Based on the results obtained from Pg wavefront imaging in active source deep seismic sounding, we propose a new ray hit analysis method for high-resolution seismic refraction profile data processing. This method can ...Based on the results obtained from Pg wavefront imaging in active source deep seismic sounding, we propose a new ray hit analysis method for high-resolution seismic refraction profile data processing. This method can be used to further determine possible refraction interface, especially spatial location of basement and its pattern characteristics in complex upper crustal structure region, making data processing for high-resolution refraction profiles more fine. We use this method to study the crystalline basement structure of east part of A＇nyemaqên suite zone at northeast side of Qinghai-Xizang Plateau and the basement patterns as well as its spreading features at the east part of Anemaqen suite zone and its adjacent region were determined.展开更多
We performed detailed time-resolved spectroscopy of bright tong gamma- ray bursts （GRBs） which show significant GeV emissions （GRB 080916C, GRB 090902B and GRB 090926A）. In addition to the standard Band model, we ...We performed detailed time-resolved spectroscopy of bright tong gamma- ray bursts （GRBs） which show significant GeV emissions （GRB 080916C, GRB 090902B and GRB 090926A）. In addition to the standard Band model, we also use a model consisting of a black body and a power law to fit the spectra. We find that for the latter model there are indications of an additional soft component in the spectra. While previous studies have shown that such models are required for GRB 090902B, here we find that a composite spectral model consisting of two blackbodies and a power law adequately fits the data of all the three bright GRBs. We investigate the evolution of the spectral parameters and find several interesting features that appear in all three GRBs, like （a） temperatures of the blackbodies are strongly correlated with each other, （b） fluxes in the black body components are strongly correlated with each other, （c） the temperatures of the black body trace the profile of the individual pulses of the GRBs, and （d） the characteristics of power law components like the spectral index and the delayed onset bear a close similarity to the emission characteristics in the GeV regions. We discuss the implications of these results and the possibility of identifying the radiation mechanisms during the prompt emission of GRBs.展开更多
An imported energy spectrum analyzer is powerful, but English operation interface is not easy to use. According to actual work needs, preliminary design of the Chinese energy spectrum analysis system is introduced in ...An imported energy spectrum analyzer is powerful, but English operation interface is not easy to use. According to actual work needs, preliminary design of the Chinese energy spectrum analysis system is introduced in the paper.展开更多
We investigate the relationship between the rise width and the full width of gamma-ray burst pulses. Theoretical analysis shows that either width is proportional to Г^-2△τθ,FWHMRc/c（Г the Lorentz factor of the b...We investigate the relationship between the rise width and the full width of gamma-ray burst pulses. Theoretical analysis shows that either width is proportional to Г^-2△τθ,FWHMRc/c（Г the Lorentz factor of the bulk motion, △τθ,FWHM a local pulse＇s width, Rc the radius of fireballs and c the velocity of light）. We study the relationship for four samples of observed pulses. We find： （1） merely the curvature effect could reproduce the relationship between the rise and full widths with the same slope as derived from the model of Qin et al.; （2） gamma-ray burst pulses, selected from both the short and long GRBs, follow the same sequence in the rise width vs. full width diagram, with the shorter pulses at one end; （3） all GRBs may intrinsically result from local Gaussian pulses. These features place constraints on the physical mechanism（s） for producing long and short GRBs.展开更多
New high performance grouts with high volume stability and good fluidity were prepared with Portland cement and a multifunctional admixture (MFA). The theological characteristics and mechanical performance of the grou...New high performance grouts with high volume stability and good fluidity were prepared with Portland cement and a multifunctional admixture (MFA). The theological characteristics and mechanical performance of the grouts were investigated. The addition of MFA effectively improves the pseudo-plasticity of the grout. The Ma cone flow time decreases obviously, and the bleeding rate tends to be zero. The deformation behaviors of fresh mixture and hardened grout are systematically studied. Mercury injection method (MIP), scanning electron microscopy (SEM) and X-ray diffractory analysis experiments are used to analyze the microstructure evolution of the grouts, which manifests that the co-action of the early bubble reaction and the latter ettringite crystallization ensure the volume stability throughout the whole hydration process and result in refined pore structure of the grout.展开更多
Have developed a Bi-Pb-Sr-Ca-Cu-O superconductor with an onset Tc of 108K and a zero resistance temperature Tco of 104K. There are at least five different phases: the high Tc and low Tc ones and three minor ones. The ...Have developed a Bi-Pb-Sr-Ca-Cu-O superconductor with an onset Tc of 108K and a zero resistance temperature Tco of 104K. There are at least five different phases: the high Tc and low Tc ones and three minor ones. The high Tc and low Tc phases have the face - centered orthorhombic structure with a = 0.540nm, b = 0.545nm, c = 3.669nm and a = 0.540nm b = 0.546nm, c = 3.077nm, respectively. The former has the superstructure of 3.24nm, and the latter has the superstructure of 2.7nm and is incommensurate in the b direction.展开更多
Splat foils with 30-35 μm thickness and spum ribbon with 50-55 μm thickness of Mo-4Th-0.4B and Mo-8Th-0.8B were made by arc melt hammer-anvil and melt spinning techniques. Both alloys have high hardness and a strong...Splat foils with 30-35 μm thickness and spum ribbon with 50-55 μm thickness of Mo-4Th-0.4B and Mo-8Th-0.8B were made by arc melt hammer-anvil and melt spinning techniques. Both alloys have high hardness and a strong age hardening response, especially Mo-8Th-0.8B. The precipitates associated with age hardening were ThB4(tetragon) and Mo2B (C16, BTC). The times for reaching a age hardening peak for both alloys are not the same and depended on the precipitation extent of Th and B solutes from the metastable solid solution. Grain refinement was observed. The work indicates that new high strength Mo alloys can be developed by rapid solidification.展开更多
Calcium hydroxytitanate formed in the Bayer digestion process of Chinese diasporic bauxite was studied. Interplanar spacings of calcium hydroxytitanate crystal were determined by XRD analysis. Only one endothermic pea...Calcium hydroxytitanate formed in the Bayer digestion process of Chinese diasporic bauxite was studied. Interplanar spacings of calcium hydroxytitanate crystal were determined by XRD analysis. Only one endothermic peak occurs at 550-560°C on the DTA curve. IR spectrometry has revealed that hydroxyl exists in calcium hydroxytitanate instead of crystal water. Observation under SEM has indicated that the crystal grains are in the shape of regular hexagonal plates 2-8 μm in edge length and less than 1 μm in thickness. The influences of various digestion conditions on the formation and transformation of calcium hydroxytitanate and other Ca-Ti-containing compounds such as lime addition, content and distribution state of TiO2 in bauxite, digestion temperature and retention time were studied.展开更多
This paper summarizes the new developments in the study of barium rare-earth fluor-carbonate mineral structures .The second order superstructure of cebaite -(Ce ) was solved by using high power X-ray single crystal di...This paper summarizes the new developments in the study of barium rare-earth fluor-carbonate mineral structures .The second order superstructure of cebaite -(Ce ) was solved by using high power X-ray single crystal diffractometer . Five kinds of coordination forms were found . All atoms in the cell , including C and F , were properly located . In the process of study in a cordylite-(Ce ), a new mineral was discovered , whose chemical formula is (Ca0.5□0.5) BaCe2 (CO3)4F . It is isostructural with baiyuneboite - (Ce ), but different in composition (Na in baiyuneboite- (Ce ) is substituted by Ca disorderly ) . On the basis of the studies a proposal to re-define cordylite-(Ce )as a mineral group name is put forth by the authors . Finally a new type of twinning of huanghoite-(Ce ) was found on the systematical absence of diffraction data by means of a single crystal diffractometer .展开更多
The forms and structures of the phases in Fe-Ni-Co-Nb-Ti-Si low expansion superal-loys have been studied using analytical electron microscopy, high resolution electron microscopy, chemical phase analysis, X-ray diffra...The forms and structures of the phases in Fe-Ni-Co-Nb-Ti-Si low expansion superal-loys have been studied using analytical electron microscopy, high resolution electron microscopy, chemical phase analysis, X-ray diffraction, etc. The effects of yttrium on the microstructures and properties in the superalloys have also been investigated. The results reveal that trace yttrium mainly located in the platelet precipitates makes the crystal structure changed. The platelet precipitates become smaller, denser and rather homogeneous with appropriate yttrium addition. Compared with the conventional low expansion superalloy, the misfit of the platelet phase with the matrix in the yttrium-containing low expansion superalloy decreases from 0.7% to 0.07%, which indicates very low stress at the interface.展开更多
Thin film methods and X ray energy dispersive technique were applied to analyze sulfate-containing particles inBeijing in order to examine their features and sources. Atmospheric aerosol particles were collected on el...Thin film methods and X ray energy dispersive technique were applied to analyze sulfate-containing particles inBeijing in order to examine their features and sources. Atmospheric aerosol particles were collected on electron microscope meshes according to two size ranges: coarse particles (r>0.5μm) and fine particles (0.5μm>r>0. 1μm) by using a two-stage impactor. It was found that more than seventy percent of the fine particles and about twenty percentof the coarse particles were sulfate-containing particles. These particles were formed mainly through heterogeneousnucleation. The element composition analyses revealed that the atmospheric aerosol particles in Beijing were domi-nated by crustal particles and construction dust.展开更多
An Al62.5Cu25Fe12.5 quasi-crystalline alloy was prepared by are melting. X-ray diffraction and scanning electron microscopy were used to study the microstructure of the quasi-crystalline alloy. Isothermal weight gain ...An Al62.5Cu25Fe12.5 quasi-crystalline alloy was prepared by are melting. X-ray diffraction and scanning electron microscopy were used to study the microstructure of the quasi-crystalline alloy. Isothermal weight gain of the Al-Cu-Fe quasi-crystal at elevated temperature in dry air was measured by means of a thermal balance and the oxidation behavior was evaluated by oxidation kinetic curves, from which it was deduced that the quasi-crystal exhibits good oxidation resistance. The surface morphologies of the Al-Cu-Fe quasi-crystal after isothermal oxidation at 700°C and 800°C for different times were observed. The oxidation resistance of quasi-crystalline powder and normal crystalline powder in the Al-Cu-Fe system was also quantitatively compared in quantity.展开更多
Indium oxide(In_2O_3) films were prepared on Al_2O_3(0001) substrates at 700 °C by metal-organic chemical vapor deposition(MOCVD).Then the samples were annealed at 800 °C,900 °C and 1 000 °C,respec...Indium oxide(In_2O_3) films were prepared on Al_2O_3(0001) substrates at 700 °C by metal-organic chemical vapor deposition(MOCVD).Then the samples were annealed at 800 °C,900 °C and 1 000 °C,respectively.The X-ray diffraction(XRD) analysis reveals that the samples were polycrystalline films before and after annealing treatment.Triangle or quadrangle grains can be observed,and the corner angle of the grains becomes smooth after annealing.The highest Hall mobility is obtained for the sample annealed at 900 °C with the value about 24.74 cm^2·V^(-1)·s^(-1).The average transmittance for the films in the visible range is over 90%.The optical band gaps of the samples are about 3.73 e V,3.71 e V,3.70 eV and 3.69 eV corresponding to the In_2O_3 films deposited at 700 °C and annealed at 800 °C,900 °C and 1 000 °C,respectively.展开更多
By citrate sol-gel auto-combustion method,the nanophase M-type planar hexagonal ferrite is prepared.The transmission electron microscopy(TEM),X-ray diffraction(XRD) and thermal analysis are used to study the grain siz...By citrate sol-gel auto-combustion method,the nanophase M-type planar hexagonal ferrite is prepared.The transmission electron microscopy(TEM),X-ray diffraction(XRD) and thermal analysis are used to study the grain size,phase composition,microstructure and crystallization process.The results show that the nanophase M-type Sr-ferrite prepared by this method is single,and its grain size is smaller than 100 nm.Moreover,most of the grains present hexagonal sheet shape.Tests are carried out for its attenuation to 1.06 mm laser.It is found that the extinction capability of the nanophase M-type Sr-ferrite smoke is good,and its mass extinction coefficient is 1.628 m2/g.展开更多
The seismic data obtained from high resolution seismic refraction profile in Jiashi strong earthquake swarm area in Xinjiang, China were further processed with ray hit analysis method and more complete basement interf...The seismic data obtained from high resolution seismic refraction profile in Jiashi strong earthquake swarm area in Xinjiang, China were further processed with ray hit analysis method and more complete basement interface structural characteristics beneath Jiashi strong earthquake swarm area were determined. The results show that there are two clear basement interfaces at the upper crust in Jiashi strong earthquake swarm area. The first one with buried depth ranging from 2.6 km to 3.3 km presents integral and continuous structure, and it appears an inclined plane interface and smoothly rises up toward Tianshan Mountain. The second basement interface with buried depth from 8.5 km to 11.8 km, is the antiquated crystalline basement of Tarim basin. Near the post number of 37 km, the buried depth of the crystalline basement changed abruptly by 2.5 km, which maybe result from an ultra crystalline basement fault. If taking this fault as a boundary, the crystalline basement could be divided into two parts, i.e. the southwestern segment with buried depth about 11.5 km, and the northeastern segment with buried depth approxi-mately from 8.5 km to 9.0 km. That is to say, in each segment, the buried depth changes not too much. The northeast segment rises up as a whole and upheaves slightly from southwest to northeast, which reflects the upper crustal deformation characteristics under the special tectonic background at the northwestern edge of Tarim basin.展开更多
ZnSe multipod-based structures,including tetrapod-like microrods,long microwires,and short nanorods,are selectively prepared by atmospheric pressure thermal evaporation of ZnSe nanoparticles without using any catalyst...ZnSe multipod-based structures,including tetrapod-like microrods,long microwires,and short nanorods,are selectively prepared by atmospheric pressure thermal evaporation of ZnSe nanoparticles without using any catalyst.The morphologies could be well controlled by simply adjusting the deposition position.The phase structures,morphologies,and optical properties of the products are investigated by X-ray diffraction(XRD),scanning electron microscopy(SEM),high-resolution transmission electron microscopy(TEM),and photoluminescence(PL) spectroscopy.A vapor-liquid mechanism is proposed for the formation of ZnSe multipod-based structures.The presented route is expected to be applied to the synthesis of other Ⅱ-Ⅵ groups or other group's semiconductor materials with controllable morphologies.展开更多
A new high spectral resolution crystal spectrometer is designed to measure very low emissive X-ray spectra of laser-produced plasma in 0.5-0.9 nm range. A large open aperture （30 ×20 （mm）） mica （002） spheri...A new high spectral resolution crystal spectrometer is designed to measure very low emissive X-ray spectra of laser-produced plasma in 0.5-0.9 nm range. A large open aperture （30 ×20 （mm）） mica （002） spherically bent crystal with curvature radius R = 380 mm is used as dispersive and focusing element. The imaging plate is employed to obtain high spectral resolution with effective area of 30 × 80 （mm）. The long designed path of the X-ray spectrometer beam is 980 mm from the source to the detector via the crystal. Experiment is carried out at a 20-J laser facility. X-ray spectra in an absolute intensity scale is obtained from Al laserproduced plasmas created by laser energy of 6.78 J. Samples of spectra obtained with spectral resolution of up to E/△E - 1500 are presented. The results clearly show that the device is good to diagnose laser high-density plasmas.展开更多
A Princeton Instruments PI-LCX 1300 charge-coupled device （CCD） camera used for X-ray spectrum measurements in laser-plasma experiments is calibrated using three radioactive sources and investigated with the Monte C...A Princeton Instruments PI-LCX 1300 charge-coupled device （CCD） camera used for X-ray spectrum measurements in laser-plasma experiments is calibrated using three radioactive sources and investigated with the Monte Carlo code Geant4. The exposure level is controlled to make the CCD work in single photon counting mode. A summation algorithm for obtaining accurate X-ray spectra is developed to reconstruct the X-ray spectra, and the results show that the developed algorithm effectively reduces the low-energy tail caused by split pixel events. The obtained CCD energy response shows good linearity. The detection efficiency curves from both Monte Carlo simulations and the manufacturer agree well with the experimental results. This consistency demonstrates that event losses in charge collection processes are negligible when the developed summation algorithm of sDlit Dixel events is emDloved.展开更多
基金National Natural Science Foundation of China (40334040) and Joint Seismological Science Foundation of China (106076)
文摘Based on the results obtained from Pg wavefront imaging in active source deep seismic sounding, we propose a new ray hit analysis method for high-resolution seismic refraction profile data processing. This method can be used to further determine possible refraction interface, especially spatial location of basement and its pattern characteristics in complex upper crustal structure region, making data processing for high-resolution refraction profiles more fine. We use this method to study the crystalline basement structure of east part of A＇nyemaqên suite zone at northeast side of Qinghai-Xizang Plateau and the basement patterns as well as its spreading features at the east part of Anemaqen suite zone and its adjacent region were determined.
文摘We performed detailed time-resolved spectroscopy of bright tong gamma- ray bursts （GRBs） which show significant GeV emissions （GRB 080916C, GRB 090902B and GRB 090926A）. In addition to the standard Band model, we also use a model consisting of a black body and a power law to fit the spectra. We find that for the latter model there are indications of an additional soft component in the spectra. While previous studies have shown that such models are required for GRB 090902B, here we find that a composite spectral model consisting of two blackbodies and a power law adequately fits the data of all the three bright GRBs. We investigate the evolution of the spectral parameters and find several interesting features that appear in all three GRBs, like （a） temperatures of the blackbodies are strongly correlated with each other, （b） fluxes in the black body components are strongly correlated with each other, （c） the temperatures of the black body trace the profile of the individual pulses of the GRBs, and （d） the characteristics of power law components like the spectral index and the delayed onset bear a close similarity to the emission characteristics in the GeV regions. We discuss the implications of these results and the possibility of identifying the radiation mechanisms during the prompt emission of GRBs.
文摘An imported energy spectrum analyzer is powerful, but English operation interface is not easy to use. According to actual work needs, preliminary design of the Chinese energy spectrum analysis system is introduced in the paper.
基金Supported by the National Natural Science Foundation of China
文摘We investigate the relationship between the rise width and the full width of gamma-ray burst pulses. Theoretical analysis shows that either width is proportional to Г^-2△τθ,FWHMRc/c（Г the Lorentz factor of the bulk motion, △τθ,FWHM a local pulse＇s width, Rc the radius of fireballs and c the velocity of light）. We study the relationship for four samples of observed pulses. We find： （1） merely the curvature effect could reproduce the relationship between the rise and full widths with the same slope as derived from the model of Qin et al.; （2） gamma-ray burst pulses, selected from both the short and long GRBs, follow the same sequence in the rise width vs. full width diagram, with the shorter pulses at one end; （3） all GRBs may intrinsically result from local Gaussian pulses. These features place constraints on the physical mechanism（s） for producing long and short GRBs.
文摘New high performance grouts with high volume stability and good fluidity were prepared with Portland cement and a multifunctional admixture (MFA). The theological characteristics and mechanical performance of the grouts were investigated. The addition of MFA effectively improves the pseudo-plasticity of the grout. The Ma cone flow time decreases obviously, and the bleeding rate tends to be zero. The deformation behaviors of fresh mixture and hardened grout are systematically studied. Mercury injection method (MIP), scanning electron microscopy (SEM) and X-ray diffractory analysis experiments are used to analyze the microstructure evolution of the grouts, which manifests that the co-action of the early bubble reaction and the latter ettringite crystallization ensure the volume stability throughout the whole hydration process and result in refined pore structure of the grout.
文摘Have developed a Bi-Pb-Sr-Ca-Cu-O superconductor with an onset Tc of 108K and a zero resistance temperature Tco of 104K. There are at least five different phases: the high Tc and low Tc ones and three minor ones. The high Tc and low Tc phases have the face - centered orthorhombic structure with a = 0.540nm, b = 0.545nm, c = 3.669nm and a = 0.540nm b = 0.546nm, c = 3.077nm, respectively. The former has the superstructure of 3.24nm, and the latter has the superstructure of 2.7nm and is incommensurate in the b direction.
文摘Splat foils with 30-35 μm thickness and spum ribbon with 50-55 μm thickness of Mo-4Th-0.4B and Mo-8Th-0.8B were made by arc melt hammer-anvil and melt spinning techniques. Both alloys have high hardness and a strong age hardening response, especially Mo-8Th-0.8B. The precipitates associated with age hardening were ThB4(tetragon) and Mo2B (C16, BTC). The times for reaching a age hardening peak for both alloys are not the same and depended on the precipitation extent of Th and B solutes from the metastable solid solution. Grain refinement was observed. The work indicates that new high strength Mo alloys can be developed by rapid solidification.
文摘Calcium hydroxytitanate formed in the Bayer digestion process of Chinese diasporic bauxite was studied. Interplanar spacings of calcium hydroxytitanate crystal were determined by XRD analysis. Only one endothermic peak occurs at 550-560°C on the DTA curve. IR spectrometry has revealed that hydroxyl exists in calcium hydroxytitanate instead of crystal water. Observation under SEM has indicated that the crystal grains are in the shape of regular hexagonal plates 2-8 μm in edge length and less than 1 μm in thickness. The influences of various digestion conditions on the formation and transformation of calcium hydroxytitanate and other Ca-Ti-containing compounds such as lime addition, content and distribution state of TiO2 in bauxite, digestion temperature and retention time were studied.
文摘This paper summarizes the new developments in the study of barium rare-earth fluor-carbonate mineral structures .The second order superstructure of cebaite -(Ce ) was solved by using high power X-ray single crystal diffractometer . Five kinds of coordination forms were found . All atoms in the cell , including C and F , were properly located . In the process of study in a cordylite-(Ce ), a new mineral was discovered , whose chemical formula is (Ca0.5□0.5) BaCe2 (CO3)4F . It is isostructural with baiyuneboite - (Ce ), but different in composition (Na in baiyuneboite- (Ce ) is substituted by Ca disorderly ) . On the basis of the studies a proposal to re-define cordylite-(Ce )as a mineral group name is put forth by the authors . Finally a new type of twinning of huanghoite-(Ce ) was found on the systematical absence of diffraction data by means of a single crystal diffractometer .
基金financially supported by the Project of the Science and Technology Creative Team of Universities in Jiangxi Province,China(No.00008713)the Open Foundation of Jiangxi Key Laboratory for Advanced Copper and Tungsten Materials(No.2013-KLP-04)
基金Chinese foundation of aeronautical science( N o.96 G2 10 0 3)
文摘The forms and structures of the phases in Fe-Ni-Co-Nb-Ti-Si low expansion superal-loys have been studied using analytical electron microscopy, high resolution electron microscopy, chemical phase analysis, X-ray diffraction, etc. The effects of yttrium on the microstructures and properties in the superalloys have also been investigated. The results reveal that trace yttrium mainly located in the platelet precipitates makes the crystal structure changed. The platelet precipitates become smaller, denser and rather homogeneous with appropriate yttrium addition. Compared with the conventional low expansion superalloy, the misfit of the platelet phase with the matrix in the yttrium-containing low expansion superalloy decreases from 0.7% to 0.07%, which indicates very low stress at the interface.
文摘Thin film methods and X ray energy dispersive technique were applied to analyze sulfate-containing particles inBeijing in order to examine their features and sources. Atmospheric aerosol particles were collected on electron microscope meshes according to two size ranges: coarse particles (r>0.5μm) and fine particles (0.5μm>r>0. 1μm) by using a two-stage impactor. It was found that more than seventy percent of the fine particles and about twenty percentof the coarse particles were sulfate-containing particles. These particles were formed mainly through heterogeneousnucleation. The element composition analyses revealed that the atmospheric aerosol particles in Beijing were domi-nated by crustal particles and construction dust.
基金financially supported by the High-Tech Research and Development Program of China(No.SS2013AA031305)the Key Technologies R&D Program of Tianjin(No.12ZCDGGX49100)
文摘An Al62.5Cu25Fe12.5 quasi-crystalline alloy was prepared by are melting. X-ray diffraction and scanning electron microscopy were used to study the microstructure of the quasi-crystalline alloy. Isothermal weight gain of the Al-Cu-Fe quasi-crystal at elevated temperature in dry air was measured by means of a thermal balance and the oxidation behavior was evaluated by oxidation kinetic curves, from which it was deduced that the quasi-crystal exhibits good oxidation resistance. The surface morphologies of the Al-Cu-Fe quasi-crystal after isothermal oxidation at 700°C and 800°C for different times were observed. The oxidation resistance of quasi-crystalline powder and normal crystalline powder in the Al-Cu-Fe system was also quantitatively compared in quantity.
基金supported by the National Natural Science Foundation of China(Nos.6127411311204212 and 61404091)+5 种基金the Program for New Century Excellent Talents in University(No.NCET-11-1064)the Tianjin Natural Science Foundation(Nos.13JCYBJC1570013JCZDJC2610014JCZDJC31500 and 14JCQNJC00800)the Tianjin Science and Technology Developmental Funds of Universities and Colleges(Nos.2010070320130701 and 20130702)
文摘Indium oxide(In_2O_3) films were prepared on Al_2O_3(0001) substrates at 700 °C by metal-organic chemical vapor deposition(MOCVD).Then the samples were annealed at 800 °C,900 °C and 1 000 °C,respectively.The X-ray diffraction(XRD) analysis reveals that the samples were polycrystalline films before and after annealing treatment.Triangle or quadrangle grains can be observed,and the corner angle of the grains becomes smooth after annealing.The highest Hall mobility is obtained for the sample annealed at 900 °C with the value about 24.74 cm^2·V^(-1)·s^(-1).The average transmittance for the films in the visible range is over 90%.The optical band gaps of the samples are about 3.73 e V,3.71 e V,3.70 eV and 3.69 eV corresponding to the In_2O_3 films deposited at 700 °C and annealed at 800 °C,900 °C and 1 000 °C,respectively.
文摘By citrate sol-gel auto-combustion method,the nanophase M-type planar hexagonal ferrite is prepared.The transmission electron microscopy(TEM),X-ray diffraction(XRD) and thermal analysis are used to study the grain size,phase composition,microstructure and crystallization process.The results show that the nanophase M-type Sr-ferrite prepared by this method is single,and its grain size is smaller than 100 nm.Moreover,most of the grains present hexagonal sheet shape.Tests are carried out for its attenuation to 1.06 mm laser.It is found that the extinction capability of the nanophase M-type Sr-ferrite smoke is good,and its mass extinction coefficient is 1.628 m2/g.
基金Foundation item: Joint Seismological Foundation of China (106076)National Natural Science Foundation of China (40474049, 40334040).
文摘The seismic data obtained from high resolution seismic refraction profile in Jiashi strong earthquake swarm area in Xinjiang, China were further processed with ray hit analysis method and more complete basement interface structural characteristics beneath Jiashi strong earthquake swarm area were determined. The results show that there are two clear basement interfaces at the upper crust in Jiashi strong earthquake swarm area. The first one with buried depth ranging from 2.6 km to 3.3 km presents integral and continuous structure, and it appears an inclined plane interface and smoothly rises up toward Tianshan Mountain. The second basement interface with buried depth from 8.5 km to 11.8 km, is the antiquated crystalline basement of Tarim basin. Near the post number of 37 km, the buried depth of the crystalline basement changed abruptly by 2.5 km, which maybe result from an ultra crystalline basement fault. If taking this fault as a boundary, the crystalline basement could be divided into two parts, i.e. the southwestern segment with buried depth about 11.5 km, and the northeastern segment with buried depth approxi-mately from 8.5 km to 9.0 km. That is to say, in each segment, the buried depth changes not too much. The northeast segment rises up as a whole and upheaves slightly from southwest to northeast, which reflects the upper crustal deformation characteristics under the special tectonic background at the northwestern edge of Tarim basin.
文摘ZnSe multipod-based structures,including tetrapod-like microrods,long microwires,and short nanorods,are selectively prepared by atmospheric pressure thermal evaporation of ZnSe nanoparticles without using any catalyst.The morphologies could be well controlled by simply adjusting the deposition position.The phase structures,morphologies,and optical properties of the products are investigated by X-ray diffraction(XRD),scanning electron microscopy(SEM),high-resolution transmission electron microscopy(TEM),and photoluminescence(PL) spectroscopy.A vapor-liquid mechanism is proposed for the formation of ZnSe multipod-based structures.The presented route is expected to be applied to the synthesis of other Ⅱ-Ⅵ groups or other group's semiconductor materials with controllable morphologies.
基金supported by the National Natural Science Foundation of China under Grant No.10576041
文摘A new high spectral resolution crystal spectrometer is designed to measure very low emissive X-ray spectra of laser-produced plasma in 0.5-0.9 nm range. A large open aperture （30 ×20 （mm）） mica （002） spherically bent crystal with curvature radius R = 380 mm is used as dispersive and focusing element. The imaging plate is employed to obtain high spectral resolution with effective area of 30 × 80 （mm）. The long designed path of the X-ray spectrometer beam is 980 mm from the source to the detector via the crystal. Experiment is carried out at a 20-J laser facility. X-ray spectra in an absolute intensity scale is obtained from Al laserproduced plasmas created by laser energy of 6.78 J. Samples of spectra obtained with spectral resolution of up to E/△E - 1500 are presented. The results clearly show that the device is good to diagnose laser high-density plasmas.
基金supported by the National Natural Science Foundation of China(Nos.10975121,10905051,10902051,and 11174259)the Foundation of CAEP(Nos.2009A0102003 and 2011B0102021)the Foundation of Science and Technology on Plasma Physics Laboratory(No.9140C6802041004)
文摘A Princeton Instruments PI-LCX 1300 charge-coupled device （CCD） camera used for X-ray spectrum measurements in laser-plasma experiments is calibrated using three radioactive sources and investigated with the Monte Carlo code Geant4. The exposure level is controlled to make the CCD work in single photon counting mode. A summation algorithm for obtaining accurate X-ray spectra is developed to reconstruct the X-ray spectra, and the results show that the developed algorithm effectively reduces the low-energy tail caused by split pixel events. The obtained CCD energy response shows good linearity. The detection efficiency curves from both Monte Carlo simulations and the manufacturer agree well with the experimental results. This consistency demonstrates that event losses in charge collection processes are negligible when the developed summation algorithm of sDlit Dixel events is emDloved.
