This study proposes a class of augmented subspace schemes for the weak Galerkin(WG)finite element method used to solve eigenvalue problems.The augmented subspace is built with the conforming linear finite element spac...This study proposes a class of augmented subspace schemes for the weak Galerkin(WG)finite element method used to solve eigenvalue problems.The augmented subspace is built with the conforming linear finite element space defined on the coarse mesh and the eigen-function approximations in the WG finite element space defined on the fine mesh.Based on this augmented subspace,solving the eigenvalue problem in the fine WG finite element space can be reduced to the solution of the linear boundary value problem in the same WG finite element space and a low dimensional eigenvalue problem in the augmented sub-space.The proposed augmented subspace techniques have the second order convergence rate with respect to the coarse mesh size,as demonstrated by the accompanying error esti-mates.Finally,a few numerical examples are provided to validate the proposed numerical techniques.展开更多
The existing researches of the evaluation method of ride comfort of vehicle mainly focus on the level of human feelings to vibration. The level of human feelings to vibration is influenced by many factors, however, th...The existing researches of the evaluation method of ride comfort of vehicle mainly focus on the level of human feelings to vibration. The level of human feelings to vibration is influenced by many factors, however, the ride comfort according to the common principle of probability and statistics and simple binary logic is tmable to reflect these uncertainties. The random fuzzy evaluation model from people subjective response to vibration is adopted in the paper, these uncertainties are analyzed from the angle of psychological physics. Discussing the traditional evaluation of ride comfort during vehicle vibration, a fuzzily random evaluation model on the basis of annoyance rate is proposed for the human body＇s subjective response to vibration, with relevant fuzzy membership function and probability distribution given. A half-car four degrees of freedom suspension vibration model is described, subject to irregular excitations from the road surface, with the aid of software Matlab/Simulink. A new kind of evaluation method for ride comfort of vehicles is proposed in the paper, i.e., the annoyance rate evaluation method. The genetic algorithm and neural network control theory are used to control the system. Simulation results are obtained, such as the comparison of comfort reaction to vibration environments between before and after control, relationship of annoyance rate to vibration frequency and weighted acceleration, based on ISO 2631 / 1 （1982）, ISO 2631-1 （1997） and annoyance rate evaluation method, respectively. Simulated assessment results indicate that the proposed active suspension systems prove to be effective in the vibration isolation of the suspension system, and the subjective response of human being can be promoted from very uncomfortable to a little uncomfortable. Furthermore, the novel evaluation method based on annoyance rate can further estimate quantitatively the number of passengers who feel discomfort due to vibration. A new analysis method of vehicle comfort is presented.展开更多
Monodisperse spherical SiO2 particles were successfully synthesized in 2-propanol-H2O-NH3 system by the microwave hydrothermal method using ammonia as catalyst. To investigate the influences on the size of spherical S...Monodisperse spherical SiO2 particles were successfully synthesized in 2-propanol-H2O-NH3 system by the microwave hydrothermal method using ammonia as catalyst. To investigate the influences on the size of spherical SiO2 particles, factors such as ammonia concentration, reaction temperature, stirring intensity and reactants mol ratio have been studied. The orthogonal experiments were carried out. The as-prepared SiO2 particles were characterized by X-ray diffraction （XRD）, transmission electron microscopy （TEM）, Fourier transform infrared spectroscopy （FTIR） and differential thermal analysis （DTA）. The results indicated that the size of SiO2 particles increased greatly with the increase in ammonia concentration, temperature and reactants mol ratio, but increased slightly with the increase in stirring intensity. Monodisperse spherical Si02 particles were amorphous with perfect sphere and uniform size. Hydroxyl was detected in SiO2. Kinetic parameters were calculated, and finally the reaction rate equation of dehydrated hydroxyl was obtained.展开更多
A new electrical method of conductive carbon-film(with waterproof and anticorrosion ability)was proposed to continuously measure crack propagation rate of brittle rock under THMC coupling condition.A self-designed cou...A new electrical method of conductive carbon-film(with waterproof and anticorrosion ability)was proposed to continuously measure crack propagation rate of brittle rock under THMC coupling condition.A self-designed coupling testing system was used to conduct THMC coupling fracture tests of the pre-cracked red sandstone specimens(where the temperature is only changed)by this new electrical method of conductive carbon-film.Calculation results obtained by the energy method coincide well with the test results.And the higher the temperature is,the earlier the crack is initiated and the larger the crack propagation rate and accelerated velocity are,which can prove the validity of the new electrical method.This new electrical method has advantages of continuously measuring crack propagation rate over the conventional electrical,optical and acoustic methods,and can provide important basis for safety assessment and cracking-arrest design of deep rock mass engineering.展开更多
This paper presents anew regularization method for solving operator equations of the first kind; the convergence rate of the regularized solution is improved, as compared with the ordinary Tikhonov regularization.
An accelerator storage ring needs clean ultrahigh vacuum.A TiZrV non-evaporable getter(NEG) film deposited on interior walls of the chamber can realize distributed pumping,effective vacuum improvement and reduced long...An accelerator storage ring needs clean ultrahigh vacuum.A TiZrV non-evaporable getter(NEG) film deposited on interior walls of the chamber can realize distributed pumping,effective vacuum improvement and reduced longitudinal pressure gradient.But accumulation of pollutants such as N_2 and O_2 will decrease the adsorption ability of the NEG,leading to a reduction of NEG lifetime.Therefore,an NEG thin film coated with a layer of Pd,which has high diffusion rate and absorption ability for H_2,can extend the service life of NEG and improve the pumping rate of H_2 as well.In this paper,with argon as discharge gas,a magnetron sputtering method is adopted to prepare TiZrV-Pd films in a long straight pipe.By SEM measurement,deposition rates of TiZrV-Pd films are analyzed under different deposition parameters,such as magnetic field strength,gas flow rate,discharge current,discharge voltage and working pressure.By comparing the experimental results with the simulation results based on Sigmund's theory,the Pd deposition rate C can be estimated by the sputtered depth.展开更多
[Objectives ] The paper was to explore enzyme inhibition rate method for rapid detection of organophosphorus and carbamate pesticides in cowpea. [ Methods ] Acetylcholinesterase （ACHE） was added to cowpea extract, t...[Objectives ] The paper was to explore enzyme inhibition rate method for rapid detection of organophosphorus and carbamate pesticides in cowpea. [ Methods ] Acetylcholinesterase （ACHE） was added to cowpea extract, to determine the inhibition rate of extract against enzyme. The influences of different sampiing methods and sampling parts on detection results were compared. [ Results] The positive rate of standard sampling was 18.18% higher than that of non-stand- ard sampling, and the positive rate of samples collected from cowpea tail was 16.67% higher than that collected from other parts. [ Condmions] Enzyme inhibi- tion rate method is suitable for rapid detection of organophosphorus and carbamate pesticides in cowpea.展开更多
The castings defects are affected by the melting volume change rate of material.The change rate has an important effect on running safety of the high temperature thermal storage chamber,too.But the characteristics of ...The castings defects are affected by the melting volume change rate of material.The change rate has an important effect on running safety of the high temperature thermal storage chamber,too.But the characteristics of existing measuring installations are complex structure,troublesome operation and low precision.In order to measure the melting volume change rate of material accurately and conveniently,a self-designed measuring instrument,self-heating probe instrument,and measuring method are described.Temperature in heating cavity is controlled by PID temperature controller;melting volume change rateυand molten density are calculated based on the melt volume which is measured by the instrument.Positive and negativeυrepresent expansion and shrinkage of the sample volume after melting,respectively.Taking eutectic LiF+CaF2 for example,its melting volume change rate and melting density at 1123 K are-20.6%and 2651 kg/m–3 measured by this instrument,which is only 0.71%smaller than literature value.Density and melting volume change rate of industry pure aluminum at 973 K and analysis pure NaCl at 1123 K are detected by the instrument too.The measure results are agreed with report values.Measuring error sources are analyzed and several improving measures are proposed.In theory,the measuring errors of the change rate and molten density which are measured by the self-designed instrument is nearly 1/20-1/50 of that measured by the refitted mandril thermal expansion instrument.The self-designed instrument and method have the advantages of simple structure,being easy to operate,extensive applicability for material,relatively high accuracy,and most importantly,temperature and sample vapor pressure have little effect on the measurement accuracy.The presented instrument and method solve the problems of complicated structure and procedures,and large measuring errors for the samples with high vapor pressure by existing installations.展开更多
Fatigue crack propagation characteristics of a diesel engine crankshaft are studied by measuring the fatigue crack growth rate using a frequency sweep method on a resonant fatigue test rig. Based on the phenomenon tha...Fatigue crack propagation characteristics of a diesel engine crankshaft are studied by measuring the fatigue crack growth rate using a frequency sweep method on a resonant fatigue test rig. Based on the phenomenon that the system frequency will change when the crack becomes large, this method can be directly applied to a complex component or structure. Finite element analyses （FEAs） are performed to calibrate the relation between the frequency change and the crack size, and to obtain the natural frequency of the test rig and the stress intensity factor （SIF） of growing cracks. The crack growth rate i.e. da/dN-AK of each crack size is obtained by combining the testing-time monitored data and FEA results. The results show that the crack growth rate of engine crankshaft, which is a component with complex geometry and special surface treatment, is quite different from that of a pure material. There is an apparent turning point in the Paris＇s crack partition. The cause of the fatigue crack growth is also discussed.展开更多
Ce^(3+)as the active site on the CeO_(2)abrasive surface is the key to enhancing the material removal rate(MRR).The CeO_(2)abrasives with high chemical activity were prepared by the molten salt method under a reducing...Ce^(3+)as the active site on the CeO_(2)abrasive surface is the key to enhancing the material removal rate(MRR).The CeO_(2)abrasives with high chemical activity were prepared by the molten salt method under a reducing atmosphere.The crystal structure and morphology of CeO_(2)abrasive s were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM),Fourier transform infrared spectroscopy(FT-IR),ultraviolet—visible diffuse reflectance spectroscopy(UV-Vis DRS),and X-ray photoelectron spectroscopy(XPS).The CeO_(2)abrasives were obtained under different atmospheres(Air,Ar,and Ar/H_(2)).With the enhancement of the reducing atmosphere,the morphology of the abrasives transforms from spherical to octahedral,while more oxygen vacancies and Ce^(3+)are generated on the surface of CeO_(2)abrasives.The CMP experiments show that the MRRs of the CeO_(2)-Air,CeO_(2)-Ar,and CeO_(2)-Ar/H_(2)abrasives on SiO_(2)substrates are 337.60,578.74,and 691.28 nm/min,respectively.Moreover,as confirmed by atomic force microscopy(AFM),the substrate surfaces exhibit low roughness(20.5 nm)after being polished using all of the prepared samples.Especially,the MRR of CeO_(2)-Ar/H_(2)abrasives is increased by 104.76%compared with CeO_(2)-air abrasives.The improved CMP performance is attributed to the increased Ce^(3+)concentration and the octahedral morphology of the abrasives enhancing the chemical reaction and mechanical removal at the abrasive-substrate interface.展开更多
The aim of this study is to evaluate the uncertainty of 2πα and 2πβ surface emission rates using the windowless multiwire proportional counter method.This study used the Monte Carlo method (MCM) to validate the co...The aim of this study is to evaluate the uncertainty of 2πα and 2πβ surface emission rates using the windowless multiwire proportional counter method.This study used the Monte Carlo method (MCM) to validate the conventional Guide to the Expression of Uncertainty in Measurement (GUM) method.A dead time measurement model for the two-source method was established based on the characteristics of a single-channel measurement system,and the voltage threshold correction factor measurement function was indirectly obtained by fitting the threshold correction curve.The uncertainty in the surface emission rate was calculated using the GUM method and the law of propagation of uncertainty.The MCM provided clear definitions for each input quantity and its uncertainty distribution,and the simulation training was realized with a complete and complex mathematical model.The results of the surface emission rate uncertainty evaluation for four radioactive plane sources using both methods showed the uncertainty’s consistency E_(n)<0.070 for the comparison of each source,and the uncertainty results of the GUM were all lower than those of the MCM.However,the MCM has a more objective evaluation process and can serve as a validation tool for GUM results.展开更多
Radar interferograms are usually influenced by factors such as atmospheric artifacts,orbital errors,and terrain errors.It is difficult to reduce the influence by using the conventional small baseline subset(SBAS)metho...Radar interferograms are usually influenced by factors such as atmospheric artifacts,orbital errors,and terrain errors.It is difficult to reduce the influence by using the conventional small baseline subset(SBAS)method when determining the deformation rate.This study uses the adjustment model with systematic parameters to improve the conventional SBAS method and employs it to determine the interseismic deformation rate of the Haiyuan fault system,providing a data reference for exploring the locking depth,strain accumulation state,and potential seismic risk assessment of different segments of the Haiyuan fault system.The results are as follows:(1)the simulation experiment verifies the feasibility and robustness of the modified SBAS method.This method can effectively reduce the influence of residual signals such as atmospheric artifacts,orbital errors and terrain errors in the interferograms.The deformation rate map can be significantly improved;(2)the deformation rate field in the radar’s Line of Sight(LOS)direction shows that there are obvious differences between the north and south sides of Haiyuan fault system,which is consistent with the characteristics of the left-lateral strike-slip movement of the Haiyuan fault system.The deformation rate field and profiles reflect the complex trends among different segments of Haiyuan fault system in detail.(3)the deformation rate of the Jingtai pull-apart basin is higher than that of the surrounding areas,possibly indicating strong regional activity,which provides a reference for studying the seismic risk of the Jingtai pull-apart basin;and(4)the interseismic deformation rate and profiles across the fault show that the middle section of the Lao Hu Shan(LHS)segment and the western and middle sections of the Haiyuan segment are locked.展开更多
The interfacial oxygen transfer rate is one of the main factors to control the composition of alloys.The commonly employed method of studying the interfacial oxygen transfer rate is the chemical composition analysis;h...The interfacial oxygen transfer rate is one of the main factors to control the composition of alloys.The commonly employed method of studying the interfacial oxygen transfer rate is the chemical composition analysis;however,it is difficult to be studied in situ.Here,a new method of measuring the oxygen transfer rate at the gas-slag and slag-metal interfaces was reported based on electrochemical analyses.The interfacial oxygen transfer rate in the smelting process of Inconel 718 superalloy was investigated at 1723,1773,1823,and 1873 K.The experimental results show that the electrochemical method can measure the real-time oxygen content;hence,this method is promising in controlling the oxygen content in alloys.As the temperature increased,both the equilibrium oxygen content and the rate of oxygen absorption increased significantly,and the increase was the most obvious when the temperature was 1873 K.The possible reason is that the increase in temperature weakens the mass transfer resistance of the electric double layer at the interface,thus accelerating the oxygen transfer rate.展开更多
This paper givers an estimated formula of convergence rate for parallel multisplitting iterative method.Using the formula,we can simplify and unify the proof of convergence of PMI_method.
For an upper bound of the spectral radius of the QHSS (quasi Hermitian and skew-Hermitian splitting) iteration matrix which can also bound the contraction factor of the QHSS iteration method,we give its minimum point ...For an upper bound of the spectral radius of the QHSS (quasi Hermitian and skew-Hermitian splitting) iteration matrix which can also bound the contraction factor of the QHSS iteration method,we give its minimum point under the conditions which guarantee that the upper bound is strictly less than one. This provides a good choice of the involved iteration parameters,so that the convergence rate of the QHSS iteration method can be significantly improved.展开更多
We discuss estimates for the rate of convergence of the method of successive subspace corrections in terms of condition number estimate for the method of parallel subspace corrections.We provide upper bounds and in a ...We discuss estimates for the rate of convergence of the method of successive subspace corrections in terms of condition number estimate for the method of parallel subspace corrections.We provide upper bounds and in a special case,a lower bound for preconditioners defined via the method of successive subspace corrections.展开更多
A kinetic study of biogas production from Urban Solid Waste (USW) generated in Dar es Salaam city (Tanzania) is presented. An experimental bioreactor simulating mesophilic conditions of most USW landfills was develope...A kinetic study of biogas production from Urban Solid Waste (USW) generated in Dar es Salaam city (Tanzania) is presented. An experimental bioreactor simulating mesophilic conditions of most USW landfills was developed. The goal of the study was to generate the kinetic order of reaction with respect to biodegradable organic waste and use it to model biogas production from food residues mixed with fruit waste. Anaerobic biodegradation was employed under temperature range of 28℃ - 38℃. The main controls were leachate recirculation and pH adjustments to minimize acid inhibitory effects and accelerate waste biodegradation. The experimental setup comprised of three sets of bioreactors. A biodegradation rate law in differential form was proposed and the numerical values of kinetic order and rate constant were determined using initial rate method as 0.994 and 0.3093 mol0.006·day-1, respectively. Results obtained were consistent with that found in literature and model predictions were in reasonable agreement with experimental data.展开更多
A new method of the multiple rates isotemperature is proposed to define the most probable mechanismg(α) of thermal anlaysis; the iterative isoconversional procedure has been employed to estimate apparent activation e...A new method of the multiple rates isotemperature is proposed to define the most probable mechanismg(α) of thermal anlaysis; the iterative isoconversional procedure has been employed to estimate apparent activation energyE; the pre-exponential factorA is obtained on the basis ofE andg(α). By this new method, the thermal analysis kinetics triplet of dehydration of cobalt oxalate dihydrate is determined, apparent activation energyE is 99.84 kJ·mol?1; pre-exponential factorA is 3.427×109–3.872×109 s?1 and the most probable mechanism belongs to nucleation and growth,A m model, the range ofm is from 1.50 to 1.70. Key words multiple rates isotemperature method - isoconversional method - cobalt oxalate dihydrate - accomodation function - differential scanning calorimetry (DSC) CLC number O 636.1 Foundation item: Supported by the Key Foundation of the Science and Technology Committee of Hubei Province (2001ABA009)Biography: Li Li-qing (1977-), female, Master candidate, research direction: material synthesize and thermal analysis kinetics.展开更多
AIM To evaluate the influence of creatinine methodology on the performance of chronic kidney disease(CKD)-Epidemiology Collaboration Group-calculated estimated glomerular filtration rate(CKD-EPI-eGFR) for CKD diagnosi...AIM To evaluate the influence of creatinine methodology on the performance of chronic kidney disease(CKD)-Epidemiology Collaboration Group-calculated estimated glomerular filtration rate(CKD-EPI-eGFR) for CKD diagnosis/staging in a large cohort of diabetic patients. METHODS Fasting blood samples were taken from diabetic patients attending our clinic for their regular annual examination, including laboratory measurement of serum creatinine and eGFR.RESULTS Our results indicated an overall excellent agreement in CKD staging(kappa = 0.918) between the Jaffé serum creatinine-and enzymatic serum creatinine-based CKDEPI-eGFR, with 9% of discordant cases. As compared to the enzymatic creatinine, the majority of discordances(8%) were positive, i.e., associated with the more advanced CKD stage re-classification, whereas only 1% of cases were negatively discordant if Jaffé creatinine was used for eGFR calculation. A minor proportion of the discordant cases(3.5%) were re-classified into clinically relevant CKD stage indicating mildly to moderately decreased kidney function(< 60 m L/min per 1.73 m^2). Significant acute and chronic hyperglycaemia, assessedas plasma glucose and Hb A1 c levels far above the recommended glycaemic goals, was associated with positively discordant cases. Due to a very low frequency, positive discordance is not likely to present a great burden for the health-care providers, while intensified medical care may actually be beneficial for the small number of discordant patients. On the other hand, a very low proportion of negatively discordant cases(1%) at the 60 m L/min per 1.73 m^2 eGFR level indicate a negligible possibility to miss the CKD diagnosis, which could be the most prominent clinical problem affecting patient care, considering high risk of CKD for adverse patient outcomes. CONCLUSION This study indicate that compensated Jaffé creatinine procedure, in spite of the glucose-dependent bias, is not inferior to enzymatic creatinine in CKD diagnosis/staging and therefore may provide a reliable and cost-effective tool for the renal function assessment in diabetic patients.展开更多
A term structure model bearing features of stochastic volatility and stochastic mean drift with jump （SVJ-SD model for short） is built in the paper to describe the stochastic behavior of interest rates.Based on samp...A term structure model bearing features of stochastic volatility and stochastic mean drift with jump （SVJ-SD model for short） is built in the paper to describe the stochastic behavior of interest rates.Based on sample data of an interest rate of national bond repurchase,maximum likelihood （ML）,linear Kalman filter and efficient method of moments （EMM） are used to estimate the model.While ML works well for simple models,it may lead to considerable deviation in parameter estimation when dynamic risks of interest rates are considered in them.Linear Kalman filter is a tractable and reasonably accurate technique for estimation cases where ML was not feasible.Moreover,when compared with the first two approaches,using EMM can obtain better parameter estimates for complex models with non-affine structures.展开更多
基金partly supported by the Beijing Natural Science Foundation(Grant No.Z200003)by the National Natural Science Foundation of China(Grant Nos.12331015,12301475,12301465)+1 种基金by the National Center for Mathematics and Interdisciplinary Science,Chinese Academy of Sciencesby the Research Foundation for the Beijing University of Technology New Faculty(Grant No.006000514122516).
文摘This study proposes a class of augmented subspace schemes for the weak Galerkin(WG)finite element method used to solve eigenvalue problems.The augmented subspace is built with the conforming linear finite element space defined on the coarse mesh and the eigen-function approximations in the WG finite element space defined on the fine mesh.Based on this augmented subspace,solving the eigenvalue problem in the fine WG finite element space can be reduced to the solution of the linear boundary value problem in the same WG finite element space and a low dimensional eigenvalue problem in the augmented sub-space.The proposed augmented subspace techniques have the second order convergence rate with respect to the coarse mesh size,as demonstrated by the accompanying error esti-mates.Finally,a few numerical examples are provided to validate the proposed numerical techniques.
基金supported by National University Basic Scientific Research Fund of China(Grant No.N100403009)National Natural Science Foundation of China(Grant No.50875041)
文摘The existing researches of the evaluation method of ride comfort of vehicle mainly focus on the level of human feelings to vibration. The level of human feelings to vibration is influenced by many factors, however, the ride comfort according to the common principle of probability and statistics and simple binary logic is tmable to reflect these uncertainties. The random fuzzy evaluation model from people subjective response to vibration is adopted in the paper, these uncertainties are analyzed from the angle of psychological physics. Discussing the traditional evaluation of ride comfort during vehicle vibration, a fuzzily random evaluation model on the basis of annoyance rate is proposed for the human body＇s subjective response to vibration, with relevant fuzzy membership function and probability distribution given. A half-car four degrees of freedom suspension vibration model is described, subject to irregular excitations from the road surface, with the aid of software Matlab/Simulink. A new kind of evaluation method for ride comfort of vehicles is proposed in the paper, i.e., the annoyance rate evaluation method. The genetic algorithm and neural network control theory are used to control the system. Simulation results are obtained, such as the comparison of comfort reaction to vibration environments between before and after control, relationship of annoyance rate to vibration frequency and weighted acceleration, based on ISO 2631 / 1 （1982）, ISO 2631-1 （1997） and annoyance rate evaluation method, respectively. Simulated assessment results indicate that the proposed active suspension systems prove to be effective in the vibration isolation of the suspension system, and the subjective response of human being can be promoted from very uncomfortable to a little uncomfortable. Furthermore, the novel evaluation method based on annoyance rate can further estimate quantitatively the number of passengers who feel discomfort due to vibration. A new analysis method of vehicle comfort is presented.
基金supported by the National Basic Research Program of China (Grant No.2007CB613603)
文摘Monodisperse spherical SiO2 particles were successfully synthesized in 2-propanol-H2O-NH3 system by the microwave hydrothermal method using ammonia as catalyst. To investigate the influences on the size of spherical SiO2 particles, factors such as ammonia concentration, reaction temperature, stirring intensity and reactants mol ratio have been studied. The orthogonal experiments were carried out. The as-prepared SiO2 particles were characterized by X-ray diffraction （XRD）, transmission electron microscopy （TEM）, Fourier transform infrared spectroscopy （FTIR） and differential thermal analysis （DTA）. The results indicated that the size of SiO2 particles increased greatly with the increase in ammonia concentration, temperature and reactants mol ratio, but increased slightly with the increase in stirring intensity. Monodisperse spherical Si02 particles were amorphous with perfect sphere and uniform size. Hydroxyl was detected in SiO2. Kinetic parameters were calculated, and finally the reaction rate equation of dehydrated hydroxyl was obtained.
基金Projects(51474251,51874351) supported by the National Natural Science Foundation of China
文摘A new electrical method of conductive carbon-film(with waterproof and anticorrosion ability)was proposed to continuously measure crack propagation rate of brittle rock under THMC coupling condition.A self-designed coupling testing system was used to conduct THMC coupling fracture tests of the pre-cracked red sandstone specimens(where the temperature is only changed)by this new electrical method of conductive carbon-film.Calculation results obtained by the energy method coincide well with the test results.And the higher the temperature is,the earlier the crack is initiated and the larger the crack propagation rate and accelerated velocity are,which can prove the validity of the new electrical method.This new electrical method has advantages of continuously measuring crack propagation rate over the conventional electrical,optical and acoustic methods,and can provide important basis for safety assessment and cracking-arrest design of deep rock mass engineering.
文摘This paper presents anew regularization method for solving operator equations of the first kind; the convergence rate of the regularized solution is improved, as compared with the ordinary Tikhonov regularization.
基金supported by the National Natural Science Funds of China(No.11205155)Fundamental Research Funds for the Central Universities(WK2310000041)
文摘An accelerator storage ring needs clean ultrahigh vacuum.A TiZrV non-evaporable getter(NEG) film deposited on interior walls of the chamber can realize distributed pumping,effective vacuum improvement and reduced longitudinal pressure gradient.But accumulation of pollutants such as N_2 and O_2 will decrease the adsorption ability of the NEG,leading to a reduction of NEG lifetime.Therefore,an NEG thin film coated with a layer of Pd,which has high diffusion rate and absorption ability for H_2,can extend the service life of NEG and improve the pumping rate of H_2 as well.In this paper,with argon as discharge gas,a magnetron sputtering method is adopted to prepare TiZrV-Pd films in a long straight pipe.By SEM measurement,deposition rates of TiZrV-Pd films are analyzed under different deposition parameters,such as magnetic field strength,gas flow rate,discharge current,discharge voltage and working pressure.By comparing the experimental results with the simulation results based on Sigmund's theory,the Pd deposition rate C can be estimated by the sputtered depth.
文摘[Objectives ] The paper was to explore enzyme inhibition rate method for rapid detection of organophosphorus and carbamate pesticides in cowpea. [ Methods ] Acetylcholinesterase （ACHE） was added to cowpea extract, to determine the inhibition rate of extract against enzyme. The influences of different sampiing methods and sampling parts on detection results were compared. [ Results] The positive rate of standard sampling was 18.18% higher than that of non-stand- ard sampling, and the positive rate of samples collected from cowpea tail was 16.67% higher than that collected from other parts. [ Condmions] Enzyme inhibi- tion rate method is suitable for rapid detection of organophosphorus and carbamate pesticides in cowpea.
基金supported by Gansu Provincial Critical Patented Projects of China(Grant No.1101ZSB117)Gansu Provincial Science and Technology Pillar Program of China(Grant No.1002ZSB018)
文摘The castings defects are affected by the melting volume change rate of material.The change rate has an important effect on running safety of the high temperature thermal storage chamber,too.But the characteristics of existing measuring installations are complex structure,troublesome operation and low precision.In order to measure the melting volume change rate of material accurately and conveniently,a self-designed measuring instrument,self-heating probe instrument,and measuring method are described.Temperature in heating cavity is controlled by PID temperature controller;melting volume change rateυand molten density are calculated based on the melt volume which is measured by the instrument.Positive and negativeυrepresent expansion and shrinkage of the sample volume after melting,respectively.Taking eutectic LiF+CaF2 for example,its melting volume change rate and melting density at 1123 K are-20.6%and 2651 kg/m–3 measured by this instrument,which is only 0.71%smaller than literature value.Density and melting volume change rate of industry pure aluminum at 973 K and analysis pure NaCl at 1123 K are detected by the instrument too.The measure results are agreed with report values.Measuring error sources are analyzed and several improving measures are proposed.In theory,the measuring errors of the change rate and molten density which are measured by the self-designed instrument is nearly 1/20-1/50 of that measured by the refitted mandril thermal expansion instrument.The self-designed instrument and method have the advantages of simple structure,being easy to operate,extensive applicability for material,relatively high accuracy,and most importantly,temperature and sample vapor pressure have little effect on the measurement accuracy.The presented instrument and method solve the problems of complicated structure and procedures,and large measuring errors for the samples with high vapor pressure by existing installations.
文摘Fatigue crack propagation characteristics of a diesel engine crankshaft are studied by measuring the fatigue crack growth rate using a frequency sweep method on a resonant fatigue test rig. Based on the phenomenon that the system frequency will change when the crack becomes large, this method can be directly applied to a complex component or structure. Finite element analyses （FEAs） are performed to calibrate the relation between the frequency change and the crack size, and to obtain the natural frequency of the test rig and the stress intensity factor （SIF） of growing cracks. The crack growth rate i.e. da/dN-AK of each crack size is obtained by combining the testing-time monitored data and FEA results. The results show that the crack growth rate of engine crankshaft, which is a component with complex geometry and special surface treatment, is quite different from that of a pure material. There is an apparent turning point in the Paris＇s crack partition. The cause of the fatigue crack growth is also discussed.
基金the National Natural Science Foundation of China(51905324)the Scientific Research Program Funded by Shaanxi Provincial Education Department(20JK0545)the Doctoral Scientific Research Startup Foundation of Shaanxi University of Science and Technology(2018BJ-14)。
文摘Ce^(3+)as the active site on the CeO_(2)abrasive surface is the key to enhancing the material removal rate(MRR).The CeO_(2)abrasives with high chemical activity were prepared by the molten salt method under a reducing atmosphere.The crystal structure and morphology of CeO_(2)abrasive s were characterized by X-ray diffraction(XRD),scanning electron microscopy(SEM),transmission electron microscopy(TEM),Fourier transform infrared spectroscopy(FT-IR),ultraviolet—visible diffuse reflectance spectroscopy(UV-Vis DRS),and X-ray photoelectron spectroscopy(XPS).The CeO_(2)abrasives were obtained under different atmospheres(Air,Ar,and Ar/H_(2)).With the enhancement of the reducing atmosphere,the morphology of the abrasives transforms from spherical to octahedral,while more oxygen vacancies and Ce^(3+)are generated on the surface of CeO_(2)abrasives.The CMP experiments show that the MRRs of the CeO_(2)-Air,CeO_(2)-Ar,and CeO_(2)-Ar/H_(2)abrasives on SiO_(2)substrates are 337.60,578.74,and 691.28 nm/min,respectively.Moreover,as confirmed by atomic force microscopy(AFM),the substrate surfaces exhibit low roughness(20.5 nm)after being polished using all of the prepared samples.Especially,the MRR of CeO_(2)-Ar/H_(2)abrasives is increased by 104.76%compared with CeO_(2)-air abrasives.The improved CMP performance is attributed to the increased Ce^(3+)concentration and the octahedral morphology of the abrasives enhancing the chemical reaction and mechanical removal at the abrasive-substrate interface.
文摘The aim of this study is to evaluate the uncertainty of 2πα and 2πβ surface emission rates using the windowless multiwire proportional counter method.This study used the Monte Carlo method (MCM) to validate the conventional Guide to the Expression of Uncertainty in Measurement (GUM) method.A dead time measurement model for the two-source method was established based on the characteristics of a single-channel measurement system,and the voltage threshold correction factor measurement function was indirectly obtained by fitting the threshold correction curve.The uncertainty in the surface emission rate was calculated using the GUM method and the law of propagation of uncertainty.The MCM provided clear definitions for each input quantity and its uncertainty distribution,and the simulation training was realized with a complete and complex mathematical model.The results of the surface emission rate uncertainty evaluation for four radioactive plane sources using both methods showed the uncertainty’s consistency E_(n)<0.070 for the comparison of each source,and the uncertainty results of the GUM were all lower than those of the MCM.However,the MCM has a more objective evaluation process and can serve as a validation tool for GUM results.
基金supported by the National Natural Science Foundation of China(41874011,41861134009)the National Key Research and Development Program of China(2018YFC1503603)
文摘Radar interferograms are usually influenced by factors such as atmospheric artifacts,orbital errors,and terrain errors.It is difficult to reduce the influence by using the conventional small baseline subset(SBAS)method when determining the deformation rate.This study uses the adjustment model with systematic parameters to improve the conventional SBAS method and employs it to determine the interseismic deformation rate of the Haiyuan fault system,providing a data reference for exploring the locking depth,strain accumulation state,and potential seismic risk assessment of different segments of the Haiyuan fault system.The results are as follows:(1)the simulation experiment verifies the feasibility and robustness of the modified SBAS method.This method can effectively reduce the influence of residual signals such as atmospheric artifacts,orbital errors and terrain errors in the interferograms.The deformation rate map can be significantly improved;(2)the deformation rate field in the radar’s Line of Sight(LOS)direction shows that there are obvious differences between the north and south sides of Haiyuan fault system,which is consistent with the characteristics of the left-lateral strike-slip movement of the Haiyuan fault system.The deformation rate field and profiles reflect the complex trends among different segments of Haiyuan fault system in detail.(3)the deformation rate of the Jingtai pull-apart basin is higher than that of the surrounding areas,possibly indicating strong regional activity,which provides a reference for studying the seismic risk of the Jingtai pull-apart basin;and(4)the interseismic deformation rate and profiles across the fault show that the middle section of the Lao Hu Shan(LHS)segment and the western and middle sections of the Haiyuan segment are locked.
基金gratefully express their appreciation to National Natural Science Foundation of China(Nos.51974153 and U1960203)the Joint Fund of State Key Laboratory of Marine Engineering and University of Science and Technology Liaoning(SKLMEA-USTL-201707)the China Scholarship Council(201908210457).
文摘The interfacial oxygen transfer rate is one of the main factors to control the composition of alloys.The commonly employed method of studying the interfacial oxygen transfer rate is the chemical composition analysis;however,it is difficult to be studied in situ.Here,a new method of measuring the oxygen transfer rate at the gas-slag and slag-metal interfaces was reported based on electrochemical analyses.The interfacial oxygen transfer rate in the smelting process of Inconel 718 superalloy was investigated at 1723,1773,1823,and 1873 K.The experimental results show that the electrochemical method can measure the real-time oxygen content;hence,this method is promising in controlling the oxygen content in alloys.As the temperature increased,both the equilibrium oxygen content and the rate of oxygen absorption increased significantly,and the increase was the most obvious when the temperature was 1873 K.The possible reason is that the increase in temperature weakens the mass transfer resistance of the electric double layer at the interface,thus accelerating the oxygen transfer rate.
文摘This paper givers an estimated formula of convergence rate for parallel multisplitting iterative method.Using the formula,we can simplify and unify the proof of convergence of PMI_method.
基金the National Natural Science Foundation (No.11671393),China.
文摘For an upper bound of the spectral radius of the QHSS (quasi Hermitian and skew-Hermitian splitting) iteration matrix which can also bound the contraction factor of the QHSS iteration method,we give its minimum point under the conditions which guarantee that the upper bound is strictly less than one. This provides a good choice of the involved iteration parameters,so that the convergence rate of the QHSS iteration method can be significantly improved.
文摘We discuss estimates for the rate of convergence of the method of successive subspace corrections in terms of condition number estimate for the method of parallel subspace corrections.We provide upper bounds and in a special case,a lower bound for preconditioners defined via the method of successive subspace corrections.
文摘A kinetic study of biogas production from Urban Solid Waste (USW) generated in Dar es Salaam city (Tanzania) is presented. An experimental bioreactor simulating mesophilic conditions of most USW landfills was developed. The goal of the study was to generate the kinetic order of reaction with respect to biodegradable organic waste and use it to model biogas production from food residues mixed with fruit waste. Anaerobic biodegradation was employed under temperature range of 28℃ - 38℃. The main controls were leachate recirculation and pH adjustments to minimize acid inhibitory effects and accelerate waste biodegradation. The experimental setup comprised of three sets of bioreactors. A biodegradation rate law in differential form was proposed and the numerical values of kinetic order and rate constant were determined using initial rate method as 0.994 and 0.3093 mol0.006·day-1, respectively. Results obtained were consistent with that found in literature and model predictions were in reasonable agreement with experimental data.
文摘A new method of the multiple rates isotemperature is proposed to define the most probable mechanismg(α) of thermal anlaysis; the iterative isoconversional procedure has been employed to estimate apparent activation energyE; the pre-exponential factorA is obtained on the basis ofE andg(α). By this new method, the thermal analysis kinetics triplet of dehydration of cobalt oxalate dihydrate is determined, apparent activation energyE is 99.84 kJ·mol?1; pre-exponential factorA is 3.427×109–3.872×109 s?1 and the most probable mechanism belongs to nucleation and growth,A m model, the range ofm is from 1.50 to 1.70. Key words multiple rates isotemperature method - isoconversional method - cobalt oxalate dihydrate - accomodation function - differential scanning calorimetry (DSC) CLC number O 636.1 Foundation item: Supported by the Key Foundation of the Science and Technology Committee of Hubei Province (2001ABA009)Biography: Li Li-qing (1977-), female, Master candidate, research direction: material synthesize and thermal analysis kinetics.
文摘AIM To evaluate the influence of creatinine methodology on the performance of chronic kidney disease(CKD)-Epidemiology Collaboration Group-calculated estimated glomerular filtration rate(CKD-EPI-eGFR) for CKD diagnosis/staging in a large cohort of diabetic patients. METHODS Fasting blood samples were taken from diabetic patients attending our clinic for their regular annual examination, including laboratory measurement of serum creatinine and eGFR.RESULTS Our results indicated an overall excellent agreement in CKD staging(kappa = 0.918) between the Jaffé serum creatinine-and enzymatic serum creatinine-based CKDEPI-eGFR, with 9% of discordant cases. As compared to the enzymatic creatinine, the majority of discordances(8%) were positive, i.e., associated with the more advanced CKD stage re-classification, whereas only 1% of cases were negatively discordant if Jaffé creatinine was used for eGFR calculation. A minor proportion of the discordant cases(3.5%) were re-classified into clinically relevant CKD stage indicating mildly to moderately decreased kidney function(< 60 m L/min per 1.73 m^2). Significant acute and chronic hyperglycaemia, assessedas plasma glucose and Hb A1 c levels far above the recommended glycaemic goals, was associated with positively discordant cases. Due to a very low frequency, positive discordance is not likely to present a great burden for the health-care providers, while intensified medical care may actually be beneficial for the small number of discordant patients. On the other hand, a very low proportion of negatively discordant cases(1%) at the 60 m L/min per 1.73 m^2 eGFR level indicate a negligible possibility to miss the CKD diagnosis, which could be the most prominent clinical problem affecting patient care, considering high risk of CKD for adverse patient outcomes. CONCLUSION This study indicate that compensated Jaffé creatinine procedure, in spite of the glucose-dependent bias, is not inferior to enzymatic creatinine in CKD diagnosis/staging and therefore may provide a reliable and cost-effective tool for the renal function assessment in diabetic patients.
基金Sponsored by the National Natural Science Foundation of China(60979010)
文摘A term structure model bearing features of stochastic volatility and stochastic mean drift with jump （SVJ-SD model for short） is built in the paper to describe the stochastic behavior of interest rates.Based on sample data of an interest rate of national bond repurchase,maximum likelihood （ML）,linear Kalman filter and efficient method of moments （EMM） are used to estimate the model.While ML works well for simple models,it may lead to considerable deviation in parameter estimation when dynamic risks of interest rates are considered in them.Linear Kalman filter is a tractable and reasonably accurate technique for estimation cases where ML was not feasible.Moreover,when compared with the first two approaches,using EMM can obtain better parameter estimates for complex models with non-affine structures.
