Powder metallurgy（PM） Ti–22Al–24Nb–0.5Mo（at.%） alloys were prepared by hot isostatic pressing. In order to study the feasibility of PM ＋ ring rolling combined process for preparing Ti_2AlNb rings, thermal mech...Powder metallurgy（PM） Ti–22Al–24Nb–0.5Mo（at.%） alloys were prepared by hot isostatic pressing. In order to study the feasibility of PM ＋ ring rolling combined process for preparing Ti_2AlNb rings, thermal mechanical simulation tests of PM Ti_2AlNb alloys were conducted and two rectangular PM rings（150 mm in height, 75 mm in thickness,350 mm in external diameter） were rolled as a validation experiment. Experimental results show that the flow stress of Ti_2AlNb alloys exhibited a significant drop at the very beginning of the deformation（true strain／0.1）, and became stable with the increase in strain. Stress instability phenomenon of PM Ti_2AlNb alloys was more obvious than that of wrought alloy. Flow stress fluctuation at the initial stage of deformation is related to phase transition of Ti_2AlNb alloys which strongly depends on heat treatment and thermal mechanical deformation process. Processing windows during initial stage of ring rolling process is very crucial. A sound PM Ti_2AlNb rectangular ring blank（height = 150 mm, thickness = 30 mm, external diameter = 750 mm） was successfully rolled in two passes by using the improved heat preservation method and optimized rolling parameters. Tensile properties of PM Ti_2AlNb alloy were improved, and the porosity was reduced after ring rolling.展开更多
A 1040°C-hot-deformed Ti_2AlNb-based alloy solution-treated at 950°C and aged at different temperatures was quantitatively investigated. The microstructure, size of the phase, and microhardness of the deform...A 1040°C-hot-deformed Ti_2AlNb-based alloy solution-treated at 950°C and aged at different temperatures was quantitatively investigated. The microstructure, size of the phase, and microhardness of the deformed alloys were measured. The results indicated that the microstructure of the deformed Ti_2AlNb-based alloy specimens comprise coarse O lath, fine O lath, equiaxed O/α_2, and acicular O phase. More O phase was generated in the deformed alloy after heat treatment because the acicular O phase was more likely to nucleate and grow along the deformation-induced crystal defects such as dislocations and subgrain boundaries. After deformation and subsequent heat treatment, the acicular O phase of the resultant alloy became finer compared to that of the undeformed alloy, and the acicular O phase became coarser and longer with the elevated aging temperature, while the width of the O lath exhibited unobvious variations. The hot deformation facilitated the dissolution of the O lath but accelerated the precipitation of the acicular O phase. When the 950°C-solution-treated deformed Ti_2AlNb-based alloy was then aged at 750°C for different periods, the phase content was nearly invariable, O and B2 phases eventually reached equilibrium, and the microstructure became stable and homogeneous.展开更多
文摘Powder metallurgy（PM） Ti–22Al–24Nb–0.5Mo（at.%） alloys were prepared by hot isostatic pressing. In order to study the feasibility of PM ＋ ring rolling combined process for preparing Ti_2AlNb rings, thermal mechanical simulation tests of PM Ti_2AlNb alloys were conducted and two rectangular PM rings（150 mm in height, 75 mm in thickness,350 mm in external diameter） were rolled as a validation experiment. Experimental results show that the flow stress of Ti_2AlNb alloys exhibited a significant drop at the very beginning of the deformation（true strain／0.1）, and became stable with the increase in strain. Stress instability phenomenon of PM Ti_2AlNb alloys was more obvious than that of wrought alloy. Flow stress fluctuation at the initial stage of deformation is related to phase transition of Ti_2AlNb alloys which strongly depends on heat treatment and thermal mechanical deformation process. Processing windows during initial stage of ring rolling process is very crucial. A sound PM Ti_2AlNb rectangular ring blank（height = 150 mm, thickness = 30 mm, external diameter = 750 mm） was successfully rolled in two passes by using the improved heat preservation method and optimized rolling parameters. Tensile properties of PM Ti_2AlNb alloy were improved, and the porosity was reduced after ring rolling.
基金the National Natural Science Foundation of China(Nos.51474156 and U1660201)the National Magnetic Confinement Fusion Energy Research Program of China(No.2015GB119001)for their grants and financial supports
文摘A 1040°C-hot-deformed Ti_2AlNb-based alloy solution-treated at 950°C and aged at different temperatures was quantitatively investigated. The microstructure, size of the phase, and microhardness of the deformed alloys were measured. The results indicated that the microstructure of the deformed Ti_2AlNb-based alloy specimens comprise coarse O lath, fine O lath, equiaxed O/α_2, and acicular O phase. More O phase was generated in the deformed alloy after heat treatment because the acicular O phase was more likely to nucleate and grow along the deformation-induced crystal defects such as dislocations and subgrain boundaries. After deformation and subsequent heat treatment, the acicular O phase of the resultant alloy became finer compared to that of the undeformed alloy, and the acicular O phase became coarser and longer with the elevated aging temperature, while the width of the O lath exhibited unobvious variations. The hot deformation facilitated the dissolution of the O lath but accelerated the precipitation of the acicular O phase. When the 950°C-solution-treated deformed Ti_2AlNb-based alloy was then aged at 750°C for different periods, the phase content was nearly invariable, O and B2 phases eventually reached equilibrium, and the microstructure became stable and homogeneous.
