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Hydrothermal Synthesis of V<sub>3</sub>O<sub>7</sub>.<sup>.</sup>H<sub>2</sub>O Nanobelts and Study of Their Electrochemical Properties 被引量:1
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作者 Mohamed Kamel Chine Faouzi Sediri Neji Gharbi 《Materials Sciences and Applications》 2011年第8期964-970,共7页
Vanadium oxide hydrate V3O7..H2O (H2V3O8) nanobelts have been synthesized by hydrothermal approach using V2O5 as vanadium source and phenolphthalein as structure-directing agent. Techniques X-ray powder diffraction (X... Vanadium oxide hydrate V3O7..H2O (H2V3O8) nanobelts have been synthesized by hydrothermal approach using V2O5 as vanadium source and phenolphthalein as structure-directing agent. Techniques X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), infrared spectroscopy and nitrogen adsorption/desorption isotherms have been used to characterize the structure, morphology and composition of the nanobelts. The V3O7. H2O nanobelts are up to several hundreds of nanometers, the widths and thicknesses are 90 and 40 nm, respectively. The electroactivity of the nanobelts has been investigated. The as-synthesized material is promising for chemical and energy-related applications such as catalysts, electrochemical device and it may be applied in rechargeable lithium-ion batteries. 展开更多
关键词 NANOBELTS v3o7..h2o PHENOLPHTHALEIN HYDROTHERMAL Synthesis ELECTROACTIVITY
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水热合成V_3O_7·H_2O纳米带及其电化学性能研究 被引量:3
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作者 黄文达 高绍康 魏明灯 《华南师范大学学报(自然科学版)》 CAS 北大核心 2009年第A02期10-12,共3页
通过简单的水热法合成法制备出形貌均一、纯度高的V3O7.H2O纳米带.运用XRD、SEM、TEM、TG等手段对合成产物的结构和晶相进行了表征.结果表明材料具有优异的电化学性能.在电流密度为0.02 A/g条件下,首次放电比容量达到391 mAh/g,经过50... 通过简单的水热法合成法制备出形貌均一、纯度高的V3O7.H2O纳米带.运用XRD、SEM、TEM、TG等手段对合成产物的结构和晶相进行了表征.结果表明材料具有优异的电化学性能.在电流密度为0.02 A/g条件下,首次放电比容量达到391 mAh/g,经过50次循环仍然能够稳定在220 mAh/g. 展开更多
关键词 v3o7·h2o纳米带 水热合成 电化学性能
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