To explore the formation mechanism of anisotropy in Ti-6Al-4V alloy fabricated by selective laser melting(SLM),the compressive mechanical properties,microhardness,microstructure,and crystallographic orientation of the...To explore the formation mechanism of anisotropy in Ti-6Al-4V alloy fabricated by selective laser melting(SLM),the compressive mechanical properties,microhardness,microstructure,and crystallographic orientation of the alloy across different planes were investigated.The anisotropy of SLM-fabricated Ti-6Al-4V alloys was analyzed,and the electron backscatter diffraction technique was used to investigate the influence of different grain types and orientations on the stress-strain distribution at various scales.Results reveal that in room-temperature compression tests at a strain rate of 10^(-3) s^(-1),both the compressive yield strength and microhardness vary along the deposition direction,indicating a certain degree of mechanical property anisotropy.The alloy exhibits a columnar microstructure;along the deposition direction,the grains appear equiaxed,and they have internal hexagonal close-packed(hcp)α/α'martensitic structure.α'phase has a preferential orientation approximately along the<0001>direction.Anisotropy arises from the high aspect ratio of columnar grains,along with the weak texture of the microstructure and low symmetry of the hcp crystal structure.展开更多
Al-Cu-Mn-Mg合金因其优异的综合性能,被广泛应用于航空航天和轨道交通等领域。然而,该合金在铸造过程中容易出现热裂缺陷,严重影响铸件的质量和可靠性。因此,提高合金的晶粒细化效果,对于改善合金的铸造性能具有重要意义。Al-Ti-B细化...Al-Cu-Mn-Mg合金因其优异的综合性能,被广泛应用于航空航天和轨道交通等领域。然而,该合金在铸造过程中容易出现热裂缺陷,严重影响铸件的质量和可靠性。因此,提高合金的晶粒细化效果,对于改善合金的铸造性能具有重要意义。Al-Ti-B细化剂是铝合金铸造中最常用的晶粒细化剂,但不同Ti/B质量比的Al-Ti-B细化剂对晶粒细化效果及热裂机制尚未系统研究。采用X射线衍射仪(XRD)、光学显微镜(OM)、扫描电镜(SEM)和CRC(constrained rod cast)金属型约束热裂棒模具等,分析了不同Ti/B质量比的Al-Ti-B细化剂对铸造Al-Cu-Mn-Mg合金微观组织和热裂倾向性的影响。实验结果表明,4种Ti/B比的Al-Ti-B细化剂中Al_3Ti和TiB_2相的含量存在显著差异。在B含量均为0.3%(质量分数)的条件下,添加Al-3Ti-1B、Al-4Ti-1B、Al-5Ti-1B和Al-5Ti-2B的Al-5Cu-0.7Mn-0.55Mg合金的平均晶粒尺寸分别为162.07、113.73、107.81和88.00μm,对应的热裂纹倾向性指数依次为112、136、96和24。微观机制分析表明,Ti B_(2)相的含量对晶粒细化效果和热裂倾向性具有显著影响。特别是Al-5Ti-2B细化剂,在晶粒细化的同时,显著降低了合金的热裂倾向性,展现出优异的性能。展开更多
目的:拟采用超微血管成像技术(superb microvascular imaging,SMI)和超声造影(contrast-enhanced ultrasound,CEUS)相结合的方法,对甲状腺4a及4b级结节进行TI-RADS(thyroid imaging reporting and data system)分级。方法:对27例超声造...目的:拟采用超微血管成像技术(superb microvascular imaging,SMI)和超声造影(contrast-enhanced ultrasound,CEUS)相结合的方法,对甲状腺4a及4b级结节进行TI-RADS(thyroid imaging reporting and data system)分级。方法:对27例超声造影证实的甲状腺结节进行回顾性分析,术前分别行2 D灰阶超声、超微血管显像和超声造影,并对其进行分组、定量计分,得到各组的工作特性曲线(receiver operating characteristic,ROC)。结果:(1)27例行超声造影检查的甲状腺结节中:TI-RADS分级联合超微血管成像与TI-RADS分级联合超声造影曲线下面积相比较(Z=-0.206,P=0.175),诊断效能差异无统计学意义(P>0.05),表明SMI与CEUS诊断效能近似;(2)27例行超声造影检查的甲状腺结节中:TI-RADS分级联合超微血管成像和超声造影与TI-RADS分级曲线下面积相比较(Z=-1.242,P=0.011),诊断效能差异有统计学意义(P<0.05)。结论:TI-RADS分级联合超微血管成像结合超声造影能够提高甲状腺结节诊断的准确性,能够为临床诊治提供较为准确指导;超微血管成像与超声造影在鉴别诊断甲状腺结节良恶性方面具有较高一致性。展开更多
基金National Natural Science Foundation of China(51504138,51674118,52271177)Hunan Provincial Natural Science Foundation of China(2023JJ50181)Supported by State Key Laboratory of Materials Processing and Die&Mould Technology,Huazhong University of Science and Technology(P2024-022)。
文摘To explore the formation mechanism of anisotropy in Ti-6Al-4V alloy fabricated by selective laser melting(SLM),the compressive mechanical properties,microhardness,microstructure,and crystallographic orientation of the alloy across different planes were investigated.The anisotropy of SLM-fabricated Ti-6Al-4V alloys was analyzed,and the electron backscatter diffraction technique was used to investigate the influence of different grain types and orientations on the stress-strain distribution at various scales.Results reveal that in room-temperature compression tests at a strain rate of 10^(-3) s^(-1),both the compressive yield strength and microhardness vary along the deposition direction,indicating a certain degree of mechanical property anisotropy.The alloy exhibits a columnar microstructure;along the deposition direction,the grains appear equiaxed,and they have internal hexagonal close-packed(hcp)α/α'martensitic structure.α'phase has a preferential orientation approximately along the<0001>direction.Anisotropy arises from the high aspect ratio of columnar grains,along with the weak texture of the microstructure and low symmetry of the hcp crystal structure.
文摘Al-Cu-Mn-Mg合金因其优异的综合性能,被广泛应用于航空航天和轨道交通等领域。然而,该合金在铸造过程中容易出现热裂缺陷,严重影响铸件的质量和可靠性。因此,提高合金的晶粒细化效果,对于改善合金的铸造性能具有重要意义。Al-Ti-B细化剂是铝合金铸造中最常用的晶粒细化剂,但不同Ti/B质量比的Al-Ti-B细化剂对晶粒细化效果及热裂机制尚未系统研究。采用X射线衍射仪(XRD)、光学显微镜(OM)、扫描电镜(SEM)和CRC(constrained rod cast)金属型约束热裂棒模具等,分析了不同Ti/B质量比的Al-Ti-B细化剂对铸造Al-Cu-Mn-Mg合金微观组织和热裂倾向性的影响。实验结果表明,4种Ti/B比的Al-Ti-B细化剂中Al_3Ti和TiB_2相的含量存在显著差异。在B含量均为0.3%(质量分数)的条件下,添加Al-3Ti-1B、Al-4Ti-1B、Al-5Ti-1B和Al-5Ti-2B的Al-5Cu-0.7Mn-0.55Mg合金的平均晶粒尺寸分别为162.07、113.73、107.81和88.00μm,对应的热裂纹倾向性指数依次为112、136、96和24。微观机制分析表明,Ti B_(2)相的含量对晶粒细化效果和热裂倾向性具有显著影响。特别是Al-5Ti-2B细化剂,在晶粒细化的同时,显著降低了合金的热裂倾向性,展现出优异的性能。
