以碳纤维纸为电热材料,通过三聚氰胺改性脲醛树脂胶与纤维板基材叠层热压制备电热功能复合板,采用全因子试验方法探究热压压力及施胶量的影响。结果表明:热压压力对复合板电阻下降率(Drop rate of resistance,DRR)的影响不显著;施胶量...以碳纤维纸为电热材料,通过三聚氰胺改性脲醛树脂胶与纤维板基材叠层热压制备电热功能复合板,采用全因子试验方法探究热压压力及施胶量的影响。结果表明:热压压力对复合板电阻下降率(Drop rate of resistance,DRR)的影响不显著;施胶量的影响则极显著,胶黏剂的增加明显干扰电热层碳纤维搭接界面,两者呈高度线性下降关系,DRR变化范围在24%~40%。综合考虑内结合强度等性能,确定较优工艺参数为:压力0.8 MPa,双面施胶量130 g/m^2。展开更多
Objective： This study explored the effects of different light curing modes and ethanol-wet bonding on dentin bonding strength and durability. Methods： A total of 54 molars were randomly divided into three groups： S...Objective： This study explored the effects of different light curing modes and ethanol-wet bonding on dentin bonding strength and durability. Methods： A total of 54 molars were randomly divided into three groups： Single Bond 2, Gluma Comfort Bond, and N-Bond. Based on the three light-curing modes and presence or absence of eth- anol pretreatment, the samples were assigned to six subgroups： high-light mode, ethanol pretreatment＋high-light mode, soft-start mode, ethanol pretreatment＋soft-start mode, standard mode, and ethanol pretreatment＋standard mode. All samples were bonded with resin based on the experimental groups. After 24 h and 6 months of water storage, a universal testing machine was used to measure microtensile bond strength. Scanning electron microscopy （SEM） was applied to observe mixed layer morphology. Results： The 24-h and 6-month microtensile bond strengths of the ethanol pretreatment groups were significantly higher than those of the non-ethanol pretreatment groups at the same light modes （P〈0.05）. With or without ethanol pretreatment, the microtensile bond strengths of the high-light modes were significantly lower than those of the soft-start modes and standard modes （P〈0.05）. The microtensile bond strengths of samples from the 6-month water storage group significantly decreased compared with those of samples from the 24-h water storage group （P〈0.05）. The soft-start groups and standard groups formed better mixed layers than the high-light mode groups, whereas the ethanol pretreatment groups formed more uniform mixed layers than those without ethanol pretreatment. Conclusions： Ethanol-wet bonding technique, soft-start, and standard modes could improve dentin bonding properties.展开更多
基金Project supported by the Science and Technology Research Project of the Education Department of Jilin Province of China(No.(2015)527)
文摘Objective： This study explored the effects of different light curing modes and ethanol-wet bonding on dentin bonding strength and durability. Methods： A total of 54 molars were randomly divided into three groups： Single Bond 2, Gluma Comfort Bond, and N-Bond. Based on the three light-curing modes and presence or absence of eth- anol pretreatment, the samples were assigned to six subgroups： high-light mode, ethanol pretreatment＋high-light mode, soft-start mode, ethanol pretreatment＋soft-start mode, standard mode, and ethanol pretreatment＋standard mode. All samples were bonded with resin based on the experimental groups. After 24 h and 6 months of water storage, a universal testing machine was used to measure microtensile bond strength. Scanning electron microscopy （SEM） was applied to observe mixed layer morphology. Results： The 24-h and 6-month microtensile bond strengths of the ethanol pretreatment groups were significantly higher than those of the non-ethanol pretreatment groups at the same light modes （P〈0.05）. With or without ethanol pretreatment, the microtensile bond strengths of the high-light modes were significantly lower than those of the soft-start modes and standard modes （P〈0.05）. The microtensile bond strengths of samples from the 6-month water storage group significantly decreased compared with those of samples from the 24-h water storage group （P〈0.05）. The soft-start groups and standard groups formed better mixed layers than the high-light mode groups, whereas the ethanol pretreatment groups formed more uniform mixed layers than those without ethanol pretreatment. Conclusions： Ethanol-wet bonding technique, soft-start, and standard modes could improve dentin bonding properties.
