A new Shift bases was synthesized by the reaction of p-dimetyl-amino-benzylaldehide and α-naftyl-amine. All synthesized compounds were characterized by elemental analysis, IR （infra red） spectroscopy and NMR （nucl...A new Shift bases was synthesized by the reaction of p-dimetyl-amino-benzylaldehide and α-naftyl-amine. All synthesized compounds were characterized by elemental analysis, IR （infra red） spectroscopy and NMR （nuclear magnetic resonance） spectroscopy and evaluated for their in vitro antifungal activities of the compounds tested against Pseudomonas aeruginosa, Mycobacterium lacticolium, Aspergillus niger, Cladasporium resinale, Penicillium chrosegenum, Chastorniurn gloloodium and Trichoderma virideh. These derivatives have vast range of biological activities which benefit us.展开更多
We demonstrate an adjustable pure dispersion slope compensating-module based on strain-chirped fiber Bragg gratings. The center wavelength of the module is preserved while the pure dispersion slope is tuned.
The effect of potassium-decoration was studied on the activity of water-gas shift （WGS） reaction over the Co-Mo-based catalysts supported on active carbon （AC）, which was prepared by incipient wetness co-impregnat...The effect of potassium-decoration was studied on the activity of water-gas shift （WGS） reaction over the Co-Mo-based catalysts supported on active carbon （AC）, which was prepared by incipient wetness co-impregnation method. The decoration of potassium on active carbon in advance enhances the activities of the CoMo-K/AC catalysts for WGS reaction. Highest activity （about 92% conversion） was obtained at 250 ？ C for the catalyst with an optimum K 2 O/AC weight ratio in the range from 0.12 to 0.15. The catalysts were characterized by TPR and EPR, and the results show that activated carbon decorated with potassium makes Co-Mo species highly dispersed, and thus easily reduced and sulfurized. XRD results show that an appropriate content of potassium-decoration on active carbon supports may favors the formation of highly dispersed Co 9 S 8 -type structures which are situated on the edge or a site in contact with MoS 2 , K-Mo-O-S, Mo-S-K phase. Those active species are responsible for the high activity of CoMo-K/AC catalysts.展开更多
The preparation of the iron-based catalysts promoted by cobalt with a small amount of copper and aluminum for the high temperature shift reaction （HTS） with different sequences of adding catalyst raw materials durin...The preparation of the iron-based catalysts promoted by cobalt with a small amount of copper and aluminum for the high temperature shift reaction （HTS） with different sequences of adding catalyst raw materials during neutralization and precipitation was investigated. XRD, BET and particle size distribution （PSD） were used to characterize the prepared catalysts. It was found that the catalyst crystals were all γ-Fe2O3, and the intermediate of the catalyst after aging was Fe3O4. The crystallographic form of the catalyst and its intermediate was not affected by the addition sequence in the neutralization and precipitation process. The results showed that the specific surface area and the particle size of the catalysts depended on the addition sequence to the mother liquor. Cobalt with a small amount of copper and aluminum could increase the specific surface area and decrease the particle size of catalysts.展开更多
Use of multidisciplinary analysis in reliabilitybased design optimization(RBDO) results in the emergence of the important method of reliability-based multidisciplinary design optimization(RBMDO). To enhance the effici...Use of multidisciplinary analysis in reliabilitybased design optimization(RBDO) results in the emergence of the important method of reliability-based multidisciplinary design optimization(RBMDO). To enhance the efficiency and convergence of the overall solution process,a decoupling algorithm for RBMDO is proposed herein.Firstly, to decouple the multidisciplinary analysis using the individual disciplinary feasible(IDF) approach, the RBMDO is converted into a conventional form of RBDO. Secondly,the incremental shifting vector(ISV) strategy is adopted to decouple the nested optimization of RBDO into a sequential iteration process composed of design optimization and reliability analysis, thereby improving the efficiency significantly. Finally, the proposed RBMDO method is applied to the design of two actual electronic products: an aerial camera and a car pad. For these two applications, two RBMDO models are created, each containing several finite element models(FEMs) and relatively strong coupling between the involved disciplines. The computational results demonstrate the effectiveness of the proposed method.展开更多
An improved approach for J-value segmentation （JSEG） is presented for unsupervised color image segmentation. Instead of color quantization algorithm, an automatic classification method based on adaptive mean shift ...An improved approach for J-value segmentation （JSEG） is presented for unsupervised color image segmentation. Instead of color quantization algorithm, an automatic classification method based on adaptive mean shift （AMS） based clustering is used for nonparametric clustering of image data set. The clustering results are used to construct Gaussian mixture modelling （GMM） of image data for the calculation of soft J value. The region growing algorithm used in JSEG is then applied in segmenting the image based on the multiscale soft J-images. Experiments show that the synergism of JSEG and the soft classification based on AMS based clustering and GMM overcomes the limitations of JSEG successfully and is more robust.展开更多
文摘A new Shift bases was synthesized by the reaction of p-dimetyl-amino-benzylaldehide and α-naftyl-amine. All synthesized compounds were characterized by elemental analysis, IR （infra red） spectroscopy and NMR （nuclear magnetic resonance） spectroscopy and evaluated for their in vitro antifungal activities of the compounds tested against Pseudomonas aeruginosa, Mycobacterium lacticolium, Aspergillus niger, Cladasporium resinale, Penicillium chrosegenum, Chastorniurn gloloodium and Trichoderma virideh. These derivatives have vast range of biological activities which benefit us.
文摘We demonstrate an adjustable pure dispersion slope compensating-module based on strain-chirped fiber Bragg gratings. The center wavelength of the module is preserved while the pure dispersion slope is tuned.
文摘The effect of potassium-decoration was studied on the activity of water-gas shift （WGS） reaction over the Co-Mo-based catalysts supported on active carbon （AC）, which was prepared by incipient wetness co-impregnation method. The decoration of potassium on active carbon in advance enhances the activities of the CoMo-K/AC catalysts for WGS reaction. Highest activity （about 92% conversion） was obtained at 250 ？ C for the catalyst with an optimum K 2 O/AC weight ratio in the range from 0.12 to 0.15. The catalysts were characterized by TPR and EPR, and the results show that activated carbon decorated with potassium makes Co-Mo species highly dispersed, and thus easily reduced and sulfurized. XRD results show that an appropriate content of potassium-decoration on active carbon supports may favors the formation of highly dispersed Co 9 S 8 -type structures which are situated on the edge or a site in contact with MoS 2 , K-Mo-O-S, Mo-S-K phase. Those active species are responsible for the high activity of CoMo-K/AC catalysts.
文摘The preparation of the iron-based catalysts promoted by cobalt with a small amount of copper and aluminum for the high temperature shift reaction （HTS） with different sequences of adding catalyst raw materials during neutralization and precipitation was investigated. XRD, BET and particle size distribution （PSD） were used to characterize the prepared catalysts. It was found that the catalyst crystals were all γ-Fe2O3, and the intermediate of the catalyst after aging was Fe3O4. The crystallographic form of the catalyst and its intermediate was not affected by the addition sequence in the neutralization and precipitation process. The results showed that the specific surface area and the particle size of the catalysts depended on the addition sequence to the mother liquor. Cobalt with a small amount of copper and aluminum could increase the specific surface area and decrease the particle size of catalysts.
基金supported by the Major Program of the National Natural Science Foundation of China (Grant 51490662)the Funds for Distinguished Young Scientists of Hunan Province (Grant 14JJ1016)+1 种基金the State Key Program of the National Science Foundation of China (11232004)the Heavy-duty Tractor Intelligent Manufacturing Technology Research and System Development (Grant 2016YFD0701105)
文摘Use of multidisciplinary analysis in reliabilitybased design optimization(RBDO) results in the emergence of the important method of reliability-based multidisciplinary design optimization(RBMDO). To enhance the efficiency and convergence of the overall solution process,a decoupling algorithm for RBMDO is proposed herein.Firstly, to decouple the multidisciplinary analysis using the individual disciplinary feasible(IDF) approach, the RBMDO is converted into a conventional form of RBDO. Secondly,the incremental shifting vector(ISV) strategy is adopted to decouple the nested optimization of RBDO into a sequential iteration process composed of design optimization and reliability analysis, thereby improving the efficiency significantly. Finally, the proposed RBMDO method is applied to the design of two actual electronic products: an aerial camera and a car pad. For these two applications, two RBMDO models are created, each containing several finite element models(FEMs) and relatively strong coupling between the involved disciplines. The computational results demonstrate the effectiveness of the proposed method.
文摘An improved approach for J-value segmentation （JSEG） is presented for unsupervised color image segmentation. Instead of color quantization algorithm, an automatic classification method based on adaptive mean shift （AMS） based clustering is used for nonparametric clustering of image data set. The clustering results are used to construct Gaussian mixture modelling （GMM） of image data for the calculation of soft J value. The region growing algorithm used in JSEG is then applied in segmenting the image based on the multiscale soft J-images. Experiments show that the synergism of JSEG and the soft classification based on AMS based clustering and GMM overcomes the limitations of JSEG successfully and is more robust.
