties and the recrystallization texture of magnetostrictive 0.1 at% Nb C-doped Fe83 Ga17 alloys were investigated. The directionally solidified columnar-grained structure substantially enhanced the tensile elongation at intermediate temperatures by suppressing fracture along the transverse boundaries. Compared with tensile elongations of 1.0% at 300℃ and 12.0% at 500℃ of the hot-forged equiaxed-grained alloys, the columnar-grained alloys exhibited substantially increased tensile elongations of 21.6% at 300℃ and 46.6% at 500℃. In the slabs for rolling, the introduction of 〈001〉-oriented columnar grains also promotes the secondary recrystallization of Goss grains in the finally annealed sheets, resulting in an improvement of the saturation magnetostriction. For the columnar-grained specimens, the inhomogeneous microstructure and disadvantage in number and size of Goss grains are improved in the primarily annealed sheets, which is beneficial to the abnormal growth of Goss grains during the final annealing process. 展开更多
关键词 MAGNETOSTRICTION iron-gallium alloys columnar grain DUCTILITY abnormal grain growth
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Mechanism of Grain Refinement in Ferritic Stainless Steel Welds: Between Dendrite Fragmentation, Grain Detachment and Heterogeneous Nucleation 被引量:1
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作者 Amuda Muhammed Olawale Hakeem Mridha Shahjahan 《材料科学与工程(中英文A版)》 2011年第3X期321-327,共7页
关键词 不锈钢焊接 形核机制 晶粒细化 异质形核 钢焊缝 铁素体 条块分割 粮食
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Grain Refinement During Directionally Solidifying GCr18Mo Steel at Low Pulling Speeds Under an Axial Static Magnetic Field 被引量:3
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作者 Yuan Hou Zhen-Qiang Zhang +3 位作者 Wei-Dong Xuan Jiang Wang Jian-Bo Yu Zhong-Ming Ren 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2018年第7期681-691,共11页
The present work investigates how axial static magnetic field affects the solidification structure and the solute distribution in directionally solidified GCr18Mo steel. Experimental results show that grain refinement... The present work investigates how axial static magnetic field affects the solidification structure and the solute distribution in directionally solidified GCr18Mo steel. Experimental results show that grain refinement and the colunmar to equiaxed transition is enhanced with the increases in the magnetic field intensity (B) and temperature gradient (G) and the decrease in the growth speed. This phenomenon is simultaneously accompanied by more uniformly distributed alloying elements. The corresponding numerical simulations verify a thermoelectric (TE) magnetic convection pattern in the mushy zone due to the interaction between the magnetic field and TE current. The TE magnetic convection in the liquid should be responsible for the motion of dendrite fragments. The TE magnetic force acting on the dendrite is one of the driving forces trigging fragmentation. 展开更多
关键词 GCr18Mo steel grain refinement Axial static magnetic field columnar to equiaxed transitionThermoelectric magnetic force
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平面流铸制备Fe-3%Si硅钢微观组织的数值模拟 被引量:1
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作者 宫晓威 常庆明 +1 位作者 常佳琦 鲍思前 《材料导报》 北大核心 2025年第2期220-226,共7页
针对平面流铸工艺的特点,通过元胞自动机和有限元模型模拟分析Fe-3%Si硅钢平面流铸过程的传热、凝固和晶粒生长过程。当熔潭达到稳定时,在熔潭内部的上、下半月面附近观察到不同程度的涡流现象;熔体接触冷却辊开始凝固并形成稳定薄带;... 针对平面流铸工艺的特点,通过元胞自动机和有限元模型模拟分析Fe-3%Si硅钢平面流铸过程的传热、凝固和晶粒生长过程。当熔潭达到稳定时,在熔潭内部的上、下半月面附近观察到不同程度的涡流现象;熔体接触冷却辊开始凝固并形成稳定薄带;薄带组织主要由贴辊面附近先形成的等轴晶薄层和随后形成的柱状晶组成;贴辊面晶粒尺寸为3~5μm,自由面晶粒尺寸为7~11μm。增大过热度和喷嘴速度都会使晶粒尺寸增大,柱状晶比例增大;而提高换热系数和冷却辊转速会使晶粒尺寸减小,柱状晶比例减小。 展开更多
关键词 平面流铸 数值模拟 硅钢 微观组织 柱状晶
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激光熔敷氧化锆热障涂层微观结构研究 被引量:12
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作者 高阳 解仑 +2 位作者 佟百运 梁勇 师昌绪 《航空材料学报》 EI CAS CSCD 2003年第3期1-4,共4页
采用5KW连续CO_2激光器对Ni基高温合金上二次重熔NiCoCrAlY和ZrO_2陶瓷层进行了研究。结果表明:激光快速熔化和凝固获得定向外延生长、紧密堆积的柱状晶氧化锆陶瓷层。NiCoCrAlY结合层与柱状晶之间存在氧化铝层,保证了柱状晶与NiCoCrAl... 采用5KW连续CO_2激光器对Ni基高温合金上二次重熔NiCoCrAlY和ZrO_2陶瓷层进行了研究。结果表明:激光快速熔化和凝固获得定向外延生长、紧密堆积的柱状晶氧化锆陶瓷层。NiCoCrAlY结合层与柱状晶之间存在氧化铝层,保证了柱状晶与NiCoCrAlY层的联结。激光重熔ZrO_2层由四方相和立方相组成,经快速冷却由高温保留至室温。 展开更多
关键词 激光熔敷 氧化锆 热障涂层 微观结构 等离子喷涂
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高温合金双性能整体叶盘铸造技术 被引量:9
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作者 汤鑫 曹腊梅 +3 位作者 盖其东 李爱兰 张勇 刘发信 《航空材料学报》 EI CAS CSCD 2006年第3期93-98,共6页
介绍铸造高温合金双性能整体叶盘的铸造工艺,包括双性能合金材料的选择、整体叶盘组织的形成方法、控制措施和浇注工艺参数以及热处理制度对双性能整体叶盘力学性能的影响。结果表明,当浇注过热度ΔT=160~290℃,铸型搅动转数n=K+270~K+3... 介绍铸造高温合金双性能整体叶盘的铸造工艺,包括双性能合金材料的选择、整体叶盘组织的形成方法、控制措施和浇注工艺参数以及热处理制度对双性能整体叶盘力学性能的影响。结果表明,当浇注过热度ΔT=160~290℃,铸型搅动转数n=K+270~K+300(rpm)时,整体叶盘叶片为定向柱晶组织、轮盘为等轴晶组织,初步获得双性能叶盘的热处理制度为1180℃/2h+1230℃/3h,AC+1100℃/4h,AC+870℃/20h,AC。 展开更多
关键词 合金材料 整体叶盘 双性能 定向柱晶 等轴晶 热处理
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不锈钢上激光熔敷涂层结构特征与质量研究 被引量:8
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作者 高阳 佟百运 +1 位作者 梁勇 师昌绪 《材料科学与工艺》 EI CAS CSCD 2003年第4期347-350,共4页
采用5kW连续CO2激光器对经等离子喷涂的NiCoCrAlY结合层和ZrO2陶瓷层进行二次重熔处理,并利用金相显微镜、扫描电镜、电子探针和显微硬度计对激光熔敷涂层进行了显微结构、元素分布以及显微硬度观察与测试.结果表明:多道搭接工艺能降低... 采用5kW连续CO2激光器对经等离子喷涂的NiCoCrAlY结合层和ZrO2陶瓷层进行二次重熔处理,并利用金相显微镜、扫描电镜、电子探针和显微硬度计对激光熔敷涂层进行了显微结构、元素分布以及显微硬度观察与测试.结果表明:多道搭接工艺能降低熔敷涂层气孔率.ZrO2陶瓷层稀释度低,与基体结合完好.并观察到NiCoCrAlY合金层中存在明显的对流图案.加入了TiO2-Al-Ti添加剂的ZrO2陶瓷层激光重熔后得到了无裂纹的定向生长柱状晶,并且呈现一次枝晶平均间距为2 3μm的表层和平均间距为3 8μm的次表层结构. 展开更多
关键词 不锈钢 激光熔敷涂层 二氧化碳激光器 显微结构 元素分布 硬度 陶瓷热障涂层
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连续柱状晶组织铜及铜合金的超延展变形行为与塑性提高机制 被引量:26
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作者 谢建新 王宇 黄海友 《中国有色金属学报》 EI CAS CSCD 北大核心 2011年第10期2324-2336,共13页
以本文作者所在课题组近年来的工作为基础,介绍了高性能连续柱状晶组织纯铜的室温超延展性、热交换用连续柱状晶组织BFe10-1-1管材的高塑性以及高弹高导Cu-12%Al(质量分数)合金的室温塑性提升。研究发现,连续柱状晶组织的高取向性、平... 以本文作者所在课题组近年来的工作为基础,介绍了高性能连续柱状晶组织纯铜的室温超延展性、热交换用连续柱状晶组织BFe10-1-1管材的高塑性以及高弹高导Cu-12%Al(质量分数)合金的室温塑性提升。研究发现,连续柱状晶组织的高取向性、平直的低能小角晶界以及在强塑性变形过程中高组分的(001)"软"取向织构及不同于普通多晶组织的动态回复、组织演化特征,是其塑性提升、具有超延展变形能力的主要原因,总结了连续柱状晶组织塑性提高与超延展变形性的相关机制。研究结果为改善材料尤其是脆性材料和难加工材料的室温塑性与可加工性能提供了理论依据和新思路。 展开更多
关键词 连续柱状晶组织 室温超延展性 塑性提升 变形机制 织构 晶界 组织演化
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柱状晶对Fe-3%Si电工钢再结晶织构演变规律的影响 被引量:15
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作者 张宁 杨平 毛卫民 《金属学报》 SCIE EI CAS CSCD 北大核心 2012年第3期307-314,共8页
在对长轴分别平行于板法向(ND)、轧向(RD)、横向(TD)的柱状晶样品冷轧组织及织构演变规律分析的基础上,利用XRD与EBSD技术,对不同退火温度下各样品再结晶织构的形成规律进行分析.结果表明,柱状晶样品再结晶织构的演变,一方面体现了初始... 在对长轴分别平行于板法向(ND)、轧向(RD)、横向(TD)的柱状晶样品冷轧组织及织构演变规律分析的基础上,利用XRD与EBSD技术,对不同退火温度下各样品再结晶织构的形成规律进行分析.结果表明,柱状晶样品再结晶织构的演变,一方面体现了初始取向晶粒的"遗传性",即立方织构与Goss织构的形成;另一方面又展示了柱状晶样品不同于单晶及多晶的"特殊性",即{113}织构的形成、Goss晶粒大大超过立方晶粒的生长能力及TD样品中{110}〈110〉取向晶粒的消失.退火温度的变化在不同样品中可造成立方织构的增强或减弱,这取决于再结晶时的形核及长大环境,分析认为TD样品低温时形成最强的立方织构与其在冷轧过程中最强的晶界阻力有关.综合考虑各再结晶织构的转变规律,其形成与定向形核及定向长大均相关.研究还证实,3种柱状晶样品中等压下量冷轧并退火后都可抑制γ线织构的形成. 展开更多
关键词 电工钢 柱状晶 织构 再结晶
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对柱状多晶硅薄膜的制备研究 被引量:10
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作者 张丽伟 赵新蕖 +3 位作者 卢景霄 郜小勇 陈永生 靳瑞敏 《人工晶体学报》 EI CAS CSCD 北大核心 2006年第5期1159-1162,共4页
在多晶硅薄膜(Poly-S i)生长理论的基础上,用等离子体化学气相沉积(RF-PECVD)系统,配合快速光热退火装置(RTP),在玻璃衬底和石英衬底上制备了柱状结构的多晶硅薄膜。借助于扫描电子显微镜(SEM)等测试手段,对薄膜的表面形貌和断面形貌进... 在多晶硅薄膜(Poly-S i)生长理论的基础上,用等离子体化学气相沉积(RF-PECVD)系统,配合快速光热退火装置(RTP),在玻璃衬底和石英衬底上制备了柱状结构的多晶硅薄膜。借助于扫描电子显微镜(SEM)等测试手段,对薄膜的表面形貌和断面形貌进行了分析。结果发现:(1)柱晶的形成对薄膜的厚度有一定要求,而且薄膜越厚,柱晶直径越容易长得更大。本实验中,薄膜厚度达到2.5μm左右时,柱晶直径达到了1.5μm以上;(2)再结晶过程是从靠近光源的薄膜表面开始进而到薄膜内部的。再次说明RTP中再结晶的发生,与光和物质的相互作用密切相关。 展开更多
关键词 SEM RTP 柱晶 多晶硅薄膜
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3D-CAFE法凝固参数对430不锈钢凝固组织的影响 被引量:8
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作者 庞瑞朋 王福明 +2 位作者 王金龙 李长荣 张国庆 《材料热处理学报》 EI CAS CSCD 北大核心 2013年第12期188-195,共8页
采用3D-CAFE法与实验相结合的方法,研究形核参数(n v,max,ΔT v,max)和过热度对430铁素体不锈钢凝固组织的影响。本文条件下得到nv,max越大,ΔTv,max越小,晶粒越细小。计算得到最佳过热度值为20℃,并进行了过热度为20℃的实验室实验,试... 采用3D-CAFE法与实验相结合的方法,研究形核参数(n v,max,ΔT v,max)和过热度对430铁素体不锈钢凝固组织的影响。本文条件下得到nv,max越大,ΔTv,max越小,晶粒越细小。计算得到最佳过热度值为20℃,并进行了过热度为20℃的实验室实验,试样的凝固组织几乎全部为球形等轴晶,晶粒的平均直径从表面到中心依次增加。实验室试样的晶粒平均直径为918.07μm,3D-CAFE模型计算20℃过热度试样的晶粒平均直径为920.13μm。计算得到的凝固组织与实验结果基本一致。 展开更多
关键词 过热度 柱状晶 等轴晶 3D—CAFE
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柱状晶对Fe-3%Si电工钢冷轧织构演变规律的影响 被引量:13
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作者 张宁 杨平 毛卫民 《金属学报》 SCIE EI CAS CSCD 北大核心 2012年第7期782-788,共7页
Fe-3%Si电工钢铸锭中普遍存在柱状晶,其晶体学及形状各向异性对随后的热轧、冷轧及退火织构产生很大的影响.利用xRD与EBSD技术对长轴分别平行于轧面法向(ND),轧制方向(RD)和横向(TD)的柱状晶冷轧样品的织构及组织进行了研究,并对晶界的... Fe-3%Si电工钢铸锭中普遍存在柱状晶,其晶体学及形状各向异性对随后的热轧、冷轧及退火织构产生很大的影响.利用xRD与EBSD技术对长轴分别平行于轧面法向(ND),轧制方向(RD)和横向(TD)的柱状晶冷轧样品的织构及组织进行了研究,并对晶界的特殊作用进行了分析.结果表明,中等压下量下,3种柱状晶样品具有不同程度的{001}织构遗传性,即3种样品均不同程度的摆脱了{111}线织构的形成;柱状晶长轴平行于ND和TD时,{001}取向在冷轧时得到大的保留;柱状晶长轴平行于RD时,得到最强的{111}〈112〉织构;柱状晶长轴平行于TD时,冷轧组织中旋转立方织构及{111}〈110〉织构较强.此外,3种样品的织构均表现出由立方→{001}〈130〉→{113}〈251〉的过渡路径,与等轴多晶样品沿α线和γ线转动的路径不同.不同方向的柱状晶晶界对冷轧变形过程中晶粒转动的作用不同,但因晶粒尺寸大而作用有限,且与初始取向相关. 展开更多
关键词 电工钢 柱状晶 织构 冷轧
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