Slagging and calcium treatment are commonly used methods to control cleanliness and inclusions in steel.However,the inappropriate slagging and calcium treatment operations resulted in the generation of large-sized inc...Slagging and calcium treatment are commonly used methods to control cleanliness and inclusions in steel.However,the inappropriate slagging and calcium treatment operations resulted in the generation of large-sized inclusions and deterioration of steel cleanliness;meanwhile,changed inclusions from Al_(2)O_(3)–SiO_(2)–MnO type to Al_(2)O_(3)–SiO_(2)–CaO type after the calcium treatment during the production of an H-beam steel.Combining the thermodynamic analysis and industrial trials,measurements including reducing the basicity of refining slag to be less than 2.0 and the Al_(2)O_(3)content in slag to be less than 10 wt.%and the cancelation of calcium treatment under the total content less than 15×10^(−6)have been taken.After optimization,the content of total oxygen in tundish decreased by 24%;meanwhile,inclusions were changed from the Al_(2)O_(3)–SiO_(2)–CaO system to the Al_(2)O_(3)–SiO_(2)–MnO system with a low-melting point and a obvious decrease in the number density,area fraction,and maximum size of inclusions.It has achieved the improvement of steel cleanliness while reducing production costs.展开更多
Objective:Magnetically controlled capsule gastroscopy(MCCG)is an effective method for screening gastric diseases;however,its performance may be affected by gastric cleanliness.We aimed to explore the correlation betwe...Objective:Magnetically controlled capsule gastroscopy(MCCG)is an effective method for screening gastric diseases;however,its performance may be affected by gastric cleanliness.We aimed to explore the correlation between Helicobacter pylori infection and the degree of gastric cleanliness in the MCCG.Methods:This retrospective study enrolled 297 participants from October 2020 to April 2024 at Sir Run Run Shaw Hospital,Zhejiang University School of Medicine.Participant characteristics,MCCG examination results,and(13)C-urea breath test(C13-UBT)results were collected.The gastric cleanliness in MCCG examinations was assessed using a gastric cleanliness score.Binary logistic regression was used to analyze the relationships among participant characteristics,H.pylori infection,and gastric cleanliness.Chi-square tests and Fisher's exact tests were used to analyze the relationships among gastric lesions,H.pylori infection,and gastric cleanliness.Results:Among the participants,24.2%had H.pylori infection,and 17.5%had poor gastric cleanliness.Hypertension(odds ratio[OR]:2.63;95%confidence interval[CI]:1.36e5.09;p?0.004)was associated with a greater likelihood of H.pylori infection.H.pylori infection(OR:3.76;95%CI:1.99e7.09;p<0.001)was an independent risk factor for poor gastric cleanliness in the MCCG.A significant disparity was noted in the prevalence of focal erosions(p<0.001),gastric ulcers(p?0.001),and positive gastric lesions(p?0.027)between the 2 groups with and without H.pylori infection.The proportion of positive gastric lesions was not significantly different between the good gastric cleanliness group and the poor gastric cleanliness group(25.7%vs.21.2%;p?0.490).Conclusion:The findings of this study revealed that H.pylori infection was associated with hypertension.H.pylori infection may lead to poor gastric cleanliness.Institutions are advised to perform C13-UBT before MCCG,and participants should be informed of the risk of poor gastric cleanliness if the results are positive.The decision to perform H.pylori eradication before MCCG should take into account patient willingness and the benefit-to-risk ratio.展开更多
The effect of pre-melting refining slag containing different contents of Ce2O3 on the absorption and modification of Al2O3 inclusion in an Al-killed steel was investigated through the slag/steel reaction experiment at...The effect of pre-melting refining slag containing different contents of Ce2O3 on the absorption and modification of Al2O3 inclusion in an Al-killed steel was investigated through the slag/steel reaction experiment at 1600 oC.It was found that the replacement of 10 wt.% Al2O3 with Ce2O3 for 50 wt.%CaO-33 wt.%Al2O3-7 wt.%MgO-10 wt.%SiO2 refining slag promoted the slag absorption ability of alumina inclusion,which made the total oxygen content determined by infrared absorption method decrease from 100 to 25 ppm in 15 min.The Mg-Al-Ce-O type inclusion was also detected in the as-solidified samples by scanning electron microscopy(SEM).Thermodynamic analysis indicated that the Ce2O3.Al2O3 type inclusions would be formed with the cerium content in the range of 6.9 ppb to 3.6 ppm when the content of aluminum was 0.01 wt.%.展开更多
During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH)...During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH) process was low: heating by Al addition during the RH decarburization process and final deoxidation at the end of the RH decarburization process(process-Ⅰ), and increasing the oxygen content at the end of RH decarburization, heating and final deoxidation by one-time Al addition(process-Ⅱ). Temperature increases of 10°C by different processes were studied; the results showed that the two heating processes could achieve the same heating effect. The T.[O] content in the slab and the refining process was better controlled by process-Ⅰ than by process-Ⅱ. Statistical analysis of inclusions showed that the numbers of inclusions in the slab obtained by process-Ⅰ were substantially less than those in the slab obtained by process-Ⅱ. For process-Ⅰ, the Al_2O_3 inclusions produced by Al added to induce heating were substantially removed at the end of decarburization. The amounts of inclusions were substantially greater for process-Ⅱ than for process-Ⅰ at different refining stages because of the higher dissolved oxygen concentration in process-Ⅱ. Industrial test results showed that process-Ⅰ was more beneficial for improving the cleanliness of molten steel.展开更多
To investigate inclusion formation in each step during steel making process, several samples were taken in different steps of the production of steel at Mobarakeh Steel Co of Esfahan to measure the oxygen chemical pot...To investigate inclusion formation in each step during steel making process, several samples were taken in different steps of the production of steel at Mobarakeh Steel Co of Esfahan to measure the oxygen chemical potential of the molten steel in each stage. The chemical compositions of the inclusions in samples were investigated by scanning electron microscope. The chemical composition of the slag was analyzed. With the use of thermodnamic calculations and chemical analysis of the melt, at the working temperature, the relationship between dissolved oxygen and other elements were determined. Finally, it was found that there is a close relationship between inclusions formed in each step with the oxygen partial pressure.展开更多
The equilibrium reaction between CaO-Al2O3-SiO2-MgO slag and 28MnCr5 molten steel was calculated to obtain the suitable slag composition which is effective for decreasing the oxygen content in molten steel. The dissol...The equilibrium reaction between CaO-Al2O3-SiO2-MgO slag and 28MnCr5 molten steel was calculated to obtain the suitable slag composition which is effective for decreasing the oxygen content in molten steel. The dissolved oxygen content [O] in molten steel un- der different top slag conditions was calculated using a thermodynamic model and was measured using an electromotive force method in slag-steel equilibrium experiments at 1873 K. The relations among [O], the total oxygen content (T.O), and the composition of the slag were investigated. The experimental results show that both [O] and T.O decrease with decreasing SiO2 content of the slag and exhibit different trends with the changes in the CaO/Al2O3 mass ratio of the slag. Increasing the CaO/Al2O3 mass ratio results in a decrease in [O] and an in- crease in T.O. To ensure that T.O ≤ 20 ppm and [O] ≤ 10 ppm, the SiO2 content should be controlled to 〈5wt%, and the CaO/AI203 mass ratio should be in the range from 1.2 to 1.6.展开更多
To make high integrity lightweight metal castings,best practices are required in various stages of casting and heat treatment processes,including liquid metal composition and quality control,casting and gating/riser s...To make high integrity lightweight metal castings,best practices are required in various stages of casting and heat treatment processes,including liquid metal composition and quality control,casting and gating/riser system design,and process optimization.This paper presents best practices for liquid metal processing and quality assurance of molten metal in both melting and mold filling.Best practices for other aspects of lightweight metal casting will be published separately.展开更多
BACKGROUND The vaginal microbiome plays a critical role in the health of pregnant women and their newborns.Group B Streptococcus(GBS)and vaginal cleanliness significantly affect the vaginal microecosystem and are clos...BACKGROUND The vaginal microbiome plays a critical role in the health of pregnant women and their newborns.Group B Streptococcus(GBS)and vaginal cleanliness significantly affect the vaginal microecosystem and are closely associated with vaginal diseases.AIM To explore the effects of GBS status and vaginal cleanliness on vaginal microecosystems.METHODS We collected 160 vaginal swabs from pregnant women and divided them into the following four groups based on GBS status and vaginal cleanliness:GBS-positive+vaginal cleanliness I–II degree,GBS-negative+vaginal cleanliness I–II degree,GBS-positive+vaginal cleanliness III–IV degree,and GBS-negative+vaginal cleanliness III–IV degree.Samples were subjected to 16S rRNA gene amplicon sequencing.RESULTS Alpha diversity analysis showed that the Shannon index did not significantly differ between the four groups.We identified significant variation in taxa abundance between the GBS-positive and GBS-negative groups and between the vaginal cleanliness I–II degree and III–IV degree groups.Principal coordinate analysis and non-metric multidimensional scaling analysis further confirmed the microbial diversity of the four groups.Moreover,the linear discriminant analysis demonstrated that Lactobacillus jensenii and Actinobacteria were strongly associated with GBS-positive status,and Lactobacillus iners,Lactobacillaceae,Lactobacillus,Lactobacillales,Bacilli and Firmicutes were closely correlated with GBS-negative status.CONCLUSION GBS status and vaginal cleanliness significantly affect vaginal microbiome differences in pregnant women.Our findings provide instructional information for clinical antibiotic treatment in pregnant women with different GBS statuses and vaginal cleanliness degrees.展开更多
Based on analysis of a large data set and supplementary sampling and analysis for hazardous trace elements in coal samples from the Huainan Coalfield,a generalized contrast-weighted scale index method was used to esta...Based on analysis of a large data set and supplementary sampling and analysis for hazardous trace elements in coal samples from the Huainan Coalfield,a generalized contrast-weighted scale index method was used to establish a model to evaluate the grade of coal cleanliness and its regional distribution in the main coal seam(No.13-1)The results showed that:(1)The contents of Cr,Mn and Ni in the coal seam are relatively high and the average values are greater than 20μg/g.The contents of Se and Hg are at a high level while most other trace elements are at normal levels.(2)The cleanliness grade of the coal seam is mainly grade III-IV,which corresponds to a relatively good-medium coal cleanliness grade.However,some parts of the seam are at grade V(relatively poor coal cleanliness).(3)Coal of relatively good cleanliness grade(grade III)is distributed mainly in the regions corresponding to the Zhuji-Dingji-Gubei coal mines and in the eastern periphery of the Panji coal mine.Coal of medium cleanliness(grade IV)is distributed mainly in the regions of the Panji-Xiejiaji and Kouzidong coalmines.Relatively poor grade coal(grade V)is distributed in the southwest regions of the coalfield and the contents of Cr,As and Hg in coal collected from the relatively poor coal cleanliness regions often exceed the regulatory standards for the maximum concentration limits.展开更多
Shot-peened,case-hardened gears can fail in the tooth root due to crack initiation below the surface of the steel matrix.Here,the crack is initiated at a non-metallic inclusion in the center of a so-called fisheye.Thi...Shot-peened,case-hardened gears can fail in the tooth root due to crack initiation below the surface of the steel matrix.Here,the crack is initiated at a non-metallic inclusion in the center of a so-called fisheye.This failure type can lead to a reduced endurance fatigue limit of the gears.It is for this reason that,over the last decade,much effort has been invested by steel manufacturers to reduce the non-metallic inclusion content of gear steels so as to mitigate or even completely prevent such crack initiation.These ultra-clean gear steels were achieved by various measures in the steel production process.However,as a result,the remaining non-metallic inclusions are inhomogeneously distributed in the steel volume in terms of both size and location.However,due to the inhomogeneity of ultra-clean steels,the question arose if the values derived according to the standards are still representative of ultra-clean steel batches.The results show that the standards can still be applied,but more effort must be applied.To determine the degree of cleanliness,six microsections are currently evaluated according to steel test specification(SEP)1571,method K.It is shown that an examination of 24 microsections starting from size class 0 seems beneficial to get more reliable and comparable results of the degree of cleanliness of these ultra-clean gear steels.In addition,it is shown that a high degree of cleanliness has been achieved for all steel batches investigated with the measures taken in the steel production process.展开更多
The effect of the axial static magnetic field(ASMF)on cleanliness and microstructure in magnetically controlled electroslag remelted GCr15 bearing steel ingots was investigated experimentally.The results show that a m...The effect of the axial static magnetic field(ASMF)on cleanliness and microstructure in magnetically controlled electroslag remelted GCr15 bearing steel ingots was investigated experimentally.The results show that a magnetically controlled spin-vibration induced by the interaction of the ASMFs and the remelting current exists at the consumable electrode tip,resulting in thinner liquid melt film and smaller droplets.With the increase in magnetic flux density,the optimization effect of ASMFs on electroslag remelting process increases and reaches the peak with a 40 mT ASMF,then decreases.The cleanliness of the ingots was improved,and the count of inclusions larger than 5μm was reduced.The microstructure of the ingots processed with a 40 mT ASMF was significantly refined.The depth of the metallic molten pool was reduced from 45.2 to 17.5 mm with the application of 40 mT ASMF.The tensile strength,impact toughness,and Rockwell hardness of the ingots obtained under the 40 mT ASMF were significantly improved.The mechanisms of the spin-vibration occurring at the electrode tip end were interpreted in detail to elucidate the effect of ASMFs.展开更多
A testing system for evaluating cleanliness of ventilation ducts was constructed. Comparisons of four evaluation methods for quantifying the amount of dust on the inner surface of ventilation ducts are presented. The ...A testing system for evaluating cleanliness of ventilation ducts was constructed. Comparisons of four evaluation methods for quantifying the amount of dust on the inner surface of ventilation ducts are presented. The experimental results show that the wiping by solvent method is more efficient than that by the wiping method,especially used on low cleanliness duct surface. The gravimetric tape method is an efficient method of collecting dust samples on the duct surface with low amounts of dust,particularly used to check the cleanliness level after the cleaning work. The optical method can be set up rapidly and is useful for fieldwork measurements.展开更多
To clarify the effect of the tundish lining on the steel cleanliness,the MgO based and Al2 O3 based gunning materials( GM) were used as the lining of the alumina crucibles,respectively,in which about 200 g of ultra-...To clarify the effect of the tundish lining on the steel cleanliness,the MgO based and Al2 O3 based gunning materials( GM) were used as the lining of the alumina crucibles,respectively,in which about 200 g of ultra-low carbon steel was charged at 1 823 K for 2 h in pure argon atmosphere. The chemical analysis was carried out to investigate the change of chemical composition of steel in contact with GM after high temperatures holding experiments. The steel cleanliness in terms of inclusion number density,inclusion size and inclusion size distribution was evaluated by SEM and EDS. It was found that the MgO GM provided more oxygen and showed a stronger oxidizing capacity due to its higher content of reducible oxides( 10. 5 mass% SiO2+ 2 mass%Fe2 O3). The use of Al2 O3 GM resulted in an improved steel cleanliness and consequently Al2 O3 GM could be a promising refractory material in the tundish lining.展开更多
The key manufacturing technologies associated with composition, microstructure, mechanical properties, casting quality and key process control for large martensitic stainless steel castings are involved in this paper....The key manufacturing technologies associated with composition, microstructure, mechanical properties, casting quality and key process control for large martensitic stainless steel castings are involved in this paper. The achievements fully satisfeid the technical requirements of the large 700 MW stainless steel hydraulic turbine runner for the Three Gorges Hydropower Station, and become the major technical support for the design and manufacture of the largest 700 MW hydraulic turbine generator unit in the world developed through our own efforts. The characteristics of a new high yield to tensile strength (R p0.2/R m ) ratio and high obdurability martensitic stainless steel with ultra low carbon and high cleanliness are also described. Over the next ten years, the large martensitic stainless steel castings and advanced manufacturing technologies will see a huge demand in clean energy industry such as nuclear power, hydraulic power at home and abroad. Therefore, the new high yield o tensile strength (R p0.2/R m ) ratio and high obdurability martensitic stainless steel materials, the fast and flexible manufacturing technologies of large size castings, and new environment friendly sustainable process will face new challenges and opportunities.展开更多
Objective:To evaluate the performance parameters of adenosine triphosphat(ATP)bioluminescence detection technology in assessing surface cleanliness in surgical environments and on hand surfaces.Methods:Samples were co...Objective:To evaluate the performance parameters of adenosine triphosphat(ATP)bioluminescence detection technology in assessing surface cleanliness in surgical environments and on hand surfaces.Methods:Samples were collected from 20 orthopedic surgeons at five hand sites(fingertips,hypothenar eminence,thenar eminence,nail grooves of the index/middle fingers,and nail matrices)before and after handwashing.ATP bioluminescence assays and agar plate colony counting were performed to measure relative light unit(RLU)values and logarithmic total colony counts,respectively.Differences in RLU and colony counts across hand sites were compared.Linear regression analysis was conducted to assess the correlation between RLU values and log-transformed colony counts at each site.The water Raman signal-to-noise ratio(S/N)and detection limits were also determined.Results:A significant linear positive correlation was observed between RLU values and log colony counts on surgeons'hands,with the regression equation:y=-0.4580+0.127x(p<0.001,R^(2)=0.947).The sodium fluorescein standard demonstrated a water Raman S/N of 935.67 and detection limits of 0.86-51.53 RFU,both exceeding blank controls,with a wide linear range.Conclusion:ATP bioluminescence technology exhibits high sensitivity and precision for evaluating hand surface cleanliness,showing strong linear correlation with colony counts.Its detection limits surpass conventional standards,making it a robust tool for surgical hygiene monitoring.展开更多
The Macao Science Satellite-1(MSS-1)is the first space science satellite jointly developed on the Chinese mainland and in Macao region.It comprises two satellites,named MSS-1A and MSS-1B,and holds considerable importa...The Macao Science Satellite-1(MSS-1)is the first space science satellite jointly developed on the Chinese mainland and in Macao region.It comprises two satellites,named MSS-1A and MSS-1B,and holds considerable importance in China’s space exploration endeavors.Among these,MSS-1A is the world’s first high-precision scientific satellite dedicated to exploring the geomagnetic field and space environment at low latitudes.Equipped with two high-precision vector magnetometers and one scalar magnetometer,which are integrally installed on a highly stable nonmagnetic optical bench,the MSS-1A enables simultaneous high-precision measurements of both the Earth’s vector magnetic field and its scalar components.Its design integrates several state-of-the-art technologies,including arc-second-level thermal stability control,nonmagnetic thermal control for the optical bench,and ultra-high magnetic cleanliness control.These innovations effectively minimize magnetic interference originating from the satellite itself,thereby substantially improving the precision of geomagnetic field measurements and establishing a robust technical foundation for future magnetic survey satellite constellations.展开更多
目的比较硫酸镁钠钾口服液(OSS)与复方聚乙二醇电解质散(PEG)在结肠镜检查前肠道准备中的安全性和有效性。方法回顾性分析2023月9月-2024年9月该院采用OSS与PEG在肠镜检查行前肠道准备的患者2000例。根据不同肠道准备药物,将患者分为OSS...目的比较硫酸镁钠钾口服液(OSS)与复方聚乙二醇电解质散(PEG)在结肠镜检查前肠道准备中的安全性和有效性。方法回顾性分析2023月9月-2024年9月该院采用OSS与PEG在肠镜检查行前肠道准备的患者2000例。根据不同肠道准备药物,将患者分为OSS组(1000例,口服OSS)和PEG组(1000例,口服4 L PEG)。比较两组患者肠道清洁度、清洁效果、肠腔气泡、结肠镜检查阳性率和不良反应发生率。结果OSS组肠道准备成功率为92.5%(925/1000),PEG组肠道准备成功率为91.7%(917/1000),两组患者比较,差异无统计学意义(P>0.05);两组患者左侧结肠波士顿肠道准备量表(BBPS)评分比较,差异无统计学意义(P>0.05),OSS组BBPS总分,以及中段和右侧结肠BBPS评分明显高于PEG组,差异均有统计学意义(P<0.05);OSS组气泡评估满意率为96.2%,高于PEG组的90.3%,差异有统计学意义(P<0.05);两组患者结肠镜检查阳性率和不良反应发生率比较,差异均无统计学意义(P>0.05)。结论OSS在肠道准备方面具有较好的去泡效果,清洁效果与PEG相当,且有较高的安全性。展开更多
基金support from the National Key R&D Program(Nos.2023YFB3506802 and 2023YFB3709900)the National Natural Science Foundation of China(Grant Nos.52174293 and U22A20171)+1 种基金the Fundamental Research Funds for the Central Universities(Grant No.FRF-BD-20-04A)the High Steel Center(HSC)at North China University of Technology.
文摘Slagging and calcium treatment are commonly used methods to control cleanliness and inclusions in steel.However,the inappropriate slagging and calcium treatment operations resulted in the generation of large-sized inclusions and deterioration of steel cleanliness;meanwhile,changed inclusions from Al_(2)O_(3)–SiO_(2)–MnO type to Al_(2)O_(3)–SiO_(2)–CaO type after the calcium treatment during the production of an H-beam steel.Combining the thermodynamic analysis and industrial trials,measurements including reducing the basicity of refining slag to be less than 2.0 and the Al_(2)O_(3)content in slag to be less than 10 wt.%and the cancelation of calcium treatment under the total content less than 15×10^(−6)have been taken.After optimization,the content of total oxygen in tundish decreased by 24%;meanwhile,inclusions were changed from the Al_(2)O_(3)–SiO_(2)–CaO system to the Al_(2)O_(3)–SiO_(2)–MnO system with a low-melting point and a obvious decrease in the number density,area fraction,and maximum size of inclusions.It has achieved the improvement of steel cleanliness while reducing production costs.
基金supported by the General Research Project of the Department of Education of Zhejiang Province,China(No.Y202351338)the Soft Science Project of the Department of Science and Technology of Zhejiang Province,China(No.2024C35054).
文摘Objective:Magnetically controlled capsule gastroscopy(MCCG)is an effective method for screening gastric diseases;however,its performance may be affected by gastric cleanliness.We aimed to explore the correlation between Helicobacter pylori infection and the degree of gastric cleanliness in the MCCG.Methods:This retrospective study enrolled 297 participants from October 2020 to April 2024 at Sir Run Run Shaw Hospital,Zhejiang University School of Medicine.Participant characteristics,MCCG examination results,and(13)C-urea breath test(C13-UBT)results were collected.The gastric cleanliness in MCCG examinations was assessed using a gastric cleanliness score.Binary logistic regression was used to analyze the relationships among participant characteristics,H.pylori infection,and gastric cleanliness.Chi-square tests and Fisher's exact tests were used to analyze the relationships among gastric lesions,H.pylori infection,and gastric cleanliness.Results:Among the participants,24.2%had H.pylori infection,and 17.5%had poor gastric cleanliness.Hypertension(odds ratio[OR]:2.63;95%confidence interval[CI]:1.36e5.09;p?0.004)was associated with a greater likelihood of H.pylori infection.H.pylori infection(OR:3.76;95%CI:1.99e7.09;p<0.001)was an independent risk factor for poor gastric cleanliness in the MCCG.A significant disparity was noted in the prevalence of focal erosions(p<0.001),gastric ulcers(p?0.001),and positive gastric lesions(p?0.027)between the 2 groups with and without H.pylori infection.The proportion of positive gastric lesions was not significantly different between the good gastric cleanliness group and the poor gastric cleanliness group(25.7%vs.21.2%;p?0.490).Conclusion:The findings of this study revealed that H.pylori infection was associated with hypertension.H.pylori infection may lead to poor gastric cleanliness.Institutions are advised to perform C13-UBT before MCCG,and participants should be informed of the risk of poor gastric cleanliness if the results are positive.The decision to perform H.pylori eradication before MCCG should take into account patient willingness and the benefit-to-risk ratio.
基金Project supported by the National Natural Science Foundation of China (50734008)
文摘The effect of pre-melting refining slag containing different contents of Ce2O3 on the absorption and modification of Al2O3 inclusion in an Al-killed steel was investigated through the slag/steel reaction experiment at 1600 oC.It was found that the replacement of 10 wt.% Al2O3 with Ce2O3 for 50 wt.%CaO-33 wt.%Al2O3-7 wt.%MgO-10 wt.%SiO2 refining slag promoted the slag absorption ability of alumina inclusion,which made the total oxygen content determined by infrared absorption method decrease from 100 to 25 ppm in 15 min.The Mg-Al-Ce-O type inclusion was also detected in the as-solidified samples by scanning electron microscopy(SEM).Thermodynamic analysis indicated that the Ce2O3.Al2O3 type inclusions would be formed with the cerium content in the range of 6.9 ppb to 3.6 ppm when the content of aluminum was 0.01 wt.%.
基金financially supported by the National Natural Science Foundation of China (No.51404022)
文摘During the production of Ti-bearing Al-killed ultra-low-carbon(ULC) steel, two different heating processes were used when the converter tapping temperature or the molten steel temperature in the Ruhrstahl–Heraeus(RH) process was low: heating by Al addition during the RH decarburization process and final deoxidation at the end of the RH decarburization process(process-Ⅰ), and increasing the oxygen content at the end of RH decarburization, heating and final deoxidation by one-time Al addition(process-Ⅱ). Temperature increases of 10°C by different processes were studied; the results showed that the two heating processes could achieve the same heating effect. The T.[O] content in the slab and the refining process was better controlled by process-Ⅰ than by process-Ⅱ. Statistical analysis of inclusions showed that the numbers of inclusions in the slab obtained by process-Ⅰ were substantially less than those in the slab obtained by process-Ⅱ. For process-Ⅰ, the Al_2O_3 inclusions produced by Al added to induce heating were substantially removed at the end of decarburization. The amounts of inclusions were substantially greater for process-Ⅱ than for process-Ⅰ at different refining stages because of the higher dissolved oxygen concentration in process-Ⅱ. Industrial test results showed that process-Ⅰ was more beneficial for improving the cleanliness of molten steel.
文摘To investigate inclusion formation in each step during steel making process, several samples were taken in different steps of the production of steel at Mobarakeh Steel Co of Esfahan to measure the oxygen chemical potential of the molten steel in each stage. The chemical compositions of the inclusions in samples were investigated by scanning electron microscope. The chemical composition of the slag was analyzed. With the use of thermodnamic calculations and chemical analysis of the melt, at the working temperature, the relationship between dissolved oxygen and other elements were determined. Finally, it was found that there is a close relationship between inclusions formed in each step with the oxygen partial pressure.
基金financially supported by the Program for New Century Excellent Talents in Universities of China(No.NCET-07-0650)
文摘The equilibrium reaction between CaO-Al2O3-SiO2-MgO slag and 28MnCr5 molten steel was calculated to obtain the suitable slag composition which is effective for decreasing the oxygen content in molten steel. The dissolved oxygen content [O] in molten steel un- der different top slag conditions was calculated using a thermodynamic model and was measured using an electromotive force method in slag-steel equilibrium experiments at 1873 K. The relations among [O], the total oxygen content (T.O), and the composition of the slag were investigated. The experimental results show that both [O] and T.O decrease with decreasing SiO2 content of the slag and exhibit different trends with the changes in the CaO/Al2O3 mass ratio of the slag. Increasing the CaO/Al2O3 mass ratio results in a decrease in [O] and an in- crease in T.O. To ensure that T.O ≤ 20 ppm and [O] ≤ 10 ppm, the SiO2 content should be controlled to 〈5wt%, and the CaO/AI203 mass ratio should be in the range from 1.2 to 1.6.
文摘To make high integrity lightweight metal castings,best practices are required in various stages of casting and heat treatment processes,including liquid metal composition and quality control,casting and gating/riser system design,and process optimization.This paper presents best practices for liquid metal processing and quality assurance of molten metal in both melting and mold filling.Best practices for other aspects of lightweight metal casting will be published separately.
文摘BACKGROUND The vaginal microbiome plays a critical role in the health of pregnant women and their newborns.Group B Streptococcus(GBS)and vaginal cleanliness significantly affect the vaginal microecosystem and are closely associated with vaginal diseases.AIM To explore the effects of GBS status and vaginal cleanliness on vaginal microecosystems.METHODS We collected 160 vaginal swabs from pregnant women and divided them into the following four groups based on GBS status and vaginal cleanliness:GBS-positive+vaginal cleanliness I–II degree,GBS-negative+vaginal cleanliness I–II degree,GBS-positive+vaginal cleanliness III–IV degree,and GBS-negative+vaginal cleanliness III–IV degree.Samples were subjected to 16S rRNA gene amplicon sequencing.RESULTS Alpha diversity analysis showed that the Shannon index did not significantly differ between the four groups.We identified significant variation in taxa abundance between the GBS-positive and GBS-negative groups and between the vaginal cleanliness I–II degree and III–IV degree groups.Principal coordinate analysis and non-metric multidimensional scaling analysis further confirmed the microbial diversity of the four groups.Moreover,the linear discriminant analysis demonstrated that Lactobacillus jensenii and Actinobacteria were strongly associated with GBS-positive status,and Lactobacillus iners,Lactobacillaceae,Lactobacillus,Lactobacillales,Bacilli and Firmicutes were closely correlated with GBS-negative status.CONCLUSION GBS status and vaginal cleanliness significantly affect vaginal microbiome differences in pregnant women.Our findings provide instructional information for clinical antibiotic treatment in pregnant women with different GBS statuses and vaginal cleanliness degrees.
基金the Key Research and Development Projects in Anhui Province(201904a07020071)the Science and Technology Project of the Department of Land and Resources of Anhui Province(2016-K-16)the Key Research and Development Projects in Anhui Province(1804a0802198).
文摘Based on analysis of a large data set and supplementary sampling and analysis for hazardous trace elements in coal samples from the Huainan Coalfield,a generalized contrast-weighted scale index method was used to establish a model to evaluate the grade of coal cleanliness and its regional distribution in the main coal seam(No.13-1)The results showed that:(1)The contents of Cr,Mn and Ni in the coal seam are relatively high and the average values are greater than 20μg/g.The contents of Se and Hg are at a high level while most other trace elements are at normal levels.(2)The cleanliness grade of the coal seam is mainly grade III-IV,which corresponds to a relatively good-medium coal cleanliness grade.However,some parts of the seam are at grade V(relatively poor coal cleanliness).(3)Coal of relatively good cleanliness grade(grade III)is distributed mainly in the regions corresponding to the Zhuji-Dingji-Gubei coal mines and in the eastern periphery of the Panji coal mine.Coal of medium cleanliness(grade IV)is distributed mainly in the regions of the Panji-Xiejiaji and Kouzidong coalmines.Relatively poor grade coal(grade V)is distributed in the southwest regions of the coalfield and the contents of Cr,As and Hg in coal collected from the relatively poor coal cleanliness regions often exceed the regulatory standards for the maximum concentration limits.
基金The underlying research work was funded in equal proportions by the“Arbeitsgemeinschaft industrieller Forschungsvereinigungen e.V.(AiF)”,the German Federal Ministry of Economics and Technology(BMWi,IGF no.16662 N)and the FVA.The results presented in this paper were taken from the FVA research project 293 III“Späte Zahnfußbrüche/Reinheitsgrad”.More detailed information on the influence of non-metallic inclusions is given in the final report.
文摘Shot-peened,case-hardened gears can fail in the tooth root due to crack initiation below the surface of the steel matrix.Here,the crack is initiated at a non-metallic inclusion in the center of a so-called fisheye.This failure type can lead to a reduced endurance fatigue limit of the gears.It is for this reason that,over the last decade,much effort has been invested by steel manufacturers to reduce the non-metallic inclusion content of gear steels so as to mitigate or even completely prevent such crack initiation.These ultra-clean gear steels were achieved by various measures in the steel production process.However,as a result,the remaining non-metallic inclusions are inhomogeneously distributed in the steel volume in terms of both size and location.However,due to the inhomogeneity of ultra-clean steels,the question arose if the values derived according to the standards are still representative of ultra-clean steel batches.The results show that the standards can still be applied,but more effort must be applied.To determine the degree of cleanliness,six microsections are currently evaluated according to steel test specification(SEP)1571,method K.It is shown that an examination of 24 microsections starting from size class 0 seems beneficial to get more reliable and comparable results of the degree of cleanliness of these ultra-clean gear steels.In addition,it is shown that a high degree of cleanliness has been achieved for all steel batches investigated with the measures taken in the steel production process.
基金This work is supported by the National Key Research and Development Program of China under Grant numbers of 2016YFB0300401,2018YFF0109404,and 2016YFB0301401the National Natural Science Foundation of China under Grant numbers of U1860202,U1732276,50134010,51704193,51904184,and 52004156the Users with Excellence Program of Hefei Science Center CAS under Grant number of 2019HSC-UE010,and the Changjiang Scholar Program of Chinese Ministry of Education.
文摘The effect of the axial static magnetic field(ASMF)on cleanliness and microstructure in magnetically controlled electroslag remelted GCr15 bearing steel ingots was investigated experimentally.The results show that a magnetically controlled spin-vibration induced by the interaction of the ASMFs and the remelting current exists at the consumable electrode tip,resulting in thinner liquid melt film and smaller droplets.With the increase in magnetic flux density,the optimization effect of ASMFs on electroslag remelting process increases and reaches the peak with a 40 mT ASMF,then decreases.The cleanliness of the ingots was improved,and the count of inclusions larger than 5μm was reduced.The microstructure of the ingots processed with a 40 mT ASMF was significantly refined.The depth of the metallic molten pool was reduced from 45.2 to 17.5 mm with the application of 40 mT ASMF.The tensile strength,impact toughness,and Rockwell hardness of the ingots obtained under the 40 mT ASMF were significantly improved.The mechanisms of the spin-vibration occurring at the electrode tip end were interpreted in detail to elucidate the effect of ASMFs.
基金Project(2006BAJ02A10) supported by the National Key Technologies R&D Program
文摘A testing system for evaluating cleanliness of ventilation ducts was constructed. Comparisons of four evaluation methods for quantifying the amount of dust on the inner surface of ventilation ducts are presented. The experimental results show that the wiping by solvent method is more efficient than that by the wiping method,especially used on low cleanliness duct surface. The gravimetric tape method is an efficient method of collecting dust samples on the duct surface with low amounts of dust,particularly used to check the cleanliness level after the cleaning work. The optical method can be set up rapidly and is useful for fieldwork measurements.
基金the Major State Basic Research Development Program of China(Grant No.2014CB660800)
文摘To clarify the effect of the tundish lining on the steel cleanliness,the MgO based and Al2 O3 based gunning materials( GM) were used as the lining of the alumina crucibles,respectively,in which about 200 g of ultra-low carbon steel was charged at 1 823 K for 2 h in pure argon atmosphere. The chemical analysis was carried out to investigate the change of chemical composition of steel in contact with GM after high temperatures holding experiments. The steel cleanliness in terms of inclusion number density,inclusion size and inclusion size distribution was evaluated by SEM and EDS. It was found that the MgO GM provided more oxygen and showed a stronger oxidizing capacity due to its higher content of reducible oxides( 10. 5 mass% SiO2+ 2 mass%Fe2 O3). The use of Al2 O3 GM resulted in an improved steel cleanliness and consequently Al2 O3 GM could be a promising refractory material in the tundish lining.
文摘The key manufacturing technologies associated with composition, microstructure, mechanical properties, casting quality and key process control for large martensitic stainless steel castings are involved in this paper. The achievements fully satisfeid the technical requirements of the large 700 MW stainless steel hydraulic turbine runner for the Three Gorges Hydropower Station, and become the major technical support for the design and manufacture of the largest 700 MW hydraulic turbine generator unit in the world developed through our own efforts. The characteristics of a new high yield to tensile strength (R p0.2/R m ) ratio and high obdurability martensitic stainless steel with ultra low carbon and high cleanliness are also described. Over the next ten years, the large martensitic stainless steel castings and advanced manufacturing technologies will see a huge demand in clean energy industry such as nuclear power, hydraulic power at home and abroad. Therefore, the new high yield o tensile strength (R p0.2/R m ) ratio and high obdurability martensitic stainless steel materials, the fast and flexible manufacturing technologies of large size castings, and new environment friendly sustainable process will face new challenges and opportunities.
文摘Objective:To evaluate the performance parameters of adenosine triphosphat(ATP)bioluminescence detection technology in assessing surface cleanliness in surgical environments and on hand surfaces.Methods:Samples were collected from 20 orthopedic surgeons at five hand sites(fingertips,hypothenar eminence,thenar eminence,nail grooves of the index/middle fingers,and nail matrices)before and after handwashing.ATP bioluminescence assays and agar plate colony counting were performed to measure relative light unit(RLU)values and logarithmic total colony counts,respectively.Differences in RLU and colony counts across hand sites were compared.Linear regression analysis was conducted to assess the correlation between RLU values and log-transformed colony counts at each site.The water Raman signal-to-noise ratio(S/N)and detection limits were also determined.Results:A significant linear positive correlation was observed between RLU values and log colony counts on surgeons'hands,with the regression equation:y=-0.4580+0.127x(p<0.001,R^(2)=0.947).The sodium fluorescein standard demonstrated a water Raman S/N of 935.67 and detection limits of 0.86-51.53 RFU,both exceeding blank controls,with a wide linear range.Conclusion:ATP bioluminescence technology exhibits high sensitivity and precision for evaluating hand surface cleanliness,showing strong linear correlation with colony counts.Its detection limits surpass conventional standards,making it a robust tool for surgical hygiene monitoring.
文摘The Macao Science Satellite-1(MSS-1)is the first space science satellite jointly developed on the Chinese mainland and in Macao region.It comprises two satellites,named MSS-1A and MSS-1B,and holds considerable importance in China’s space exploration endeavors.Among these,MSS-1A is the world’s first high-precision scientific satellite dedicated to exploring the geomagnetic field and space environment at low latitudes.Equipped with two high-precision vector magnetometers and one scalar magnetometer,which are integrally installed on a highly stable nonmagnetic optical bench,the MSS-1A enables simultaneous high-precision measurements of both the Earth’s vector magnetic field and its scalar components.Its design integrates several state-of-the-art technologies,including arc-second-level thermal stability control,nonmagnetic thermal control for the optical bench,and ultra-high magnetic cleanliness control.These innovations effectively minimize magnetic interference originating from the satellite itself,thereby substantially improving the precision of geomagnetic field measurements and establishing a robust technical foundation for future magnetic survey satellite constellations.
文摘目的比较硫酸镁钠钾口服液(OSS)与复方聚乙二醇电解质散(PEG)在结肠镜检查前肠道准备中的安全性和有效性。方法回顾性分析2023月9月-2024年9月该院采用OSS与PEG在肠镜检查行前肠道准备的患者2000例。根据不同肠道准备药物,将患者分为OSS组(1000例,口服OSS)和PEG组(1000例,口服4 L PEG)。比较两组患者肠道清洁度、清洁效果、肠腔气泡、结肠镜检查阳性率和不良反应发生率。结果OSS组肠道准备成功率为92.5%(925/1000),PEG组肠道准备成功率为91.7%(917/1000),两组患者比较,差异无统计学意义(P>0.05);两组患者左侧结肠波士顿肠道准备量表(BBPS)评分比较,差异无统计学意义(P>0.05),OSS组BBPS总分,以及中段和右侧结肠BBPS评分明显高于PEG组,差异均有统计学意义(P<0.05);OSS组气泡评估满意率为96.2%,高于PEG组的90.3%,差异有统计学意义(P<0.05);两组患者结肠镜检查阳性率和不良反应发生率比较,差异均无统计学意义(P>0.05)。结论OSS在肠道准备方面具有较好的去泡效果,清洁效果与PEG相当,且有较高的安全性。