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Accurate closed-form flutter eigensolutions of three-dimensional composite laminates with shear deformation
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作者 Dezhuang PAN Yufeng XING 《Chinese Journal of Aeronautics》 2026年第1期230-246,共17页
According to the Mindlin plate theory and the first-order piston theory,this work obtains accurate closed-form eigensolutions for the flutter problem of three-dimensional(3D)rectangular laminated panels.The governing ... According to the Mindlin plate theory and the first-order piston theory,this work obtains accurate closed-form eigensolutions for the flutter problem of three-dimensional(3D)rectangular laminated panels.The governing differential equations are derived by the Hamilton's variational principle,and then solved by the iterative Separation-of-Variable(i SOV)method,which are applicable to arbitrary combinations of homogeneous Boundary Conditions(BCs).However,only the simply-support,clamped and cantilever panels are considered in this work for the sake of clarity.With the closed-form eigensolutions,the flutter frequency,flutter mode and flutter boundary are presented,and the effect of shear deformation and aerodynamic damping on flutter frequencies is investigated.Besides,the relation between panel energy and the work of aerodynamic load is discussed.The numerical comparisons reveal the following.(A)The flutter eigenvalues obtained by the present method are accurate,validated by the Finite Element Method(FEM)and the Galerkin method.(B)When the span-chord ratio is larger than 3,simplifying a 3D panel to 2D(two-dimensional)panel is reasonable and the relative differences of the flutter points predicted by the two models are less than one percent.(C)The reciprocal relationship between the mechanical energy of the panel and the work done by aerodynamic load is verified by using the present flutter eigenvalues and modes,further indicating the high accuracy of the present solutions.(D)The coupling of shear deformation and aerodynamic damping prevents frequency coalescing. 展开更多
关键词 closed-form eigensolutions The first-order piston theory The Mindlin plate theory Three-dimensional panel flutter Separation-of-variable method
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Closed-form solution to thin-walled box girders considering effects of shear deformation and shear lag 被引量:18
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作者 周旺保 蒋丽忠 +1 位作者 刘志杰 刘小洁 《Journal of Central South University》 SCIE EI CAS 2012年第9期2650-2655,共6页
Considering three longitudinal displacement functions and uniform axial displacement functions for shear lag effect and uniform axial deformation of thin-walled box girder with varying depths,a simple and efficient me... Considering three longitudinal displacement functions and uniform axial displacement functions for shear lag effect and uniform axial deformation of thin-walled box girder with varying depths,a simple and efficient method with high precision to analyze the shear lag effect of thin-walled box girders was proposed.The governing differential equations and boundary conditions of the box girder under lateral loading were derived based on the energy-variational method,and closed-form solutions to stress and deflection corresponding to lateral loading were obtained.Analysis and calculations were carried out with respect to a trapezoidal box girder under concentrated loading or uniform loading and a rectangular box girder under concentrated loading.The analytical results were compared with numerical solutions derived according to the high order finite strip element method and the experimental results.The investigation shows that the closed-form solution is in good agreement with the numerical solutions derived according to the high order finite strip method and the experimental results,and has good stability.Because of the shear lag effect,the stress in cross-section centroid is no longer zero,thus it is not reasonable enough to assume that the strain in cross-section centroid is zero without considering uniform axial deformation. 展开更多
关键词 shear lag effect thin-walled box girder energy-variational method shear deformation closed-form solution
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基于组件颜色信息的谱方法Matting
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作者 王甲卓 李翠华 《厦门大学学报(自然科学版)》 CAS CSCD 北大核心 2010年第4期495-500,共6页
将组件的颜色信息引入谱方法Matting中,利用组件颜色信息,通过对比各个组件之间的颜色相似性,对组件进行分组,从而提取出前景物体.这样做有两个好处:第一是可以摒弃传统的Matting问题解决方法中利用Trimap图进行半监督学习的过程,而是... 将组件的颜色信息引入谱方法Matting中,利用组件颜色信息,通过对比各个组件之间的颜色相似性,对组件进行分组,从而提取出前景物体.这样做有两个好处:第一是可以摒弃传统的Matting问题解决方法中利用Trimap图进行半监督学习的过程,而是利用颜色相似性信息作为约束条件或者启发式信息应用到无监督的学习过程中,降低了自动提取前景物体的盲目性.第二是获得颜色相似性信息后只需要再结合很少的前、背景提示信息,就可以使得无法确定为前景还是背景的组件进一步减少,从而完成一个半监督的学习过程,而不用像传统方法那样引入大量的用户操作才能完成半监督的学习过程. 展开更多
关键词 谱方法 matting 颜色直方图 无监督学习 半监督学习
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Comparison of the local pivotal method and systematic sampling for national forest inventories 被引量:1
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作者 Minna Räty Mikko Kuronen +3 位作者 Mari Myllymäki Annika Kangas Kai Mäkisara Juha Heikkinen 《Forest Ecosystems》 SCIE CSCD 2020年第4期716-732,共17页
Background:The local pivotal method(LPM)utilizing auxiliary data in sample selection has recently been proposed as a sampling method for national forest inventories(NFIs).Its performance compared to simple random samp... Background:The local pivotal method(LPM)utilizing auxiliary data in sample selection has recently been proposed as a sampling method for national forest inventories(NFIs).Its performance compared to simple random sampling(SRS)and LPM with geographical coordinates has produced promising results in simulation studies.In this simulation study we compared all these sampling methods to systematic sampling.The LPM samples were selected solely using the coordinates(LPMxy)or,in addition to that,auxiliary remote sensing-based forest variables(RS variables).We utilized field measurement data(NFI-field)and Multi-Source NFI(MS-NFI)maps as target data,and independent MS-NFI maps as auxiliary data.The designs were compared using relative efficiency(RE);a ratio of mean squared errors of the reference sampling design against the studied design.Applying a method in NFI also requires a proven estimator for the variance.Therefore,three different variance estimators were evaluated against the empirical variance of replications:1)an estimator corresponding to SRS;2)a Grafström-Schelin estimator repurposed for LPM;and 3)a Matérn estimator applied in the Finnish NFI for systematic sampling design.Results:The LPMxy was nearly comparable with the systematic design for the most target variables.The REs of the LPM designs utilizing auxiliary data compared to the systematic design varied between 0.74–1.18,according to the studied target variable.The SRS estimator for variance was expectedly the most biased and conservative estimator.Similarly,the Grafström-Schelin estimator gave overestimates in the case of LPMxy.When the RS variables were utilized as auxiliary data,the Grafström-Schelin estimates tended to underestimate the empirical variance.In systematic sampling the Matérn and Grafström-Schelin estimators performed for practical purposes equally.Conclusions:LPM optimized for a specific variable tended to be more efficient than systematic sampling,but all of the considered LPM designs were less efficient than the systematic sampling design for some target variables.The Grafström-Schelin estimator could be used as such with LPMxy or instead of the Matérn estimator in systematic sampling.Further studies of the variance estimators are needed if other auxiliary variables are to be used in LPM. 展开更多
关键词 Auxiliary data Bias Local pivotal method matérn estimator National forest inventory Sampling efficiency Simple random sampling Spatially balanced sampling Systematic sampling Variance
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Numerical analysis of the stability and minimum required strength of sill mats considering creep behavior of rock mass
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作者 Chuan Fan Li Li +4 位作者 Guangsheng Liu Xiaocong Yang Weidong Song Lijie Guo Ruofan Wang 《International Journal of Minerals,Metallurgy and Materials》 2025年第7期1471-1482,共12页
The underhand cut-and-fill mining method is widely employed in underground mines,especially when the quality of surrounding rock mass or ore body is inferior or subjected to high stresses.Such a method typically requi... The underhand cut-and-fill mining method is widely employed in underground mines,especially when the quality of surrounding rock mass or ore body is inferior or subjected to high stresses.Such a method typically requires the construction of sill mats with cemented backfill to provide operators with safe artificial roofs.Accurate estimation of the minimum required strength of the sill mat is crucial to minimize binder consumption and ensure its stability upon base exposure.Over the years,only a few publications were devoted to determining the minimum required cohesion(cmin)of sill mats.None of them considered rock wall closure to be associated with the creep of surrounding rock mass.Moreover,the effect of rock wall closure associated with rock creep on the cminof the sill mat remains unknown.Thus,a series of numerical simulations was performed to fill this gap.The influence of rock creep on the cminof base-exposed sill mat was investigated for the first time.The numerical results indicate that Mitchell’s models could be suitable for sill mats subjected to negligible wall closure.However,this scenario is rare,especially when mine depth is large.In general,the cminof sill mats increases as mine depth increases.Neglecting rock creep would significantly underestimate the cminof sill mats.When mine depth is large and the rock mass exhibits severe creep,cemented backfill with ductile behavior(i.e.,with low stiffness but enough strength)should be considered to reduce binder consumption and prevent crushing failure.In all cases,promptly filling the mined-out stope below the sill mat can improve its stability and reduce its cminvalue. 展开更多
关键词 underhand cut-and-fill mining method sill mat cemented backfill rock creep wall closure FLAC3D
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线性方程组的迭代解法及其Matlab实现程序 被引量:1
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作者 花威 《长江工程职业技术学院学报》 CAS 2009年第4期85-87,共3页
介绍了求解线性方程组的迭代法的基本思想和两种常见迭代方法,推论出迭代的收敛条件,并且用Matlab软件编制出迭代法的实现程序。
关键词 线性方程组 迭代法 matLAB软件
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联合时间反演与代数迭代的感应式磁声成像重建
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作者 窦靓玉 周海龙 商博 《通信与信息技术》 2026年第1期25-30,共6页
感应式磁声成像(Magneto-Acoustic Tomography with Magnetic Induction,MAT-MI)是具备高对比度与高空间分辨率优势的多物理场耦合的新型成像技术,但其逆问题,即重建过程中存在的弧状伪影、噪声敏感干扰限制了成像精度。为此,本文提出... 感应式磁声成像(Magneto-Acoustic Tomography with Magnetic Induction,MAT-MI)是具备高对比度与高空间分辨率优势的多物理场耦合的新型成像技术,但其逆问题,即重建过程中存在的弧状伪影、噪声敏感干扰限制了成像精度。为此,本文提出一种时间反演-代数迭代(Algebraic Reconstruction Technique,ART)融合重建算法,通过结合声波传播的物理聚焦机制与正则化数值优化,以声学均匀生物组织模型为研究对象,通过仿真计算得到声压分布,结合时间反演-代数迭代融合重建算法实现声源图像重建。仿真实验表明,本文提出的重建算法能准确有效地重建出声学均匀介质中的声源图像,研究结果对磁声成像实验设计和后续研究提供研究基础。 展开更多
关键词 mat-MI 时间反演 代数迭代 图像重建
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Closed-Form Solutions of Stress Intensity Factors for Semi-elliptical Surface Cracks in a Cylindrical Bar Under Pure Tension
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作者 M.K.Ramezani S.Ramesh +1 位作者 J.Purbolaksono R.Das 《Acta Mechanica Solida Sinica》 SCIE EI CSCD 2022年第2期344-356,共13页
In this work,the stress intensity factors(SIFs)for a wide range of semi-elliptical surface cracks with different inclination angles in a cylindrical bar subjected to pure tension were investigated numerically.The main... In this work,the stress intensity factors(SIFs)for a wide range of semi-elliptical surface cracks with different inclination angles in a cylindrical bar subjected to pure tension were investigated numerically.The main parameters considered to evaluate the SIFs were the crack size ratio(a/d),the crack aspect ratio(a/c),and the crack inclination angle(0).The dual-boundary element met hod implemented in software BEASY was used to compute the SIF values for cracks.Furt her more,the general closed-form solutions were proposed to evaluate the corresponding SIFs for Mode I,Mode II and Mode III types of fracture through curve fitting approaches.These solutions can provide accurate and reliable values of stress intensity factors for a crack on a cylindrical bar under pure tension in a rapid way compared to those obtained using computational models.In addition,these results can be used as inputs for failure studies and life evaluations of cracked cylinder under working conditions. 展开更多
关键词 Stress intensity factor Surface crack Solid cylinder closed-form solution Dual-boundary element method
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Closed-form internal impedance model and characterization of mixed carbon nanotube bundles for three-dimensional integrated circuits
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作者 卢启军 朱樟明 +2 位作者 杨银堂 丁瑞雪 李跃进 《Chinese Physics B》 SCIE EI CAS CSCD 2018年第1期520-525,共6页
Based on the complex effective conductivity method, a closed-form expression for the internal impedance of mixed carbon nanotube (CNT) bundles, in which the number of CNTs for a given diameter follows a Gaussian dis... Based on the complex effective conductivity method, a closed-form expression for the internal impedance of mixed carbon nanotube (CNT) bundles, in which the number of CNTs for a given diameter follows a Gaussian distribution, is proposed in this paper. It can appropriately capture the skin effect as well as the temperature effect of mixed CNT bundles. The results of the closed-form expression and the numerical calculation are compared with various mean diameters, standard deviations, and temperatures. It is shown that the proposed model has very high accuracy in the whole frequency range considered, with maximum errors of 1% and 2.3% for the resistance and the internal inductance, respectively. Moreover, by using the proposed model, the high-frequency electrical characteristics of mixed CNT bundles are deeply analyzed to provide helpful design guidelines for their application in future high-performance three-dimensional integrated circuits. 展开更多
关键词 mixed carbon nanotube (CNT) bundle internal impedance closed-form expression complex ef-fective conductivity method
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New structures for closed-form wave solutions for the dynamical equations model related to the ion sound and Langmuir waves
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作者 Md Nur Alam M S Osman 《Communications in Theoretical Physics》 SCIE CAS CSCD 2021年第3期1-13,共13页
This treatise analyzes the coupled nonlinear system of the model for the ion sound and Langmuir waves.The modified(G'/G)-expansion procedure is utilized to raise new closed-form wave solutions.Those solutions are ... This treatise analyzes the coupled nonlinear system of the model for the ion sound and Langmuir waves.The modified(G'/G)-expansion procedure is utilized to raise new closed-form wave solutions.Those solutions are investigated through hyperbolic,trigonometric and rational function.The graphical design makes the dynamics of the equations noticeable.It provides the mathematical foundation in diverse sectors of underwater acoustics,electromagnetic wave propagation,design of specific optoelectronic devices and physics quantum mechanics.Herein,we concluded that the studied approach is advanced,meaningful and significant in implementing many solutions of several nonlinear partial differential equations occurring in applied sciences. 展开更多
关键词 the modified(G'/G)-expansion method ion sound wave Langmuir wave closed-form wave solutions
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基于热压法制备环保型防潮软木地垫的优化研究
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作者 周文娟 吴昊 《佳木斯大学学报(自然科学版)》 2025年第12期171-173,4,共4页
随着室内装饰对环保建材需求攀升,软木地垫因多孔结构引发的吸湿问题与传统化学处理带来的污染隐患亟待解决。为开发兼具高防潮性与环保性的软木地垫创新制备体系,研究采用物理热压成型工艺,以可再生栓皮栎软木颗粒为基材,搭配复配胶粘... 随着室内装饰对环保建材需求攀升,软木地垫因多孔结构引发的吸湿问题与传统化学处理带来的污染隐患亟待解决。为开发兼具高防潮性与环保性的软木地垫创新制备体系,研究采用物理热压成型工艺,以可再生栓皮栎软木颗粒为基材,搭配复配胶粘剂构建环保材料体系,并通过双层复合结构与正交实验优化热压参数。实验显示,150℃/10 MPa/15 min工艺组合下,地垫密度较传统溶剂型地垫提升31.0%,回弹率增加2.7%,尺寸稳定性改进77.8%。且24 h吸水率仅3.5%,40次湿热循环后膨胀率为1.7%。结果表明,该研究实现了软木地垫环保性与防潮性的突破,为室内装饰领域提供了绿色、耐用的建材选择,推动了建材行业的环保可持续发展。 展开更多
关键词 热压法 软木地垫 防潮性能 环保材料 工艺优化
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小孔节流空气静压轴承设计与性能分析 被引量:1
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作者 仇德中 雷卫宁 薛亚平 《机械强度》 北大核心 2025年第11期42-50,共9页
针对单节流孔空气静压轴承的性能,深入研究了其设计参数对承载力和刚度的影响,旨在优化空气静压轴承的结构设计和性能表现。采用有限元方法对单节流孔空气静压轴承进行参数化建模,分析了气腔设计、节流孔直径、供气压力、气膜厚度、节... 针对单节流孔空气静压轴承的性能,深入研究了其设计参数对承载力和刚度的影响,旨在优化空气静压轴承的结构设计和性能表现。采用有限元方法对单节流孔空气静压轴承进行参数化建模,分析了气腔设计、节流孔直径、供气压力、气膜厚度、节流孔深度、气腔厚度、气腔直径等因素对轴承性能的影响。将仿真模拟与试验平台测试结合,验证了各设计参数对轴承性能的影响规律。研究表明,节流孔直径、气膜厚度、供气压力和气腔直径等参数对轴承的承载力具有显著影响,而节流孔深度和气腔厚度对承载力的影响较小。节流孔直径、供气压力、气腔直径和气腔厚度与承载力成正相关,而气膜厚度、节流孔深度等参数与承载力成负相关。此外,具有气腔结构的空气静压轴承在承载力和刚度方面远超无气腔结构的轴承。仿真结果与试验数据的一致性良好,验证了所建仿真模型的可靠性与准确性。 展开更多
关键词 小孔节流 气浮垫 有限元方法 承载能力 刚度
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玻璃纤维增强二氧化硅气凝胶毡的低成本制备及性能
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作者 薛子航 蹇思豪 +5 位作者 韩敏航 李波 郝瑞鑫 马超 苗洋 高峰 《应用化学》 北大核心 2025年第10期1361-1374,共14页
二氧化硅气凝胶因其独特的三维网状结构而具备优异的隔热性能、低密度等优势,受到广泛关注。然而,其力学性能差、易碎裂,以及传统制备工艺流程复杂、周期长和成本高的问题限制了其大规模应用。本文以廉价的水玻璃为硅源、玻璃纤维为增... 二氧化硅气凝胶因其独特的三维网状结构而具备优异的隔热性能、低密度等优势,受到广泛关注。然而,其力学性能差、易碎裂,以及传统制备工艺流程复杂、周期长和成本高的问题限制了其大规模应用。本文以廉价的水玻璃为硅源、玻璃纤维为增强材料,通过溶胶-凝胶法和常压干燥工艺制备玻璃纤维增强的二氧化硅气凝胶复合毡。探讨了老化时间、去离子水用量和浸泡时间、三甲基氯硅烷用量和改性时间对玻璃纤维增强二氧化硅气凝胶复合材料性能的影响。在老化时间为10 h,去离子水用量为200 mL,浸泡2次,时间设置为(24+12) h,三甲基氯硅烷用量为18 mL,改性时间为60 h时,所制备的二氧化硅气凝胶毡比表面积达776.38 m2/g,密度为0.228 g/cm3,导热系数为0.0218 W/(m·K),抗压强度为2.4 MPa,抗拉强度为0.5 MPa。该材料还表现出良好的高温稳定性和疏水性,疏水角为141.5(°),为其在隔热领域的工业化应用提供了新的实践方向。 展开更多
关键词 SiO2气凝胶毡 玻璃纤维 隔热性能 溶胶-凝胶法 常压干燥
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两种隔断的石笼网垫单元体冲刷数值模拟研究
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作者 王迪 周成 +2 位作者 黄良誉 何宁 钟启明 《水道港口》 2025年第1期87-95,共9页
石笼网垫生态护岸因其良好的整体性、透水性、耐腐蚀性、抗冲刷性和环境适应性,被广泛应用于我国河道岸坡治理中,但是传统石笼网垫是用网片作为隔断,需耗费大量人力绑扎和填石料,施工困难。为此,研发设计了新型石笼网垫,将传统的网片隔... 石笼网垫生态护岸因其良好的整体性、透水性、耐腐蚀性、抗冲刷性和环境适应性,被广泛应用于我国河道岸坡治理中,但是传统石笼网垫是用网片作为隔断,需耗费大量人力绑扎和填石料,施工困难。为此,研发设计了新型石笼网垫,将传统的网片隔断替换为胶结碎石格构隔断,这样碎石填料和隔断可以一起碾压,能极大提高施工效率。为了探究新型石笼网垫的抗冲蚀性,利用CFD_DEM耦合分析软件,开展了石笼网垫单元体的冲刷数值模拟研究,探究传统与新型石笼网垫单元体的逊径流失累积量随冲刷时间的变化规律,并得出流失的逊径颗粒在冲刷流失过程中的运动轨迹线及其在流失过程中的流速,同时进一步开展了探究不同冲刷流速、岸坡倾角下新型石笼网垫单元体抗冲刷效果的数值模拟。研究结果为推广新型石笼网垫护岸结构的设计与施工提供参考。 展开更多
关键词 生态护岸 石笼网垫 单元体冲刷 数值模拟 离散元 EDEM模型
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系列无光釉的研制 被引量:11
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作者 沈华荣 洪琛 +1 位作者 曹春娥 陈云霞 《陶瓷学报》 CAS 北大核心 2009年第4期511-515,共5页
通过对光泽度、白度及抗热震稳定性等多种性能的测试分析,探讨了硅铝比、无光剂种类、釉料细度及冷却方式对无光釉釉面质量的影响,并确定了其最佳配方和制备工艺。结果表明:钙质、镁质的最佳SiO2/Al2O3范围分别为4~6、5,钡质、复合无... 通过对光泽度、白度及抗热震稳定性等多种性能的测试分析,探讨了硅铝比、无光剂种类、釉料细度及冷却方式对无光釉釉面质量的影响,并确定了其最佳配方和制备工艺。结果表明:钙质、镁质的最佳SiO2/Al2O3范围分别为4~6、5,钡质、复合无光釉的最佳SiO2/Al2O3为5,锌质的最佳SiO2/Al2O3范围为4~9;在高温阶段适当保温和缓慢冷却所得样品效果较好。 展开更多
关键词 无光釉 无光剂 硅铝比 冷却方式
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后处理在数字抠像中的应用与解析 被引量:4
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作者 姚桂林 刘绍辉 +2 位作者 李敏 姚鸿勋 胡文 《电子学报》 EI CAS CSCD 北大核心 2017年第3期719-729,共11页
数字抠像是将一幅图像中的前景物体与背景进行分离的问题,它的关键在于Alpha通道的计算.以往通过采样方法求得的Alpha中,由于采用逐点计算的离散化方式,求解出的Alpha通常不连续,并且包含很多噪声,因而需要对Alpha进行后处理,这不仅会增... 数字抠像是将一幅图像中的前景物体与背景进行分离的问题,它的关键在于Alpha通道的计算.以往通过采样方法求得的Alpha中,由于采用逐点计算的离散化方式,求解出的Alpha通常不连续,并且包含很多噪声,因而需要对Alpha进行后处理,这不仅会增强Alpha在视觉上的平滑性,而且能够进一步提高Alpha的精确度.在目前国际上,有关数字抠像后处理领域已经进行了许多研究,但缺少相关的综述性文献,并且对后处理后的Alpha如何进行定量的评价也仍未系统解决.本文首先将数字抠像中的后处理方法分为2类:与仿射类方法相结合的方式及自平滑方式,其次,对两类方法进行了全面的总结和梳理,并对方法的优缺点进行了分析,对将来研究方向提出了建议,最后,针对后处理后的Alpha结果进行了全面的量化比较,弥补了传统方法基本上仅在视觉层面上进行比较的缺陷. 展开更多
关键词 图像分割 图像抠像 后处理 Laplacian抠像矩阵 Nonlocal方法 自平滑
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高温环境样品总DNA直接和间接提取方法的比较 被引量:7
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作者 刘宏伟 彭谦 +11 位作者 李沁元 肖炜 崔晓龙 林连兵 刘志坚 姜成林 徐丽华 陈义光 王治刚 任禛 邓岚 文孟良 《微生物学报》 CAS CSCD 北大核心 2006年第6期1018-1022,共5页
分别采用两种环境总DNA直接提取法和一种间接提取法从6种温泉菌席样品中提取总DNA,以DNA粗产物的纯度、能否用于后续PCR扩增及PCR-DGGE(变性梯度凝胶电泳)所反映的微生物多样性为评价指标对两类方法进行比较和评价。研究发现,虽然间接... 分别采用两种环境总DNA直接提取法和一种间接提取法从6种温泉菌席样品中提取总DNA,以DNA粗产物的纯度、能否用于后续PCR扩增及PCR-DGGE(变性梯度凝胶电泳)所反映的微生物多样性为评价指标对两类方法进行比较和评价。研究发现,虽然间接提取法效率低下,但对于高温极端环境中生物量较小的样品,间接法能得到有研究价值的、纯度较高的环境样品总DNA,而直接法得到的DNA量小且不适于PCR扩增操作。在使用这2类方法都能得到可用于研究操作的DNA的情况下,间接提取法能更好的体现环境样品中微生物的多样性。 展开更多
关键词 菌席 环境DNA 间接DNA提取法 PCR—DGGE
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二氧化硅消光剂的合成与表征 被引量:6
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作者 孔庆刚 钱海燕 +5 位作者 孙兴菊 董婷 刘凯 章翔宇 李俊 高桂枝 《中国粉体技术》 CAS 北大核心 2012年第2期50-54,共5页
为了获得性能指标符合消光剂要求的二氧化硅产品,通过正交实验L16(45)对沉淀法合成二氧化硅的过程进行优化,研究各因素对二氧化硅中位径、吸油值的影响规律,利用X射线衍射、扫描电镜对二氧化硅粒子的结构、形貌进行表征。结果表明,制备... 为了获得性能指标符合消光剂要求的二氧化硅产品,通过正交实验L16(45)对沉淀法合成二氧化硅的过程进行优化,研究各因素对二氧化硅中位径、吸油值的影响规律,利用X射线衍射、扫描电镜对二氧化硅粒子的结构、形貌进行表征。结果表明,制备的二氧化硅为无定形产物,颗粒呈球形,一次颗粒粒径约为30 nm,各项指标与进口产品相近。 展开更多
关键词 液相沉淀法 二氧化硅消光剂 合成 表征
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球状纳米二氧化钛/石墨烯复合材料的合成及导电性能 被引量:7
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作者 刘琳 李莹 +4 位作者 鄂涛 杨姝宜 姜志刚 许丽岩 张天琪 《材料工程》 EI CAS CSCD 北大核心 2019年第8期97-102,共6页
采用改进的水热法制备二氧化钛/石墨烯(TiO2/G)复合导电材料,并研究水热温度以及石墨烯用量对TiO2/G复合材料导电性的影响。利用傅里叶变换红外(FTIR)光谱、X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)和电化学阻抗谱等测试手段对复... 采用改进的水热法制备二氧化钛/石墨烯(TiO2/G)复合导电材料,并研究水热温度以及石墨烯用量对TiO2/G复合材料导电性的影响。利用傅里叶变换红外(FTIR)光谱、X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)和电化学阻抗谱等测试手段对复合材料的结构,微观形貌以及导电性能进行表征,并确定最佳的水热温度以及石墨烯的最佳添加量。结果表明:石墨烯添加量为5%(质量分数),水热温度为160℃,TiO2/G复合材料的导电性最佳,其电阻率为13.46Ω·cm。复合材料中TiO2纳米颗粒为球状的锐钛矿相,直径为100~200nm左右,且均匀生长在石墨烯片层表面。其中,TiO2纳米颗粒生长于石墨烯片层上,有效地阻止石墨烯片层的聚集,有利于石墨烯片层间形成导电网络,提高电子迁移效率,赋予二氧化钛复合材料优异的导电性能。 展开更多
关键词 石墨烯 二氧化钛 导电性 水热法 复合导电材料
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沉淀二氧化硅消光剂的制备研究 被引量:5
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作者 玉显恒 李婧 +1 位作者 李蓉 李立新 《化学研究与应用》 CAS CSCD 北大核心 2007年第10期1134-1137,共4页
The precipitated silica matting agent was synthesized by chem-deposit method,sodium silicate and sulfurric acid as raw materials,appending dispersant and surfactant.The optimal parameters for the required precipitated... The precipitated silica matting agent was synthesized by chem-deposit method,sodium silicate and sulfurric acid as raw materials,appending dispersant and surfactant.The optimal parameters for the required precipitated silica with excellent properties are temperature 70~85℃,pH value 9,reaction liquid mass concentration 20%,the calcined temperature between 450~480℃.The result shows that the prepared precipitated silica pore volume is 1.0~1.3cm3/g,the partical size is smaller than 10um,D50 approximately 5um.The surface area is 320~430m2/g,the pore size is between 147~388. 展开更多
关键词 化学沉淀法 二氧化硅 消光剂 工艺条件
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