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Dynamics Analysis of Close-coupling Multiple Helicopters System 被引量:9
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作者 赵志刚 吕恬生 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2008年第1期71-78,共8页
The particularity and practicality of harmony operations of close-coupling multiple helicopters indicate that the researches on it are urgent and necessary, Using the model that describes two hovering helicopters carr... The particularity and practicality of harmony operations of close-coupling multiple helicopters indicate that the researches on it are urgent and necessary, Using the model that describes two hovering helicopters carrying one heavy load, an inertia coordinate system and body coordinate systems of each sub-system are established. A nonlinear force model is established too. The equilibrium computation results can be regarded as the reference control inputs of the flight control system under hovering or low-speed flight condition. After the establishment of a translation kinematics model and a posture kinematics model, a coupling dynamics model of the multiple helicopter system is set up. The results can also be regarded as the base to analyze stabilization and design a controller for a close-coupling multiple helicopters harmony operation system. 展开更多
关键词 close-coupling multiple helicopters harmony operation equilibrium computation kinematics analysis dynamics analysis
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A novel optimization method for dynamic response analysis of HSERs via a field-circuit coupling mathematical model 被引量:1
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作者 Jiaxin YOU Xiangqian CUI +2 位作者 Xu CHEN Ding DING Guofu ZHAI 《Chinese Journal of Aeronautics》 2025年第7期467-478,共12页
In the aerospace sector,the soft magnetic materials of Hermetically Sealed Electromagnetic Relays(HSERs)are critical in forming magnetic circuits.Conventional soft magnetic materials,primarily magnetic iron,have been ... In the aerospace sector,the soft magnetic materials of Hermetically Sealed Electromagnetic Relays(HSERs)are critical in forming magnetic circuits.Conventional soft magnetic materials,primarily magnetic iron,have been unable to meet the development trend of fast-response,miniaturized,and lightweight aerospace and aviation systems.This paper applies circuit theory and electromagnetics theory to establish a Field-Circuit Coupling Mathematical Model(FCCMM)for dynamic response analysis of HSERs.This model centers on inductance calculation,with the core's permeability and saturation magnetic flux density as critical parameters.Based on this model,for a specific type of HSER,this paper introduced three alloys with key parameters different from magnetic iron,then tested the magnetic characteristic curves of these four soft magnetic materials,followed by simulations to obtain the electromagnetic characteristics of digital mock-ups corresponding to these four materials,compared and validated the dynamic responses corresponding to these four soft magnetic materials finally.Based on the theoretical model analysis results,this paper designed a lightweight coil to minimize response time,made prototypes,set up test systems,and tested dynamic characteristics.The experimental results indicate that the nanocrystalline alloy1K107B exhibits the most significant optimization,reducing the closing time by 40.48%and achieving a weight reduction of 6.53%. 展开更多
关键词 Field-circuit coupling Dynamic response Hermetically Sealed Electromagnetic Relay(HSER) Soft magnetic materials Inductance calculation Closing time
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Novel Closed-Form Solution for Analyzing Mutual Coupling Between Cylindrical Comformal Rectangular Microstrip Patch Antennas
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作者 何芒 徐晓文 《Journal of Beijing Institute of Technology》 EI CAS 2003年第2期129-133,共5页
Based on the integral equation formulations and the moment method, a novel closed form solution for analyzing the mutual coupling effect between the cylindrical comformal rectangular microstrip patch antennas is pres... Based on the integral equation formulations and the moment method, a novel closed form solution for analyzing the mutual coupling effect between the cylindrical comformal rectangular microstrip patch antennas is presented. By using this algorithm, the elements of the impedance matrix and exciting vector are cast into closed forms, thus the computational efficiency is improved dramatically. Numerical results are presented to verify the validity and reliability of the algorithm. 展开更多
关键词 conformal microstrip antenna mutual coupling moment method closed form solution
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Close coupling calculations for excitation partial cross sections in Ne-HF collisions
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作者 余春日 《Chinese Physics B》 SCIE EI CAS CSCD 2008年第6期2097-2102,共6页
This paper reports that an exact quantum close coupling calculation is carried out for rotational excitation in Ne HF collisions on the available anisotropic potential. Partial cross sections are obtained separately a... This paper reports that an exact quantum close coupling calculation is carried out for rotational excitation in Ne HF collisions on the available anisotropic potential. Partial cross sections are obtained separately at the incident energies of 48.35, 75, 120 and 150meV. The reliability of the results is demonstrated by comparison with previously published theoretical findings. Based on the calculations, the effect of the potential energy surface on the excitation partial cross sections is discussed in detail. 展开更多
关键词 close coupling calculation excitation partial cross section Ne HF collision
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The determination of 52 elements in marine geological samples by an inductively coupled plasma optical emission spectrometry and an inductively coupled plasma mass spectrometry with a high-pressure closed digestion method 被引量:16
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作者 GAO Jingjing LIU Jihua +3 位作者 LI Xianguo YAN Quanshu WANG Xiaojing WANG Hongmin 《Acta Oceanologica Sinica》 SCIE CAS CSCD 2017年第1期109-117,共9页
An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method(HPCD), is stud... An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method(HPCD), is studied by an inductively coupled plasma optical emission spectrometry(ICP-OES) and an inductively coupled plasma mass spectrometry(ICP-MS). The operating parameters of the instruments are optimized, and the optimal analytical parameters are determined. The influences of optical spectrum and mass spectrum interferences, digestion methods and acid systems on the analytical results are investigated. The optimal spectral lines and isotopes are chosen, and internal standard element of rhodium is selected to compensate for matrix effects and analytical signals drifting. Compared with the methods of an electric heating plate digestion and a microwave digestion, a high-pressure closed digestion method is optimized with less acid, complete digestion,less damage for digestion process. The marine geological samples are dissolved completely by a HF-HCl-HNO_3 system, the relative error(RE) for the analytical results are all less than 6.0%. The method detection limits are 2–40μg/g by the ICP-OES, and 6–80 ng/g by ICP-MS. The methods are used to determine the marine sediment reference materials(GBW07309, GBW07311, GBW07313), rock reference materials(GBW07103, GBW07104,GBW07105), and cobalt-rich crust reference materials(GBW07337, GBW07338, GBW07339), the obtained analytical results are in agreement with the certified values, and both of the relative standard deviation(RSD) and the relative error(RE) are less than 6.0%. The analytical method meets the requirements for determining 52 elements contents of bulk marine geological samples. 展开更多
关键词 marine geological sample high-pressure closed digestion method inductively coupled plasma optical emission spectrometry inductively coupled plasma mass spectrometry major element minor element trace element
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Influence of melt superheat on breakup process of close-coupled gas atomization 被引量:3
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作者 欧阳鸿武 陈欣 黄伯云 《中国有色金属学会会刊:英文版》 EI CSCD 2007年第5期967-973,共7页
In close-coupled gas atomization(CCGA), the influences of melt superheat on breakup process are fundamental to obtain desired or finer powder. Based on a series of Cu atomization experiment under different superheatin... In close-coupled gas atomization(CCGA), the influences of melt superheat on breakup process are fundamental to obtain desired or finer powder. Based on a series of Cu atomization experiment under different superheating conditions, the influences of melt superheat on breakup process were studied. Experimental results indicate that as the melt superheat is increased to 150, 200, 250 and 300 K, the mean particle size (D50) decreases consequently to 34.9, 32.3, 30.9 and 19.7 μm. Theoretical analysis reveals that the primary breakup and secondary breakup processes are close coupled, and the melt superheat radically influences the melt properties, and plays a crucial role on governing the filming process of primary breakup and the atomization modes of secondary breakup. There exists a strong nonlinear decrease of contact angle of melt to nozzle orifice wall when the superheat is increased from 250 K to 300 K, leading to a marked fall of the film thickness formed in primary breakup, and D50 of copper powders is therefore sharply reduced. However, the log-normal distribution feature of particle size has not been substantially improved. 展开更多
关键词 气体雾化 耦合 喷嘴 颗粒尺寸 金属融化
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Melt metal sheet breaking mechanism of close-coupled gas atomization 被引量:2
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作者 欧阳鸿武 黄伯云 +1 位作者 陈欣 余文焘 《中国有色金属学会会刊:英文版》 EI CSCD 2005年第5期985-992,共8页
The gas atomization is the process that a liquid mass is disintegrated into a collection of liquid melt droplets by the impact of high velocity gas stream and solidified into metal particles. However, the liquid melt ... The gas atomization is the process that a liquid mass is disintegrated into a collection of liquid melt droplets by the impact of high velocity gas stream and solidified into metal particles. However, the liquid melt sheet breaking mechanism has not been fully understood. So the experimental research was carried out under the condition of lower melt superheat. The results reveal that there are three approaches about melt metal sheet’s breakage: from the edges of sheets, from inner surface of sheets, and disrupted by other droplets and sheets. The approach of melt sheet breakage is dependent on its thickness. The thicker sheets (above 25μm) are disintegrated mainly by the way of droplet’s departing from edges, and the thinner sheets (below 10μm) are chiefly breaking from the inner surface. 展开更多
关键词 粉末冶金 流动结构 气压雾化 过热处理
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Pd Close Coupled Catalyst
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作者 Zhong Hua SHI Mao Chu GONG Yao Qiang CHEN 《Chinese Chemical Letters》 SCIE CAS CSCD 2006年第9期1271-1274,共4页
A catalyst comprised novel high surface area alumina support was prepared to control emission of automobiles. The results showed that prepared catalyst could satisfy the requirements of a high performance close couple... A catalyst comprised novel high surface area alumina support was prepared to control emission of automobiles. The results showed that prepared catalyst could satisfy the requirements of a high performance close coupled catalyst for its good catalytic activity at low temperature and good stability at high temperature. 展开更多
关键词 close coupled catalyst cold start high surface area support exhaust gas.
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Effect of high temperature pretreatment on the thermal resistance properties of Pd/CeO2/Al2O3 close-coupled catalysts 被引量:3
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作者 黄木兰 王苏宁 +3 位作者 兰丽 张海龙 史忠华 陈耀强 《Journal of Rare Earths》 SCIE EI CAS CSCD 2017年第2期149-157,共9页
Fresh Pd/CeO/AlOclose coupled catalyst was prepared by the stepwise impregnation method and calcined at 550 °C for 3 h, which was then pretreated at 700, 800, and 900 °C for 3 h, respectively. Finally, these... Fresh Pd/CeO/AlOclose coupled catalyst was prepared by the stepwise impregnation method and calcined at 550 °C for 3 h, which was then pretreated at 700, 800, and 900 °C for 3 h, respectively. Finally, these pretreated catalysts were aged at 1000 °C for 3 h to study their anti-aging properties. The catalytic activities of the catalysts were investigated detailedly, and the results showed that the catalyst pretreated at 800 °C before aging treatment possessed the best anti-aging performance for CHoxidation. XRD and XPS results indicated that well-crystallized CeOparticles were formed during calcinations at 800 °C, which made CeOan effective promoter. HRTEM revealed that Pd particles found on the edge of CeOover the aged catalyst pretreated at 800 °C were relatively smaller than those over the catalysts without pretreatment. H-TPR and XPS results also implied that the interaction between well-crystallized CeOand Pd suppressed the deactivation of PdO sites and further enhanced the catalytic performance. 展开更多
关键词 pretreatment temperature C_3H_8 oxidation anti-aging properties close-coupled catalyst rare earths
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Close Coupled Showerhead Reactors for the Growth of Group Ⅲ Nitrides
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作者 Thrush E J Kappers M +5 位作者 Considine L Mullins J T Saywell V Bentham F C Sharma N Humphreys C J 《发光学报》 EI CAS CSCD 北大核心 2001年第z1期103-106,共4页
The group Ⅲ nitrides are an important class of materials with aplications in UV and visible optoelectronics,high temperature electronics,cold cathodes and solar blind detectors.In recent years,with the realisation of... The group Ⅲ nitrides are an important class of materials with aplications in UV and visible optoelectronics,high temperature electronics,cold cathodes and solar blind detectors.In recent years,with the realisation of nitride based LEDs,the use of GaN IED has the potential to compete with 1raditional filament and discharge lamps,for the provision of white lighting,and there has been an explosion of interest in the MOCVD growth of GaN based materials with an increasing focus on large area multiwafer reactors and wafer uniforrmity.This paper will review the design philosophy and characteristics of close-coupled showerhead reactors,relating these to the requirements of group Ⅲ-nitride growth,and will present a selection of data resulting from the operation of such equipment.These results suggest that the close coupled showerhead style of reactor is very suitable for the growth of GaN based structures in both research and production environments. 展开更多
关键词 MOCVD close coupled showerhead reactor growth of groupⅢnitrides
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基于ANSYS的摆动轴漂移热误差消减设计研究
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作者 杨红军 李清耀 慕道增 《机床与液压》 北大核心 2026年第1期56-61,共6页
为解决五轴加工中心摆动回转轴因热变形引起的定位漂移问题,通过热误差分析与结构优化提升轴系精度稳定性。通过多种工况测试及ANSYS热-结构耦合有限元分析,确定定位漂移的根源在于冷却介质温度变化引起主轴周期性热变形。通过约束热变... 为解决五轴加工中心摆动回转轴因热变形引起的定位漂移问题,通过热误差分析与结构优化提升轴系精度稳定性。通过多种工况测试及ANSYS热-结构耦合有限元分析,确定定位漂移的根源在于冷却介质温度变化引起主轴周期性热变形。通过约束热变形及降低系统热变形内应力,重新设计多种编码器支撑结构,并利用ANSYS对新结构的热误差和灵敏度进行仿真分析,并采用最优结构方案进行实际应用验证。新摆动回转轴精度采用验棒和动态采样两种方式检测,结果表明:新结构使热漂移量从5.4″降至0.18″;实际测试中最小进给单位0.0001°(0.36″)下轴系响应灵敏无超调。改进后的回转轴定位稳定、灵敏度优良,漂移热误差问题得到解决,验证了分析与改进设计的有效性。 展开更多
关键词 摆动回转轴 漂移热误差 闭环控制 灵敏度 热-结构耦合分析
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柴油机双SCR系统氨干扰DOC氧化性研究
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作者 刘如月 吕志华 +3 位作者 孙楠楠 王琛 闫彩彩 于姗姗 《内燃机学报》 北大核心 2026年第2期144-154,共11页
为研究柴油机双选择性还原(SCR)后处理系统中紧耦合SCR催化器氨泄漏在柴油氧化催化剂(DOC)中的反应和其对CO、HC和NO氧化的影响,基于Langmuir-Hinshelwood机理建立CO、C_(3)H_(6)、NO和NH_(3)在DOC中氧化转化的全局动力学模型,并通过13... 为研究柴油机双选择性还原(SCR)后处理系统中紧耦合SCR催化器氨泄漏在柴油氧化催化剂(DOC)中的反应和其对CO、HC和NO氧化的影响,基于Langmuir-Hinshelwood机理建立CO、C_(3)H_(6)、NO和NH_(3)在DOC中氧化转化的全局动力学模型,并通过13组不同组分和体积分数的试验边界对模型进行了校准,试验空速为120000 h^(-1),温度范围为120~500℃.再利用世界统一瞬态循环(WHTC)工况验证模型,模型氧化率仿真误差小于15%.试验和模拟均表明NH_(3)在DOC中氧化形成N_(2)O、NO和NO_(2)共3种污染物,且在入口有NO_(x)(包括NO和NO_(2))存在时产生了大量N_(2)O.另外,通过仿真发现,NH_(3)对CO、C_(3)H_(6)和NO的氧化均存在抑制作用,体积分数为50×10^(-6)的NH_(3)使CO和C_(3)H_(6)起燃温度分别升高9℃和57℃,350℃以下NO氧化为NO_(2)的体积分数约降低20%.明确了DOC中NH_(3)干扰行为,并为带紧耦合SCR的柴油机后处理系统设计提供DOC模型基础. 展开更多
关键词 柴油机 紧耦合选择性还原 氨泄漏 柴油氧化催化剂
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柴油机后处理ccSCR路线N_(2)O排放特性研究
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作者 殷雪梅 李顺红 +3 位作者 吕志华 马江丽 常仕英 于飞 《内燃机学报》 北大核心 2026年第1期58-67,共10页
为研究柴油机后处理紧耦合选择性催化还原(ccSCR)路线的一氧化二氮(N_(2)O)排放特性,研究了柴油机在世界统一瞬态循环(WHTC)、世界统一稳态循环(WHSC)和低负荷循环(LLC)下不同催化剂、不同尿素喷射量和电加热(EHC)对N_(2)O排放的影响.... 为研究柴油机后处理紧耦合选择性催化还原(ccSCR)路线的一氧化二氮(N_(2)O)排放特性,研究了柴油机在世界统一瞬态循环(WHTC)、世界统一稳态循环(WHSC)和低负荷循环(LLC)下不同催化剂、不同尿素喷射量和电加热(EHC)对N_(2)O排放的影响.结果表明:氨泄漏催化剂(ASC)对N_(2)O生成的分担率最大,高达50%;增加尿素喷射量利于降低ASC后NO_(x)排放,但增加ASC后NH_(3)和N_(2)O排放风险.WHTC、WHSC和LLC循环下开启EHC,尿素喷射量增加,ASC后NO_(x)排放下降、NH_(3)和N_(2)O排放增加;随EHC加热时间增加,ccSCR和SCR入口平均温度均提升,NO_(x)、NH3和N_(2)O排放降低;WHTC、WHSC和LLC循环下开启EHC,尿素喷射量增加是导致ASC后N_(2)O排放增加的主要原因.针对带EHC的ccSCR国Ⅶ后处理路线,建议优化尿素喷射策略并搭配低N_(2)O型ASC催化剂后处理系统,以实现降低NOx同时降低N_(2)O排放. 展开更多
关键词 柴油机 紧耦合选择性催化还原催化剂 尿素喷射量 氨泄漏催化剂 氨气排放 一氧化二氮排放
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制丝车间解包线智能照明系统的研究
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作者 卓亮 张伟 +5 位作者 郑义 何林洋 葛泽江 刘鹏 昝义涛 王海韵 《中国照明电器》 2026年第1期109-112,共4页
针对卷烟厂制丝车间解包线传统照明系统能耗高、传统照明控制系统与制丝车间生产线控制系统无法协同等问题,本研究提出基于PLC控制的三级闭环智能照明系统。通过构建“控制中枢-区域控制-现场执行”架构,融合区域状态耦合算法,实现解包... 针对卷烟厂制丝车间解包线传统照明系统能耗高、传统照明控制系统与制丝车间生产线控制系统无法协同等问题,本研究提出基于PLC控制的三级闭环智能照明系统。通过构建“控制中枢-区域控制-现场执行”架构,融合区域状态耦合算法,实现解包线照明系统与解包线生产流程深度耦合。工厂现场数据显示,解包线智能照明系统投用后解包线照明能耗降低48.5%,本文详细阐述系统设计、核心算法、工程实施及效益评估,为烟草行业绿色制造提供完整技术解决方案。 展开更多
关键词 PLC控制 三级闭环 智能照明系统 区域状态耦合 生产流程 能耗
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Numerical study on failure propagation between two closely spaced tunnels 被引量:1
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作者 Gang ZHENG Rui ZHU +4 位作者 Ji-bin SUN Tian-qi ZHANG Jing-bo TONG Rui-kun WANG Yu DIAO 《Journal of Zhejiang University-Science A(Applied Physics & Engineering)》 SCIE EI CAS CSCD 2021年第11期894-908,共15页
An increasing number of engineering accidents have shown that the failure of a tunnel can propagate to a neighbouring tunnel.However,due to the complex interaction between the failed tunnel structure and the soil medi... An increasing number of engineering accidents have shown that the failure of a tunnel can propagate to a neighbouring tunnel.However,due to the complex interaction between the failed tunnel structure and the soil medium,the mechanism by which the failure is propagated between two closely spaced tunnels remains unclear.In this study,the coupled EulerianLagrangian(CEL)modelling technique was adopted to investigate the influence of a failed tunnel(FT)on an adjacent tunnel,which was termed an“influenced tunnel”(IT).The safety of the IT was analysed in detail under different circumstances,such as different failure positions of the FT,different failure degrees of the FT,and different spatial relationships between the two tunnels.The simulation results indicated that the most adverse case may occur when the two tunnels are arranged as offsets and the IT is the upper tunnel.Under this circumstance,significant shear deformation may occur in IT because IT is located at the shear band of the FT. 展开更多
关键词 Failure propagation closely spaced tunnels coupled Eulerian-Lagrangian(CEL)
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高压密闭消解-电感耦合等离子体发射光谱法测定铜矿石中的银 被引量:3
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作者 袁润蕾 李小辉 +3 位作者 郭家凡 于亚辉 刘春霞 赵冲 《现代化工》 北大核心 2025年第S1期407-411,415,共6页
为便捷、准确测定大批量铜矿石中银(Ag)含量,建立了高压密闭消解结合电感耦合等离子体发射光谱仪测定铜矿石中Ag元素的方法。对消解酸的选择、消解酸比例、消解时间等试验条件进行优化,确定了最佳前处理消解条件。通过模拟矿石消解液试... 为便捷、准确测定大批量铜矿石中银(Ag)含量,建立了高压密闭消解结合电感耦合等离子体发射光谱仪测定铜矿石中Ag元素的方法。对消解酸的选择、消解酸比例、消解时间等试验条件进行优化,确定了最佳前处理消解条件。通过模拟矿石消解液试验,确定了Ag 328.068 nm作为测定银的最佳特征谱线。结果表明,本方法对Ag元素具有良好的线性关系(y=2203.5x+219.02),线性相关系数r在0.999以上;对不同含量的国家一级铜矿石标准物质进行测定,检出限为0.021μg/g,相对误差(RE)为-0.62%~0.19%,相对标准偏差(RSD)为0.59%~1.38%,回收率在95%~105%之间,满足地质矿产行业标准(DZ/T 0130—2006)对Ag元素的质控要求。 展开更多
关键词 高压密闭消解 电感耦合等离子体发射光谱法 铜矿石
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Analysis of thermal-mechanical coupled characteristics of vehicle twin-tube shock absorber
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作者 么鸣涛 龙凯 贺李平 《Journal of Beijing Institute of Technology》 EI CAS 2014年第2期203-209,共7页
A comprehensive model that included mechanical dynamics of the shock absorber coupled with its thermal properties was proposed innovatively.Moreover a thermal-mechanical coupled model which reflected the closed-loop p... A comprehensive model that included mechanical dynamics of the shock absorber coupled with its thermal properties was proposed innovatively.Moreover a thermal-mechanical coupled model which reflected the closed-loop positive feedback system was established by using MATLAB/SIMULINK,and some curves of shock absorber temperature rising characteristic were obtained by simulation &computation under several operating modes and different parameters conditions.Research results show that:shock absorber design parameters,external excitations,and thermo-physical properties parameter,such as oil density have effect on the shock absorber temperature rising characteristic.However other thermo-physical properties parameters,such as oil specific heat,cylinder density,cylinder specific heat,and cylinder thermal conductivity,have no effect on it.The results may be used for studying reliability design of the shock absorber. 展开更多
关键词 shock absorber thermal-mechanical coupled model temperature rising closed-loop positive feedback
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多自由度耦合振动环境下的近距激光通信系统设计与验证
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作者 何晓垒 王振 +2 位作者 钱阳 苏瑞芝 邱成 《光通信技术》 北大核心 2025年第4期68-71,共4页
针对商业航天器舱段间在极端震动环境下的高可靠性通信需求,提出一种抗多自由度耦合振动的近距激光通信系统。通过采用复合光路补偿结构、大发散角光学系统和基于深度学习的自适应控制算法,有效解决了多自由度振动导致的光学元件形变和... 针对商业航天器舱段间在极端震动环境下的高可靠性通信需求,提出一种抗多自由度耦合振动的近距激光通信系统。通过采用复合光路补偿结构、大发散角光学系统和基于深度学习的自适应控制算法,有效解决了多自由度振动导致的光学元件形变和光路失稳等技术难题。实验结果表明:在旋转20°、200 mm通信距离和10 mm偏移的极端工况,系统仍能保持稳定通信性能,接收功率波动小于2 dBm;在200 mm通信距离且同时存在10 mm偏移和20°旋转的最恶劣条件下,接收功率稳定在-10.84 dBm以上。 展开更多
关键词 多自由度 耦合震动 近距 激光通信 光学稳定性
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ICP-MS-紧密内插法快速测定食用菌及香辛料中的有害元素研究
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作者 郭楠楠 刘雁陇 《中国调味品》 北大核心 2025年第11期181-186,共6页
为建立一种快速且能够准确检测食品中不同有害元素的新方法,以食用菌和香辛料为研究对象,分别采用电感耦合等离子体质谱法(ICP-MS)-紧密内插法与标准曲线法对照测定样品中Pb、Cd、Cr、Hg、As、Mn、Cu 7种元素的含量。结果表明,ICP-MS-... 为建立一种快速且能够准确检测食品中不同有害元素的新方法,以食用菌和香辛料为研究对象,分别采用电感耦合等离子体质谱法(ICP-MS)-紧密内插法与标准曲线法对照测定样品中Pb、Cd、Cr、Hg、As、Mn、Cu 7种元素的含量。结果表明,ICP-MS-紧密内插法的检出限在0.0218~0.279 ng/mL之间,定量限在0.0728~0.930 ng/mL之间。样品的平均加标回收率为83.7%~99.7%,相对标准偏差在0.2%~1.8%之间。与国家标准中标准曲线法(国标法)相比,这两种方法之间不存在显著性差异(P>0.05)。结论:ICP-MS-紧密内插法线性关系较好,检测时间减少,且无需绘制标准溶液工作曲线和测定空白溶液,推广应用前景较好。 展开更多
关键词 电感耦合等离子体质谱法(ICP-MS) 紧密内插法 有害元素 食用菌 香辛料
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薄壁铁路桥梁在移动荷载列作用下的横向弯曲-扭转耦合振动
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作者 蔡勇 潘焰琛 《铁道学报》 北大核心 2025年第10期154-161,共8页
除垂直振动外,铁路桥梁上列车往往偏离桥梁横截面中心线行驶,也会导致桥梁产生横向和扭转振动;已有研究大多聚焦于桥梁竖向振动,对弯曲-扭转耦合振动理论的研究相对匮乏。为解决这一问题,提出一种用于分析列车荷载作用下薄壁铁路桥梁弯... 除垂直振动外,铁路桥梁上列车往往偏离桥梁横截面中心线行驶,也会导致桥梁产生横向和扭转振动;已有研究大多聚焦于桥梁竖向振动,对弯曲-扭转耦合振动理论的研究相对匮乏。为解决这一问题,提出一种用于分析列车荷载作用下薄壁铁路桥梁弯曲-扭转耦合振动的闭合解方法。将列车简化为两个具有恒定间隔的车轮载荷子系统叠加的移动荷载列模型,基于弗拉索夫的薄壁梁理论,建立桥梁振动微分方程。使用Fourier正弦变换、Laplace-Carson变换及其逆变换求解桥梁振动微分方程,得到列车荷载作用下薄壁梁横向弯曲-扭转耦合响应。验证闭合解可靠性后进一步开展参数分析,可得以下结论:附加扭转力矩在薄壁梁扭转振动中起重要作用;梁的弯曲-扭转耦合响应幅值随速度、车桥比增大表现出类似正弦波的形式逐渐变大;列车轴载增大会引起响应增大,当荷载等级从250 kN增加到300 kN时,梁扭转和横向振动幅值均增加20%。 展开更多
关键词 移动荷载列 薄壁梁 弯曲-扭转耦合振动 动力响应 闭合解
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