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Microstructural Evolution and Strengthening Mechanisms of Shoulderless Micro-friction Stir Welded Joints of 1060-H24 Pure Aluminum
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作者 Zhang Changqing Ma Dongdong +3 位作者 Gu Huaizhuang Wang Dong Liu Enrong Zhang Pengsheng 《稀有金属材料与工程》 北大核心 2025年第11期2757-2767,共11页
The differences between shouldered and shoulderless tools in the micro-friction stir welding of 0.8 mm thin plates were evaluated.Employing a suite of advanced characterization methods,including white light interferom... The differences between shouldered and shoulderless tools in the micro-friction stir welding of 0.8 mm thin plates were evaluated.Employing a suite of advanced characterization methods,including white light interferometry,electron backscatter diffraction(EBSD),and scanning electron microscopy,the formation of weld surface,joint microstructure distribution,and fracture characteristics were studied.The enhancement mechanism of mechanical properties was explained through the Hall-Petch relationship and Taylor's hardening law.Results indicate that the main reason for the increased yield strength observed in shoulderless tool joints is the combined mechanism of dislocation strengthening and fine-grain strengthening.Specifically,the utilization of shouldered tools results in a smooth weld surface,with an average grain size of 11.24μm and a high-angle grain boundary content of 16.80%in the nugget zone.The primary texture components are the{011}<100>Goss and{112}<111>copper textures,yielding a maximum texture strength of 3.70.Simultaneously,the fracture dimples exhibit a reduction in size and an increase in depth.Whereas the welds produced with shoulderless tools display slight burrs on the surface.The experimental results demonstrate that the average grain size in the nugget zone of these joints is significantly reduced to 0.59μm,while the high-angle grain boundary content reaches 34.34%.This process is accompanied by the formation of{111}<110>Shear textures and{001}<110>rotated cubic textures as the main components,resulting in a significant increase in maximum texture strength to 6.65. 展开更多
关键词 micro-friction stir welding stirring tool EBSD mechanical properties
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Melt flow, heat transfer and solidification in bloom continuous casting with combined vertical linear electromagnetic stirring and rotary electromagnetic stirring
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作者 Ze-peng Wang En-gang Wang Zhong-xin Zhai 《Journal of Iron and Steel Research International》 2025年第4期950-960,共11页
An opposite combined vertical linear electromagnetic stirring(CV-LEMS)was proposed,which is applied in the final solidification zone of bloom continuous casting.The melt flow,heat transfer,and solidification under CV-... An opposite combined vertical linear electromagnetic stirring(CV-LEMS)was proposed,which is applied in the final solidification zone of bloom continuous casting.The melt flow,heat transfer,and solidification under CV-LEMS were investigated by establishing a three-dimensional numerical simulation model and a pilot continuous casting simulation experiment and compared with the conventional rotary electromagnetic stirring(REMS).The results show that a longitudinally symmetric linear magnetic field is formed in the liquid core of the bloom by applying CV-LEMS,which induces a strong longitudinal circulation flow both on the inner arc side and the outer arc side in the liquid core of the bloom.The height of the melt longitudinal effective mixing range under CV-LEMS reaches 0.9 m,which is greater than that of the REMS and makes up for the deficiency of REMS sensitivity to the position of the final solidification zone.CV-LEMS strongly promotes the mixing of upper melt with high temperature and the lower part melt with low temperature in the liquid core,improves the uniformity of melt temperature distribution and significantly increases the melt temperature near the solidification front,and the width of the liquid core increases by 4.2 mm at maximum.This shows that the appliction of CV-LEMS is more helpful to strengthen the feeding effect of the upper melt to the solidification shrinkage of the lower melt than the conventional REMS and inhibits the formation of porosity,shrinkage cavity and crack defects in the center of the bloom. 展开更多
关键词 Combined vertical linear electromagnetic stirring Final rotary electromagnetic stirring Longitudinal circulation flow Feeding ability Bloom continuous casting
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Dissimilar Friction Stir Lap Welding of Ti Alloy and Al-Li Alloy:Microstructure and Mechanical Property 被引量:1
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作者 Zhang Wenxin Zhang Xiankun +3 位作者 Shi Lei Li Shengli Jiang Yuanning Wu Chuansong 《稀有金属材料与工程》 北大核心 2025年第2期311-318,共8页
Friction stir lap welding of AA2195 Al-Li alloy and Ti alloy was conducted to investigate the formation,microstructure,and mechanical properties of the joints.Results show that under different welding parameters,with ... Friction stir lap welding of AA2195 Al-Li alloy and Ti alloy was conducted to investigate the formation,microstructure,and mechanical properties of the joints.Results show that under different welding parameters,with the decrease in welding heat input,the weld surface is smoother.The Ti/Al joint interface is flat without obvious Ti and Al mixed structure,and the hook structure is not formed under optimal parameters.Due to the enhanced breaking effect of the stirring head,the hook structural defects and intermetallic compounds are more likely to form at the Ti/Al interface at high rotational speed of 1000 r/min,thereby deteriorating the mechanical properties of joints.Decreasing the heat input is beneficial to hardness enhancement of the aluminum alloy in the weld nugget zone.Under the optimal parameters of rotation speed of 800 r/min and welding speed of 120 mm/min,the maximum tensile shear strength of joint is 289 N/mm. 展开更多
关键词 Ti/Al dissimilar welding friction stir lap welding Ti alloy Al-Li alloy interface bonding mechanical property
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Elucidating the process mechanism in Mg-to-Al friction stir lap welding enhanced by ultrasonic vibration 被引量:3
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作者 Ming Zhai Lei Shi ChuanSong Wu 《Journal of Magnesium and Alloys》 2025年第1期338-355,共18页
The composite structures/components made by friction stir lap welding(FSLW)of Mg alloy sheet and Al alloy sheet are of wide application potentials in the manufacturing sector of transportation vehicles.To further impr... The composite structures/components made by friction stir lap welding(FSLW)of Mg alloy sheet and Al alloy sheet are of wide application potentials in the manufacturing sector of transportation vehicles.To further improve the joint quality,the ultrasonic vibration(UV)is exerted in FSLW,and the UV enhanced FSLW(UVeFSLW)was developed for making Mg-to-Al dissimilar joints.The numerical analysis and experimental investigation were combined to study the process mechanism in Mg/Al UVeFSLW.An equation related to the temperature and strain rate was derived to calculate the grain size at different locations of the weld nugget zone,and the effect of grain size distribution on the threshold thermal stress was included,so that the prediction accuracy of flow stress was further improved.With such modified constitutive equation,the numerical simulation was conducted to compare the heat generation,temperature profiles and material flow behaviors in Mg/Al UVeFSLW/FSLW processes.It was found that the exerted UV decreased the temperature at two checking points on the tool/workpiece interface from 707/671 K in FSLW to 689/660 K in UVeFSLW,which suppressed the IMCs thickness at Mg-Al interface from 1.7μm in FSLW to 1.1μm in UVeFSLW.The exerted UV increased the horizontal materials flow ability,and decreased the upward flow ability,which resulted in the increase of effective sheet thickness/effective lap width from 2.01/3.70 mm in FSLW to 2.04/4.84 mm in UVeFSLW.Therefore,the ultrasonic vibration improved the tensile shear strength of Mg-to-Al lap joints by 18%. 展开更多
关键词 Friction stir lap welding Mg-to-Al dissimilar alloys Ultrasonic vibration Numerical simulation Experimental investigation
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Properties and structure investigation of the friction stir welding seam of the AA6061-T6 plates 被引量:2
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作者 M.Soukieh W.Harara +2 位作者 H.Koudaimi M.Halak M.Kassem 《China Welding》 2025年第2期132-138,共7页
Friction stir welding(FSW)is a relatively new welding technique that has significant advantages compared to the fusion welding techniques in joining non weld able alloys by fusion,such as aluminum alloys.Three FSW sea... Friction stir welding(FSW)is a relatively new welding technique that has significant advantages compared to the fusion welding techniques in joining non weld able alloys by fusion,such as aluminum alloys.Three FSW seams of AA6061-T6 plates were made us-ing different FSW parameters.The structure of the FSW seams was investigated using X-ray diffraction(XRD),scanning electron mi-croscope(SEM)and non destructive testing(NDT)techniques and their hardness was also measured.The dominated phase in the AA6061-T6 alloy and the FSW seams was theα-Al.The FSW seam had lower content of the secondary phases than the AA6061-T6 al-loy.The hardness of the FSW seams was decreased by about 30%compared to the AA6061-T6 alloy.The temperature distributions in the weld seams were also studied experimentally and numerically modeled and the results were in a good agreement. 展开更多
关键词 AA6061-T6 Friction stir welding welding parameters temperature distribution numerical modeling FSW weld seam
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Superplastic behavior of fine-grained Ti-10V-2Fe-3Al alloy fabricated by friction stir processing 被引量:1
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作者 Kai Wang Wenjing Zhang +3 位作者 Takuya Ogura Yoshiaki Morisada Xinqing Zhao Hidetoshi Fujii 《Journal of Materials Science & Technology》 2025年第3期26-36,共11页
Ti-10V-2Fe-3Al alloy with fine-grainedβphases was fabricated by friction stir processing with opti-mized processing parameters.The superplastic behavior of the specimens was investigated by tensile deformation at dif... Ti-10V-2Fe-3Al alloy with fine-grainedβphases was fabricated by friction stir processing with opti-mized processing parameters.The superplastic behavior of the specimens was investigated by tensile deformation at different strain rates and temperatures,and an optimal superplastic elongation of 634%was achieved at 700℃ and 3×10^(-4)/s.An annealing treatment at 650℃ for 60 min showed a mi-crostructure withαprecipitates distributed in theβmatrix in the friction stir specimen.Such pre-heat treatment improves the superplasticity of the specimen,achieving an elongation of up to 807%at 750℃ and 3×10^(-4)/s.The influences of tensile temperatures and strain rates on the microstructural evolution,such as grain size variation,grain morphology,and phase transformations,were discussed.The super-plastic deformation behavior of fine-grained Ti-10V-2Fe-3Al alloy is controlled by grain boundary sliding and accompanied by dynamic phase transformation and recrystallization. 展开更多
关键词 Ti-10V-2Fe-3Al alloy Friction stir processing SUPERPLASTICITY Microstructural evolution Pre-heat treatment
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Revealing stir zone heterogeneities in friction stir-welded and annealed AZ31 alloy
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作者 Hiba Azzeddine Salaheddine Sadi +3 位作者 Farazila Yusof François Brisset Thierry Baudin Megumi Kawasaki 《Journal of Magnesium and Alloys》 2025年第8期3986-4004,共19页
The difference in the microstructure,texture in the stir zone(SZ)of the AZ31(Mg-3 Al-1 Zn,wt.%)alloy after friction stir welding(FSW)and subsequent annealing at 400℃for 1 h was characterized by scanning electron micr... The difference in the microstructure,texture in the stir zone(SZ)of the AZ31(Mg-3 Al-1 Zn,wt.%)alloy after friction stir welding(FSW)and subsequent annealing at 400℃for 1 h was characterized by scanning electron microscopy(SEM)with electron backscatter diffraction(EBSD)measurements at the surface and core regions.The findings indicate that FSW produced grain refinement where the mean grain size decreases from 19μm(base metal)to 5.1 and 3.5μm at the surface and core regions,respectively.The c-axis of the grains at the surface region was aligned with the normal direction(<0001>//ND)due to the additional strain of the tool shoulder.In contrast,the core region shows a typical shear texture,where the c-axis tends to be oriented parallel to the welding direction(<0001>//WD).The Vickers microhardness mapping across the SZ revealed that the core region was soften than the surface region due to the dynamic recrystallization and texture weakening.The microstructure of the SZ remains principally deformed after annealing treatment except for the development of massive Mg_(17)Al_(12)precipitates and the abnormal grain growth of a few grains with<11-20>//WD orientation at the upper side of the surface region.The c-axis of the grains at the surface region was tilted about 10°toward WD,while an inclined<0001>//WD orientation about 30°from WD was developed at the core region.Consequently,the distribution of microhardness values across the SZ was more heterogeneous than the FSW sample.The results were discussed in the light of grain boundary misorientation,dislocation density and the pinning effect of Mg_(17)Al_(12)precipitates.Additionally,Schmid factor analysis was used to examine the activation of the basal slip mode to characterize the associated mechanical response. 展开更多
关键词 EBSD FSW Magnesium Microstructure Texture stir zone
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Low-Temperature Superplastic Deformation Behavior of Bimodal Microstructure of Friction Stir Processed Ti-6Al-4V Alloy
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作者 H.Q.Dai N.Li +6 位作者 L.H.Wu J.Wang P.Xue F.C.Liu D.R.Ni B.L.Xiao Z.Y.Ma 《Acta Metallurgica Sinica(English Letters)》 2025年第9期1559-1569,共11页
For a long time,the conventional superplastic forming temperature for Ti alloys is generally too high(~900-920℃),which leads to too long production cycles,heavy surface oxidation,and property reduction.In this study,... For a long time,the conventional superplastic forming temperature for Ti alloys is generally too high(~900-920℃),which leads to too long production cycles,heavy surface oxidation,and property reduction.In this study,an ultrafine bimodal microstructure,consisting of ultrafine equiaxed microstructure(0.66μm)and 43.3%lamellar microstructure,was achieved in the Ti-6Al-4V alloy by friction stir processing(FSP).The low-temperature superplastic behavior and deformation mechanism of the FSP Ti-6Al-4V alloy were investigated at temperatures of 550-675℃and strain rates ranging from 1×10^(−4)to 3×10^(−3)s^(−1).The FSP alloy exhibited superplastic elongations of>200%at the temperature range from 550 to 650℃,and an optimal superplastic elongation of 611%was achieved at 625℃and 1×10^(−4)s^(−1).This is the first time to report the low-temperature superplasticity of the bimodal microstructure in Ti alloys.Grain boundary sliding was identified as the dominant deformation mechanism,which was effectively accommodated by the comprehensive effect of dislocation-inducedβphase precipitation and dynamic spheroidization of the lamellar structure.This study provides a novel insight into the low-temperature superplastic deformation behavior of the bimodal microstructure. 展开更多
关键词 Titanium alloys Friction stir processing SUPERPLASTICITY Bimodal microstructure SPHEROIDIZATION
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Optimizing mold electromagnetic stirring parameters for coordinated control of initial shell solidification quality in large round blooms under four-port submerged entry nozzle for feeding
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作者 Tao Wang Chang-jun Xu +3 位作者 Chong Lei Lu-hao Ren Wen Wang Hong-lin Guo 《Journal of Iron and Steel Research International》 2025年第8期2389-2402,共14页
A coupled computational model of molten steel within the mold was developed,encompassing electromagnetic fields,fluid flow,heat transfer,shell formation,stress,and strain.The model was verified through comparison with... A coupled computational model of molten steel within the mold was developed,encompassing electromagnetic fields,fluid flow,heat transfer,shell formation,stress,and strain.The model was verified through comparison with plant measurements,showing reasonable agreement in electromagnetic field distribution,solidification endpoint,and shell thickness.Results indicate that coordinating the submerged entry nozzle(SEN)and mold electromagnetic stirring(M-EMS)effectively regulates the solidification quality of the initial shell.Adjusting M-EMS current frequency changes the impact position of the molten steel jet from the four-port SEN,while increasing current intensity reduces the jet impact intensity.Adjusting the M-EMS parameters can enhance the initial shell uniformity.Furthermore,in areas directly impacted by the steel jet from the four-port SEN,a relationship between brittle temperature range(BTR)width and total mechanical strain was found,and the larger the BTR width,the smaller the corresponding total mechanical strain.The BTR width provides a discriminant method to avoid hot tearing.Appropriate M-EMS parameters are obtained and applied,and the plant trials show a significant improvement in hot tearing near the surface of round blooms. 展开更多
关键词 Mold electromagnetic stirring Large-size round bloom Hot tearing SOLIDIFICATION Alloy steel
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Improvement on the distribution uniformity of hydrodynamics in a stirred tank with an H-like fractal impeller
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作者 Hui Li Pan You +2 位作者 Xiaoyang Chen Huiming Yang Peicheng Luo 《Chinese Journal of Chemical Engineering》 2025年第6期83-94,共12页
Fractal theory provides a new strategy for equipment design.In this work,we propose a novel H-like fractal(HLF)impeller to improve the uniformity of the distribution of hydrodynamics in stirred tanks.The impellers are... Fractal theory provides a new strategy for equipment design.In this work,we propose a novel H-like fractal(HLF)impeller to improve the uniformity of the distribution of hydrodynamics in stirred tanks.The impellers are constructed by replacing two vertical blades or four legs with two or four H-like subblades by fractal iterations,respectively.Flow characteristics including velocity and turbulent kinetic energy(TKE)distributions,vortices,power number,are predicted by large eddy simulation.Compared with Rushton turbine(RT)impeller when H/T=1(or dual RTs when H/T=1.5,triple RTs when H/T=2),the HLF impeller can produce a flow field with more uniform distributions of larger velocities and TKE level.The impeller with more fractal iteration times can further improve the distribution uniformity of hydrodynamics in the case of high H/T.Power analysis shows that this is mainly due to the improved energy utilization efficiency by the fractal structure design. 展开更多
关键词 FRACTAL IMPELLER Mixing stirred tank Large eddy simulation(LES)
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Robust interfacial bonding achieved via phase separation induced by enhanced Al diffusion during AZ31/high-entropy alloy friction stir welding
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作者 Gaohui Li Haining Yao +4 位作者 Boyuan Fu Ke Chen Katsuyoshi Kondoh Nannan Chen Min Wang 《Journal of Magnesium and Alloys》 2025年第3期1012-1019,共8页
Welding high-entropy alloy(HEA)to Mg alloy has gained increasing attention for multi-metal structure design,while intrinsic sluggish diffusion kinetics of HEA confines diffusion-controlled interfacial reactions and mak... Welding high-entropy alloy(HEA)to Mg alloy has gained increasing attention for multi-metal structure design,while intrinsic sluggish diffusion kinetics of HEA confines diffusion-controlled interfacial reactions and makes it challenging to establish robust metallurgical bonding.This study investigated welding of FeCoCrNiMn HEA to commercial AZ31 as a model combination to pioneer thisfield.Interfacial phase separation phenomenon was observed,with the diffusion accelerated by in-situ engineering a submicron-scale thick(∼400–500 nm)HEA nearby the interface into nanocrystalline-structure during friction stir welding.Abundant grain boundaries generated in this nanocrystalline-interlayer serve as diffusion short-circuits and energetically preferred nucleation-sites,which promoted Al in AZ31 to diffuse into HEA and triggered quick separation into body-centered cubic AlNi-type and tetragonal FeCr-type intermetallics.HEA and AZ31 were thus metallurgically bonded by these interfacial intermetallics.The joint shows exceptional strength in tensile lap-shear testing with fracture largely occurred within AZ31 rather than right along interface as commonly reported previously for dissimilar joints. 展开更多
关键词 High-entropy alloy Mg alloy Friction stir welding DIFFUSION Phase separation
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Achieving excellent strength-ductility synergy of wire-arc additive manufactured Mg-Gd-Y-Zr alloy via friction stir processing
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作者 Wenzhe Yang Kuitong Yang +3 位作者 Haiou Yang Zihong Wang Chenghui Hu Xin Lin 《Journal of Magnesium and Alloys》 2025年第6期2500-2508,共9页
Friction stir processing(FSP)was applied to wire-arc additively manufactured(WAAM)Mg-9.54Gd-1.82Y-0.44Zr(GW92K)alloy to address coarse microstructure and porosity defects inherent to layer-by-layer deposition.FSP indu... Friction stir processing(FSP)was applied to wire-arc additively manufactured(WAAM)Mg-9.54Gd-1.82Y-0.44Zr(GW92K)alloy to address coarse microstructure and porosity defects inherent to layer-by-layer deposition.FSP induced complete dissolution of the coarse Mg_(5)(Gd,Y)eutectic network(initial size:3.3±0.5μm)and triggered dynamic recrystallization,achieving a 69.5%grain refinement from 16.4μm(WAAMed)to 5.0μm(FSPed).This microstructural transformation enhanced ultimate tensile strength(UTS)by 32%(217±3 MPa→286±2 MPa),yield strength(YS)by 46%(124±2 MPa→182±7 MPa),and elongation(EL)by 35%(9.7±1.1%→13.1±1.4%).Quantitative analysis via Hall-Petch relationship confirmed that grain refinement contributed~50 MPa(79%)of the total YS increment,while nano-precipitation(β/βphases<20 nm)effects accounted for the remaining~13 MPa.The simultaneous strength-ductility enhancement originates from FSP-induced defect elimination(porosity reduction:1.75%→0.18%)and dual-phase grain boundary pinning by Zr particles andβ-Mg_(5)(Gd,Y)precipitates.These findings establish FSP as a viable post-treatment for overcoming WAAM limitations in high-performance Mg-RE alloy fabrication. 展开更多
关键词 Additive manufacturing Friction stir processing Mg-Gd-y-Zr alloy Microstructure Mechanical properties.
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Eulerian-Lagrangian simulation of dispersed liquid flow in turbulent stirred tanks
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作者 Jingchang Zhang Xiaoping Guan +1 位作者 Ning Yang Maximilian Lackner 《Chinese Journal of Chemical Engineering》 2025年第7期182-190,共9页
Liquid-liquid dispersion is often performed in stirred tanks,which are valued for their ease of operation,high droplet generation rate and effective droplet dispersion.Many relevant simulations use the Eulerian-Euleri... Liquid-liquid dispersion is often performed in stirred tanks,which are valued for their ease of operation,high droplet generation rate and effective droplet dispersion.Many relevant simulations use the Eulerian-Eulerian method,combining population balance equations with statistical models to forecast droplet breakage.Conversely,the Eulerian-Lagrangian(E-L)method provides precise tracking of individual droplets,which is crucial for simulating dispersion processes.However,E-L simulation faces challenges in integrating droplet breakage effectively.To address this issue,our research introduces a probabilistic approach for droplet breakages.It assumes that a longer time increases the likelihood of breakup;a droplet breaks if the calculated probability exceeds a random value from 0 to 1.Consequently,the simulated breakage frequency becomes independent of the Lagrangian time step.The Sauter mean diameter and droplet size distribution can be accurately predicted by this probabilistic approach.By closely monitoring droplet motion,we reveal the complexity of droplet trajectories and the detailed patterns of circulation in stirred tanks.These insights contribute to a deeper understanding of liquidliquid dispersion dynamics. 展开更多
关键词 Eulerian-Lagrangian method Liquid-liquid dispersion Droplet breakage stirred vessel Turbulent flow Computational fluid dynamics
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A comprehensive review of microstructure and mechanical properties of friction stir processed magnesium alloys and composites
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作者 Maryam Mehdizade Hossein Keshavarz +3 位作者 Fatemeh Marashi-Najafi Morteza Tayebi Amir Mostafaei Ali Reza Eivani 《Journal of Magnesium and Alloys》 2025年第9期4089-4129,共41页
Friction stir processing(FSP)induces severe plastic deformation,generating intense strains and localized heating,which modifies the surface and enables the fabrication of magnesium(Mg)-based composites.This technique ... Friction stir processing(FSP)induces severe plastic deformation,generating intense strains and localized heating,which modifies the surface and enables the fabrication of magnesium(Mg)-based composites.This technique refines the microstructure of Mg alloys,enhancing mechanical properties—particularly ductility,a key limitation of these HCP alloys.This review addresses the underlying microstructural evolution during FSP of Mg alloys and Mg-matrix composites,including(i)grain refinement via continuous and discontinuous dynamic recrystallization(CDRX and DDRX),(ii)fragmentation and redistribution of secondary phases and intermetallics,(iii)transformation of low-and high-angle grain boundaries,and(iv)additional microstructural changes induced by external reinforcements.This review provides a comprehensive analysis of the strengthening mechanisms and their impact on the mechanical properties of FSP Mg alloys and Mgmatrix composites(MMCs).The paper examines the correlation between FSP processing parameters,microstructural evolution,and resulting mechanical properties.It critically highlights how the type of reinforcement and the dynamic recrystallization induced by friction stir processing influence grain boundary character and,consequently,the material’s strengthening response.It includes a comparative evaluation of yield stress,ultimate tensile strength,microhardness,elongation,and fractography for various FSP-treated Mg alloys and MMCs,including AZxx,WExx,ZExx,ZKxx,AMxx,AExx,and Mg-rare earth alloys.Additionally,the novelty of this review lies in its emphasis on connecting microstructural transformations to mechanical performance trends across different alloy systems and processing strategies,an aspect that has been underexplored in previous reviews.Recent advancements in FSP techniques and their implications for improving the performance of Mg-based materials are also discussed. 展开更多
关键词 Mg-based composites Friction stir processing Surface modification Microstructure Mechanical properties Dynamic recrystallization
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Recent advances in time-series analysis methods for identifying fluid flow characteristics in stirred tank reactors
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作者 Xiaoyu Tang Facheng Qiu +3 位作者 Peiqiao Liu Yundong Wang Hong Li Zuohua Liu 《Chinese Journal of Chemical Engineering》 2025年第1期310-327,共18页
Leveraging big data signal processing offers a pathway to the development of artificial intelligencedriven equipment.The analysis of fluid flow signals and the characterization of fluid flow behavior are of critical i... Leveraging big data signal processing offers a pathway to the development of artificial intelligencedriven equipment.The analysis of fluid flow signals and the characterization of fluid flow behavior are of critical in two-phase flow studies.Significant research efforts have focused on discerning flow regimes using various signal analysis methods.In this review,recent advances in time series signals analysis algorithms for stirred tank reactors have been summarized,and the detailed methodologies are categorized into the frequency domain methods,time-frequency domain methods,and state space methods.The strengths,limitations,and notable findings of each algorithm are highlighted.Additionally,the interrelationships between these methodologies have also been discussed,as well as the present progress achieved in various applications.Future research directions and challenges are also predicted to provide an overview of current research trends in data mining of time series for analyzing flow regimes and chaotic signals.This review offers a comprehensive summary for extracting and characterizing fluid flow behavior and serves as a theoretical reference for optimizing the characterization of chaotic signals in future research endeavors. 展开更多
关键词 Flow characteristics Time series analysis Flow signal Chaos analysis stirred tank reactor
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Research on strength-ductility and fracture behavior of ultra-fine bio-magnesium alloys via double-sided friction stir processing using liquid CO_(2) cooling
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作者 Kun Sheng Shaokang Guan +2 位作者 Yufeng Sun Yoshiaki Morisada Hidetoshi Fujii 《Journal of Magnesium and Alloys》 2025年第8期3725-3739,共15页
Bio-magnesium(Mg)alloys exhibit excellent biocompatibility and biodegradability,making them highly promising for implant applications.However,their limited strength-ductility balance remains a critical challenge restr... Bio-magnesium(Mg)alloys exhibit excellent biocompatibility and biodegradability,making them highly promising for implant applications.However,their limited strength-ductility balance remains a critical challenge restricting widespread use.In this study,ultra-fine-grained and homogeneous Mg alloys were fabricated using double-sided friction stir processing(DS-FSP)with liquid CO_(2) rapid cooling,leading to a significant enhancement in the strength-ductility synergy of the stirred zone.The results demonstrate that DS-FSP samples exhibit simultaneous improvements in ultimate tensile strength(UTS)and elongation,reaching 334.1±15 MPa and 28.2±7.3%,respectively.Compared to the non-uniform fine-grained microstructure obtained through single-sided friction stir processing,DS-FSP generates a uniform ultra-fine-grained structure,fundamentally altering the fracture behavior and mechanisms of Mg alloys.The DS-FSP samples exhibit irregular fracture patterns due to variations in basal slip system activation among different grains.In contrast,single-sided friction stir processing samples,characterized by a fine-grained yet heterogeneous microstructure,display flat shear fractures dominated by high-density dislocation initiation induced by twin formation,with fracture propagation dictated by the non-uniform texture.By achieving an ultra-fine grain size and homogeneous texture,DS-FSP effectively modifies the fracture mechanisms,thereby enhancing the strength-ductility balance of bio-magnesium alloys. 展开更多
关键词 Bio-magnesium alloys Double-sided friction stir processing Homogeneous microstructure Ultra-fine grain Strength-ductility Fracture behavior
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Microstructure and properties of Cu-TiB_(2) composites prepared by mechanical stirring-assisted double-melt in-situ reaction
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作者 Tao Zhou Xu Wang +7 位作者 Liu-Xin Qin Yan-Bin Jiang Meng Wang Yan-Jun Ding Bai-Rui Qi Zhu Xiao Yan-Lin Jia Zhou Li 《Rare Metals》 2025年第2期1342-1362,共21页
A novel mechanical stirring-assisted double-melt in-situ reaction casting process was developed to prepare Cu-1TiB2(wt%)composites.The effects of preparation parameters(melting reaction temperature,stirring rate and s... A novel mechanical stirring-assisted double-melt in-situ reaction casting process was developed to prepare Cu-1TiB2(wt%)composites.The effects of preparation parameters(melting reaction temperature,stirring rate and stirring time)on the microstructure and properties of Cu-1TiB2 composites were investigated.The melt viscosity and particle motion during stirring process were analyzed.The strong turbulence and shear effects generated by mechanical stirring in the melt not only significantly improve the particle distribution but also contribute to adequate in-situ reactions and precise control of the chemical composition.The optimal preparation parameters were 1200℃,a stirring rate of 100 r·min^(−1) and a stirring time of 1 min.Combined with the cold rolling process,the tensile strength,elongation and electrical conductivity of the composite reached 475 MPa,6.0%and 88.4%IACS,respectively,which were significantly better than the composite prepared by manual stirring.The good plasticity is attributed to the uniform distribution of TiB_(2) particles,effectively retarding the crack propagation.The dispersion of particles promotes heterogeneous nucleation of Cu matrix and inhibits grain growth.On the other hand,dispersed particles contribute to grain shear fracture and dislocation multiplication during cold deformation.Therefore,the composite achieves higher dislocation strengthening and grain boundary strengthening. 展开更多
关键词 stir casting In-situ reaction Microstructure Cu-TiB_(2)composites Mechanical properties
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The relationship between microstructural characteristics and galvanic effect,SCC behavior of friction stir welded joint in as-welded and heat-treated conditions
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作者 Yanming Xia Dejing Zhou +3 位作者 Da-Hai Xia Zhiming Gao Linyue Bai Wenbin Hu 《Journal of Materials Science & Technology》 2025年第20期186-207,共22页
The detailed precipitation behavior and grain structure in different sub-regions of friction stir welding(FSW)AA6061-T6 joint after post-weld solution and aging treatments were explored.And the effects of microstructu... The detailed precipitation behavior and grain structure in different sub-regions of friction stir welding(FSW)AA6061-T6 joint after post-weld solution and aging treatments were explored.And the effects of microstructural evolution on mechanical properties,macro/micro electrochemical corrosion behavior and stress corrosion cracking behavior were investigated.The inherent microstructural gradients in FSW joint lead to dramatic degradation of mechanical properties and the presence of macro-galvanic effect,with the latter exacerbating anodic dissolution in heat-affected zone(HAZ)induced by micro-galvanic corro-sion and inhibiting pitting corrosion in stirred zone(SZ).Post-weld heat treatment(PWHT)causes the formation of matrix precipitates with similar densities in different sub-regions,resulting in optimized precipitate distribution,comprehensive hardness recovery,and diminished macro-galvanic effect.Grain boundary misorientation angle,grain size and pre-existing dislocations synergistically influence the evo-lution of grain boundary precipitates(GBPs)and precipitation-free zones(PFZs)during the PWHT.As a result,pitting corrosion is the dominant corrosion form in SZ due to the narrowest PFZ width and dis-persed GBPs,while intergranular corrosion is caused by continuous GBPs in other sub-regions.This study verified the dominant role of macro-galvanic effect and micro-galvanic effect in the corrosion process of FSW joint and FSW-PWHT joint,respectively.The maximum SCC susceptibility at HAZ in As-FSWed joint is dominated by enhanced anodic dissolution due to macro-galvanic effect.The SCC sensitivity of FSW-PWHT joint is higher than that of FSW joint due to high electrochemical activity and corrosion rate caused by the severe stress concentration between sub-grains and recrystallized grains at the thermome-chanical affected zone(TMAZ)/SZ interface. 展开更多
关键词 Aluminum alloys Friction stir welding Galvanic corrosion Post-weld heat treatment Microstructure evolution
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Hole inhibition mechanisms of Mg/steel lap joint by pinless friction stir spot welding
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作者 Tao-tao Li Hong-de Ding +5 位作者 Rui-feng Li Kai Qi Zhen-guang Liu Xiao-qiang Zhang Yue Zhao Lei Qiao 《Journal of Iron and Steel Research International》 2025年第4期1085-1101,共17页
Pinless friction stir spot welding(P-FSSW)was performed to manufacture Mg/steel lap joints.Orthogonal tests for P-FSSW of Mg/steel were investigated,and the main factors affecting the properties of Mg/steel lap joints... Pinless friction stir spot welding(P-FSSW)was performed to manufacture Mg/steel lap joints.Orthogonal tests for P-FSSW of Mg/steel were investigated,and the main factors affecting the properties of Mg/steel lap joints were derived.The shear force of the Mg/steel lap joints gradually increased and then decreased as the welding time increased.Maximum shear force was 5.3 kN.Fe-Al intermetallic compound(IMC)was formed at the Mg/steel interface near the steel side,and Mg-Al IMCs were formed at the Mg/steel interface near the Mg alloy side.Mg/steel lap joint was transformed from an initial solid-state welding to fusion-brazing welding as the welding time increased.No hole defects were formed in Mg/steel solid-state welding joints,whereas hole defects appeared in Mg/steel fusion-brazing welding joints.The temperature field of Mg/steel lap joints was simulated to analyze hole defects generated during the welding process.Hole defects can be eliminated by changing the spindle deflection angle,and the shear force decreased.Excessive spindle deflection can also lead to failure to form a stable joint.Hole defects were removed because the spindle deflection angle reduced the interfacial reaction temperature,and a solid-state welding joint was formed,which resulted in an absence of fusion-brazing welding hole formation. 展开更多
关键词 Mg/steel Lap joint Pinless friction stir spot welding Hole inhibition SIMULATION
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Effect of single winding helical electromagnetic stirring on microstructure and mechanical properties of semi-solid Al-Mg_(2)Si in-situ composites
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作者 Dong Pan Qing-tao Guo +7 位作者 Yi-tong Wang Bing-jun Lu Xue-feng Tang Hua-song Liu Pei Xu Xiao-lei Zhu Chong-yi Wei Yu Zhang 《China Foundry》 2025年第4期449-462,共14页
The Al-Mg_(2)Si in-situ composite is a lightweight material with great potential for application in fields such as automotive lightweighting,aerospace,and electronic components.In this research,the modification,semi-s... The Al-Mg_(2)Si in-situ composite is a lightweight material with great potential for application in fields such as automotive lightweighting,aerospace,and electronic components.In this research,the modification,semi-solid technology coupled with different types of electromagnetic stirring was applied to regulate the undesirable solidified dendritic microstructure and facilitate the composites’mechanical properties.The spheroidization and refinement of Mg_(2)Si andα-Al matrix in SM(semi-solid)+RES(rotate electromagnetic stirring)sample and SM+SHES(single winding helical electromagnetic stirring)sample are realized under the effect of fused dendrite arm,the decreased critical nucleate radius,and the increased nucleation rate and extra supercooling degree induced by electromagnetic stirring.The Mg_(2)Si phase in the SM+RES sample and SM+SHES sample is refined by 73.4%and 75.7%,respectively compared to the AC(as-cast)sample.Besides,the single winding electromagnetic stirring can lead to more homogeneously distributed physical fields,lower temperature gradient,and more significant mass transfer,mainly responsible for the more homogeneous distributed reinforced finer Mg_(2)Si particles in the SM+SHES sample.Moreover,both the tensile properties and hardness of modified semi-solid composites are improved through electromagnetic stirring.Compared with RES,the improvement effect of SHES is more excellent.The SM+SHES sample possesses the highest Brinell hardness(124.7 HB),and its quality index of tensile properties is 5.73%and 82.2%higher than that of the SM+RES and AC samples,respectively. 展开更多
关键词 electromagnetic stirring Al-Mg_(2)Si composites SEMI-SOLID mechanical properties MODIFICATION
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