On the base of literature review and the analysis of yarn properties, yarn structure and some other facts, the abrasion resistance of both rotor spun yarn and ring spun yarns are discussed. The results show that with ...On the base of literature review and the analysis of yarn properties, yarn structure and some other facts, the abrasion resistance of both rotor spun yarn and ring spun yarns are discussed. The results show that with the same raw material and twist, the rotor spun yarn has lower abrasion resistance than that of ring spun yarn, because of the higher twist employed, the abrasion resistance of rotor spun yarn is higher than that of ring spun yarn.展开更多
In this study, the effect of wheel speed and mischmetal（MM） content on the magnetic properties of MMFeB ribbons was investigated. The samples were prepared via direct solidification technique. The nominal compositio...In this study, the effect of wheel speed and mischmetal（MM） content on the magnetic properties of MMFeB ribbons was investigated. The samples were prepared via direct solidification technique. The nominal composition of the alloy ingots is MM;Fe;B;with x varying from 9 to 15 in steps of 2. Experimental results show the overall magnetic properties of the ribbons.Analysis of the results shows that the magnetic properties first improve and then degrade with the wheel speed and MM content increasing. Increase in MM content leads to better formation of crystal texture in the ribbons, indicating that the a-Fe phase might undermine the formation of crystal texture. Magnetic properties results show that the coercivity of the ribbons rises with an appropriate increase in both MM content and wheel speed during melt-spun process. The strongest magnetic properties of the ribbons(remanence of M;= 0.72 T, intrinsic coercivity of H;= 352.58 kA·m;, and maximum energy product of（BH）;=72.14 kJ·m;) are obtained for compositions where x = 13 and a wheel speed of v = 20 m·s;.展开更多
Compounds with the composition SmFex（x=3–8） were prepared by melt spun method at a velocity of 40 m/s and subsequent annealing at temperature between 600–1000 ℃. The crystal structures of the as-quenched and as a...Compounds with the composition SmFex（x=3–8） were prepared by melt spun method at a velocity of 40 m/s and subsequent annealing at temperature between 600–1000 ℃. The crystal structures of the as-quenched and as annealed powders were investigated by XRD methods with following Rietveld analysis. The glass forming ability could be enhanced by the increase of Sm content to x≤5.Metastable Sm5Fe17-type structure existed when 3≤x≤5 and temperature was lower than 800 ℃. SmFe2-type structure could be stable up to 1000 ℃ when x〉3 and temperature was under 800 ℃. The content of SmFe2-type decreased with the increase of x value and increased with temperature lower than 800 ℃, from which SmFe2-type started to bring the transition to SmFe3-type. As for Sm5Fe17-type compounds with x=3.4, the highest coercivity of 33.6 kOe could be obtained under a velocity of 30 m/s and heat treated under 700 ℃×1h.展开更多
The SmxZr0.3Fe9.1-xCoo.6 （x=0.8, 0.9, 1.D） powders were prepared by melt-spun method with different quenching velocities. The phase and microstructure were studied by X-ray diffraction （XRD）, scanning electron mic...The SmxZr0.3Fe9.1-xCoo.6 （x=0.8, 0.9, 1.D） powders were prepared by melt-spun method with different quenching velocities. The phase and microstructure were studied by X-ray diffraction （XRD）, scanning electron microscopy （SEM） and transmission elec- tron microscopy （TEM）. The Th2Zn17-type structure of the as-cast state changed to TbCuv-type after quenching to a rotating molyb- denum roll under certain velocity, and the formation of TbCuT-type phase was strictly depending on the Sm content and roll speed. The SEM morphology showed that the Fe-rich Zone was typically fish-bone structure and TEM diffraction pattern indicated the nano-scale crystal size with TbCuT-structure when x=0.9, and FCC type 7-Fe on the basis of ct-Fe formed in the non-equilibrium so- lidification could be detected by selected area electron diffraction （SAED） indexing in the x=0.8 samples.展开更多
The magnetocaloric properties of melt-spun La(Fe,Si)13 and MnFePGe compounds were investigated. Very large value of magnetic entropy change ｜ΔS｜=31 and 35.4 J·(kg·K)-1 under 5 T were obtained at 201 K in ...The magnetocaloric properties of melt-spun La(Fe,Si)13 and MnFePGe compounds were investigated. Very large value of magnetic entropy change ｜ΔS｜=31 and 35.4 J·(kg·K)-1 under 5 T were obtained at 201 K in LaFe11.8Si1.2 melt-spun ribbons and at around 317 K in Mn1.1Fe0.9P0.76Ge0.24 melt-spun ribbons, respectively. The large magnetocaloric effect results from a more homogenous element distribution related to the very high cooling rate during melt-spinning. The excellent MCE properties, the low materials cost and the accelerated aging regime make the melt-spun-type La(Fe,Si)13 and MnFePGe materials an excellent candidate for magnetic refrigerant applications.展开更多
A three-dimensional electrochemical oxidation （3D-EC） reactor with introduction of activated carbon （AC） as particle micro-electrodes was apphed for the advanced treatment of secondary wastewater effluent of a wet...A three-dimensional electrochemical oxidation （3D-EC） reactor with introduction of activated carbon （AC） as particle micro-electrodes was apphed for the advanced treatment of secondary wastewater effluent of a wet-spun acrylic fiber manufacturing plant. Under the optimized conditions （current density of 500 A/m2, circulation rate of 5 mL/min, AC dosage of 50 g, and chloride concentration of 1.0 g/L）, the average removal efficiencies of chemical oxygen demand （CODer）, NH3-N, total organic carbon （TOC）, and ultraviolet absorption at 254 nm （UV2s4） of the 3D-EC reactor were 64.5%, 60.8%, 46.4%, and 64.8%, respectively; while the corresponding effluent concentrations of CODcr, NH3-N, TOC, and UV2s4 were 76.6, 20.1, and 42.5 mg/L, and 0.08 Abs/cm, respectively. The effluent concentration of CODer was less than 100 mg/L, which showed that the treated wastewater satisfied the demand of the integrated wastewater discharge standard （GB 8978-1996）. The 3D-EC process remarkably improved the treatment efficiencies with synergistic effects for CODer, NH3-N, TOC, and UV2s4 during the stable stage of 44.5%, 38.8%, 27.2%, and 10.9%, respectively, as compared with the sum of the efficiencies of a two-dimensional electrochemical oxidation （2D-EC） reactor and an AC adsorption process, which was ascribed to the numerous micro-electrodes of AC in the 3D-EC reactor. Gas chromatography mass spectrometry （GC-MS） analysis revealed that electro- chemical treatment did not generate more toxic organics, and it was proved that the increase in acute biotoxicity was caused primarily by the production of free chlorine.展开更多
This paper presents a comparison study of two models for predicting the strength of rotor spun cotton yarns from fiber properties. The adaptive neuro-fuzzy system inference （ANFIS） and Multiple Linear Regression mod...This paper presents a comparison study of two models for predicting the strength of rotor spun cotton yarns from fiber properties. The adaptive neuro-fuzzy system inference （ANFIS） and Multiple Linear Regression models are used to predict the rotor spun yarn strength. Fiber properties and yam count are used as inputs to train the two models and the count-strength-product （CSP） was the targel. The predictive performances of the two models are estimated and compared. We found that the ANFIS has a better predictive power in comparison with linear multiple regression model. The impact of each fiber property is also illustrated.展开更多
In this study, the alloy ingots with nominal compositions of （Nd1_xCex）31FebalCoo.2Gao.1B （x = 0, 0.1 wt%, 0.2 wt%, 0.3 wt%, 0.4 wt%, 0.5 wt%） were prepared and then melt-spun to form nanocrystalline ribbons at th...In this study, the alloy ingots with nominal compositions of （Nd1_xCex）31FebalCoo.2Gao.1B （x = 0, 0.1 wt%, 0.2 wt%, 0.3 wt%, 0.4 wt%, 0.5 wt%） were prepared and then melt-spun to form nanocrystalline ribbons at the wheel speed of 20 m/s. XRD results show that all melt-spun ribbons exhibit the tetragonal structure （Nd,Ce）2Fe14B phase with the space group P42]rnmm. The Curie temperature and lattice constant decrease with the increase of Ce content. The Curie temperature decreases gradually from 306 to 247 ~C with the increase of Ce content. Those results indicate that Ce element has been incorporated into Nd2Fe14B main crystalline phase and formed （Ce,Nd）-Fe-B hard magnetic phase. It is also found that the remanence ratio （Mr/Ms） decreases from 0.693 to 0.663 and the coercivity （Hc） decreases from 18.7 to 14.2 kOe with the increase of Ce content. However, a relatively high coercivity of 18.3 kOe for （Ndl xCex）31FebalCoo.2Gao.lB （x = 0.2） melt-spun ribbon is achieved. The coercivity is sensitive to microstructure. The AFM patterns show the sample （x - 0.2） has the most uniform and finest micro- structure. The magnetization reversal behavior （0M plots） is discussed in detail. The positive 0M value is observed in every sample, which confirms the existence of exchange coupling interaction. Evidently, the OM maximum value reaches 0.9 in the sample （x - 0.2）. It is indicated that the intergranular exchange coupling effect is the strongest, which is consistent with coercivity enhancing.展开更多
Melt-spun ribbons which are the important raw material for hot-deformed magnets can be prepared by single-roller melt-spinning. In order to prepare well-structured ribbons, the model of temperature field for single-ro...Melt-spun ribbons which are the important raw material for hot-deformed magnets can be prepared by single-roller melt-spinning. In order to prepare well-structured ribbons, the model of temperature field for single-roller melt-spinning process was constructed in this work. The heat conduction in this process was simplified as one dimensional heat conduction problem. It was shown by modeling that, the temperature field in the melt-spinning before solidification in this model could be described as this equa-tionT（x,t）=Tmoexp[-k（x-x0）-k2αt]＋T0. The temperatureT（x,t） of the alloy melts decreased with increased positionx and cooling timet exponentially from the wheel-free surface to the wheel-side surface. The constantk determined the decrease speed of alloy tempera-tureT（x,t）, which was proportional to the interfacial heat transfer coefficienth and the interfacial area of heat conductionA0, but in-versely proportional to the thermal conductivityK.x0 was the thickness of the alloy melt. With increasedx0, the temperature differ-ence between wheel-free surface and the wheel-side surface became larger, which would lead to larger difference in grain size. In ex-periments, the influence of melt-spinning process parameters on the temperature field model was discussed, such as cooling roller materials, wheel speed, and so on. Melt-spun ribbons prepared by single-roller melt spinning at different wheel speed were investi-gated and magnetic properties of die-upset magnets from melt-spun ribbons on different cooling roller were analyzed. The variation of grain size in the depth direction consisted with temperature field model. This model provided directions for the preparation of melt-spun ribbons with uniformly distributed fine grains, which were very necessary for producing hot-deformed magnets with high magnetic performance.展开更多
Amorphous （Nd,Pr）13Fe80Nb1B6 ribbons were crystallized at 670-730°C for 5-25 min to study the effects of isothermal crystallization on their behavior and magnetic properties. XRD results indicate that the isoth...Amorphous （Nd,Pr）13Fe80Nb1B6 ribbons were crystallized at 670-730°C for 5-25 min to study the effects of isothermal crystallization on their behavior and magnetic properties. XRD results indicate that the isothermal incubation time is 12, 5, and less than 5 min at 670, 700, and 730°C, respectively. High coercivities, with the maximum value of iHc = 1616 kA/m at 700°C for 19 min, measured by a physical property measurement system, are obtained in the crystallized ribbons. This is mainly attributed to the addition of Pr and Nb, because Pr2Fe14B has a higher anisotropic field than Nd2Fe14B, and Nb enriched in the grain boundary regions can not only reduce the exchange-coupling effects among hard grains, but also impede grain growth during the crystallization process. In addition, it should also be related to the characteristics of the furnace that the authors designed.展开更多
Generally, ring spun yarns are manufactured from roving which is produced by roving frame. In this paper, an experiment has been done producing ring spun cotton yarn directly from finisher drawn sliver eliminatin...Generally, ring spun yarns are manufactured from roving which is produced by roving frame. In this paper, an experiment has been done producing ring spun cotton yarn directly from finisher drawn sliver eliminating the roving frame. Total 3 types of yarn with the various linear density of 8 Ne, 10 Ne & 12 Ne were produced using a roving frame and without using a roving frame. In the next step, physical and mechanical properties of those yarns including unevenness, imperfections, hairiness & tenacity were investigated. The result showed that ring spun cotton yarns produced from sliver exhibited inferior physical and mechanical properties compared with samples from the conventional ring spinning system.展开更多
Highly textured Heusler alloy Mn_（46）Ni_（42）Sn_（11）Sb_1 ribbons were prepared by melt spinning. The annealed high Mn content Mn46Ni42Sn11Sb1 ribbon cross-section microstructure, crystal structure, martensitic tr...Highly textured Heusler alloy Mn_（46）Ni_（42）Sn_（11）Sb_1 ribbons were prepared by melt spinning. The annealed high Mn content Mn46Ni42Sn11Sb1 ribbon cross-section microstructure, crystal structure, martensitic transformation（MT）, and magnetoresistance（MR） properties were investigated. The MR in the annealed ribbon was assessed by the magnetic field direction perpendicular to the ribbon surface with the magnetic field up to 30 k Oe. The large negative value of 25% for MR was obtained at 244 K. The exchange bias（EB） effects of the as-spun and annealed ribbons were investigated. After annealing, the EB effects have been improved by about 25 Oe at the temperature of 50 K. The magnetizations have increased approximately by 10% more than the as-spun ribbon.展开更多
The lower strength of friction spun yarns has became a key problem that hinder the develop-ment of friction spinning,especially in high speeds and fine yarns.In this paper a project aimed atincreasing the strength of ...The lower strength of friction spun yarns has became a key problem that hinder the develop-ment of friction spinning,especially in high speeds and fine yarns.In this paper a project aimed atincreasing the strength of friction spun yarns by using a false twist process has been made.In re-ported experiment false twist was inserted into the yarn which has been formed on a friction spin-ning machine,so that it made the yarn untwist at first,then regain the twist.In the meantime draftwas applied to generate more tension than that which had been experienced during yarn formationon the friction spinning machine.It made the yarn reforming and the loosely bound fibres in thefriction spun yarn formed due to extremely low tension on the friction spinning machine becametighter.Results indicate that with the proper draft,tension and false twist the tenacity of processedyarn will increase more than 10%.This project is an attempt to discover whether improvements can be made and whether it isworth pursuing research into modifications of yarn structure.The results imply that if the yarntension can be raised during yarn formation on the friction spinning machine or a chance is offeredto the yarn to reform after the yarn formation the yarn tenacity will be increased obviously.展开更多
The rotor spun yarn(OE yarn),twist of which is calledlayering twist,was added a few involving twist,and itsstructure and properties were measured.The experimen-tal results have shown that the morphological structure o...The rotor spun yarn(OE yarn),twist of which is calledlayering twist,was added a few involving twist,and itsstructure and properties were measured.The experimen-tal results have shown that the morphological structure ofthe rotor spun yarn with modified twist was changed andits tensile properties and abrasion resistance were im-proved.展开更多
This paper described the physical behaviour of three types of denim cloths produced from rotor yarn, ring yarn and modified rotor yarn (prepared by adding conventional twist to rotor yarn) respectively. Experimental w...This paper described the physical behaviour of three types of denim cloths produced from rotor yarn, ring yarn and modified rotor yarn (prepared by adding conventional twist to rotor yarn) respectively. Experimental work showed that denim cloth produced from the modified rotor yarn has superior properties over conventional rotor yarn in terms of surface texture and appearance,tearing strength and resistance to abrasion.展开更多
A model was deveIoped to investigate impregnation behavior of thermoplastic resin into filament bundle based on Darcy's law. Consolidation processes of unidirectional laminate were performed to evaluate the validi...A model was deveIoped to investigate impregnation behavior of thermoplastic resin into filament bundle based on Darcy's law. Consolidation processes of unidirectional laminate were performed to evaluate the validity of the model. Friction spun core yarns were used in the experiments with polypropylene fiber sheath and glass filament core. The processing conditions, such as temperature and pressure, and filament parameters were taken into consideration. A good agreement was found between theoretical prediction and experiment data.展开更多
In this paper, fibrillation properties of solvent - spun cellulose fiber and some influencing factors are analyzed based on the experiment results. It is pointed out that special textile styles and aesthetic appearanc...In this paper, fibrillation properties of solvent - spun cellulose fiber and some influencing factors are analyzed based on the experiment results. It is pointed out that special textile styles and aesthetic appearance could be obtained by controlling the fibrillation.展开更多
It is believed that gel spun polyethylene(PE)fibers have a somewhat extended chain crystalstructure,because of the disentangling of the chains which takes place in semi-dilute solutionand the ultra high draw ratio use...It is believed that gel spun polyethylene(PE)fibers have a somewhat extended chain crystalstructure,because of the disentangling of the chains which takes place in semi-dilute solutionand the ultra high draw ratio used.Ten years ago,PE shish-kebabs grown from dilute solutionwere proved to have extended chain backbone which causes the raising of its melting point.These crystals were found to have a triclinic crystal phase,This study shows a different result forgel spun ultra high drawn PE fiber.The unit cell remains orthorhombic even if the draw ratioreaches 50;as the draw ratio increases,the length in a and b axes are shortened while that in c ax-is changes quite insignificantly.When the draw ratio is over 10,two endothermic melting peakscan be seen in the DSC curves with corresponding peak temperature of 136.7-145.3℃.The lat-ter peak is attributed to the amount of extended chain crystal.展开更多
文摘On the base of literature review and the analysis of yarn properties, yarn structure and some other facts, the abrasion resistance of both rotor spun yarn and ring spun yarns are discussed. The results show that with the same raw material and twist, the rotor spun yarn has lower abrasion resistance than that of ring spun yarn, because of the higher twist employed, the abrasion resistance of rotor spun yarn is higher than that of ring spun yarn.
基金financially supported by the National Natural Science Foundation of China (Nos. 51461033, 51571126, 51541105, and 11547032)the Inner Mongolia Innovative Research Team (No. 3400102)+3 种基金the Inner Mongolia Science Foundation (No. 2013MS0110)the Provincial Major Science and Technology Project of Inner Mongolia (No. 2009J1006)the Baotou Major Research Project Special for Rare Earth (No. 2012R1006)the Inner Mongolia University of Science and Technology Innovation Fund
文摘In this study, the effect of wheel speed and mischmetal（MM） content on the magnetic properties of MMFeB ribbons was investigated. The samples were prepared via direct solidification technique. The nominal composition of the alloy ingots is MM;Fe;B;with x varying from 9 to 15 in steps of 2. Experimental results show the overall magnetic properties of the ribbons.Analysis of the results shows that the magnetic properties first improve and then degrade with the wheel speed and MM content increasing. Increase in MM content leads to better formation of crystal texture in the ribbons, indicating that the a-Fe phase might undermine the formation of crystal texture. Magnetic properties results show that the coercivity of the ribbons rises with an appropriate increase in both MM content and wheel speed during melt-spun process. The strongest magnetic properties of the ribbons(remanence of M;= 0.72 T, intrinsic coercivity of H;= 352.58 kA·m;, and maximum energy product of（BH）;=72.14 kJ·m;) are obtained for compositions where x = 13 and a wheel speed of v = 20 m·s;.
基金supported by the National High Technology Research and Development Program of China(863 Program)(2011AA03A402)
文摘Compounds with the composition SmFex（x=3–8） were prepared by melt spun method at a velocity of 40 m/s and subsequent annealing at temperature between 600–1000 ℃. The crystal structures of the as-quenched and as annealed powders were investigated by XRD methods with following Rietveld analysis. The glass forming ability could be enhanced by the increase of Sm content to x≤5.Metastable Sm5Fe17-type structure existed when 3≤x≤5 and temperature was lower than 800 ℃. SmFe2-type structure could be stable up to 1000 ℃ when x〉3 and temperature was under 800 ℃. The content of SmFe2-type decreased with the increase of x value and increased with temperature lower than 800 ℃, from which SmFe2-type started to bring the transition to SmFe3-type. As for Sm5Fe17-type compounds with x=3.4, the highest coercivity of 33.6 kOe could be obtained under a velocity of 30 m/s and heat treated under 700 ℃×1h.
基金supported by the National High Technology Research and Development Program of China (863 Program) (2011AA03A402)the International Scientific and Technological Cooperation Projects (2010DFB53520)
文摘The SmxZr0.3Fe9.1-xCoo.6 （x=0.8, 0.9, 1.D） powders were prepared by melt-spun method with different quenching velocities. The phase and microstructure were studied by X-ray diffraction （XRD）, scanning electron microscopy （SEM） and transmission elec- tron microscopy （TEM）. The Th2Zn17-type structure of the as-cast state changed to TbCuv-type after quenching to a rotating molyb- denum roll under certain velocity, and the formation of TbCuT-type phase was strictly depending on the Sm content and roll speed. The SEM morphology showed that the Fe-rich Zone was typically fish-bone structure and TEM diffraction pattern indicated the nano-scale crystal size with TbCuT-structure when x=0.9, and FCC type 7-Fe on the basis of ct-Fe formed in the non-equilibrium so- lidification could be detected by selected area electron diffraction （SAED） indexing in the x=0.8 samples.
文摘The magnetocaloric properties of melt-spun La(Fe,Si)13 and MnFePGe compounds were investigated. Very large value of magnetic entropy change ｜ΔS｜=31 and 35.4 J·(kg·K)-1 under 5 T were obtained at 201 K in LaFe11.8Si1.2 melt-spun ribbons and at around 317 K in Mn1.1Fe0.9P0.76Ge0.24 melt-spun ribbons, respectively. The large magnetocaloric effect results from a more homogenous element distribution related to the very high cooling rate during melt-spinning. The excellent MCE properties, the low materials cost and the accelerated aging regime make the melt-spun-type La(Fe,Si)13 and MnFePGe materials an excellent candidate for magnetic refrigerant applications.
基金supported by the Major Science and Technology Program for Water Pollution Control and Treatment (No. 2012ZX07201002-6)
文摘A three-dimensional electrochemical oxidation （3D-EC） reactor with introduction of activated carbon （AC） as particle micro-electrodes was apphed for the advanced treatment of secondary wastewater effluent of a wet-spun acrylic fiber manufacturing plant. Under the optimized conditions （current density of 500 A/m2, circulation rate of 5 mL/min, AC dosage of 50 g, and chloride concentration of 1.0 g/L）, the average removal efficiencies of chemical oxygen demand （CODer）, NH3-N, total organic carbon （TOC）, and ultraviolet absorption at 254 nm （UV2s4） of the 3D-EC reactor were 64.5%, 60.8%, 46.4%, and 64.8%, respectively; while the corresponding effluent concentrations of CODcr, NH3-N, TOC, and UV2s4 were 76.6, 20.1, and 42.5 mg/L, and 0.08 Abs/cm, respectively. The effluent concentration of CODer was less than 100 mg/L, which showed that the treated wastewater satisfied the demand of the integrated wastewater discharge standard （GB 8978-1996）. The 3D-EC process remarkably improved the treatment efficiencies with synergistic effects for CODer, NH3-N, TOC, and UV2s4 during the stable stage of 44.5%, 38.8%, 27.2%, and 10.9%, respectively, as compared with the sum of the efficiencies of a two-dimensional electrochemical oxidation （2D-EC） reactor and an AC adsorption process, which was ascribed to the numerous micro-electrodes of AC in the 3D-EC reactor. Gas chromatography mass spectrometry （GC-MS） analysis revealed that electro- chemical treatment did not generate more toxic organics, and it was proved that the increase in acute biotoxicity was caused primarily by the production of free chlorine.
文摘This paper presents a comparison study of two models for predicting the strength of rotor spun cotton yarns from fiber properties. The adaptive neuro-fuzzy system inference （ANFIS） and Multiple Linear Regression models are used to predict the rotor spun yarn strength. Fiber properties and yam count are used as inputs to train the two models and the count-strength-product （CSP） was the targel. The predictive performances of the two models are estimated and compared. We found that the ANFIS has a better predictive power in comparison with linear multiple regression model. The impact of each fiber property is also illustrated.
基金Project supported by the National Basic Research Program of China(973 Program)(2014CB643701)the National Natural Science Foundation of China(51571064,51331003)
文摘In this study, the alloy ingots with nominal compositions of （Nd1_xCex）31FebalCoo.2Gao.1B （x = 0, 0.1 wt%, 0.2 wt%, 0.3 wt%, 0.4 wt%, 0.5 wt%） were prepared and then melt-spun to form nanocrystalline ribbons at the wheel speed of 20 m/s. XRD results show that all melt-spun ribbons exhibit the tetragonal structure （Nd,Ce）2Fe14B phase with the space group P42]rnmm. The Curie temperature and lattice constant decrease with the increase of Ce content. The Curie temperature decreases gradually from 306 to 247 ~C with the increase of Ce content. Those results indicate that Ce element has been incorporated into Nd2Fe14B main crystalline phase and formed （Ce,Nd）-Fe-B hard magnetic phase. It is also found that the remanence ratio （Mr/Ms） decreases from 0.693 to 0.663 and the coercivity （Hc） decreases from 18.7 to 14.2 kOe with the increase of Ce content. However, a relatively high coercivity of 18.3 kOe for （Ndl xCex）31FebalCoo.2Gao.lB （x = 0.2） melt-spun ribbon is achieved. The coercivity is sensitive to microstructure. The AFM patterns show the sample （x - 0.2） has the most uniform and finest micro- structure. The magnetization reversal behavior （0M plots） is discussed in detail. The positive 0M value is observed in every sample, which confirms the existence of exchange coupling interaction. Evidently, the OM maximum value reaches 0.9 in the sample （x - 0.2）. It is indicated that the intergranular exchange coupling effect is the strongest, which is consistent with coercivity enhancing.
基金Project supported by Major State Basic Research Development Program of China(2010AA03A401)the National High-tech R&D Program of China(50931001,51241009)
文摘Melt-spun ribbons which are the important raw material for hot-deformed magnets can be prepared by single-roller melt-spinning. In order to prepare well-structured ribbons, the model of temperature field for single-roller melt-spinning process was constructed in this work. The heat conduction in this process was simplified as one dimensional heat conduction problem. It was shown by modeling that, the temperature field in the melt-spinning before solidification in this model could be described as this equa-tionT（x,t）=Tmoexp[-k（x-x0）-k2αt]＋T0. The temperatureT（x,t） of the alloy melts decreased with increased positionx and cooling timet exponentially from the wheel-free surface to the wheel-side surface. The constantk determined the decrease speed of alloy tempera-tureT（x,t）, which was proportional to the interfacial heat transfer coefficienth and the interfacial area of heat conductionA0, but in-versely proportional to the thermal conductivityK.x0 was the thickness of the alloy melt. With increasedx0, the temperature differ-ence between wheel-free surface and the wheel-side surface became larger, which would lead to larger difference in grain size. In ex-periments, the influence of melt-spinning process parameters on the temperature field model was discussed, such as cooling roller materials, wheel speed, and so on. Melt-spun ribbons prepared by single-roller melt spinning at different wheel speed were investi-gated and magnetic properties of die-upset magnets from melt-spun ribbons on different cooling roller were analyzed. The variation of grain size in the depth direction consisted with temperature field model. This model provided directions for the preparation of melt-spun ribbons with uniformly distributed fine grains, which were very necessary for producing hot-deformed magnets with high magnetic performance.
基金supported by the National Natural Science Foundation of China (No. 50744014)the National Basic Research Foundation (No. 2004CCA04000)+3 种基金Science and Technology Department of Zhejiang Province (Nos. 2008C21046 and 2008C11086-1)the Natural Science Foundation of Zhejiang Province,China (No. Y406389)the Research and Development Program of Ningbo Bureau of Science and Technology (No. 2006B100054)K.C.Wong Magna Found in Ningbo University
文摘Amorphous （Nd,Pr）13Fe80Nb1B6 ribbons were crystallized at 670-730°C for 5-25 min to study the effects of isothermal crystallization on their behavior and magnetic properties. XRD results indicate that the isothermal incubation time is 12, 5, and less than 5 min at 670, 700, and 730°C, respectively. High coercivities, with the maximum value of iHc = 1616 kA/m at 700°C for 19 min, measured by a physical property measurement system, are obtained in the crystallized ribbons. This is mainly attributed to the addition of Pr and Nb, because Pr2Fe14B has a higher anisotropic field than Nd2Fe14B, and Nb enriched in the grain boundary regions can not only reduce the exchange-coupling effects among hard grains, but also impede grain growth during the crystallization process. In addition, it should also be related to the characteristics of the furnace that the authors designed.
文摘Generally, ring spun yarns are manufactured from roving which is produced by roving frame. In this paper, an experiment has been done producing ring spun cotton yarn directly from finisher drawn sliver eliminating the roving frame. Total 3 types of yarn with the various linear density of 8 Ne, 10 Ne & 12 Ne were produced using a roving frame and without using a roving frame. In the next step, physical and mechanical properties of those yarns including unevenness, imperfections, hairiness & tenacity were investigated. The result showed that ring spun cotton yarns produced from sliver exhibited inferior physical and mechanical properties compared with samples from the conventional ring spinning system.
基金Project supported by the National Basic Research Program of China(Grant No.2012CB722801)the Postdoctoral Science Foundation of China(Grant No.2015M571285)+3 种基金the National Natural Science Foundation of China(Grant No.51401140)the Postdoctoral Research Station Foundation of Taiyuan University of Science and Technology,China(Grant Nos.20142014,20152041,and 20151082)the Natural Science Foundation of Shanxi Province,China(Grants Nos.2015021019,2015091011,and 2015081011)the Key Team of Scientific and Technological Innovation of Shanxi Province,China(Grant No.2013131009)
文摘Highly textured Heusler alloy Mn_（46）Ni_（42）Sn_（11）Sb_1 ribbons were prepared by melt spinning. The annealed high Mn content Mn46Ni42Sn11Sb1 ribbon cross-section microstructure, crystal structure, martensitic transformation（MT）, and magnetoresistance（MR） properties were investigated. The MR in the annealed ribbon was assessed by the magnetic field direction perpendicular to the ribbon surface with the magnetic field up to 30 k Oe. The large negative value of 25% for MR was obtained at 244 K. The exchange bias（EB） effects of the as-spun and annealed ribbons were investigated. After annealing, the EB effects have been improved by about 25 Oe at the temperature of 50 K. The magnetizations have increased approximately by 10% more than the as-spun ribbon.
文摘The lower strength of friction spun yarns has became a key problem that hinder the develop-ment of friction spinning,especially in high speeds and fine yarns.In this paper a project aimed atincreasing the strength of friction spun yarns by using a false twist process has been made.In re-ported experiment false twist was inserted into the yarn which has been formed on a friction spin-ning machine,so that it made the yarn untwist at first,then regain the twist.In the meantime draftwas applied to generate more tension than that which had been experienced during yarn formationon the friction spinning machine.It made the yarn reforming and the loosely bound fibres in thefriction spun yarn formed due to extremely low tension on the friction spinning machine becametighter.Results indicate that with the proper draft,tension and false twist the tenacity of processedyarn will increase more than 10%.This project is an attempt to discover whether improvements can be made and whether it isworth pursuing research into modifications of yarn structure.The results imply that if the yarntension can be raised during yarn formation on the friction spinning machine or a chance is offeredto the yarn to reform after the yarn formation the yarn tenacity will be increased obviously.
文摘The rotor spun yarn(OE yarn),twist of which is calledlayering twist,was added a few involving twist,and itsstructure and properties were measured.The experimen-tal results have shown that the morphological structure ofthe rotor spun yarn with modified twist was changed andits tensile properties and abrasion resistance were im-proved.
文摘This paper described the physical behaviour of three types of denim cloths produced from rotor yarn, ring yarn and modified rotor yarn (prepared by adding conventional twist to rotor yarn) respectively. Experimental work showed that denim cloth produced from the modified rotor yarn has superior properties over conventional rotor yarn in terms of surface texture and appearance,tearing strength and resistance to abrasion.
基金Funded by the Research Fund for the Doctoral Program of High Education
文摘A model was deveIoped to investigate impregnation behavior of thermoplastic resin into filament bundle based on Darcy's law. Consolidation processes of unidirectional laminate were performed to evaluate the validity of the model. Friction spun core yarns were used in the experiments with polypropylene fiber sheath and glass filament core. The processing conditions, such as temperature and pressure, and filament parameters were taken into consideration. A good agreement was found between theoretical prediction and experiment data.
文摘In this paper, fibrillation properties of solvent - spun cellulose fiber and some influencing factors are analyzed based on the experiment results. It is pointed out that special textile styles and aesthetic appearance could be obtained by controlling the fibrillation.
基金This project is supported by National Science Foundation of China
文摘It is believed that gel spun polyethylene(PE)fibers have a somewhat extended chain crystalstructure,because of the disentangling of the chains which takes place in semi-dilute solutionand the ultra high draw ratio used.Ten years ago,PE shish-kebabs grown from dilute solutionwere proved to have extended chain backbone which causes the raising of its melting point.These crystals were found to have a triclinic crystal phase,This study shows a different result forgel spun ultra high drawn PE fiber.The unit cell remains orthorhombic even if the draw ratioreaches 50;as the draw ratio increases,the length in a and b axes are shortened while that in c ax-is changes quite insignificantly.When the draw ratio is over 10,two endothermic melting peakscan be seen in the DSC curves with corresponding peak temperature of 136.7-145.3℃.The lat-ter peak is attributed to the amount of extended chain crystal.
