In the aerospace sector,the soft magnetic materials of Hermetically Sealed Electromagnetic Relays(HSERs)are critical in forming magnetic circuits.Conventional soft magnetic materials,primarily magnetic iron,have been ...In the aerospace sector,the soft magnetic materials of Hermetically Sealed Electromagnetic Relays(HSERs)are critical in forming magnetic circuits.Conventional soft magnetic materials,primarily magnetic iron,have been unable to meet the development trend of fast-response,miniaturized,and lightweight aerospace and aviation systems.This paper applies circuit theory and electromagnetics theory to establish a Field-Circuit Coupling Mathematical Model(FCCMM)for dynamic response analysis of HSERs.This model centers on inductance calculation,with the core's permeability and saturation magnetic flux density as critical parameters.Based on this model,for a specific type of HSER,this paper introduced three alloys with key parameters different from magnetic iron,then tested the magnetic characteristic curves of these four soft magnetic materials,followed by simulations to obtain the electromagnetic characteristics of digital mock-ups corresponding to these four materials,compared and validated the dynamic responses corresponding to these four soft magnetic materials finally.Based on the theoretical model analysis results,this paper designed a lightweight coil to minimize response time,made prototypes,set up test systems,and tested dynamic characteristics.The experimental results indicate that the nanocrystalline alloy1K107B exhibits the most significant optimization,reducing the closing time by 40.48%and achieving a weight reduction of 6.53%.展开更多
The particularity and practicality of harmony operations of close-coupling multiple helicopters indicate that the researches on it are urgent and necessary, Using the model that describes two hovering helicopters carr...The particularity and practicality of harmony operations of close-coupling multiple helicopters indicate that the researches on it are urgent and necessary, Using the model that describes two hovering helicopters carrying one heavy load, an inertia coordinate system and body coordinate systems of each sub-system are established. A nonlinear force model is established too. The equilibrium computation results can be regarded as the reference control inputs of the flight control system under hovering or low-speed flight condition. After the establishment of a translation kinematics model and a posture kinematics model, a coupling dynamics model of the multiple helicopter system is set up. The results can also be regarded as the base to analyze stabilization and design a controller for a close-coupling multiple helicopters harmony operation system.展开更多
Based on the integral equation formulations and the moment method, a novel closed form solution for analyzing the mutual coupling effect between the cylindrical comformal rectangular microstrip patch antennas is pres...Based on the integral equation formulations and the moment method, a novel closed form solution for analyzing the mutual coupling effect between the cylindrical comformal rectangular microstrip patch antennas is presented. By using this algorithm, the elements of the impedance matrix and exciting vector are cast into closed forms, thus the computational efficiency is improved dramatically. Numerical results are presented to verify the validity and reliability of the algorithm.展开更多
This paper reports that an exact quantum close coupling calculation is carried out for rotational excitation in Ne HF collisions on the available anisotropic potential. Partial cross sections are obtained separately a...This paper reports that an exact quantum close coupling calculation is carried out for rotational excitation in Ne HF collisions on the available anisotropic potential. Partial cross sections are obtained separately at the incident energies of 48.35, 75, 120 and 150meV. The reliability of the results is demonstrated by comparison with previously published theoretical findings. Based on the calculations, the effect of the potential energy surface on the excitation partial cross sections is discussed in detail.展开更多
An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method（HPCD）, is stud...An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method（HPCD）, is studied by an inductively coupled plasma optical emission spectrometry（ICP-OES） and an inductively coupled plasma mass spectrometry（ICP-MS）. The operating parameters of the instruments are optimized, and the optimal analytical parameters are determined. The influences of optical spectrum and mass spectrum interferences, digestion methods and acid systems on the analytical results are investigated. The optimal spectral lines and isotopes are chosen, and internal standard element of rhodium is selected to compensate for matrix effects and analytical signals drifting. Compared with the methods of an electric heating plate digestion and a microwave digestion, a high-pressure closed digestion method is optimized with less acid, complete digestion,less damage for digestion process. The marine geological samples are dissolved completely by a HF-HCl-HNO_3 system, the relative error（RE） for the analytical results are all less than 6.0%. The method detection limits are 2–40μg/g by the ICP-OES, and 6–80 ng/g by ICP-MS. The methods are used to determine the marine sediment reference materials（GBW07309, GBW07311, GBW07313）, rock reference materials（GBW07103, GBW07104,GBW07105）, and cobalt-rich crust reference materials（GBW07337, GBW07338, GBW07339）, the obtained analytical results are in agreement with the certified values, and both of the relative standard deviation（RSD） and the relative error（RE） are less than 6.0%. The analytical method meets the requirements for determining 52 elements contents of bulk marine geological samples.展开更多
In close-coupled gas atomization(CCGA), the influences of melt superheat on breakup process are fundamental to obtain desired or finer powder. Based on a series of Cu atomization experiment under different superheatin...In close-coupled gas atomization(CCGA), the influences of melt superheat on breakup process are fundamental to obtain desired or finer powder. Based on a series of Cu atomization experiment under different superheating conditions, the influences of melt superheat on breakup process were studied. Experimental results indicate that as the melt superheat is increased to 150, 200, 250 and 300 K, the mean particle size (D50) decreases consequently to 34.9, 32.3, 30.9 and 19.7 μm. Theoretical analysis reveals that the primary breakup and secondary breakup processes are close coupled, and the melt superheat radically influences the melt properties, and plays a crucial role on governing the filming process of primary breakup and the atomization modes of secondary breakup. There exists a strong nonlinear decrease of contact angle of melt to nozzle orifice wall when the superheat is increased from 250 K to 300 K, leading to a marked fall of the film thickness formed in primary breakup, and D50 of copper powders is therefore sharply reduced. However, the log-normal distribution feature of particle size has not been substantially improved.展开更多
The gas atomization is the process that a liquid mass is disintegrated into a collection of liquid melt droplets by the impact of high velocity gas stream and solidified into metal particles. However, the liquid melt ...The gas atomization is the process that a liquid mass is disintegrated into a collection of liquid melt droplets by the impact of high velocity gas stream and solidified into metal particles. However, the liquid melt sheet breaking mechanism has not been fully understood. So the experimental research was carried out under the condition of lower melt superheat. The results reveal that there are three approaches about melt metal sheet’s breakage: from the edges of sheets, from inner surface of sheets, and disrupted by other droplets and sheets. The approach of melt sheet breakage is dependent on its thickness. The thicker sheets (above 25μm) are disintegrated mainly by the way of droplet’s departing from edges, and the thinner sheets (below 10μm) are chiefly breaking from the inner surface.展开更多
A catalyst comprised novel high surface area alumina support was prepared to control emission of automobiles. The results showed that prepared catalyst could satisfy the requirements of a high performance close couple...A catalyst comprised novel high surface area alumina support was prepared to control emission of automobiles. The results showed that prepared catalyst could satisfy the requirements of a high performance close coupled catalyst for its good catalytic activity at low temperature and good stability at high temperature.展开更多
Fresh Pd/CeO/AlOclose coupled catalyst was prepared by the stepwise impregnation method and calcined at 550 °C for 3 h, which was then pretreated at 700, 800, and 900 °C for 3 h, respectively. Finally, these...Fresh Pd/CeO/AlOclose coupled catalyst was prepared by the stepwise impregnation method and calcined at 550 °C for 3 h, which was then pretreated at 700, 800, and 900 °C for 3 h, respectively. Finally, these pretreated catalysts were aged at 1000 °C for 3 h to study their anti-aging properties. The catalytic activities of the catalysts were investigated detailedly, and the results showed that the catalyst pretreated at 800 °C before aging treatment possessed the best anti-aging performance for CHoxidation. XRD and XPS results indicated that well-crystallized CeOparticles were formed during calcinations at 800 °C, which made CeOan effective promoter. HRTEM revealed that Pd particles found on the edge of CeOover the aged catalyst pretreated at 800 °C were relatively smaller than those over the catalysts without pretreatment. H-TPR and XPS results also implied that the interaction between well-crystallized CeOand Pd suppressed the deactivation of PdO sites and further enhanced the catalytic performance.展开更多
The group Ⅲ nitrides are an important class of materials with aplications in UV and visible optoelectronics,high temperature electronics,cold cathodes and solar blind detectors.In recent years,with the realisation of...The group Ⅲ nitrides are an important class of materials with aplications in UV and visible optoelectronics,high temperature electronics,cold cathodes and solar blind detectors.In recent years,with the realisation of nitride based LEDs,the use of GaN IED has the potential to compete with 1raditional filament and discharge lamps,for the provision of white lighting,and there has been an explosion of interest in the MOCVD growth of GaN based materials with an increasing focus on large area multiwafer reactors and wafer uniforrmity.This paper will review the design philosophy and characteristics of close-coupled showerhead reactors,relating these to the requirements of group Ⅲ-nitride growth,and will present a selection of data resulting from the operation of such equipment.These results suggest that the close coupled showerhead style of reactor is very suitable for the growth of GaN based structures in both research and production environments.展开更多
准确测定赤泥中微量金属元素含量对于评估赤泥的环境风险和资源化利用具有重要意义。为此,本文采用HNO_(3)+HF(体积比3:1)、HNO_(3)+水2次高压密闭消解,电感耦合等离子体质谱(ICP-MS)法测定赤泥中微量金属元素。实验结果表明:在0.1 g 10...准确测定赤泥中微量金属元素含量对于评估赤泥的环境风险和资源化利用具有重要意义。为此,本文采用HNO_(3)+HF(体积比3:1)、HNO_(3)+水2次高压密闭消解,电感耦合等离子体质谱(ICP-MS)法测定赤泥中微量金属元素。实验结果表明:在0.1 g 100目赤泥样品中加入3 mL HNO_(3)、1 mL HF,180℃高压密闭消解24 h后,将聚四氟乙烯消解罐取出,赶酸至近干,然后再在样品中加入1 mL HNO_(3)、1 mL超纯水,再次放入不锈钢套中,在烘箱中180℃再消解8 h,赤泥消解完全。本方法各元素检出限为0.02~0.2 mg/kg,加标回收率为91%~104%,相对标准偏差(RSD)为1.0%~3.3%。该方法可准确、批量检测赤泥样品中V、Cr、Mn等微量金属元素。展开更多
基金supported by the National Natural Science Foundation of China(No.52177134)。
文摘In the aerospace sector,the soft magnetic materials of Hermetically Sealed Electromagnetic Relays(HSERs)are critical in forming magnetic circuits.Conventional soft magnetic materials,primarily magnetic iron,have been unable to meet the development trend of fast-response,miniaturized,and lightweight aerospace and aviation systems.This paper applies circuit theory and electromagnetics theory to establish a Field-Circuit Coupling Mathematical Model(FCCMM)for dynamic response analysis of HSERs.This model centers on inductance calculation,with the core's permeability and saturation magnetic flux density as critical parameters.Based on this model,for a specific type of HSER,this paper introduced three alloys with key parameters different from magnetic iron,then tested the magnetic characteristic curves of these four soft magnetic materials,followed by simulations to obtain the electromagnetic characteristics of digital mock-ups corresponding to these four materials,compared and validated the dynamic responses corresponding to these four soft magnetic materials finally.Based on the theoretical model analysis results,this paper designed a lightweight coil to minimize response time,made prototypes,set up test systems,and tested dynamic characteristics.The experimental results indicate that the nanocrystalline alloy1K107B exhibits the most significant optimization,reducing the closing time by 40.48%and achieving a weight reduction of 6.53%.
基金National Natural Science Foundation of China(60475039)
文摘The particularity and practicality of harmony operations of close-coupling multiple helicopters indicate that the researches on it are urgent and necessary, Using the model that describes two hovering helicopters carrying one heavy load, an inertia coordinate system and body coordinate systems of each sub-system are established. A nonlinear force model is established too. The equilibrium computation results can be regarded as the reference control inputs of the flight control system under hovering or low-speed flight condition. After the establishment of a translation kinematics model and a posture kinematics model, a coupling dynamics model of the multiple helicopter system is set up. The results can also be regarded as the base to analyze stabilization and design a controller for a close-coupling multiple helicopters harmony operation system.
文摘Based on the integral equation formulations and the moment method, a novel closed form solution for analyzing the mutual coupling effect between the cylindrical comformal rectangular microstrip patch antennas is presented. By using this algorithm, the elements of the impedance matrix and exciting vector are cast into closed forms, thus the computational efficiency is improved dramatically. Numerical results are presented to verify the validity and reliability of the algorithm.
基金Project supported by the Natural Science Foundation of the Anhui Education Bureau of Chinathe National Natural Science Foundation of China (Grant No 10676025)
文摘This paper reports that an exact quantum close coupling calculation is carried out for rotational excitation in Ne HF collisions on the available anisotropic potential. Partial cross sections are obtained separately at the incident energies of 48.35, 75, 120 and 150meV. The reliability of the results is demonstrated by comparison with previously published theoretical findings. Based on the calculations, the effect of the potential energy surface on the excitation partial cross sections is discussed in detail.
基金The China Ocean Mineral Resources Research and Development Association Research Program of the State Oceanic Administration of China under contract No.DY125-13-R-07the National Natural Science Foundation of China under contract Nos 41322036 and 41230960+1 种基金the Shandong Provincial Natural Science Foundation of China under contract No.ZR2014DP009the Special Basic Research Funds for Central Public Research Institutes for The First Institute of Oceanography,State Oceanic Administration of China under contract Nos GY0213G06 and GY02-2012G35
文摘An improved analytical method to determine the content of 52 major, minor and trace elements in marine geological samples, using a HF-HCl-HNO_3 acid system with a high-pressure closed digestion method（HPCD）, is studied by an inductively coupled plasma optical emission spectrometry（ICP-OES） and an inductively coupled plasma mass spectrometry（ICP-MS）. The operating parameters of the instruments are optimized, and the optimal analytical parameters are determined. The influences of optical spectrum and mass spectrum interferences, digestion methods and acid systems on the analytical results are investigated. The optimal spectral lines and isotopes are chosen, and internal standard element of rhodium is selected to compensate for matrix effects and analytical signals drifting. Compared with the methods of an electric heating plate digestion and a microwave digestion, a high-pressure closed digestion method is optimized with less acid, complete digestion,less damage for digestion process. The marine geological samples are dissolved completely by a HF-HCl-HNO_3 system, the relative error（RE） for the analytical results are all less than 6.0%. The method detection limits are 2–40μg/g by the ICP-OES, and 6–80 ng/g by ICP-MS. The methods are used to determine the marine sediment reference materials（GBW07309, GBW07311, GBW07313）, rock reference materials（GBW07103, GBW07104,GBW07105）, and cobalt-rich crust reference materials（GBW07337, GBW07338, GBW07339）, the obtained analytical results are in agreement with the certified values, and both of the relative standard deviation（RSD） and the relative error（RE） are less than 6.0%. The analytical method meets the requirements for determining 52 elements contents of bulk marine geological samples.
基金Projects(10476043 50574103) supported by National Natural Science Foundation of China
文摘In close-coupled gas atomization(CCGA), the influences of melt superheat on breakup process are fundamental to obtain desired or finer powder. Based on a series of Cu atomization experiment under different superheating conditions, the influences of melt superheat on breakup process were studied. Experimental results indicate that as the melt superheat is increased to 150, 200, 250 and 300 K, the mean particle size (D50) decreases consequently to 34.9, 32.3, 30.9 and 19.7 μm. Theoretical analysis reveals that the primary breakup and secondary breakup processes are close coupled, and the melt superheat radically influences the melt properties, and plays a crucial role on governing the filming process of primary breakup and the atomization modes of secondary breakup. There exists a strong nonlinear decrease of contact angle of melt to nozzle orifice wall when the superheat is increased from 250 K to 300 K, leading to a marked fall of the film thickness formed in primary breakup, and D50 of copper powders is therefore sharply reduced. However, the log-normal distribution feature of particle size has not been substantially improved.
文摘The gas atomization is the process that a liquid mass is disintegrated into a collection of liquid melt droplets by the impact of high velocity gas stream and solidified into metal particles. However, the liquid melt sheet breaking mechanism has not been fully understood. So the experimental research was carried out under the condition of lower melt superheat. The results reveal that there are three approaches about melt metal sheet’s breakage: from the edges of sheets, from inner surface of sheets, and disrupted by other droplets and sheets. The approach of melt sheet breakage is dependent on its thickness. The thicker sheets (above 25μm) are disintegrated mainly by the way of droplet’s departing from edges, and the thinner sheets (below 10μm) are chiefly breaking from the inner surface.
基金the National Natural Science Foundation of China(No.20333030)for providing financial support for this project.
文摘A catalyst comprised novel high surface area alumina support was prepared to control emission of automobiles. The results showed that prepared catalyst could satisfy the requirements of a high performance close coupled catalyst for its good catalytic activity at low temperature and good stability at high temperature.
基金Project supported by the National Natural Science Foundation of China(21173153)the National Hi-tech Research Development Program of China(863 Program,2013AA065304)the Sichuan Science and Technology Agency Supported Project(2012FZ0008)
文摘Fresh Pd/CeO/AlOclose coupled catalyst was prepared by the stepwise impregnation method and calcined at 550 °C for 3 h, which was then pretreated at 700, 800, and 900 °C for 3 h, respectively. Finally, these pretreated catalysts were aged at 1000 °C for 3 h to study their anti-aging properties. The catalytic activities of the catalysts were investigated detailedly, and the results showed that the catalyst pretreated at 800 °C before aging treatment possessed the best anti-aging performance for CHoxidation. XRD and XPS results indicated that well-crystallized CeOparticles were formed during calcinations at 800 °C, which made CeOan effective promoter. HRTEM revealed that Pd particles found on the edge of CeOover the aged catalyst pretreated at 800 °C were relatively smaller than those over the catalysts without pretreatment. H-TPR and XPS results also implied that the interaction between well-crystallized CeOand Pd suppressed the deactivation of PdO sites and further enhanced the catalytic performance.
文摘The group Ⅲ nitrides are an important class of materials with aplications in UV and visible optoelectronics,high temperature electronics,cold cathodes and solar blind detectors.In recent years,with the realisation of nitride based LEDs,the use of GaN IED has the potential to compete with 1raditional filament and discharge lamps,for the provision of white lighting,and there has been an explosion of interest in the MOCVD growth of GaN based materials with an increasing focus on large area multiwafer reactors and wafer uniforrmity.This paper will review the design philosophy and characteristics of close-coupled showerhead reactors,relating these to the requirements of group Ⅲ-nitride growth,and will present a selection of data resulting from the operation of such equipment.These results suggest that the close coupled showerhead style of reactor is very suitable for the growth of GaN based structures in both research and production environments.
文摘准确测定赤泥中微量金属元素含量对于评估赤泥的环境风险和资源化利用具有重要意义。为此,本文采用HNO_(3)+HF(体积比3:1)、HNO_(3)+水2次高压密闭消解,电感耦合等离子体质谱(ICP-MS)法测定赤泥中微量金属元素。实验结果表明:在0.1 g 100目赤泥样品中加入3 mL HNO_(3)、1 mL HF,180℃高压密闭消解24 h后,将聚四氟乙烯消解罐取出,赶酸至近干,然后再在样品中加入1 mL HNO_(3)、1 mL超纯水,再次放入不锈钢套中,在烘箱中180℃再消解8 h,赤泥消解完全。本方法各元素检出限为0.02~0.2 mg/kg,加标回收率为91%~104%,相对标准偏差(RSD)为1.0%~3.3%。该方法可准确、批量检测赤泥样品中V、Cr、Mn等微量金属元素。
