After three-body abrasion, the hardness re-distribution near the worn surface has a close relationship with the carbon content of martensite steel. It is considered that there is a competition between the work-hardeni...After three-body abrasion, the hardness re-distribution near the worn surface has a close relationship with the carbon content of martensite steel. It is considered that there is a competition between the work-hardening and the temper softening, which results from deformation and friction heat of material. When the carbon content of martensite steel is below about 0.6%, the subsurface hardness distribution of material is a softened layer sandwiched between two hardened layers, but above 0.6%C, no softened region appears on the hardness re-distribution curve.展开更多
Re-Os法能够直接厘定内生金属矿床成矿时代,但是封闭Carius管法化学流程复杂,且有一定的危险性。本文建立了一种简便快速测定辉钼矿Re-Os年龄及其Re含量的方法。用3 m L浓硝酸在10 m L比色管中溶解5~15 mg辉钼矿样品,将溶液中的钼酸沉...Re-Os法能够直接厘定内生金属矿床成矿时代,但是封闭Carius管法化学流程复杂,且有一定的危险性。本文建立了一种简便快速测定辉钼矿Re-Os年龄及其Re含量的方法。用3 m L浓硝酸在10 m L比色管中溶解5~15 mg辉钼矿样品,将溶液中的钼酸沉淀分离后稀释定容,直接采用质谱测量187和185质量数比值（M187/M185）。利用辉钼矿Re-Os年龄标准物质JDC和HLP的M187/M185值与其年龄的正相关线性关系计算未知辉钼矿样品的Re-Os年龄,并通过185Re计数利用相对法计算Re含量。本方法应用于测量13.26~2130 Ma的辉钼矿,Re-Os年龄的测定值与推荐值的相对偏差多数在0.36%~7.42%之间,由于放射性积累较多,长年龄样品测量的准确度较高。与传统Carius管法相比,该方法不需要加入稀释剂,省去了封闭和打开Carius管环节以及Re-Os分离纯化流程,适合于辉钼矿Re-Os年龄的初步分析。展开更多
文摘After three-body abrasion, the hardness re-distribution near the worn surface has a close relationship with the carbon content of martensite steel. It is considered that there is a competition between the work-hardening and the temper softening, which results from deformation and friction heat of material. When the carbon content of martensite steel is below about 0.6%, the subsurface hardness distribution of material is a softened layer sandwiched between two hardened layers, but above 0.6%C, no softened region appears on the hardness re-distribution curve.
文摘Re-Os法能够直接厘定内生金属矿床成矿时代,但是封闭Carius管法化学流程复杂,且有一定的危险性。本文建立了一种简便快速测定辉钼矿Re-Os年龄及其Re含量的方法。用3 m L浓硝酸在10 m L比色管中溶解5~15 mg辉钼矿样品,将溶液中的钼酸沉淀分离后稀释定容,直接采用质谱测量187和185质量数比值（M187/M185）。利用辉钼矿Re-Os年龄标准物质JDC和HLP的M187/M185值与其年龄的正相关线性关系计算未知辉钼矿样品的Re-Os年龄,并通过185Re计数利用相对法计算Re含量。本方法应用于测量13.26~2130 Ma的辉钼矿,Re-Os年龄的测定值与推荐值的相对偏差多数在0.36%~7.42%之间,由于放射性积累较多,长年龄样品测量的准确度较高。与传统Carius管法相比,该方法不需要加入稀释剂,省去了封闭和打开Carius管环节以及Re-Os分离纯化流程,适合于辉钼矿Re-Os年龄的初步分析。
