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Production of titanium powder by metallothermic reduction of TiO_(2) in cold pressed pellets 被引量:2
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作者 ZHENG Hai-yan GUO Yong-chun SHEN Feng-man 《Journal of Central South University》 SCIE EI CAS CSCD 2021年第1期48-57,共10页
In order to produce low-cost titanium(Ti)with high productivity,fundamental studies on producing metallic Ti from titanium dioxide(TiO_(2))in the cold pressed pellets were conducted by metallothermic reduction with an... In order to produce low-cost titanium(Ti)with high productivity,fundamental studies on producing metallic Ti from titanium dioxide(TiO_(2))in the cold pressed pellets were conducted by metallothermic reduction with an indirect contact method.This paper focuses on discussing the mechanism of the reduction process and the relationships of RM(a revised reduction index)with reduction temperature,reduction time,and mole ratio of TiO_(2) to CaCl_(2)(nTiO_(2)/nCaCl_(2))in the pellets.The results show that metallic Ti was obtained from the reduction of TiO_(2) in the pellets by calcium(Ca)vapor;pellets were reduced homogenously and Ca vapor diffused into the porous pellets by Knudsen diffusion or the mixing diffusion of molecular diffusion and Knudsen diffusion at 1273 K;RM increased with the increases of temperature and reduction time and was 96.34%when T_(Redu)=1273 K,t_(Redu)=6 h,and nTiO_(2)/nCaCl_(2)=4;the reasonable nTiO_(2)/nCaCl_(2) value is 3−5 for the pellets with enough strength and high RM. 展开更多
关键词 titanium dioxide titanium powder metellothermic reduction cold pressed pellet reduction index
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Effect of Si Content on Mechanical Properties of a Mo and V Free Low Alloy Cast Steel for Automobile Cold Pressing Die 被引量:1
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作者 B.H.Kim J.S.Shin +4 位作者 S.M.Lee B.M.Moon H.D.Kim S.Y.Ju O.Y.Choi 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2008年第3期313-316,共4页
The effects of Si content on combinations of important properties such as hardness, hardenability, and weldability in addition to strength increment were systematically investigated to develop a Mo and V free low allo... The effects of Si content on combinations of important properties such as hardness, hardenability, and weldability in addition to strength increment were systematically investigated to develop a Mo and V free low alloy cast steel for automobile cold pressing die insert. For the evaluation of the applicability as the die insert, the mechanical properties were measured after spheroidization annealing (SA), quenching and tempering (Q/T), and flame hardening (FH) treatments, respectively. The developed 0.8%-1.6%Si containing Mo and V free alloy cast steels showed excellent matrix strengthening effect, hardenability, and weldability, fulfilling the industrial criterion of the mechanical properties for the die insert. 展开更多
关键词 Low alloy cast steel cold pressing die Die insert Matrix hardening Flame hardening
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Visualization Simulations for Cold Press Die
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作者 LIU Hong, YUAN Ju-long, JIN Jie (College of Mechanical & Electronical Engineering, Zhejiang University of Technology, Hangzhou 310014, China) 《厦门大学学报(自然科学版)》 CAS CSCD 北大核心 2002年第S1期31-32,共2页
Pressing process is a manufacturing method that obtained work piece with certain dimension, shape and capability through die forcing roughcast to produce plastic deformation or separate. This paper focuses on the key ... Pressing process is a manufacturing method that obtained work piece with certain dimension, shape and capability through die forcing roughcast to produce plastic deformation or separate. This paper focuses on the key problems of visualization simulation in pressing die. The final aim is that numerical simulation system can simulate the process of processing forming technique, which can supply some necessary and accurate key parameters for die design. The detail description of mechanical characteristic and key technique of sheet forming technique is discussed. Pressing forming method is one of the most important forming techniques of metal forming, which has special mechanical characteristics. The character of sheet pressing forming is that the deformation of thickness direction is very small in contrast to other directions. The deformation mode of sheet forming mainly has the following kinds: bi-directional stretch, plane stress, stretches, depths extend, bending and counter-bending. The essence of press forming is the transferring course that the transferring region of rough comes to deformation by outside force, which is main researching principle in forming and the transferring field. The analysis of pressing forming course, disclose the feature of stress-strain and their changing rule, then pressing process and forming parameters could be obtained. So the states of force and deformation of transferring region is key to determine character about the varieties of pressing transferring. The paper analyzes these factors, which may influence forming precision in pressing process. In traditional methods, some key parameter such as spring-back, bending radius for die design are calculated by experience formula or select from data table. The paper brings forward the calculation methods of key parameter in the case of drawing finite element method and numerical simulation into pressing die design. In order to calculate the value of key parameters based on data supplied by FEM, a numerical simulation application is finished combined with two descriptions of work piece deformation NURBS and discrete piece. The numerical simulation is programmed on Microsoft Visual C++ with OpenGL as the graphics tool. It establishes numerical simulation program, dynamically simulates the process of sheet pressing figuration, and gets good effects. 展开更多
关键词 cold press die VISUALIZATION SIMULATING
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Using Green Cold Pressing to Produce High Quality Fish Oil From Industrial Salmon Waste
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作者 Tarek Fouda 《Journal of Zoological Research》 2020年第1期14-19,共6页
The main objective of this research was to determine the amount of oil fish were extracted from fish west resulted from butchering,cutting and splitting processes before salmon smoking by using cold pressing methods.T... The main objective of this research was to determine the amount of oil fish were extracted from fish west resulted from butchering,cutting and splitting processes before salmon smoking by using cold pressing methods.The amount and the characteristics of extracted of oil were tested at Regional Centre for food and feed the USDA Agricultural Research Center laboratory.The samples were used from fresh Salmon waste about 1000g from each of the(head,skin,viscera,backbone,frames and cuts off).This waste recorded more than 22%of the total mass from salmon fish with used modern extract machine.in this experiment the results revealed the fresh salmon waste have more than 16%of oil fish per one kg of salmon waste.The oil weight from Salmon waste for(head,skin,viscera,backbone,frames and cuts off).was increased with pressing time increase as well as oil productivity increased.The optimum conditions at pressing time was 200 min,for all salmon waste components.Oil productivity fluctuated according to waste sources was 190,210,86,188,178 and 90 g.oil/1000 g.by head,skin,off cuts,terming,,viscera,and backbone frames,Salmon by-products,oil productivity was ranged between 8.60 to 21.00%at constant pressure.High contents of functional EPA(20:5ω3)and DHA(22:6ω3)for oil fish. 展开更多
关键词 SALMON Waste extract Efficiency Yield SMOKING Fish oil cold pressing Wet rendering
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Investigated Cold Press Oil Extraction from Non-Edible Oilseeds for Future Bio-Jet Fuels Production
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作者 Xianhui Zhao Lin Wei +1 位作者 James Julson Yinbin Huang 《Journal of Sustainable Bioenergy Systems》 2014年第4期199-214,共16页
Bio-jet fuel produced from non-edible oilseeds can be an alternative to fossil fuels with the benefits of increasing national energy security, reducing environmental impact, and fostering rural economic growth. Effici... Bio-jet fuel produced from non-edible oilseeds can be an alternative to fossil fuels with the benefits of increasing national energy security, reducing environmental impact, and fostering rural economic growth. Efficient oil extraction from oilseeds is critical for economic production of bio-jet fuels. Oil extractions from camelina (sativa) and canola (Brassica napus) seeds were conducted using a cold press method. The effect of the frequency controlling the screw rotation speed on the oil recovery and quality was discussed. Characterization of the produced raw vegetable oils, such as heating value, elemental content and main chemical compositions, was carried out. The results showed that the oil recovery increased when the frequency decreased. The highest oil recoveries for camelina and canola seeds were 88.2% and 84.1% respectively, both at 15 Hz. The cold press frequency and processing temperature (97.2°C - 106.0°C) had a minor influence on the qualities and recovery of both camelina and canola oils. In addition, camelina and canola oils produced at 15 Hz underwent catalytic cracking to examine potential hydrocarbon fuels production. It was observed that some of oil physicochemical properties were improved after catalytic cracking. Although more study is needed for further improvement of oil recovery and qualities, cold press could be an efficient method for oil extraction from non-edible oilseeds. Additionally, the preliminary results of upgrading the oils produced show very promising for future bio-jet fuels production. 展开更多
关键词 Camelina CANOLA cold press OIL Recovery UPGRADING
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Plastic forming simulations of cold isostatic pressing of selective laser sintered components 被引量:2
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作者 杜艳迎 史玉升 魏青松 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2011年第5期1118-1122,共5页
A combined method of selective laser sintering (SLS) and cold isostatic pressing (CIP) was applied to manufacturing metal parts rapidly. Finite element method was used to predict final dimensions and decrease cost... A combined method of selective laser sintering (SLS) and cold isostatic pressing (CIP) was applied to manufacturing metal parts rapidly. Finite element method was used to predict final dimensions and decrease cost. The simulations of CIP of selective laser sintered parts were carried out by Drucker-Prager-Cap constitutive model with ABAQUS computer program. The property of metal powder was measured by CIP experiments. The results show the rubber bag and the friction coefficient have little influence on results of simulations. The parts only have uniform shrinkage and have no obvious distortion in shape. The results of simulations show a good agreement with the experimental results and the calculated results, indicating that the Drucker-Prager-Cap model is an effective model to simulate CIP process. The simulations could give a useful direction to forming process of the CIP of selective laser sintered components. K 展开更多
关键词 cold isostatic pressing stainless steel plastic forming SIMULATION
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Manufacture and Cytotoxicity of a Lead-free Piezoelectric Ceramic as a Bone Substitute—Consolidation of Porous Lithium Sodium Potassium Niobate by Cold Isostatic Pressing 被引量:3
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作者 Qi Wang Jun Yang +4 位作者 Wu Zhang Roxanne Khoie Yi-ming Li Jian-guo Zhu Zhi-qing Chen 《International Journal of Oral Science》 SCIE CAS CSCD 2009年第2期99-104,共6页
Aim The piezoelectric properties and cytotoxicity of a porous lead-free piezoelectric ceramic for use as a direct bone substitute were investigated. Methodology Cold isostatic pressing (CIP) was applied to fabricate... Aim The piezoelectric properties and cytotoxicity of a porous lead-free piezoelectric ceramic for use as a direct bone substitute were investigated. Methodology Cold isostatic pressing (CIP) was applied to fabricate porous lithium sodium potassium niobate (Li0.06Na0.5K0.44) NbO3 specimens using a pore-forming method. The morphologies of the CIP-processed specimens were characterized and compared to those of specimens made by from conventional pressing procedures. The effects of the ceramic on the attachment and proliferation of osteoblasts isolated from the cranium of 1-day-old Sprague- Dawley rats were examined by a scanning electron microscopy (SEM) and metbylthiazol tetrazolium (MTT) assay. Results The results showed that CIP enhanced piezoelectricity and biological performance of the niobate specimen, and also promoted an extracellular matrix-like topography of it. In vitro studies showed that the CIP-enhanced material had positive effects on the attachment and proliferation of osteoblasts. Conclusion Niobate ceramic generated by CIP shows a promise for being a piezoelectric composite bone substitute. 展开更多
关键词 lead-free piezoelectric ceramic cold isostatic pressing (CIP) CYTOCOMPATIBILITY OSTEOBLAST
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粉末粒径和形貌对锆合金烧结坯密度和显微硬度的影响
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作者 强瑞 马飞 +2 位作者 刘茂 向姣 宋加成 《化工管理》 2026年第2期137-140,共4页
对锆合金粉末采用适当的筛分工艺和滚动流化改性处理工艺是得到压制密度更高的锆合金产品的关键方法之一。文章基于氢化脱氢工艺制备的锆合金粉末研究了不同粉末粒径分布和滚动流化改性处理等因素对粉末冷压成型制成的锆合金生坯相对密... 对锆合金粉末采用适当的筛分工艺和滚动流化改性处理工艺是得到压制密度更高的锆合金产品的关键方法之一。文章基于氢化脱氢工艺制备的锆合金粉末研究了不同粉末粒径分布和滚动流化改性处理等因素对粉末冷压成型制成的锆合金生坯相对密度、烧结后相对密度和显微硬度的影响。研究结果表明,粉末粒径和滚动流化时间均会影响压制成型的锆合金生坯和烧结坯的相对密度,粉末粒径对锆合金生坯相对密度的影响更加显著;三种滚动流化状态下(0 h、10 h和20 h),锆合金烧结坯均呈现粉末粒径越细小,烧结前后相对密度变化越大的现象,且超细粉制成的烧结坯显微硬度值明显高于其他两种D50径较大粉末制成的烧结坯显微硬度;对于粉末粒径分布相同的超细粉和粗粉,滚动流化时间越长,锆合金生坯相对密度越高,烧结前后相对密度差值越小。 展开更多
关键词 冷压烧结 粉末压坯 烧结密度 硬度 锆合金粉末
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耳片孔结构二次冷挤压强化残余应力分析研究
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作者 刘儒军 黄翔 +3 位作者 黄海鸿 任勇 殷超超 班许可岭 《合肥工业大学学报(自然科学版)》 北大核心 2026年第1期28-35,共8页
文章对7050铝合金耳片孔进行压合衬套二次冷挤压强化,从残余应力和显微硬度2个方面进行分析。通过X射线衍射仪(X-ray diffractometer,XRD)和显微硬度计对残余应力和显微硬度进行检测,研究压合衬套二次冷挤压强化对耳片孔残余应力和显微... 文章对7050铝合金耳片孔进行压合衬套二次冷挤压强化,从残余应力和显微硬度2个方面进行分析。通过X射线衍射仪(X-ray diffractometer,XRD)和显微硬度计对残余应力和显微硬度进行检测,研究压合衬套二次冷挤压强化对耳片孔残余应力和显微硬度的影响。结果表明:压合衬套二次冷挤压使耳片孔沿孔壁径向形成了一定深度的残余压应力层;随着相对挤压量增大,残余压应力峰值和应力层深度随之增大;当相对挤压量为2.5%时,最大残余压应力可达-400.3MPa,并形成了约14mm深的残余压应力层;同一相对挤压量下,同向压合衬套二次冷挤压试样挤出端的残余压应力大于挤入端,反向压合衬套二次冷挤压试样2个端面的残余压应力基本一致;当相对挤压量为2.5%时,强化后的试样沿孔壁径向形成了约4.5mm深的组织硬化层,最大硬度提升达到19.4%;压合衬套二次冷挤压强化后孔壁沿径向形成了残余压应力层和组织硬化层,进而提高了耳片孔的表面性能。 展开更多
关键词 二次冷挤压 压合衬套 相对挤压量 残余应力 显微硬度
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钢渣基固碳储热材料的开发及热物性研究
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作者 房洪彬 高祺 +2 位作者 金秋彤 张小霞 龚志军 《储能科学与技术》 北大核心 2026年第2期353-362,共10页
本研究以钢渣为基体,通过碳封存技术将其转化为固碳材料,并与硝酸钠相变材料复合,采用冷压烧结法制备了一种新型固碳储热一体化复合材料。通过正交试验优化碳封存条件,确定最佳反应条件为:温度75℃、CO_(2)压力0.85 MPa、液固比35、搅... 本研究以钢渣为基体,通过碳封存技术将其转化为固碳材料,并与硝酸钠相变材料复合,采用冷压烧结法制备了一种新型固碳储热一体化复合材料。通过正交试验优化碳封存条件,确定最佳反应条件为:温度75℃、CO_(2)压力0.85 MPa、液固比35、搅拌速率950 r/min。在此条件下,温度提升至95℃并反应4 h后,固碳量达到294 kgCO_(2)/t_(钢渣)。扫描电子显微镜(SEM)观察显示,硝酸钠均匀贴合于固碳钢渣孔隙之中;X射线衍射(XRD)分析表明二者具有良好的化学相容性,仅为物理混合。热物性测试结果表明,固碳钢渣/硝酸钠复合材料的最佳负载量为50%,其熔点为303.2℃,相变潜热值为81.9 J/g,导热系数为0.866 W/(m·K)。经过300次加热/冷却循环后,该复合材料展现出良好的循环稳定性。与钢渣硝酸钠复合相变储热材料相比,其储热性能更为优异。本研究不仅为固废资源的高效利用提供了新的途径,还为开发高性能复合相变储热材料提供了实验依据,推动了固碳与储热一体化技术的发展,为清洁低碳能源转型中的可再生能源储存技术提供了重要的技术支持。 展开更多
关键词 碳封存 冷压烧结 固碳储热一体化 复合相变储热材料
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热挤压铝钎焊材料粉锭制备复合铝焊丝工艺的研究
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作者 林业伟 胡泽宇 +5 位作者 蔡沛沛 蔡志红 蔡耿生 黄云帅 覃扬梁 刘福平 《材料研究与应用》 2026年第1期52-59,共8页
以设定粒度范围的粉状铝钎料和铝钎剂为原料,经均匀混合使铝钎剂充分包覆铝钎料,采用冷等静压(CIP)工艺将混合粉末压制成粉锭,再通过热挤压制备复合铝焊丝,并对冷等静压压制粉锭的工艺条件及热挤压工艺参数对挤压焊丝的影响进行研究。... 以设定粒度范围的粉状铝钎料和铝钎剂为原料,经均匀混合使铝钎剂充分包覆铝钎料,采用冷等静压(CIP)工艺将混合粉末压制成粉锭,再通过热挤压制备复合铝焊丝,并对冷等静压压制粉锭的工艺条件及热挤压工艺参数对挤压焊丝的影响进行研究。结果表明,在压制粉锭过程中,将冷等静压压力控制在80—190 MPa范围内,利于挤压过程中气体的逸出,可满足后续加热和挤压装填的要求,并且粉锭的径向收缩率比轴向收缩率高出约27.9%。在加工制备复合铝焊丝过程中,采用由挤压模具和导丝模具组成的挤丝模具,可实现连续的挤丝作业。由于焊丝从模具孔流出的速度与挤压杆速度和挤压比成正比,因此设计大挤压比利于提高出丝效率。在热挤压粉锭的过程中,若粉锭温度偏低可适当提高挤压杆速度进行挤压,反之亦然。热挤压速度分为4个阶段,即填充挤压、突破挤压、稳定挤压和终了挤压,而出丝平均速度则为突破挤压与终了挤压之间的平均速度。当突破挤压的压力为挤压机系统额定压力的80%—90%时,挤出焊丝较为顺利且质量稳定;当突破挤压压力为挤压机系统额定压力的90%—95%时,挤出焊丝的表面质量不稳定;而当突破压力超过挤压机系统额定压力的95%时,将无法挤出焊丝。在挤压比为100、挤压筒温度为(400±10)℃条件下,粉锭的加热温度宜控制在400—420℃范围,此时出丝平均速度达12.0 m·min^(−1)、最高出丝速度可达18.8 m·min^(−1),在此优化条件下挤出的复合铝焊丝表面完好且有光泽,密度达理论密度的97.8%,并可弯成直径为80 mm的圆。本研究制备的复合铝焊丝已用于火焰钎焊铝合金工艺。 展开更多
关键词 热挤压 铝钎料 钎剂 冷等静压 粉锭 复合铝焊丝 挤压温度 挤压速度 挤压比
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CLINICAL APPLICATION OF PAPER-SEPARATED PRESSING MOXIBUSTION 被引量:1
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作者 Liu Xiaomin, Jiang Zhenya, Li YingkunDepartment of Acupuncture and Moxibustion, Affiliated Hospital of Chengdu College of Traditional Chinese Medicine, Chendu 610072, ChinaOu PingDepartment of Traditional Chinese Medicine, Workers’ Hospital of Gaobalu Che 《World Journal of Acupuncture-Moxibustion》 1994年第3期3-6,共4页
31 cases of common cold were treated with paper-separated moxibustion. An ig-nited moxa-stick was quickly and repeatedly applied to press the paper-separated acupoints until theskin surrounding acupoints being flushed... 31 cases of common cold were treated with paper-separated moxibustion. An ig-nited moxa-stick was quickly and repeatedly applied to press the paper-separated acupoints until theskin surrounding acupoints being flushed.Points Fengfu (GV 16), Fengchi (GB 20), Dazhui (GV14), Dazhu (BL 11), Fengmen (BL 12) and Feishu (BL 13) were selected alternatively for moxi-bustion, once a day. Among 31 cases, 14 (45. 1 % ) were cured after one session of treatment, and 15(48. 4% ) cured after two sessions, with the total effective rate of 93.5 %. Its effect was similar tothat of the control drugs (" Xiang Feng Tea" and Sang Ju Ganmao Tablet", P】0. 05). Resultsshowed that this method was quite effective for treatment of common cold with either cold or heatsyndromes and also could reduce acute attacks of chronic bronchitis. 展开更多
关键词 COMMON cold Paper-separated pressING MOXIBUSTION
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油茶果干燥应力破蒲失水特征及冷榨原油质量的变化
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作者 徐建国 谌佳君 +3 位作者 石劲松 顾震 徐刚 张绪坤 《现代食品科技》 北大核心 2025年第12期147-155,共9页
为更好地了解油茶果干燥应力破蒲技术以实现油茶籽和果蒲(壳)的高效、高品质分离,该文通过开展干燥应力破蒲试验,考察了不同干燥温度(50、60、70、80℃)条件下干燥应力破蒲失水动力学特征以及破蒲过程对后续冷榨原油质量的影响,建立了... 为更好地了解油茶果干燥应力破蒲技术以实现油茶籽和果蒲(壳)的高效、高品质分离,该文通过开展干燥应力破蒲试验,考察了不同干燥温度(50、60、70、80℃)条件下干燥应力破蒲失水动力学特征以及破蒲过程对后续冷榨原油质量的影响,建立了干燥应力破蒲失水过程模型,开发了变温干燥应力破蒲工艺。研究发现,干燥应力破蒲过程中油茶果失水速率曲线呈阶梯状下降趋势,且存在提速段及多个近似恒速段;干燥温度升高,油茶果失水曲线变陡,到达破蒲终点湿基含水率(32.00%)时所需时间显著缩短。新建的半经验模型(R^(2)≥0.9997,RMSE≤0.4286%)可以准确模拟油茶果干燥应力破蒲失水过程。随着温度的升高,油茶籽冷榨原油酸价数值从0.08 mg/g显著增加至0.39 mg/g,总色差从76.27显著增加至83.63,出油率从23.43%显著降低至18.84%。低温干燥应力破蒲有利于提高油茶籽冷榨原油质量和出油率。经变温干燥应力破蒲后,油茶果破蒲率为98.35%,碎籽率为0%,冷榨原油酸价(以KOH计)、过氧化值分别为1.00 mg/g、0.0099 g/100 g,水分及挥发物为0.35%,出油率为21.08%。该研究可为优化油茶果干燥应力破蒲技术工艺及设备开发提供依据。 展开更多
关键词 油茶果 干燥应力 破蒲 模型 冷榨原油 质量
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液压冷榨大豆饼粕蛋白提取工艺优化及其应用现状分析
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作者 蒋林斌 黄广君 《中国调味品》 北大核心 2025年第3期125-128,共4页
随着消费者对植物蛋白的需求不断增加,在植物蛋白市场中,大豆蛋白由于其营养价值和功能特性而被广泛应用。然而,工业生产的大豆饼粕中含有机溶剂,严重制约着大豆蛋白在绿色食品和有机食品领域中的应用。大豆的压榨方式主要为螺旋压榨法... 随着消费者对植物蛋白的需求不断增加,在植物蛋白市场中,大豆蛋白由于其营养价值和功能特性而被广泛应用。然而,工业生产的大豆饼粕中含有机溶剂,严重制约着大豆蛋白在绿色食品和有机食品领域中的应用。大豆的压榨方式主要为螺旋压榨法和液压冷榨压榨法,两种压榨方法对大豆饼粕中蛋白的品质均会产生影响。该研究基于此,对比螺旋压榨法和液压冷榨压榨法对大豆饼粕蛋白提取率和品质的影响,最终确定采用液压冷榨压榨法压榨大豆,获得的大豆饼粕中蛋白提取率和品质均更高。以液压冷榨压榨法压榨的大豆饼粕为原材料,对其蛋白和脂质的提取工艺进行研究和优化。结果表明,最佳的大豆饼粕蛋白和脂质提取工艺为pH值10、提取时间45 min和料液比例1∶20。 展开更多
关键词 液压冷榨法 大豆蛋白 副产物 工艺优化
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Two-step molding of polymer coating for efficient daytime radiative cooling
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作者 Jiahao Ni Cheng Jin +3 位作者 Wenshuo Zhang Lanxin Li Gang Pei Bin Zhao 《Journal of Energy Chemistry》 2025年第8期533-539,共7页
Passive daytime radiative cooling has great potential for energy conservation and sustainable development.Polymer-based radiative cooling materials have received much attention due to their excellent cooling performan... Passive daytime radiative cooling has great potential for energy conservation and sustainable development.Polymer-based radiative cooling materials have received much attention due to their excellent cooling performance and scalable potential.However,the use of large amounts of organic solvents,the long cycle time,and the complexity of the preparation process have limited their development.Herein,we report a two-step cold-press sintering method for the preparation of a polymer radiative cooler,which is free of organic solvents.For demonstration,a polyvinylidene fluoride-hexafluoropropylene copolymer(PVDF-HFP)coating with a solar reflectance of 97.4%and an emissivity of 0.969 within the atmospheric window is prepared,which can achieve a sub-ambient cooling phenomenon with a temperature reduction of 4.8℃.Besides,the maximal radiative cooling power of 50.2 W/m^(2)is also obtained under sunlight.After the implementation of the proposed sintered PVDF-HFP coating in buildings,more than 10%of annual energy consumption can be saved in China.This work proposes a simple,environmentally friendly,and scalable processing method for the preparation of radiative cooling materials,facilitating the large-scale application of radiative cooling technology. 展开更多
关键词 cold pressing sintering Radiative cooling Polymer coating Passive cooling Building energy saving
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核桃仁及其粕中油脂提取工艺优化及品质分析 被引量:4
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作者 王国王 祁岩龙 +3 位作者 杨忠强 孙俪娜 尼格尔热依·亚迪卡尔 木丽得尔·叶尔肯 《粮食与油脂》 北大核心 2025年第2期86-92,共7页
在单因素试验的基础上,采用响应面法优化液压冷榨提取核桃仁中核桃油的工艺,并采用单因素试验进一步优化超临界CO_(2)萃取核桃粕中核桃油的工艺。比较分析了液压冷榨未脱种衣核桃仁(DPM)、液压冷榨脱种衣核桃仁(QPM)、超临界CO_(2)萃取... 在单因素试验的基础上,采用响应面法优化液压冷榨提取核桃仁中核桃油的工艺,并采用单因素试验进一步优化超临界CO_(2)萃取核桃粕中核桃油的工艺。比较分析了液压冷榨未脱种衣核桃仁(DPM)、液压冷榨脱种衣核桃仁(QPM)、超临界CO_(2)萃取脱种衣核桃粕(QPC)制取的核桃油品质。结果表明:液压冷榨最佳工艺条件为压榨压力50.0 MPa、压榨时间120 min、进料量10.0 kg,在此条件下核桃油出油率为61.53%±0.15%;超临界CO_(2)萃取的最佳工艺为萃取温度45.0℃、萃取时间5.0 h、萃取压力30.0 MPa,在此条件下核桃油萃取率为33.33%±0.25%。对比分析可知,3种处理条件下的核桃油品质均符合国家标准;不饱和脂肪酸含量均超过90%。 展开更多
关键词 核桃油 液压冷榨 超临界CO_(2)萃取 品质 脂肪酸组成
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Al/PTFE/AlH_(3)活性材料的制备及性能研究 被引量:1
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作者 邢逸凡 王存洪 +2 位作者 吴翰林 刘扬 曹玉武 《火工品》 北大核心 2025年第3期15-20,共6页
本研究旨在探讨AlH_(3)对Al/PTFE活性材料微观结构及宏观性能的影响,遴选最优组分配比及制备方法,以进一步提升活性材料的综合毁伤效能及引燃性能。通过粉末混合和冷压成型工艺,制备出4种不同配比的Al/PTFE/AlH_(3)活性材料,并对其微观... 本研究旨在探讨AlH_(3)对Al/PTFE活性材料微观结构及宏观性能的影响,遴选最优组分配比及制备方法,以进一步提升活性材料的综合毁伤效能及引燃性能。通过粉末混合和冷压成型工艺,制备出4种不同配比的Al/PTFE/AlH_(3)活性材料,并对其微观组织、元素分布、静态力学性能和终点毁伤能力进行了系统研究。研究结果显示,所制备的活性材料各组分分布均匀,基体材料能有效包覆金属颗粒,从而确保了材料的强度及均匀性。随着AlH_(3)含量的增加,该材料的屈服强度及弹性模量均呈现先上升后下降的趋势。在弹道枪加载试验中,当AlH_(3)质量分数达到21%时,活性材料的平均弹孔毁伤面积和平均准静态压力达到最大值,显示出最佳的综合毁伤效能。 展开更多
关键词 粉末混料 冷压成型 活性材料 AlH_(3) 屈服强度 准静态超压
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不同贮藏温度对低温压榨核桃油关键香气成分的影响 被引量:1
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作者 张玉壮 雷舒雯 +2 位作者 刘志晨 彭春秀 龚加顺 《中国油脂》 北大核心 2025年第9期14-19,共6页
旨在为核桃油的低温贮藏提供参考,研究了不同贮藏温度下低温压榨核桃油关键香气成分的差异。将低温压榨核桃油在25、4、-10、-20℃下贮藏8周,考察贮藏过程中其酸值和过氧化值的变化,采用电子鼻与固相微萃取-气相色谱-质谱法测定核桃油... 旨在为核桃油的低温贮藏提供参考,研究了不同贮藏温度下低温压榨核桃油关键香气成分的差异。将低温压榨核桃油在25、4、-10、-20℃下贮藏8周,考察贮藏过程中其酸值和过氧化值的变化,采用电子鼻与固相微萃取-气相色谱-质谱法测定核桃油的风味物质与挥发性成分含量,并采用相对气味活度值确定关键香气成分。结果表明:随着贮藏时间的延长与贮藏温度的升高,低温压榨核桃油的酸值和过氧化值升高,但均未超出国标限量;电子鼻分析表明,低温压榨核桃油主要含有氮氧化物、烃类、萜烯类、硫化物、醇类、醛酮类等物质,-20℃贮藏核桃油的风味与初始核桃油相似,25℃贮藏核桃油的风味与初始核桃油差别较大;核桃油中共检测出39种香气成分,包括醛类17种、烃类11种、酸类4种、醇类2种、酮类1种、其他类4种;新鲜核桃油中共检出17种关键香气成分,经25、4、-10、-20℃贮藏8周后,核桃油中分别检出12、13、12、13种关键香气成分,其中25、4、-10℃贮藏核桃油均与新鲜核桃油有7种共有的关键香气成分,而-20℃贮藏核桃油与新鲜核桃油有10种共有的关键香气成分。综上,核桃油在低温下贮藏效果较优,尤其在-20℃下贮藏时其品质和风味与新鲜核桃油更接近。 展开更多
关键词 低温压榨核桃油 低温贮藏 固相微萃取-气相色谱-质谱联用 电子鼻 关键香气成分
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冷榨和焙烤山茶油中关键香气化合物及营养成分的比较
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作者 王鹏 朱凯 +2 位作者 马建林 唐也婷 石自彬 《食品与机械》 北大核心 2025年第12期133-142,共10页
[目的]考察加工工艺对山茶油中挥发性香气化合物和营养成分的影响。[方法]采用全二维气相色谱质谱联用法(GC×GC-qMS)对冷榨和焙烤山茶油中香气化合物进行鉴定,进一步根据香气稀释(FD)因子和气味活度值(OAV)确定关键香气化合物。[结... [目的]考察加工工艺对山茶油中挥发性香气化合物和营养成分的影响。[方法]采用全二维气相色谱质谱联用法(GC×GC-qMS)对冷榨和焙烤山茶油中香气化合物进行鉴定,进一步根据香气稀释(FD)因子和气味活度值(OAV)确定关键香气化合物。[结果]在冷榨和焙烤山茶油中共检测到17种醛类、5种酮类、12种醇类、10种酸类、13种酯类、10种杂环类和8种其他类化合物。冷榨山茶油的关键香气化合物主要有己醛、2-庚醇、癸酸乙酯、苯甲酸乙酯和芳樟醇;而焙烤山茶油以己醛、辛醛、苯甲醛、(E)-2-壬烯醛、(E,E)-2,4-癸二烯醛、3-甲基-1-丁醇、乙酸、γ-丁内酯、2-戊基呋喃、2-乙基-6-甲基吡嗪和3-乙基-2,5-二甲基吡嗪为主。焙烤山茶油比冷榨山茶油具有更浓郁的焙烤、坚果和脂肪气味;而冷榨山茶油具有较高的维生素E、植物甾醇、多酚和角鲨烯。[结论]山茶油中香气化合物和营养成分与其加工工艺密切相关,焙烤有利于香气化合物的形成,而冷榨能保留更多的活性成分。 展开更多
关键词 山茶油 冷榨 焙烤 香气化合物 营养成分
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激光辐照改进MWCNTs/Ti复合块体冷阴极场发射性能研究
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作者 夏欢欢 麻华丽 +4 位作者 秦鑫垚 李鹏 曾凡光 李明玉 杨鹏 《化工新型材料》 北大核心 2025年第11期196-200,共5页
采用冷压烧结工艺制备了多壁碳纳米管/钛(MWCNTs/Ti)复合块体冷阴极,并利用二氧化碳红外激光器对其辐照;通过扫描电子显微镜(SEM)及拉曼光谱分析了不同功率模式下激光诱导对复合块体冷阴极表面形貌、结构的影响;采用二级结构研究了块体... 采用冷压烧结工艺制备了多壁碳纳米管/钛(MWCNTs/Ti)复合块体冷阴极,并利用二氧化碳红外激光器对其辐照;通过扫描电子显微镜(SEM)及拉曼光谱分析了不同功率模式下激光诱导对复合块体冷阴极表面形貌、结构的影响;采用二级结构研究了块体阴极的电子发射性能。结果表明:激光辐照可以显著改善阴极表面的MWCNTs形貌、结构,进而提高了冷阴极的场发射性能。当激光辐照功率为3W时,阴极表面的碳纳米管近似呈垂直列阵分布,在3.5V/μm的电场强度下,该阴极的场发射电流密度相对未激光诱导阴极从923μA/cm^(2)增加到2145μA/cm^(2),提高了132.4%。 展开更多
关键词 多壁碳纳米管/钛复合块体冷阴极 激光辐照 场发射 冷压烧结
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