High-temperature piezoelectric sen-sors are very important in severe environments such as fire safety,aerospace and oil drills,however,most current sensors are not heat res-istant(<300℃)and are fragile,which limit...High-temperature piezoelectric sen-sors are very important in severe environments such as fire safety,aerospace and oil drills,however,most current sensors are not heat res-istant(<300℃)and are fragile,which limits their use,especially in high-temperature environ-ments.A high-temperature resistant flexible piezoelectric film based on graphene oxide(GO)/polyacrylonitrile(PAN)composites was prepared by electrospinning and thermal treat-ment.It was packed into a micro-device,which could work continuously at 500℃.The intro-duction of GO significantly increased the mechanical properties of the PAN nanofibers because the oxygen-containing func-tional groups(electronegative groups)on the surface of the GO initiated a nucleophilic attack on the PAN molecule during heat treatment,enabling the GO to initiate the cyclization of the PAN at lower heat-treatment temperatures.In addition,the abund-ant oxygen-containing functional groups on GO acted as pro-oxidants to hasten the oxidation of PAN during heat treatment.The effects of GO content and heat treatment temperature on the properties of the nanofiber films were investigated.A GO/PAN nanofiber piezoelectric sensor heat-treated at 300℃had a 9.10 V and 2.25μA peak output,which are respectively 101.3%and 78.6%higher than those of the untreated films.Cyclic testing over 5000 cycles at 350℃confirmed the stable out-put performance of the GO/PAN nanofiber piezoelectric sensor.Furthermore,a sensor heat-treated at 400℃had a sensitivity of 1.7 V/N,which is 83.5%higher than that of an untreated one.The results show that the prepared GO/PAN nanofiber piezo-electric sensor combines high temperature resistance,high flexibility,stability and high sensitivity,and may have broad applic-ations in high temperature environments such as the aerospace and petroleum industries.展开更多
To ensure a reliable operation of the 2.5 MW gas turbine engine (GTE- 2.5) with the inlet gas temperature TIT = 1623 K, studies were performed over the thermal state of the nozzle guide vanes and rotor blades with the...To ensure a reliable operation of the 2.5 MW gas turbine engine (GTE- 2.5) with the inlet gas temperature TIT = 1623 K, studies were performed over the thermal state of the nozzle guide vanes and rotor blades with the temperatures, rates and flows of the working media and cooling air simulating all the potential turbine stage operating duties. The steady state and thermal-cyclic tests having been accomplished, there was no visible defect on the rotor blades and the nozzle vanes. Afterwards, they survived the endurance tests at the rated cooling. Therefore, the functionality of the shell thin-wall hybrid nozzle vanes and rotor blades under the variable operating duties of the gas turbine at the 'shock' and 'cyclic' loads of the working media temperature variations has been demonstrated.展开更多
文摘High-temperature piezoelectric sen-sors are very important in severe environments such as fire safety,aerospace and oil drills,however,most current sensors are not heat res-istant(<300℃)and are fragile,which limits their use,especially in high-temperature environ-ments.A high-temperature resistant flexible piezoelectric film based on graphene oxide(GO)/polyacrylonitrile(PAN)composites was prepared by electrospinning and thermal treat-ment.It was packed into a micro-device,which could work continuously at 500℃.The intro-duction of GO significantly increased the mechanical properties of the PAN nanofibers because the oxygen-containing func-tional groups(electronegative groups)on the surface of the GO initiated a nucleophilic attack on the PAN molecule during heat treatment,enabling the GO to initiate the cyclization of the PAN at lower heat-treatment temperatures.In addition,the abund-ant oxygen-containing functional groups on GO acted as pro-oxidants to hasten the oxidation of PAN during heat treatment.The effects of GO content and heat treatment temperature on the properties of the nanofiber films were investigated.A GO/PAN nanofiber piezoelectric sensor heat-treated at 300℃had a 9.10 V and 2.25μA peak output,which are respectively 101.3%and 78.6%higher than those of the untreated films.Cyclic testing over 5000 cycles at 350℃confirmed the stable out-put performance of the GO/PAN nanofiber piezoelectric sensor.Furthermore,a sensor heat-treated at 400℃had a sensitivity of 1.7 V/N,which is 83.5%higher than that of an untreated one.The results show that the prepared GO/PAN nanofiber piezo-electric sensor combines high temperature resistance,high flexibility,stability and high sensitivity,and may have broad applic-ations in high temperature environments such as the aerospace and petroleum industries.
文摘To ensure a reliable operation of the 2.5 MW gas turbine engine (GTE- 2.5) with the inlet gas temperature TIT = 1623 K, studies were performed over the thermal state of the nozzle guide vanes and rotor blades with the temperatures, rates and flows of the working media and cooling air simulating all the potential turbine stage operating duties. The steady state and thermal-cyclic tests having been accomplished, there was no visible defect on the rotor blades and the nozzle vanes. Afterwards, they survived the endurance tests at the rated cooling. Therefore, the functionality of the shell thin-wall hybrid nozzle vanes and rotor blades under the variable operating duties of the gas turbine at the 'shock' and 'cyclic' loads of the working media temperature variations has been demonstrated.
基金supported by the National Natural Science Foundation of China (52022100, 52192604,51971097, 51971239 and 92263103)the financial support from the Key R&D Program of Hubei (2022BAA023)+1 种基金Basic Research Support Program of Huazhong University of Science and Technology (5003110121)the support from the Young Elite Scientists Sponsorship Program by China Association for Science and Technology。