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Analysis and fusion methods on low light level image and ultra-violet image 被引量:10
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作者 BAI Lian-fa ZHANG Yi +2 位作者 GU Guo-hua CHEN Qian ZHANG Bao-min 《红外与激光工程》 EI CSCD 北大核心 2007年第1期113-117,共5页
on the basis of analyzing the characteristics of low light level(LLL)image and ultra-violet image and the information amount of dual channel color night vision system,the LLL and ultra-violet color night vision techni... on the basis of analyzing the characteristics of low light level(LLL)image and ultra-violet image and the information amount of dual channel color night vision system,the LLL and ultra-violet color night vision technique is put forward.The methods of gray-scale modulation,frequency field fusion,special component fusion arc tried,and the improved LLL and ultra-violet image pseudo color fusion algorithms are presented.These new algorithms include subsection gray-scale modulation,image difference picking-up,component separation based on the reflected characteristics to night skylight reflection characteristics of objects and color space mapping which embodies the spectrum response of image sensor and nature vision.Some good results are obtained. 展开更多
关键词 Imagc analysis Image fusion Low light level(LLL)image ultra-violet image DUAL-CHANNEL Color night vision system
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Material Properties and Mold Folded Core Based on Ultra-violet Cured Resins 被引量:1
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作者 Wang Zhijin Valentin Khaliulin +1 位作者 Vitality Kovalev Oskar Khamidullin 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI CSCD 2016年第5期529-535,共7页
Ultra-violet(UV)curing is an efficient method for composite molding.Firstly,thermophysical properties of UV cured glass-fiber reinforced plastics are conducted.Material properties are studied for various kinds of post... Ultra-violet(UV)curing is an efficient method for composite molding.Firstly,thermophysical properties of UV cured glass-fiber reinforced plastics are conducted.Material properties are studied for various kinds of postcuring modes.Then the UV curing method is suggested in manufacturing V-crimp folded core for sandwich panels.Two kinds of processing schemes for V-crimp folded core manufacturing using UV curing are presented.Finally,the effect of post-curing on the mechanical properties of folded core sandwiches is experimentally studied,and optimum modes of post-curing are determined.The experimental results show that the ultimate compressive strength of the folded sandwiches is increased by 60% after post-curing with the optimum post-curing mode. 展开更多
关键词 glass-fiber reinforced plastic composites ultra-violet(UV)curing V-crimp strength of folded core
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A spectroscopic study on the effect of ultra-violet solar radiation in Antarctica on the human skin fbroblast cells
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作者 Tatsuyuki Yamamoto Hideo Akiyoshi +5 位作者 Keisuke Yoshikiyo Tetsuya Takahashi Yukiko Tanabe Sakae Kudoh Satoshi Imurad Naoyuki Yamamoto 《Geoscience Frontiers》 SCIE CAS CSCD 2013年第6期647-653,共7页
A study on the effect of the solar ultra-violet radiation on the human skin fibroblast cells revealed that the production of matrix metalloproteinase-2 was inhibited by the radiation.A CO2 incubator connected by optic... A study on the effect of the solar ultra-violet radiation on the human skin fibroblast cells revealed that the production of matrix metalloproteinase-2 was inhibited by the radiation.A CO2 incubator connected by optical fibers to a reflector telescope for collecting the solar light was built at Syowa station by the 49th Japanese Antarctica Research Expedition.The direction of the telescope was continuously controlled by a sun-tracker to follow the movement of the Sun automatically.The intensity of the collected light was monitored by a portable spectrophotometer housed inside.The human skin fibroblast cells were incubated in the CO2 chamber to investigate the effect of the solar radiation at Syowa station and were compared with those reference experiments at a laboratory in Japan.The results showed cell damage by strong UV radiation.The production of matrix metalloproteinase-2 was prompted by the moderate UV-B,but was inhibited by the strong UV-B radiation,as studied under laboratory conditions in Japan.The effect of strong solar radiation at Syowa station involving the radiation of UV-B region was estimated to be of the same extent of the radiation caused by an artificial UV-B light with the intensity more than 50 mJ/cm2. 展开更多
关键词 ANTARCTICA GEOBIOLOGY ultra-violet radiation Human skin fibroblast cells Matrix metalloproteinase
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Photocatalytic Activity of Titanium Dioxide Powder Fabricated from an Anodized Titanium Sheet under Ultra-Violet and Visible Light Irradiation
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作者 Michio Kaneko Kiyonori Tokuno +2 位作者 Kazuo Yamagishi Takao Wada Tsuyoshi Hasegawa 《Journal of Surface Engineered Materials and Advanced Technology》 2017年第1期13-23,共11页
A commercially pure titanium sheet with titanium carbide (TiC) precipitated in its surface layer was anodized in NH4NO3 aqueous solution and heat treated in air. The photocatalytic activity of titanium dioxide powder ... A commercially pure titanium sheet with titanium carbide (TiC) precipitated in its surface layer was anodized in NH4NO3 aqueous solution and heat treated in air. The photocatalytic activity of titanium dioxide powder collected from the surface of the anodized titanium sheet was evaluated under ultra-violet and visible light irradiation. It showed relatively high photocatalytic activity in 0.1 mol/l potassium iodide solution, which was almost equal to the activity level of TiO2 powder (P-25) manufactured by Degussa Corporation. The better photocatalytic activity under ultra-violet irradiation is considered to be related to the formation of anatase type titanium dioxide. Photocatalytic activity under visible light irradiation was also observed, which was considered to be attributable to impurity doping, (carbon), in the titanium dioxide powder. 展开更多
关键词 Photocatalysis TITANIUM TITANIUM Dioxide POWDER Anodic Oxidation ultra-violet VISIBLE-LIGHT Response
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Detecting Ultra-Violet Radiation by Using Titanium Dioxide Nanoparticles
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作者 Naser Hatefi Kargan Mousa Aliahmad Samereh Azizi 《Soft Nanoscience Letters》 2012年第3期29-33,共5页
In this paper sensitivity of chemically synthesized titanium dioxide (TiO2) nanoparticles to ultra-violet (UV) radiation is investigated. For this purpose three types of ultra-violet photodetectors were fabricated, on... In this paper sensitivity of chemically synthesized titanium dioxide (TiO2) nanoparticles to ultra-violet (UV) radiation is investigated. For this purpose three types of ultra-violet photodetectors were fabricated, one with as-synthesized TiO2 nanoparticles, another one with TiO2 nanoparticles annealed at 600℃, and the third one with TiO2 nanoparticles annealed at 800℃. In each case the annealing time duration was one hour. The photodetectors were fabricated on glass slides where on them a thin layer of fluorine doped tin oxide (FTO) was deposited by spray pyrolysis. The results show that all photodetectors are sensitive to UV radiation where the photodetectors fabricated from annealed TiO2 nanoparticles are more sensitive than the photodetectors fabricated from as-synthesized TiO2 nanoparticles. 展开更多
关键词 ultra-violet PHOTODETECTOR TITANIUM Dioxide NANOCRYSTALS Nanoparticles
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Biological Defenses against Ultra-Violet, Visible Light, and Near-Infrared Exposure
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作者 Yohei Tanaka Hideki Motomura Masafumi Jinno 《Optics and Photonics Journal》 2016年第1期8-14,共7页
Objective: Humans are increasingly exposed to artificial light and electromagnetic wave radiation, in addition to solar radiation. Many studies have shown the biological effects of ultra-violet and near-infrared expos... Objective: Humans are increasingly exposed to artificial light and electromagnetic wave radiation, in addition to solar radiation. Many studies have shown the biological effects of ultra-violet and near-infrared exposure, but few have extensively investigated the innate biological defenses within human tissues against visible light and near-infrared exposure. Herein, we investigated spectral properties of endogenous human biological defenses against ultra-violet to near-infrared. Methods: A double-beam spectrophotometer (190 - 2700 nm) was used to measure the transmission spectra of a saline solution used to imitate perspiration, and oil to imitate sebum, as well as human skin, blood, adipose tissue, and muscle. Results: Saline (thickness, 0.5 mm) blocked 27.5% - 98.6% of ultra-violet, 13.2% - 34.3% of visible light, and 10.7% - 99.8% of near-infrared. Oil (thickness, 0.5 mm) blocked 50.5% - 100% of ultra-violet, 28.7% - 54.8% of visible light, and 19.0% - 98.3% of near-infrared. Blood thicknesses of 0.05 and 0.5 mm blocked over 97.8%, 100% of ultra-violet, over 94.6%, 99.7% of visible light, and over 75.8%, 99.4% of near-infrared, respectively. Skin thicknesses of 0.25 and 0.5 mm blocked over 99.4%, 100% of ultra-violet and over 94.3%, 99.7% of visible light, and over 74.7%, 93.5% of near-infrared, respectively. Adipose tissue thickness of 0.25 and0.5 mm blocked over 98.3%, 100% of ultra-violet, over 94.7%, 99.7% of visible light, and over 88.1%, 98.6% of near-infrared, respectively. Muscle thickness of 0.25 and0.5 mm blocked over 95.4%, 99.8% of ultra-violet, over 93.1%, 99.5% of visible light, and over 86.9%, 98.3% of near-infrared, respectively. Conclusions: Humans possess endogenous biological protection against ultra-violet, visible light and near-infrared exposure on multiple levels, including through perspiration, sebum, blood, skin, adipose tissue, and muscle. Since solar and artificial radiation affects human tissues, biological defenses made of biological materials may be induced to protect subcutaneous tissues against these wavelengths. 展开更多
关键词 Biological Defenses NEAR-INFRARED ultra-violet Visible Light
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乳酸钙结合UV-C处理对鲜切油桃贮藏品质的影响
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作者 王宏宇 林子沁 +5 位作者 杨梦娇 李娇 吕芳娥 姜瑜倩 刘杰 李喜宏 《保鲜与加工》 北大核心 2025年第5期24-31,40,共9页
为探究乳酸钙(CA-L)和短波紫外线(UV-C)联合处理对鲜切油桃贮藏品质的影响,以‘中油19’油桃为试材,采用3 g/L CA-L浸泡5 min和1.23 kJ/m2 UV-C辐照单独及联合处理,于(4±1)℃条件下贮藏10 d,定期测定鲜切油桃硬度、L^(*)值、褐变指... 为探究乳酸钙(CA-L)和短波紫外线(UV-C)联合处理对鲜切油桃贮藏品质的影响,以‘中油19’油桃为试材,采用3 g/L CA-L浸泡5 min和1.23 kJ/m2 UV-C辐照单独及联合处理,于(4±1)℃条件下贮藏10 d,定期测定鲜切油桃硬度、L^(*)值、褐变指数(BI)、可溶性固形物(TSS)含量、可滴定酸(TA)含量、丙二醛(MDA)含量、多酚氧化酶(PPO)活性、过氧化物酶(POD)活性、过氧化氢酶(CAT)活性及苯丙氨酸解氨酶(PAL)活性。结果表明,贮藏10 d时,CA-L和UV-C单独或联合处理组的硬度、L^(*)值、TSS含量、TA含量、CAT活性、PAL活性均显著高于对照组(P<0.05),BI、MDA含量、PPO活性及POD活性均显著低于对照组(P<0.05)。CA-L和UV-C单独或联合处理对鲜切油桃均有一定的保鲜效果,且两者结合效果最佳。贮藏10 d时,CA-L+UV-C处理组的硬度、L^(*)值、CAT活性、PAL活性分别比对照组高15.48%、10%、52.7%、77%,TSS含量和TA含量分别比对照组高1.13个百分点和0.52个百分点,BI、MDA含量、PPO活性和POD活性分别比对照组低15.27%、19.58%、34.57%、28.46%。综上所述,该研究证明CA-L与UV-C联合处理可以作为一种有效延缓鲜切油桃品质劣变的保鲜方式,为其在果蔬保鲜领域广泛应用奠定理论基础。 展开更多
关键词 鲜切油桃 乳酸钙 短波紫外线 贮藏品质
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紫外光谱结合化学计量学用于青稞酒的判别分析
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作者 张世芝 王茹 +1 位作者 赵玉霞 张明锦 《分析测试学报》 北大核心 2025年第6期1107-1114,共8页
青稞酒是源自青藏高原、以青稞为原料的著名酒类饮品。然而,随着其市场不断扩大、品种不断增多,掺假问题已成为亟待关注的焦点。该研究聚焦于运用紫外光谱法快速鉴别地理标志保护产品互助青稞酒,提出主成分分析-支持向量机(PCA-SVM)和... 青稞酒是源自青藏高原、以青稞为原料的著名酒类饮品。然而,随着其市场不断扩大、品种不断增多,掺假问题已成为亟待关注的焦点。该研究聚焦于运用紫外光谱法快速鉴别地理标志保护产品互助青稞酒,提出主成分分析-支持向量机(PCA-SVM)和多模型偏最小二乘判别分析(MPLS-DA)两种方法。研究涉及中国互助青稞酒(CHQL)、其他品牌青稞酒(OBQL)和非青稞白酒(NQBL)3类样品。SVM采用两个主成分解决二元分类问题,而MPLS-DA对虚拟变量Y的每一列使用PLS1算法建模后,整合子模型的预测结果。PCASVM和MPLS-DA均成功构建了CHQL的判别模型。PCA-SVM能区分CHQL与OBQL、NQBL,但无法区分OBQL和NQBL。相比之下,MPLS-DA能正确识别所有3类样品,可以解决多分类问题。结果表明,所提方法可作为CHQL的一种简便快速鉴别手段,且MPLS-DA展现出更优的样品识别能力。 展开更多
关键词 中国互助青稞酒 紫外光谱 化学计量学 判别分析
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Planar structure of organic photodetector for low dark current
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作者 Mohammad Nofil Amirul Ashraf Md Sabri +4 位作者 Fadlan Arif Natashah Tahani M Bawazeer Mohammad S Alsoufi Nur Adilah Roslan Azzuliani Supangat 《Chinese Physics B》 2025年第2期290-295,共6页
The focus of this study is on investigating the vanadyl 2,9,16,23-tetraphenoxy-29H, 31H-phthalocyanine(VOPc Ph O)and its blend with o-xylenyl C60 bis-adduct(OXCBA), for use as a lateral ultraviolet organic photodetect... The focus of this study is on investigating the vanadyl 2,9,16,23-tetraphenoxy-29H, 31H-phthalocyanine(VOPc Ph O)and its blend with o-xylenyl C60 bis-adduct(OXCBA), for use as a lateral ultraviolet organic photodetector. The research focuses on improving dark current reduction, which is a challenge in lateral organic photodetector. By integrating the OXCBA, low dark current values of 4.83 nA·cm^(-2)(D_(shot)^(*)= 1.414 × 10^(11)Jones) have been achieved as compared to the stand-alone VoPcPhO device of 14.06 nA·cm^(-2). The major contributing factors to dark current reduction are due to the efficient charge transfer at the photoactive-electrode interface, the deep highest occupied molecular orbital(HOMO)level of OXCBA, which leads to favorable energy level alignments hindering hole injection, and the occurrence of bulk heterojunction vertical phase segregation between VOPcPhO and OXCBA. These findings shed light on the relationship between the organic photoconductor's material composition, morphology, and performance metrics and open new avenues for metal phthalocyanine-based lateral ultraviolet organic photodetectors with low dark current and enhanced performance. 展开更多
关键词 small molecule dark current ultra-violet(UV)sensor device physics
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FPGA在319nm紫外单频激光系统锁频中的应用
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作者 苏雯静 卫怡荣 +3 位作者 侯晓凯 王越伟 何军 王军民 《量子光学学报》 北大核心 2025年第1期106-116,共11页
窄线宽、可连续调谐的319 nm紫外单频激光系统对铯原子的单步里德堡激发有重要意义。以高精细度超稳光学腔作为频率参考标准,结合射频位相调制边带PDH(Pound-Drever-Hall)技术、电子学边带技术、无调制HC(Hansch-Couillaud)技术,实现319... 窄线宽、可连续调谐的319 nm紫外单频激光系统对铯原子的单步里德堡激发有重要意义。以高精细度超稳光学腔作为频率参考标准,结合射频位相调制边带PDH(Pound-Drever-Hall)技术、电子学边带技术、无调制HC(Hansch-Couillaud)技术,实现319 nm紫外单频激光系统的频率锁定。然而常规反馈锁定系统存在结构较复杂、体积较庞大、成本较高等缺点,我们通过利用FPGA(Field Programmable Gate Array)代替信号发生器、锁相放大器、PID(Proportional-Integral-Derivative)放大器、示波器等分立设备来实现激光频率的锁定,对常规的反馈锁定系统进行简化和升级;基于Red Pitaya的FPGA板卡,利用射频位相调制边带PDH技术以及电子学边带技术对基频光进行锁定,并对射频位相调制边带PDH技术和无调制HC技术对四镜环形倍频腔的锁频效果进行了比较。FPGA的应用,在实验操作中不仅能够显著地降低成本、简化实验系统,并且充分节约使用空间,带来极大便利,有着较高的集成度、高度的灵活性、良好的稳定性。 展开更多
关键词 现场可编程门阵列(FPGA) 319nm单频紫外激光 PDH锁定 电子学边带锁定 HC锁定
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超声辅助酶解法提取废弃烟草活性多糖的条件优化及其结构特征分析
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作者 杨瑞丽 莫琬滢 +2 位作者 徐志强 徐毅 贺增洋 《中国烟草学报》 北大核心 2025年第4期110-116,共7页
【目的】拟优化烟草多糖的提取方法并明确其结构特征。【方法】以田间弃烤烟叶为原料,采用超声辅助酶解法提取粗多糖,采用葡聚糖层析手段进行分离纯化,分析提取条件对提取率的影响及纯化多糖的结构特征。【结果】(1)当使用料液比(质量... 【目的】拟优化烟草多糖的提取方法并明确其结构特征。【方法】以田间弃烤烟叶为原料,采用超声辅助酶解法提取粗多糖,采用葡聚糖层析手段进行分离纯化,分析提取条件对提取率的影响及纯化多糖的结构特征。【结果】(1)当使用料液比(质量体积比)1:60、超声时间20 min、超声功率200 W、温度45℃时,烟草粗多糖的提取率可达3.15%;当使用酶浓度1.5%、酶解时间80 min、温度55℃、pH 5.5时,烟草粗多糖的提取率可达4.75%。(2)对辅助酶解法的工艺顺序优化后,先酶解后超声的提取方法效果最好,粗多糖的提取率可达6.42%。(3)经过DEAE-52纤维素柱层析后,多糖纯度较高,且具有β-型异头碳的结构,主要由1,4连接的葡萄糖苷和1,4连接的甘露糖苷键组成。【结论】先酶解后超声的方法对烟草活性多糖的提取比较有利,所获得的新活性多糖具有β-型异头碳的结构特征。 展开更多
关键词 烟草多糖 超声辅助酶解法 正交分析 结构鉴定 红外光谱 紫外光谱
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单针射频联合白灵片对稳定期非节段型白癜风经络瘀阻证的治疗效果
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作者 徐婉妮 杨广智 刘靖 《贵州医科大学学报》 2025年第3期434-441,449,共9页
目的探讨单针射频联合白灵片治疗稳定期非节段型白癜风经络瘀阻证的疗效及安全性。方法将66例稳定期非节段型白癜风患者随均机分为3组,治疗组运用单针射频联合白灵片治疗,对照1组予窄谱中波紫外线(narrow bound ultra violet B light,NB... 目的探讨单针射频联合白灵片治疗稳定期非节段型白癜风经络瘀阻证的疗效及安全性。方法将66例稳定期非节段型白癜风患者随均机分为3组,治疗组运用单针射频联合白灵片治疗,对照1组予窄谱中波紫外线(narrow bound ultra violet B light,NB-UVB)联合白灵片治疗,对照2组予白灵片治疗,疗程12周;比较3组患者的一般资料、治疗后疗效,观察治疗前及治疗第4、8及12周时白斑面积、色素恢复情况(平均复色率、白斑色素积分),记录治疗期间不良反应情况;随访12周,观察预后。结果3组患者性别、年龄、病程、白斑数量及面积、白斑部位比较,差异无统计学差异(P>0.05),具有可比性;治疗组显效率明显高于对照1组和对照2组(P<0.001);治疗后,治疗组白斑面积小于对照1组及对照2组(P<0.05);治疗第4周开始,治疗组白癜风患者白斑处的复色率明显高于对照1组和对照2组(P<0.001);治疗前,治疗组与对照1组和对照2组白斑色素积分比较,差异无统计学意义(P>0.05);治疗12周,治疗组白斑色素积分明显高于与对照1组和对照2组(P<0.001);在治疗期间,所有患者均未出现严重不良反应,3组不良反应发生率比较,差异无统计学意义(P>0.05);治疗结束后随访患者12周,患者无明显新发白斑及迟发不良反应。结论单针射频联合白灵片治疗稳定期非节段型白癜风经络瘀阻证临床疗效好,不良反应少。 展开更多
关键词 白癜风 单针射频 白灵片 窄谱中波紫外线
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极紫外光刻物镜热致波前畸变及自适应光学校正
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作者 于文浩 刘畅 +2 位作者 李欣 马利婷 张之光 《激光杂志》 北大核心 2025年第10期27-33,共7页
芯片不断缩小的特征尺寸对光刻技术提出愈发严苛的要求,极紫外光刻(Extreme Ultra-Violet Lithography,EUVL)作为当前最有前景的新一代光刻技术,其性能受到物镜热致形变所引起波前畸变的严重影响。物镜吸收光源能量产生的热负荷导致镜... 芯片不断缩小的特征尺寸对光刻技术提出愈发严苛的要求,极紫外光刻(Extreme Ultra-Violet Lithography,EUVL)作为当前最有前景的新一代光刻技术,其性能受到物镜热致形变所引起波前畸变的严重影响。物镜吸收光源能量产生的热负荷导致镜面形变,进而造成光学投影系统中的热致波前畸变。针对此问题,采用ANSYS软件模拟了EUVL物镜在激光照射下的热应力和形变情况,利用光线追踪技术得到波前畸变,对比分析了采用自适应光学技术进行校正时变形镜单元数的不同对校正能力的影响。结果表明,单元数越多的变形镜具有更强的校正能力,对于畸变的主导分量第三阶Zernike模式,97单元变形镜的波前拟合残余RMS值低于0.24λ,拟合误差相较于61单元和88单元变形镜显著降低。研究为EUVL系统的性能优化提供了理论依据。 展开更多
关键词 极紫外光刻 自适应光学 热应力 光线追踪 波前畸变
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Photoionization Mass Spectrometric and Kinetic Modeling of Low-pressure Pyrolysis of Benzene 被引量:2
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作者 杨玖重 赵龙 +2 位作者 蔡江淮 齐飞 李玉阳 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2013年第3期245-251,I0003,共8页
Pyrolysis of benzene at 30 Torr was studied from 1360 K to 1820 K in this work. Synchrotron vacuum ultraviolet photoionization mass spectrometry was employed to detect the pyroly- sis products such as radicals, isomer... Pyrolysis of benzene at 30 Torr was studied from 1360 K to 1820 K in this work. Synchrotron vacuum ultraviolet photoionization mass spectrometry was employed to detect the pyroly- sis products such as radicals, isomers and polycyclic aromatic hydrocarbons, and measure their mole fraction profiles versus temperature. A low-pressure pyrolysis model of benzene was developed and validated by the experimental results. Rate of production analysis was performed to reveal the major reaction networks in both fuel decomposition and aromatic growth processes. It is concluded that benzene is mainly decomposed via H-abstraction reaction to produce phenyl and partly decomposed via unimolecular decomposition reac- tions to produce propargyl or phenyl. The decomposition process stops at the formation of acetylene and polyyne species like diacetylene and 1,3,5-hexatriyne due to their high thermal stabilities. Besides, the aromatic growth process in the low-pressure pyrolysis of benzene is concluded to initiate from benzene and phenyl, and is controlled by the even carbon growth mechanism due to the inhibited formation of C5 and C7 species which play important roles in the odd carbon growth mechanism. 展开更多
关键词 BENZENE Low-pressure pyrolysis PAH formation Synchrotron vacuum ultra-violet photoionization mass spectrometry Kinetic model
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超高效液相色谱-串联质谱法快速测定鱼类中孔雀石绿、结晶紫及其隐色代谢物残留量 被引量:1
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作者 屠瑞莹 陈东 +2 位作者 刘伟 范赛 赵榕 《食品安全质量检测学报》 2025年第14期57-63,共7页
目的建立固相萃取技术(solid-phase extraction,SPE)结合超高效液相色谱-串联质谱法(ultra performance liquid chromatography-tandem mass spectrometry,UPLC-MS/MS)测定鱼类中孔雀石绿、结晶紫、隐色孔雀石绿、隐色结晶紫的方法。方... 目的建立固相萃取技术(solid-phase extraction,SPE)结合超高效液相色谱-串联质谱法(ultra performance liquid chromatography-tandem mass spectrometry,UPLC-MS/MS)测定鱼类中孔雀石绿、结晶紫、隐色孔雀石绿、隐色结晶紫的方法。方法样品经乙腈沉淀蛋白并萃取后,过HMR-Lipid SPE柱通过式净化。以乙腈和乙酸铵溶液为流动相梯度洗脱,采用BEH shield C18色谱柱分离,电喷雾离子源正离子模式进行多反应监测(multiple reaction monitoring,MRM)扫描,内标法定量。结果4种目标化合物的线性范围在0.20~10.00 ng/mL,相关系数(r)大于0.999,检出限为0.05μg/kg。3个加标水平下(2、5、10μg/kg)的回收率为80.1%~105.2%,相对标准偏差为1.2%~14.3%。结论本方法灵敏、快速、准确,适用于鱼类中孔雀石绿、结晶紫及其的隐色代谢物的检测,可为鱼类的质量检测及市场监管提供技术支撑。 展开更多
关键词 超高效液相色谱-串联质谱法 孔雀石绿 结晶紫 隐色孔雀石绿 隐色结晶紫 鱼类
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IMPROVEMENT OF DIMENSIONAL ACCURACY FOR GOLD MICROPART PREPARED BY UV-LIGA
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作者 曲宁松 苏兴 +1 位作者 李寒松 曾永彬 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2012年第4期325-330,共6页
The swelling of SU-8 mold is one of the most important factors influencing the dimensional accuracy of a metal mieropart produced by ultra-violet lithography galvanik abformung(UV-LIGA). The isolation belt struc- tu... The swelling of SU-8 mold is one of the most important factors influencing the dimensional accuracy of a metal mieropart produced by ultra-violet lithography galvanik abformung(UV-LIGA). The isolation belt struc- ture is usually employed to enhance the dimensional accuracy of electroformed metal mieropart. However, noble metal is wasted because the isolation belt is filled with metal when noble metal mieroparts are fabricated. There- fore, a semi-isolation belt structure is presented to save noble metal. Furthermore, a high current density is also introduced to shorten the eleetroforming time, and thus the dimensional accuracy of electroformed gold micropart is improved by using the electrolyte jet. The experimental results indicate that both the semi-isolation belt and the high current density can help to enhance the dimensional accuracy of electroformed gold micropart. Its dimen- sional error is only 5 μm at the current density of 0. 6 A/dm2 while the semi-isolation belt structure is used. 展开更多
关键词 ultra-violet lithography galvanik abformung (UV-LIGA) microelectroforming micropart dimen- sional accuracy swelling of SU-8 structure
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超细CeO_2粉体的制备及其紫外线吸收性能 被引量:34
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作者 朱兆武 龙志奇 +2 位作者 崔大立 张顺利 张国成 《中国有色金属学报》 EI CAS CSCD 北大核心 2005年第3期435-440,共6页
用碳酸氢铵作沉淀剂通过添加NH4NO3和(NH4)2CO4两种不同的试剂制备了超细CeO2粉体.采用X射线衍射、BET和激光散射的方法研究了不同灼烧温度下粉体粒径的变化规律,并研究了粉体粒径对紫外线吸收的影响.结果表明:NH4NO3和(NH4)2CO4作为添... 用碳酸氢铵作沉淀剂通过添加NH4NO3和(NH4)2CO4两种不同的试剂制备了超细CeO2粉体.采用X射线衍射、BET和激光散射的方法研究了不同灼烧温度下粉体粒径的变化规律,并研究了粉体粒径对紫外线吸收的影响.结果表明:NH4NO3和(NH4)2CO4作为添加剂可以制得一次粒径在10~100 nm的纳米粉体,团聚粒径在200~300 nm分散性好的超细CeO2粉体.X射线衍射和BET测得的一次粒径随灼烧温度升高呈明显增大的趋势,激光散射测得的团聚粒径随灼烧温度变化不明显.CeO2粉体分散在去离子水中的吸收光谱研究表明,粉体一次粒径大小对光的吸收效果有明显影响,粒径小,紫外线吸收效果好,可见光穿透性强,粒径增大,粉体将失去紫外线吸收效果,紫外吸收受粉体的团聚粒径影响不大. 展开更多
关键词 超细CeO2粉体 制备 紫外吸收
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纳米TiO_2制备及其应用新进展 被引量:67
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作者 肖奇 邱冠周 +1 位作者 胡岳华 王淀佐 《材料导报》 EI CAS CSCD 北大核心 2000年第8期35-37,74,共4页
纳米二氧化钛是重要的无机化工材料之一,简单介绍了它的制备方法,着重阐述了湿化学方法制备纳米二氧化钛的研究情况,并详细探讨了它在光催化、光电转换以及紫外线屏蔽剂等新领域的应用。
关键词 光催化剂 温化学法 纳米二氧化钛 制备
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基于紫外脉冲检测的非接触式特高压验电仪 被引量:20
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作者 汪金刚 何为 +3 位作者 李青文 杨帆 杨永明 陈涛 《电工技术学报》 EI CSCD 北大核心 2008年第5期137-142,共6页
随着电压等级的升高,采用长杆上套装电压互感器的验电方式越来越难以满足高压输电系统发展的需求。本文提出一种非接触式特高压紫外验电方法,采用极高灵敏度的日盲型紫外探头,对传输线、开关等高压设备的电晕放电中的紫外脉冲数量进行... 随着电压等级的升高,采用长杆上套装电压互感器的验电方式越来越难以满足高压输电系统发展的需求。本文提出一种非接触式特高压紫外验电方法,采用极高灵敏度的日盲型紫外探头,对传输线、开关等高压设备的电晕放电中的紫外脉冲数量进行实时检测,确定线路带电状态。并基于该方法开发了UHVES?I型紫外验电仪,先后在高压大厅、西北电网西宁工区750kV官亭变电站、四川洪沟500kV变电站、重庆邮亭220kV变电站进行验电试验。试验结果表明,UHVES?I型紫外验电仪在高压电磁环境下能够稳定工作,能够准确检测高压线路、开关等关键输电设备的带电状态,其操作简便,无需登塔,检测效率高。 展开更多
关键词 紫外脉冲 电晕放电 特高压 验电仪
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锐钛矿、金红石和板钛矿降解罗丹明B光催化活性的比较(英文) 被引量:14
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作者 张静 阎松 +6 位作者 付鹿 王飞 原梦琼 罗根祥 徐倩 王翔 李灿 《催化学报》 SCIE EI CAS CSCD 北大核心 2011年第6期983-991,共9页
详细考察并比较了采用低温制备的锐钛矿、金红石和板钛矿氧化钛降解罗丹明B的光催化活性.与传统高温焙烧制备的金红石相比,低温制备的金红石粒径小,比表面积大,表面羟基数目多,因此光催化效率明显增加.更重要的是,当锐钛矿和金红石具有... 详细考察并比较了采用低温制备的锐钛矿、金红石和板钛矿氧化钛降解罗丹明B的光催化活性.与传统高温焙烧制备的金红石相比,低温制备的金红石粒径小,比表面积大,表面羟基数目多,因此光催化效率明显增加.更重要的是,当锐钛矿和金红石具有相似粒径和比表面积时,金红石具有较高的光降解罗丹明B活性.对于板钛矿氧化钛而言,虽然其表观光催化活性(单位时间内降解的罗丹明B)远低于锐钛矿或金红石的表观光催化活性,但是其本征光催化活性(单位比表面积、单位时间内降解的罗丹明B)却远远高于锐钛矿或金红石的本征光催化活性. 展开更多
关键词 氧化钛 紫外拉曼 晶相 罗丹明B 光催化 降解
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