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Progress and Development Direction of “Three-High” Oil and Gas Well Testing Technology 被引量:1
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作者 Bo Zhang Fayon Yuan +3 位作者 Hao Su Ming Cao Ruifeng Guo Chenxiang Sun 《Journal of Power and Energy Engineering》 2022年第6期1-13,共13页
By reviewing the development of “three-high” oil and gas well testing technology of Sinopec in recent years, this paper systematically summarizes the application of “three-high” oil and gas well testing technology... By reviewing the development of “three-high” oil and gas well testing technology of Sinopec in recent years, this paper systematically summarizes the application of “three-high” oil and gas well testing technology of Sinopec in engineering optimization design technology, and high temperature and high pressure testing technology, high pressure and high temperature transformation completion integration technology. Major progress has been made in seven aspects: plug removal and re-production technology of production wells in high acid gas fields;wellbore preparation technology of ultra-deep, high-pressure, and high-temperature oil and gas wells;surface metering technology;and supporting tool development technology. This paper comprehensively analyzes the challenges faced by the “three-high” oil and gas well production testing technology in four aspects: downhole tools, production testing technology, safe production testing, and the development of low-cost production test tools. Four development directions are put forward: 1) Improve ultra-deep oil and gas testing technology and strengthen integrated geological engineering research. 2) Deepen oil and gas well integrity evaluation technology to ensure the life cycle of oil and gas wells. 3) Carry out high-end, customized, and intelligent research on oil test tools to promote the low-cost and efficient development of ultra deep reservoirs. 4) Promote the fully automatic control of the surface metering process to realize the safe development of “three-high” reservoirs. 展开更多
关键词 “Three-High” oil and Gas Wells oil test Geological Engineering Integra-tion Intelligent Downhole Tools
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Test Results for Polymer Flooding in Daqing Oilfield 被引量:1
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作者 Zhang Jingcun Gao Shutang and Jiang Xiangcheng(Research Institute of Petroleum Esploration andDevelopment, Daqing Petroleum Administration) 《China Oil & Gas》 CAS 1995年第2期25-27,共3页
TestResultsforPolymerFloodinginDaqingOilfield¥ZhangJingcun;GaoShutangandJiangXiangcheng(ResearchInstituteofP... TestResultsforPolymerFloodinginDaqingOilfield¥ZhangJingcun;GaoShutangandJiangXiangcheng(ResearchInstituteofPetroleumEsplorati... 展开更多
关键词 POLYMER DRIVE PILOT testing TERTIARY oil RECOVERY
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Prediction of wax precipitation region in wellbore during deep water oil well testing 被引量:1
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作者 GAO Yonghai LIU Kai +4 位作者 ZHAO Xinxin LI Hao CUI Yanchun XIN Guizhen SUN Baojiang 《Petroleum Exploration and Development》 2018年第2期351-357,共7页
During deep water oil well testing, the low temperature environment is easy to cause wax precipitation, which affects the normal operation of the test and increases operating costs and risks. Therefore, a numerical me... During deep water oil well testing, the low temperature environment is easy to cause wax precipitation, which affects the normal operation of the test and increases operating costs and risks. Therefore, a numerical method for predicting the wax precipitation region in oil strings was proposed based on the temperature and pressure fields of deep water test string and the wax precipitation calculation model. And the factors affecting the wax precipitation region were analyzed. The results show that: the wax precipitation region decreases with the increase of production rate, and increases with the decrease of geothermal gradient, increase of water depth and drop of water-cut of produced fluid, and increases slightly with the increase of formation pressure. Due to the effect of temperature and pressure fields, wax precipitation region is large in test strings at the beginning of well production. Wax precipitation region gradually increases with the increase of shut-in time. These conclusions can guide wax prevention during the testing of deep water oil well, to ensure the success of the test. 展开更多
关键词 deep water oil and gas development oil well testing wellbore WAX PRECIPITATION temperature FIELD pressure FIELD WAX PRECIPITATION REGION PREDICTION
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Contract for Oil/Gas Testing Signed Between Jinlonghua & Esso
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作者 Wang Keyuo 《China Oil & Gas》 CAS 1996年第3期189-189,共1页
Contract for Oil/Gas Testing Signed Between Jinlonghua & EssoContractforOil/GasTestingSignedBetweenJinlonghu... Contract for Oil/Gas Testing Signed Between Jinlonghua & EssoContractforOil/GasTestingSignedBetweenJinlonghua&Esso¥WangKeyuJi... 展开更多
关键词 Contract for oil/Gas testing Signed Between Jinlonghua Esso
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Swelling/extraction test of Russian reservoir heavy oil by liquid carbon dioxide
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作者 LOBANOV A A SHHEKOLDIN K A +5 位作者 STRUCHKOV I A ZVONKOV M A HLAN M V PUSTOVA E J KOVALENKO V A ZOLOTUKHIN A B 《Petroleum Exploration and Development》 2018年第5期918-926,共9页
The mass transfer between heavy oil and liquid carbon dioxide and the changes of the heavy phase(mixture of heavy oil and CO_2) and light phase(pure CO_2) in the mixture were tested in lab with heavy oil samples from ... The mass transfer between heavy oil and liquid carbon dioxide and the changes of the heavy phase(mixture of heavy oil and CO_2) and light phase(pure CO_2) in the mixture were tested in lab with heavy oil samples from Russia. The experimental results showed that the heavy oil hardly expanded when the concentration of carbon dioxide in the mixture was 10%. When the concentration of carbon dioxide was higher than 26%, the volume of the heavy phase decreased, and the viscosity of the heavy phase increased exponentially as the light components extracted from the heavy oil exceeded the carbon dioxide saturated in the heavy oil. When the concentration of carbon dioxide in the mixture was 26%, the effect of viscosity reducing to the heavy phase was the strongest. The density of the light and heavy phases, volume factor, and solubility of gas and flash viscosity of heavy phase all increased with the rise of carbon dioxide concentration in the mixture. The best concentration of carbon dioxide in the mixture was 26%, when the heavy oil expanded the most and the viscosity of the heavy phase was the lowest. When the concentration of carbon dioxide in the mixture was between 10% and 26%, the volume of the light phase was the smallest and the oil displacement effect was the best. 展开更多
关键词 enhanced oil recovery liquid CO2 heavy oil SWELLING test EXTRACT test phase behavior
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TEST STUDY OF DETECTING OIL AND GAS BY USING REMOTE SENSING TECHNIQUE
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作者 Zhu Zhenhai, Zhang Jianzhong, Chen Baowen (Remote Sensing Application Institute, The Chinese Academy of Sciences) 《遥感信息》 CSCD 1990年第A02期37-38,共2页
Ⅰ The Indexes of Detecting Oil and Gas Resources The deeply buried reservoir which in a dynamic equilibrium state has a great pressure inside, and between it and earth surface there is a great difference of pressure.... Ⅰ The Indexes of Detecting Oil and Gas Resources The deeply buried reservoir which in a dynamic equilibrium state has a great pressure inside, and between it and earth surface there is a great difference of pressure. Therefore the hydrocarbon must spread and move vertically to the surface along the pressure gradient orientation. Hydrocarbons in the reservoir along some small rifts, cracks, joints and cleavages penetrate the overlying strata and seepage onto the surface. Thus the hydrocarbons become unvisble oil and gas signs. This process is called the phenomena of hydrocarbon microseepage of reservoir. Hydrocarbons microseepage in the process 展开更多
关键词 test STUDY OF DETECTING oil AND GAS BY USING REMOTE SENSING TECHNIQUE GAS
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lower Oil Prices Test Africa’s growth
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作者 Hannah Edinger Kira McDonald 《ChinAfrica》 2015年第1期10-11,共2页
The foundations of the "Africa rising" narrative may have increasingly been tested in recent months. Security concerns, the Ebola crisis in West Africa and conflict in Libya have been some of the stumbling blocks th... The foundations of the "Africa rising" narrative may have increasingly been tested in recent months. Security concerns, the Ebola crisis in West Africa and conflict in Libya have been some of the stumbling blocks the continent has had to face. These have continuously challenged its ability to respond to events that could derail the past years' economic growth. The impact of lower oil prices particularly could be a major shock to the region, especially for oilexporting countries. 展开更多
关键词 lower oil Prices test Africa’s growth
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The Test Area of Suizhong 36-1 Oil Field Fully Under Commission
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作者 Yan Hao 《China Oil & Gas》 CAS 1995年第3期14-14,共1页
TheTestAreaofSuizhong36-1OilFieldFullyUnderCommission¥//Suizhong36-lOilfieldlocatedin.LiaodongGulf,coveringa... TheTestAreaofSuizhong36-1OilFieldFullyUnderCommission¥//Suizhong36-lOilfieldlocatedin.LiaodongGulf,coveringanareaof48km2Theoi... 展开更多
关键词 test The test Area of Suizhong 36-1 oil Field Fully Under Commission
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航空发动机燃油泵动静压滑动轴承润滑特性与参数影响分析 被引量:2
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作者 符江锋 仲世杰 +2 位作者 罗康 刘显为 魏士杰 《推进技术》 北大核心 2025年第1期237-252,共16页
航空发动机燃油齿轮泵的滑动轴承长期工作在高温、高压和低黏介质极端工况下,极易诱发润滑失效,其润滑性能演变规律尚未完全探明。本文通过建立动静压混合润滑条件下燃油泵滑动轴承流体润滑模型,采用超声测量原理测试了燃油泵真实服役... 航空发动机燃油齿轮泵的滑动轴承长期工作在高温、高压和低黏介质极端工况下,极易诱发润滑失效,其润滑性能演变规律尚未完全探明。本文通过建立动静压混合润滑条件下燃油泵滑动轴承流体润滑模型,采用超声测量原理测试了燃油泵真实服役工况下的油膜厚度,验证了多个载荷条件滑动轴承润滑模型的油膜厚度计算准确性。最后,基于试验验证的润滑计算模型,研究了宽径比、偏心率和油槽位置对轴承润滑性能的影响规律。研究结果表明:计算的油膜厚度随工况变化规律与试验测点十分吻合,两者的平均计算误差为2.3%,此外,燃油泵负载增大会使得油膜的最小厚度向进口油槽处偏转,进而导致动压能力减弱,轴承在大负载工况的承载能力主要由静压提供。宽径比B/D由0.4增大至1.2时,会导致油膜温度沿周向降低1.2℃,而沿轴向升高0.5℃,偏心率增大会导致油膜厚度变小,混合润滑轴承中间截面处的动压提升0.43 MPa,设计滑动轴承的油槽位置应开在收敛楔形结构前端或者开扩楔形结构处,能提升轴承承载性能。 展开更多
关键词 航空发动机 燃油齿轮泵 滑动轴承 润滑 油膜测试
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Field Test of Electrochemical Degradation and Oil-Removal Technology Used the Treatment of Wastewater Containing Polymer in Offshore Oilfield
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作者 Mengying Yang Qing Li +2 位作者 Xianqing Yin Lei Zhai Bo Jing 《Journal of Water Resource and Protection》 2015年第17期1409-1415,共7页
Aimed at the current treatment status of the polymer-flooding wastewater in Bohai oilfield, electrochemical technology used for polymer-degradation and oil-removal was researched. It formed the process flow of cyclone... Aimed at the current treatment status of the polymer-flooding wastewater in Bohai oilfield, electrochemical technology used for polymer-degradation and oil-removal was researched. It formed the process flow of cyclone mixed dosing → electrochemical removal oil → inclined tube removal oil → walnut shell filter, and a set of skid mounted wastewater containing polymer treatment plant was designed and manufactured, which was used for the field test of electrochemical treatment of wastewater containing polymer in offshore oilfield. The result shows that the oil removal rate of the electrochemical treatment process is over 98%, and the synergistic effect is significant especially used in conjunction with water clarifier of BHQ-04. When the amount of water clarifier is 50 - 150 mg/L, the oil content, the median particle diameter and the suspended solids content of the filtered water is 8 - 18 mg/L, 1.9 - 2.26 μm and 1.39 - 2.04 mg/L respectively, which reach the scene water quality standards for water injection. 展开更多
关键词 ELECTROCHEMICAL Removal oil WASTEWATER CONTAINING POLYMER SYNERGISTIC Effect Field test
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非常规油气微注压降返排分析技术现状及发展趋势 被引量:1
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作者 许冬进 吴坤 +5 位作者 印文龙 王勇 郭泽辰 胡君城 魏志军 何飞鹏 《大庆石油地质与开发》 北大核心 2025年第3期151-158,共8页
微注压降返排分析(DFIT-FBA)技术是非常规油气开采中非常重要的一项新技术,通过低成本、易操作的方法来快速测算储层闭合压力、渗透率、原始地层压力等水力压裂关键参数,应用潜力巨大。基于国内外广泛的文献调研,开展了DFIT-FBA技术的... 微注压降返排分析(DFIT-FBA)技术是非常规油气开采中非常重要的一项新技术,通过低成本、易操作的方法来快速测算储层闭合压力、渗透率、原始地层压力等水力压裂关键参数,应用潜力巨大。基于国内外广泛的文献调研,开展了DFIT-FBA技术的现状、设计原则、设计方法、应用及发展趋势研究。结果表明:DFIT-FBA技术通过低速缓慢向地层注入流体、短暂关井和低速率(注入速率的2%~5%)回流返排,可显著缩短测试时间,并利用速率瞬态分析法和流动物质平衡方程,有效地估算储层压力、闭合压力并预测油气井产能。该技术不仅可以为非常规油气的压裂优化设计、储层“甜点”识别和小规模地震预防等方面提供技术支持,而且可以与大数据处理技术深度融合,实现四维智能可视化压裂监测,提高对复杂储层条件的监测、识别能力,从而为非常规油气田的开发提供更加精准的技术指导,优化压裂作业工艺参数,提高油气开采效率,同时可降低环境风险。 展开更多
关键词 非常规油气 压裂测试 微注压降返排分析(DFIT-FBA) 闭合压力 储层压力 油气井产能
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The Study of Electromagnetic Stress Testing Method on Oil-Gas Pipelines Based on WT 被引量:7
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作者 Bin Liu Wanru Sun Yiren Lin 《Geomaterials》 2014年第2期55-63,共9页
This paper proposes an effective method for early diagnosis (stress concentrating) of the oil-gas pipeline. Based on the principle of electromagnetic induction Faraday, we have designed and realized the nondestructive... This paper proposes an effective method for early diagnosis (stress concentrating) of the oil-gas pipeline. Based on the principle of electromagnetic induction Faraday, we have designed and realized the nondestructive testing system for stress concentration area of ferromagnetic materials by means of the research of metal materials inverse magnetostrictive effect mechanism. The system changes the influence degree of the stress in ferromagnetic materials’ magnetic conductance to the corresponding voltage array by using discrete wavelet analysis method to process the data, in which not only the measuring accuracy is improved, but also the stress concentration is more directly reflected. The experiments confirm that the electromagnetic stress testing method is feasible and valid. 展开更多
关键词 oil-Gas PIPELINE ELECTROMAGNETIC INDUCTION Magnetic CONDUCTANCE Stress CONCENTRATION NONDESTRUCTIVE testing
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新能源汽车绝缘纸油品兼容性方法研究 被引量:2
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作者 田晓鸿 李晋阳 《造纸科学与技术》 2025年第8期20-23,42,共5页
随着新能源汽车技术的迅猛发展,其动力系统对绝缘性能以及环境适应性的要求持续攀升。绝缘纸是保障电气安全极为重要的部分,它和冷却油、润滑油等液态介质长时间接触后,有可能致使材料性能变差,介电强度降低,甚至出现故障。基于此,依据... 随着新能源汽车技术的迅猛发展,其动力系统对绝缘性能以及环境适应性的要求持续攀升。绝缘纸是保障电气安全极为重要的部分,它和冷却油、润滑油等液态介质长时间接触后,有可能致使材料性能变差,介电强度降低,甚至出现故障。基于此,依据新能源汽车绝缘系统常见的应用场景,全面梳理了各类常见油品种类及其作用原理,剖析了不同绝缘纸材料的化学稳定性以及结构上较为脆弱的环节,还提出了一种基于多因子评价的油品兼容筛选办法。借助加速老化实验、红外光谱分析、电性能测试等方法,对典型油品给绝缘纸材料造成的影响程度加以评估,进而给出适配性评估模型与优化建议。研究所得成果能够为新能源汽车动力系统中绝缘纸和油品协同设计给予理论支撑与工程方面的依据。 展开更多
关键词 新能源汽车 绝缘纸 油品兼容性 老化试验 介电性能
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D1规格柴油机油的清净性能研究
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作者 郭鹏 成功 +3 位作者 吕会英 金志良 金鹏 赵正华 《润滑油》 2025年第3期42-45,共4页
D1规格柴油机油标准是我国自主开发的柴油机油标准,D1规格柴油机油需要通过4个发动机台架试验,其中柴油机油综合性能的评定(CA6DM3发动机台架测试)主要考察油品的高温清净性。研究介绍了3种D1规格的柴油机油,分别进行了柴油机油综合性... D1规格柴油机油标准是我国自主开发的柴油机油标准,D1规格柴油机油需要通过4个发动机台架试验,其中柴油机油综合性能的评定(CA6DM3发动机台架测试)主要考察油品的高温清净性。研究介绍了3种D1规格的柴油机油,分别进行了柴油机油综合性能的测试(CA6DM3发动机台架测试)、发动机油高温氧化沉积物测试(TEOST 33C测试)、发动机油适度高温活塞沉积物的测试(TEOST MHT测试)及板式成焦测试,研究结果表明TEOST 33C测试和板式成焦测试结果与CA6DM3台架测试结果趋势一致。此台架试验与模拟试验的对应关系,有助于节省配方开发的时间和费用,提高研发效率。 展开更多
关键词 D1规格 柴油机油 台架测试 清净性
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抗磨添加剂在航空润滑油摩擦磨损试验中作用特性研究
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作者 刘月皞 梅莉 张伟 《合成润滑材料》 2025年第1期28-31,共4页
采用测定润滑油抗磨损性能的四球法对不同品牌的5mm^(2)/s航空润滑油进行试验,对试验后的钢球表面形貌与组成特征进行研究。研究结果显示,不同配方体系,对四球试验过程抗磨添加剂行为特征影响明显,主要表现在磨斑直径、表面平滑度、边... 采用测定润滑油抗磨损性能的四球法对不同品牌的5mm^(2)/s航空润滑油进行试验,对试验后的钢球表面形貌与组成特征进行研究。研究结果显示,不同配方体系,对四球试验过程抗磨添加剂行为特征影响明显,主要表现在磨斑直径、表面平滑度、边缘平滑度以及磨斑表面化学组成变化。 展开更多
关键词 5mm^(2)/s航空润滑油 四球机试验 抗磨添加剂
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氢冷发电机气密性试验不合格原因分析与处理
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作者 徐进 刘龙 +2 位作者 苏剑 张文兵 王义 《电力安全技术》 2025年第1期56-59,共4页
通过对一起氢冷发电机气密性试验不合格的原因进行分析,从安装与制造的角度找出了影响气密性的因素,制定了处理方案并实施,使发电机气密性试验结果符合相关规范要求,保障了机组安全稳定运行。
关键词 氢冷发电机 密封油系统 气密性试验 密封瓦
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基于介质响应原理的变压器油纸绝缘测试实验平台设计 被引量:1
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作者 邹阳 黄煜 +3 位作者 方梦泓 石松浩 姚雨佳 高伟 《实验技术与管理》 北大核心 2025年第1期176-183,共8页
油纸绝缘作为电力变压器中的主绝缘设备,在工业生产和电力传输应用中尤为重要,为验证油纸绝缘的性能状态,该文研制了基于介质响应原理的现场可编程电力电子控制实验平台。平台以LabVIEW编程环境和三电极测试装置作为载体,采用状态机框... 油纸绝缘作为电力变压器中的主绝缘设备,在工业生产和电力传输应用中尤为重要,为验证油纸绝缘的性能状态,该文研制了基于介质响应原理的现场可编程电力电子控制实验平台。平台以LabVIEW编程环境和三电极测试装置作为载体,采用状态机框架设计了回复电压谱与极化谱测量流程,并嵌入聚类云模型算法实现油纸绝缘状态精准分类。该实验平台可促进理论知识与实践经验相结合的教学模式革新,满足实验探索、科学研究等多层次需求。 展开更多
关键词 油纸绝缘 实验平台设计 回复电压测试 数字编程控制
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准噶尔盆地非常规储层水力压裂监测技术进展 被引量:3
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作者 张士诚 李建民 +5 位作者 许江文 谢勃勃 王明星 吕振虎 李嘉成 杨鹏 《天然气工业》 北大核心 2025年第4期70-84,共15页
准噶尔盆地非常规油气资源丰富,勘探开发潜力巨大,但水力压裂开发过程中面临着储层改造体积有限、油气采出程度低和开发成本高等挑战,亟需明确地下储层水力裂缝展布形态,解决水力压裂优化设计难题。为此,在系统总结北美非常规储层水力... 准噶尔盆地非常规油气资源丰富,勘探开发潜力巨大,但水力压裂开发过程中面临着储层改造体积有限、油气采出程度低和开发成本高等挑战,亟需明确地下储层水力裂缝展布形态,解决水力压裂优化设计难题。为此,在系统总结北美非常规储层水力压裂监测试验关键认识的基础上,聚焦玛湖凹陷致密砾岩油藏和吉木萨尔凹陷页岩油藏开展的水力压裂现场监测试验,系统梳理井下鹰眼监测、DAS管外光纤监测和大斜度取心试验的结果,揭示了非常规油气储层增产改造机制,为国内非常规储层压裂优化设计和裂缝监测解释提供了依据。研究结果表明:①储层非均质性增强导致水平井段内各簇孔眼冲蚀程度差异更加明显,多簇裂缝扩展形态非均衡程度更强;②提升排量能够有效促进多簇裂缝均匀改造,而差异化布孔和段内暂堵压裂不能完全解决多裂缝非均衡扩展问题;③玛湖砾岩井下取心结果显示水力裂缝空间分布不均匀,人工裂缝数量远大于射孔簇数;④储层中穿砾裂缝数量是绕砾裂缝的2倍左右,两类水力裂缝均以高角度为主,裂缝走向与最大水平主应力方向一致;⑤支撑剂在水平方向上主要集中在10~23 m内,垂向上主要集中在20~25 m范围内;⑥砾石颗粒越大、砾石排列方向与裂缝扩展方向夹角越大,水力裂缝越容易穿过砾石。结论认为:压裂结束后段簇间的产液贡献能力存在动态变化,储层综合品质、压裂改造程度与压后产能的联系仍需进一步研究;现场系统监测结果对完善非常规油气藏压裂优化设计、推动水力压裂技术发展具有重要意义,技术体系还需整体谋划和系统推进水力压裂试验场研究。 展开更多
关键词 准噶尔盆地 玛湖砾岩油藏 吉木萨尔页岩油 水力压裂现场监测试验 井下鹰眼监测 分布式光纤监测 大斜度井取心试验
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劣质原油加工设备腐蚀防控关键技术挑战与对策 被引量:1
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作者 朱亚东 《炼油技术与工程》 2025年第5期61-64,共4页
以炼化企业加工劣质原油所带来的腐蚀问题为切入点,系统梳理炼化设备典型腐蚀机理、损伤形态、影响因素和控制措施,多维度分析了当前劣质原油加工设备腐蚀防控所面临的关键挑战,并提出了涵盖工程设计理念优化、原料质量管理创新、设备... 以炼化企业加工劣质原油所带来的腐蚀问题为切入点,系统梳理炼化设备典型腐蚀机理、损伤形态、影响因素和控制措施,多维度分析了当前劣质原油加工设备腐蚀防控所面临的关键挑战,并提出了涵盖工程设计理念优化、原料质量管理创新、设备选材优化、腐蚀监测与检测手段升级和腐蚀管理体系完善等内容的应对策略,旨在为炼油厂提供全面且有效的腐蚀防控思路,供其在构建高效劣质原油加工设备全流程腐蚀防控体系时借鉴。 展开更多
关键词 劣质原油 设备腐蚀 监控检测 防控措施 设计理念 原料管理 选材优化 腐蚀管理体系
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阳春砂挥发油含量测定方法的建立
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作者 蔡清梅 钟子充 +4 位作者 黄东海 汤丽云 胡国弟 黄彩沙 何国振 《核农学报》 北大核心 2025年第12期2690-2699,共10页
为建立阳春砂挥发油的专用测定方法,以解决生产和科研过程中其测定结果差异大、可重复性差的难题,本研究根据《中华人民共和国药典2020年版四部》中的水蒸气蒸馏法,选择加水量、粉碎程度、冷凝水温度、微沸时间、供试品重量5个对阳春砂... 为建立阳春砂挥发油的专用测定方法,以解决生产和科研过程中其测定结果差异大、可重复性差的难题,本研究根据《中华人民共和国药典2020年版四部》中的水蒸气蒸馏法,选择加水量、粉碎程度、冷凝水温度、微沸时间、供试品重量5个对阳春砂挥发油含量影响较大的因素,进行正交设计试验并筛选出具有显著影响的变量开展进一步试验,确定最佳的挥发油含量测定方法并用该法测定不同产地阳春砂的挥发油含量。结果表明,具有显著影响的变量为粉碎程度;不过筛,混合提取5 h时的挥发油含量最高;最佳的阳春砂挥发油含量测定工艺参数为加水量为500 mL、粉碎方式为粉碎5~40 s(不过筛,混合)冷凝水温度为28℃(或室温)、微沸时间为5 h、供试品重量为15 g。使用该法测得不同产地的挥发油含量从高到低为:西双版纳>春湾、怀集、文山二>广宁赤坑、文山一>广宁禾仓、那软、蟠龙、合水、韶关。本研究建立了阳春砂挥发油含量测定的新方法,可提高实际生产和科研过程中测定的稳定性和可重复性。 展开更多
关键词 阳春砂 挥发油 正交试验
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