A new niobate K3Sr3MoNb9O30, was synthesized for the first time by solid state reaction, and was characterized by EPMA, XRD, SEM and DTA. The X -ray powder diffraction data of K3Sr3MoNb9O30 was first reported. The res...A new niobate K3Sr3MoNb9O30, was synthesized for the first time by solid state reaction, and was characterized by EPMA, XRD, SEM and DTA. The X -ray powder diffraction data of K3Sr3MoNb9O30 was first reported. The results show that K3Sr3MoNb9O30 belongs to tetragonal tungsten bronze (TTB) structure with unit cell parameters α=12. 4292(5) A . c = 3. 9338(3) A , and space group P4bm (100), z=1. The calculated and measured densities are 4. 897 g/crr3 and 4. 890 g/cm3, respectively.展开更多
基金Fund by Grant-in-Aid project (No. 98-10) of International Centre for Diffraction Data .
文摘A new niobate K3Sr3MoNb9O30, was synthesized for the first time by solid state reaction, and was characterized by EPMA, XRD, SEM and DTA. The X -ray powder diffraction data of K3Sr3MoNb9O30 was first reported. The results show that K3Sr3MoNb9O30 belongs to tetragonal tungsten bronze (TTB) structure with unit cell parameters α=12. 4292(5) A . c = 3. 9338(3) A , and space group P4bm (100), z=1. The calculated and measured densities are 4. 897 g/crr3 and 4. 890 g/cm3, respectively.
