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漂浮型分级孔TiO_2陶瓷光催化剂的制备及应用 被引量:1
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作者 杜帆 漆胜群 +3 位作者 张琳琳 张航 于秀娟 邢子鹏 《黑龙江大学自然科学学报》 CAS 北大核心 2014年第1期106-111,共6页
利用高热稳定性介孔TiO2粉体,采用室温冷冻干燥法制备了一种漂浮型二氧化钛陶瓷光催化剂。采用X射线衍射(XRD)、扫描电镜(SEM)、N2吸附脱附等方法对陶瓷的结构进行表征。结果表明,所制备的漂浮型二氧化钛陶瓷具有大孔/介孔的分级孔结构... 利用高热稳定性介孔TiO2粉体,采用室温冷冻干燥法制备了一种漂浮型二氧化钛陶瓷光催化剂。采用X射线衍射(XRD)、扫描电镜(SEM)、N2吸附脱附等方法对陶瓷的结构进行表征。结果表明,所制备的漂浮型二氧化钛陶瓷具有大孔/介孔的分级孔结构,并且TiO2陶瓷在800℃焙烧条件下仍然能够保持锐钛矿相。对浓度为15 mg·L-1的模拟污染物亚甲基蓝(MB)进行了光催化降解研究,其去除率可达到92.2%。催化剂在循环使用6次后,降解效果依然在92%以上。另外,采用该催化剂降解罗丹明B(RhB)、甲基橙(MO)和苯酚(PhOH),去除率可以分别达到92.7%、90.2%和94.6%,表明所制备的漂浮型分级孔二氧化钛陶瓷光催化剂在实际废水处理中将有很好的应用前景。 展开更多
关键词 关键词 漂浮型光催化剂 分级孔TiO2陶瓷 冷冻干燥法 难降解有机废水 光催化
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Laparoscopic fundoplication for gastroesophageal reflux disease 被引量:16
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作者 Marzio Frazzoni Micaela Piccoli +2 位作者 Rita Conigliaro Leonardo Frazzoni Gianluigi Melotti 《World Journal of Gastroenterology》 SCIE CAS 2014年第39期14272-14279,共8页
Gastroesophageal reflux disease (GERD) is a condition that develops when the reflux of gastric contents into the esophagus leads to troublesome symptoms and/or complications. Heartburn is the cardinal symptom, often a... Gastroesophageal reflux disease (GERD) is a condition that develops when the reflux of gastric contents into the esophagus leads to troublesome symptoms and/or complications. Heartburn is the cardinal symptom, often associated with regurgitation. In patients with endoscopy-negative heartburn refractory to proton pump inhibitor (PPI) therapy and when the diagnosis of GERD is in question, direct reflux testing by impedance-pH monitoring is warranted. Laparoscopic fundoplication is the standard surgical treatment for GERD. It is highly effective in curing GERD with a 80% success rate at 20-year follow-up. The Nissen fundoplication, consisting of a total (360&#x000b0;) wrap, is the most commonly performed antireflux operation. To reduce postoperative dysphagia and gas bloating, partial fundoplications are also used, including the posterior (Toupet) fundoplication, and the anterior (Dor) fundoplication. Currently, there is consensus to advise laparoscopic fundoplication in PPI-responsive GERD only for those patients who develop untoward side-effects or complications from PPI therapy. PPI resistance is the real challenge in GERD. There is consensus that carefully selected GERD patients refractory to PPI therapy are eligible for laparoscopic fundoplication, provided that objective evidence of reflux as the cause of ongoing symptoms has been obtained. For this purpose, impedance-pH monitoring is regarded as the diagnostic gold standard. 展开更多
关键词 Gastroesophageal reflux disease Refractory gastroesophageal reflux disease Laparoscopic fundoplication Impedance-pH monitoring Proton pump inhibitors
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重大疾病与疑难病证的中医药防治研究与重点任务——中医现代化临床研究(一) 被引量:6
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作者 中医现代化科技发展战略研究课题组 《世界科学技术-中药现代化》 2001年第6期25-27,80,共3页
众所周知,中医现代化临床研究的重点领域就是探索重大疾病、疑难病、情志病等的治疗理论、方法和药物的过程。本文是科技部、国家中医药管理局重大课题“中医现代化科技发展战略研究”内容之一。本课题提出了中医临床的研究目标、发展... 众所周知,中医现代化临床研究的重点领域就是探索重大疾病、疑难病、情志病等的治疗理论、方法和药物的过程。本文是科技部、国家中医药管理局重大课题“中医现代化科技发展战略研究”内容之一。本课题提出了中医临床的研究目标、发展思路及重点任务。 展开更多
关键词 中医现代化 重大疾病 疑难病证 临床研究 中医药防治
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Laser-induced Breakdown Spectroscopy as a Powerful Tool for Online Quality Control in The Refractory Industry
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作者 Alexander BARYSHNIKOV Yoni GROISMAN +3 位作者 Nir ELIEZER Micharl GAFT Lev AKSELROD Alexey SAVCHENKO 《China's Refractories》 CAS 2016年第1期32-38,共7页
Raw materials have a signcant influence on the qu.ality of the final refractory products, as the crude ore often comes for processing with significant variations in chemical and mineralogical composition. Therefore, i... Raw materials have a signcant influence on the qu.ality of the final refractory products, as the crude ore often comes for processing with significant variations in chemical and mineralogical composition. Therefore, it is necessary to guarantee the stable quality of raw materials with pre-assigned qualitative factors. It is possible to solve these problems by separating raw materials by grades, including the rejection of the portions of material unsuitable for specific application, and by reasonable control of the processing parameters based on real-time infirmation about chemical composition of raw materials. This can be effectively achieved by MAYA laser ele- mental analyzers based on LIBS. Being applied in ex traction, beneficiation and processing of the mineral raw materials, LIBS analyzers can be used for automatic sor ting " the ore extracted or crushed and automatic dosage of components to stabilize the composition of raw material mixtures. 展开更多
关键词 LIBS online elemental analysis refracto-ries MINERALS metals minerals beneficiation qualitycontrol
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Influence Researches of Fused Calcium Hexaluminate Amount on Metal Corrosion Resistance of Alumina Refractories
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作者 Vladimir V. PRIMACHENKO Valeriy V. MARTYNENKO +2 位作者 Irina G. SHULIK Lyudmila N. ZOLOTUKHINA Andrey B. KOVALYOV 《China's Refractories》 CAS 2016年第1期1-6,共6页
Calcium hexaluminate is one from such perspective materials. It is characterized by high refractoriness ( above 1 830 ~C ) , as well as properties stability in reducing atmosphere, high alkali- and slag-resistance... Calcium hexaluminate is one from such perspective materials. It is characterized by high refractoriness ( above 1 830 ~C ) , as well as properties stability in reducing atmosphere, high alkali- and slag-resistance, low thermal conductivity and wettability by molten metals. In this work influence researches of fused calcium hexaluminate material additive in amount of 5%, 15% amt 25% on the main properties of alumina refractories were carried out. It is established that, the refractories containing the additive of 25% calcium hexaluminate material are characterized by the highest properties, slightly impregnated with metal melt and the highest metal corrosion resistance. The alumina purging plugs fi)r blowing of metal with calcium hexaluminate material additive are produced and intended to one metallurgical plant of Ukraine for carrying out tests. 展开更多
关键词 calcium hexaluminate alumina refracto-ries metal resistance purging plugs
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Effect of ZnO on Oxidation Resistance of Low Carbon MgO-C Refractories
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作者 XIE Zhaohui CHEN Liugang +1 位作者 ZHAI Pengtao ZHANG Yang 《China's Refractories》 CAS 2014年第2期7-11,共5页
Al-containing low carbon MgO - C refractories were prepared using 70% (in mass, the same hereinafter) fused magnesia ( ≤3 mm), 24% fused magnesia powder ( 〈0. 074 mm) , 3% flake graphite, 3% Al powder and 4% p... Al-containing low carbon MgO - C refractories were prepared using 70% (in mass, the same hereinafter) fused magnesia ( ≤3 mm), 24% fused magnesia powder ( 〈0. 074 mm) , 3% flake graphite, 3% Al powder and 4% phenolic resin (extra-added) as the basic formulation. Influence of ZnO addhion on oxidation resistance of the materials was investigated by adding 1% ZnO to substitute fused magnesia powder. The relationship between in-situ formed spinel and ZnO in the matrix was discussed by comparing apparent porosity, cold crushing strength, and phase evolution of the materials matrix. The oxidation resistances of the two materials were compared by observing the formed dense MgO layer between the decarburized layer and the original layer. The result shows that adding ZnO in MgO - C refractories accelerates the in-situ formation of ZnAl204 spinel and the formation of dense MgO layer, thus improves the oxidation resistance of the low carbon MgO - C refractories. 展开更多
关键词 zinc oxide magnesia - carbon refracto-ries in-situ spinel oxidation resistance
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