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猴耳环双标多测法及抗氧化、α-葡萄糖苷酶抑制活性成分快速筛选法的建立 被引量:1
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作者 吴嘉琳 李志超 +3 位作者 纪温铎 傅咏梅 张蜀 邓红 《中药材》 CAS 北大核心 2024年第2期390-397,共8页
目的:建立猴耳环中5个成分的双标多测法及其抗氧化、α-葡萄糖苷酶抑制活性成分的快速筛选法。方法:采用HPLC法,以双标线性校正法准确定位猴耳环中5个成分色谱峰,以没食子酸为参照物,计算没食子酸与其余4个成分的相对校正因子,对各成分... 目的:建立猴耳环中5个成分的双标多测法及其抗氧化、α-葡萄糖苷酶抑制活性成分的快速筛选法。方法:采用HPLC法,以双标线性校正法准确定位猴耳环中5个成分色谱峰,以没食子酸为参照物,计算没食子酸与其余4个成分的相对校正因子,对各成分进行定量,将所得结果与外标法进行比较。采用离线DPPH-HPLC法及亲和超滤液相联用法快速筛选猴耳环中具有抗氧化、α-葡萄糖苷酶抑制活性成分。结果:双标线性校正法相比于相对保留时间更能准确地预测待测组分在未知色谱柱上的保留时间;相对校正因子法和外标法结果的RSD<2.00%。采用离线DPPH-HPLC法及亲和超滤液相联用法可以快速筛选出猴耳环中7-没食子酰基特利色黄烷、杨梅苷等不同程度抗氧化活性和α-葡萄糖苷酶抑制活性的化合物。结论:该研究建立的双标多测同时测定猴耳环中5个成分的方法准确可行,采用离线DPPH-HPLC法及亲和超滤液相联用法能快速、灵敏、高通量筛选猴耳环中的抗氧化和α-葡萄糖苷酶抑制活性成分。 展开更多
关键词 猴耳环 双标多测法 离线dpph-hplc 亲和超滤液相联用法
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Peak Detection Implementation for Real-Time Signal Analysis Based on FPGA 被引量:1
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作者 Alperen Mustafa Colak Taito Manabe +1 位作者 Yuichiro Shibata Fujio Kurokawa 《Circuits and Systems》 2018年第10期148-167,共20页
In this paper a real-time peak detection method based on modified Automatic Multiscale Field Detection (AMPD) algorithm and Field Programmable Gate Arrays (FPGA) technologies of a time series data is studied, and opti... In this paper a real-time peak detection method based on modified Automatic Multiscale Field Detection (AMPD) algorithm and Field Programmable Gate Arrays (FPGA) technologies of a time series data is studied, and optimum scaling is highlighted after testing several scales. To validate the results obtained from modified algorithm, they are compared with the results of original AMPD method. As data of this study, three-phase voltage values of a power station are used. A detail detective sensitivity analysis of phase-to-phase voltage values is tried at different scales. Moreover, the original algorithm is tested regarding the off-line mode to obtain optimum scaling for real-time peak point detection. It is concluded that the peak detection of minimum and maximum points of data series achieved by modified algorithm is very close to the results of original AMPD algorithm. 展开更多
关键词 AMPD ALGORITHM off-line method FPGA PEAK Detection
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Cross-sections of the ^(238)U(n,γ) ^(239)U reaction in the 3.0-7.0 MeV energy region measured by relative activation method
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作者 温淳 韩正 罗小兵 《Chinese Physics C》 SCIE CAS CSCD 2023年第2期107-115,共9页
The reaction cross-sections of^(238)U(n,γ)^(239)U have been experimentally determined at neutron energies of6.117±0.119 MeV,4.626±0.086 MeV,and 3.622±0.348 MeV employing the relative activation approac... The reaction cross-sections of^(238)U(n,γ)^(239)U have been experimentally determined at neutron energies of6.117±0.119 MeV,4.626±0.086 MeV,and 3.622±0.348 MeV employing the relative activation approach along with the off-line γ-ray spectroscopy method.The D(d,n)3He reaction was utilized to obtain monoenergetic neutrons of the required energy,and the^(197)Au(n,γ)^(198)Au reaction cross-sections were adopted as the referential standard to ascertain the neutron capture cross-sections of^(238)U.Furthermore,the effects of low-energy scattered neutrons,neutron fluence fluctuations,counting of geometric corrections when measuring γ-rays,and neutron and γ-ray self-absorption caused by the sample thickness have been considered and revised in the present work.For a comparison with experimental results,the cross-sections of the^(238)U(n,γ)^(239)U reaction were calculated theoretically with the original parametric TALYS-1.9 program.The experimental measurements were in contrast to previous experimental re sults and the evaluation data available for ROSFOND-2010,CENDL-3.2 and ENDF/B-VIII.0. 展开更多
关键词 ^(238)U(n γ)^(239)U reaction neutron capture cross-sections off-lineγ-rays spectroscopy method TALYS-1.9 program
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