Geomechanical properties of rocks vary across different measurement scales,primarily due to heterogeneity.Micro-scale geomechanical tests,including micro-scale“scratch tests”and nano-scale nanoindentation tests,are ...Geomechanical properties of rocks vary across different measurement scales,primarily due to heterogeneity.Micro-scale geomechanical tests,including micro-scale“scratch tests”and nano-scale nanoindentation tests,are attractive at different scales.Each method requires minimal sample volume,is low cost,and includes a relatively rapid measurement turnaround time.However,recent micro-scale test results–including scratch test results and nanoindentation results–exhibit tangible variance and uncertainty,suggesting a need to correlate mineral composition mapping to elastic modulus mapping to isolate the relative impact of specific minerals.Different research labs often utilize different interpretation methods,and it is clear that future micro-mechanical tests may benefit from standardized testing and interpretation procedures.The objectives of this study are to seek options for standardized testing and interpretation procedures,through two specific objectives:(1)Quantify chemical and physical controls on micro-mechanical properties and(2)Quantify the source of uncertainties associated with nanoindentation measurements.To reach these goals,we conducted mechanical tests on three different scales:triaxial compression tests,scratch tests,and nanoindentation tests.We found that mineral phase weight percentage is highly correlated with nanoindentation elastic modulus distribution.Finally,we conclude that nanoindentation testing is a mineralogy and microstructure-based method and generally yields significant uncertainty and overestimation.The uncertainty of the testing method is largely associated with not mapping pore space a priori.Lastly,the uncertainty can be reduced by combining phase mapping and modulus mapping with substantial and random data sampling.展开更多
Microstructural heterogeneity of low-permeability sandstone roofs of deep unmineable coal seams due to diagenesis significantly affects rock mechanical behavior,greatly impacting the sealing potential of in situ CO_(2...Microstructural heterogeneity of low-permeability sandstone roofs of deep unmineable coal seams due to diagenesis significantly affects rock mechanical behavior,greatly impacting the sealing potential of in situ CO_(2) sequestration and the structural stability of the geological formation.However,little is known about how the microstructure of different mineral groups influences the multiscale mechanical behavior of deep sandstone.This study proposes a new method for quantitatively characterizing the multiscale mechanical properties of low-permeability sandstone and shows the mechanisms responsible for mechanical failure at the micro-,meso-,and macroscale.Triaxial compression tests and targeted nanoindentation tests were conducted to assess the micro-and macroscale mechanical properties of different types of sandstone.The micro-and macroscale experiments were coupled with numerical simulations of compression using a unified cohesive model based on Voronoi polygons to clarify the multiscale mechanical behavior.The results indicate that quartz,the primary mineral component of the sandstones examined,exhibits the strongest micromechanical properties,followed by feldspar,calcite,and clay minerals.Compared to polycrystalline quartz,monocrystalline quartz has a more stable microstructure and is mechanically stronger.The macro-mechanical properties of tight sandstone samples are weakened by increased microstructural inhomogeneity and larger grain size.This leads to a higher likelihood of splitting damage,characterized by a high degree of discrete and weak stress sensitivity.The major conclusion is that the positive rhythm lithofacies of medium-grained sandstone to siltstone are the most favorable for efficient CO_(2) sequestration in deep unmineable coal seams.展开更多
The elastoplastic mechanical properties of the weld and heat affected zone metals have comparatively major impact on the forming process of tailor-welded blanks. A few scholars investigated the elastoplastic mechanica...The elastoplastic mechanical properties of the weld and heat affected zone metals have comparatively major impact on the forming process of tailor-welded blanks. A few scholars investigated the elastoplastic mechanical properties of the weld and heat affected zone, but they only simply assumed that it was a uniform distribution elastoplastic material different from the base materials. Four types of tailor-welded blanks which consist of ST12 and 304 stainless steel plates are selected as the research objects, the elastoplastic mechanical properties of the tailor-welded blanks weld and heat affected zone metals are obtained based on the nanoindentation tests, and the Erichsen cupping tests are conducted by combining numerical simulation with physical experiment. The nanoindentation tests results demonstrate that the elastoplastic mechanical properties of the weld and heat affected zone metals are not only different from the base materials, but also varying between the weld metals and the heat affected zone metals. Comparing the Erichsen cupping test resulted from numerical with that from experimental method, it is found that the numerical value of Erichsen cupping test which consider the elastoplastic mechanical properties of the weld and heat affected zone metals have a good agreement with the experimental result, and the relative error is only 4.8%. The proposed research provides good solutions for the inhomogeneous elastoplastic mechanical properties of the tailor-welded blanks weld and heat affected zone metals, and improves the control performance of tailor-welded blanks forming accuracy.展开更多
To characterize the elastic-plastic properties of thin film materials on elastic-plastic substrates,a simple theory model was proposed,which included three steps:dimensionless analysis,finite element modeling and data...To characterize the elastic-plastic properties of thin film materials on elastic-plastic substrates,a simple theory model was proposed,which included three steps:dimensionless analysis,finite element modeling and data fitting.The dimensionless analysis was applied to deriving two preliminary nondimensional relationships of the material properties,and finite element modeling and data fitting were carried out to establish their explicit forms.Numerical indentation tests were carried out to examine the effectiveness of the proposed model and the good agreement shows that the proposed theory model can be applied in practice.展开更多
Fe40Ni40P14B6 bulk metallic glass rods have been prepared by water quenching the fluxed alloy. The deformation behavior was investigated by nanoindentation tests and compressing tests. The average hardness and elastic...Fe40Ni40P14B6 bulk metallic glass rods have been prepared by water quenching the fluxed alloy. The deformation behavior was investigated by nanoindentation tests and compressing tests. The average hardness and elastic modulus of the as-prepared Fe40Ni40P14B6 BMG (bulk metallic glass) measured by nanoindentation tests are 8.347 and 176.61 GPa respectively. The displace- ment-load curve shows “pop-in” characteristics which correspond to the loading rate bursts. Many shear bands around the indent were observed. The as-prepared Fe-based BMG exhibits a compressive plastic strain of 5.21%, which is much larger than that of other Fe-based glassy alloys and most of other BMGs.展开更多
Based on the elastoplastic mechanical properties of the weld and heat affected zone metals obtained by a nanoindentation test, a theoretical calculation model was established for the forming limit diagram（FLD） of ta...Based on the elastoplastic mechanical properties of the weld and heat affected zone metals obtained by a nanoindentation test, a theoretical calculation model was established for the forming limit diagram（FLD） of tailor-welded blanks（TWBs） on the basis of plastic constitutive relations and Hosford yield criteria. Hemispherical punch bulging tests were performed to verify the FLD theoretical calculation results. The results demonstrated that not only the FLD theoretical calculation of base materials but also that of TWBs had a good agreement with their experiments. Besides, poorer formability of TWBs caused its FLD significantly lower than that of base materials. The theoretical calculation model offers a reliable approach to obtain the specific FLD of TWBs.展开更多
Effects of cold rolling deformation on the microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel （HNASS） are investigated. Microstructure characterization shows that 70% cold rolli...Effects of cold rolling deformation on the microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel （HNASS） are investigated. Microstructure characterization shows that 70% cold rolling deformation results in significant refinement of the microstructure of this steel, with its average twin thickness reducing from 6.4 μm to 14 nm. Nanoindentation tests at different strain rates demonstrate that the hardness of the steel with nano-scale twins （nt-HNASS） is about 2 times as high as that of steel with micro-scale twins （mt-HNASS）. The hardness of nt-HNASS exhibits a pronounced strain rate dependence with a strain rate sensitivity （m value） of 0.0319, which is far higher than that of mt-HNASS （m = 0.0029）. nt-HNASS shows more significant load plateaus and a higher creep rate than mt-HNASS. Analysis reveals that higher hardness and larger m value of nt-HNASS arise from stronger strain hardening role, which is caused by the higher storage rate of dislocations and the interactions between dislocations and high density twins. The more significant load plateaus and higher creep rates of nt-HNASS are due to the rapid relaxation of the dislocation structures generated during loading.展开更多
Enzyme-induced carbonate precipitation(EICP)has emerged as an innovative soil stabilization technology to precipitate CaCO_(3)by catalyzing urea decomposition.Although extensive efforts have been made to increase the ...Enzyme-induced carbonate precipitation(EICP)has emerged as an innovative soil stabilization technology to precipitate CaCO_(3)by catalyzing urea decomposition.Although extensive efforts have been made to increase the calcium carbonate content(CCC)formed in the EICP process for the better biocementation effect,the cementability and micromechanical properties of CaCO_(3)are rarely known.A study of the cementitious characteristics and micromechanical properties of CaCO_(3)precipitates with different mixing percentages of crystal morphology is essential for soil improvement.In the present study,ultrasonic oscillation tests and nanoindentation tests were performed to investigate the cementability and micromechanical properties of CaCO_(3)precipitate.The results show that the cementability and micromechanical properties of CaCO_(3)precipitate are related to the composition of the crystal morphology.A high content of calcite is beneficial to improve the adhesion of calcium carbonate precipitate.Calcite has better mechanical properties(elastic modulus,hardness and ductility)than vaterite,and the presence of vaterite can significantly affect the measured value of mechanical properties in nanoindentation tests.The ductility of CaCO_(3)precipitate induced by crude soybean urease(CSU)is higher than that of CaCO_(3)precipitate induced by commercially available pure enzyme,suggesting that commercially available pure enzyme can be replaced by CSU for cost-effective field-scale engineering applications.This work can provide insight into optimizing the properties of CaCO_(3)precipitate from the micro-scale.展开更多
基金support of this project through the Southwest Regional Partnership on Carbon Sequestration(Grant No.DE-FC26-05NT42591)Improving Production in the Emerging Paradox Oil Play(Grant No.DE-FE0031775).
文摘Geomechanical properties of rocks vary across different measurement scales,primarily due to heterogeneity.Micro-scale geomechanical tests,including micro-scale“scratch tests”and nano-scale nanoindentation tests,are attractive at different scales.Each method requires minimal sample volume,is low cost,and includes a relatively rapid measurement turnaround time.However,recent micro-scale test results–including scratch test results and nanoindentation results–exhibit tangible variance and uncertainty,suggesting a need to correlate mineral composition mapping to elastic modulus mapping to isolate the relative impact of specific minerals.Different research labs often utilize different interpretation methods,and it is clear that future micro-mechanical tests may benefit from standardized testing and interpretation procedures.The objectives of this study are to seek options for standardized testing and interpretation procedures,through two specific objectives:(1)Quantify chemical and physical controls on micro-mechanical properties and(2)Quantify the source of uncertainties associated with nanoindentation measurements.To reach these goals,we conducted mechanical tests on three different scales:triaxial compression tests,scratch tests,and nanoindentation tests.We found that mineral phase weight percentage is highly correlated with nanoindentation elastic modulus distribution.Finally,we conclude that nanoindentation testing is a mineralogy and microstructure-based method and generally yields significant uncertainty and overestimation.The uncertainty of the testing method is largely associated with not mapping pore space a priori.Lastly,the uncertainty can be reduced by combining phase mapping and modulus mapping with substantial and random data sampling.
基金supported by the project from the Exploration and Development Research Institute of PetroChina Daqing Oilfield Companyfinancial support from the research by the National Natural Science Foundation of China(42402148)+1 种基金Sichuan Provincial Fund(24NSFSC4997)Guizhou Outstanding Young Science and Technology Talent Program(YQK[2023]012).
文摘Microstructural heterogeneity of low-permeability sandstone roofs of deep unmineable coal seams due to diagenesis significantly affects rock mechanical behavior,greatly impacting the sealing potential of in situ CO_(2) sequestration and the structural stability of the geological formation.However,little is known about how the microstructure of different mineral groups influences the multiscale mechanical behavior of deep sandstone.This study proposes a new method for quantitatively characterizing the multiscale mechanical properties of low-permeability sandstone and shows the mechanisms responsible for mechanical failure at the micro-,meso-,and macroscale.Triaxial compression tests and targeted nanoindentation tests were conducted to assess the micro-and macroscale mechanical properties of different types of sandstone.The micro-and macroscale experiments were coupled with numerical simulations of compression using a unified cohesive model based on Voronoi polygons to clarify the multiscale mechanical behavior.The results indicate that quartz,the primary mineral component of the sandstones examined,exhibits the strongest micromechanical properties,followed by feldspar,calcite,and clay minerals.Compared to polycrystalline quartz,monocrystalline quartz has a more stable microstructure and is mechanically stronger.The macro-mechanical properties of tight sandstone samples are weakened by increased microstructural inhomogeneity and larger grain size.This leads to a higher likelihood of splitting damage,characterized by a high degree of discrete and weak stress sensitivity.The major conclusion is that the positive rhythm lithofacies of medium-grained sandstone to siltstone are the most favorable for efficient CO_(2) sequestration in deep unmineable coal seams.
基金Supported by National Natural Science Foundation of China(Grant No.51275444)Specialized Research Fund for the Doctoral Program of Higher Education(Grant No.20121333110003)Natural Science Foundation-Steel and Iron Foundation of Hebei Province,China(Grant No.E2014203271)
文摘The elastoplastic mechanical properties of the weld and heat affected zone metals have comparatively major impact on the forming process of tailor-welded blanks. A few scholars investigated the elastoplastic mechanical properties of the weld and heat affected zone, but they only simply assumed that it was a uniform distribution elastoplastic material different from the base materials. Four types of tailor-welded blanks which consist of ST12 and 304 stainless steel plates are selected as the research objects, the elastoplastic mechanical properties of the tailor-welded blanks weld and heat affected zone metals are obtained based on the nanoindentation tests, and the Erichsen cupping tests are conducted by combining numerical simulation with physical experiment. The nanoindentation tests results demonstrate that the elastoplastic mechanical properties of the weld and heat affected zone metals are not only different from the base materials, but also varying between the weld metals and the heat affected zone metals. Comparing the Erichsen cupping test resulted from numerical with that from experimental method, it is found that the numerical value of Erichsen cupping test which consider the elastoplastic mechanical properties of the weld and heat affected zone metals have a good agreement with the experimental result, and the relative error is only 4.8%. The proposed research provides good solutions for the inhomogeneous elastoplastic mechanical properties of the tailor-welded blanks weld and heat affected zone metals, and improves the control performance of tailor-welded blanks forming accuracy.
基金Projects(50531060,10525211,10828205)supported by the National Natural Science Foundation of ChinaProject(10525211)supported by National Science Found for Distinguished Young Scholars of ChinaProject(076044)supported by the Cultivation Fund of the Key Scientific and Technical Innovation Project,Ministry of Education of China
文摘To characterize the elastic-plastic properties of thin film materials on elastic-plastic substrates,a simple theory model was proposed,which included three steps:dimensionless analysis,finite element modeling and data fitting.The dimensionless analysis was applied to deriving two preliminary nondimensional relationships of the material properties,and finite element modeling and data fitting were carried out to establish their explicit forms.Numerical indentation tests were carried out to examine the effectiveness of the proposed model and the good agreement shows that the proposed theory model can be applied in practice.
文摘Fe40Ni40P14B6 bulk metallic glass rods have been prepared by water quenching the fluxed alloy. The deformation behavior was investigated by nanoindentation tests and compressing tests. The average hardness and elastic modulus of the as-prepared Fe40Ni40P14B6 BMG (bulk metallic glass) measured by nanoindentation tests are 8.347 and 176.61 GPa respectively. The displace- ment-load curve shows “pop-in” characteristics which correspond to the loading rate bursts. Many shear bands around the indent were observed. The as-prepared Fe-based BMG exhibits a compressive plastic strain of 5.21%, which is much larger than that of other Fe-based glassy alloys and most of other BMGs.
基金Project(51275444) supported by the National Natural Science Foundation of ChinaProject(20121333110003) supported by the Specialized Research Fund for the Doctoral Program of Higher Education,China+1 种基金Project(E2014203271) supported by the Natural Science Foundation–Steel and Iron Foundation of Hebei ProvinceChina
文摘Based on the elastoplastic mechanical properties of the weld and heat affected zone metals obtained by a nanoindentation test, a theoretical calculation model was established for the forming limit diagram（FLD） of tailor-welded blanks（TWBs） on the basis of plastic constitutive relations and Hosford yield criteria. Hemispherical punch bulging tests were performed to verify the FLD theoretical calculation results. The results demonstrated that not only the FLD theoretical calculation of base materials but also that of TWBs had a good agreement with their experiments. Besides, poorer formability of TWBs caused its FLD significantly lower than that of base materials. The theoretical calculation model offers a reliable approach to obtain the specific FLD of TWBs.
基金Project supported by the National Natural Science Foundations of China (Grant Nos.51371089 and 51201068)the National Key Basic Research and Development Program of China (Grant No.2010CB631001)
文摘Effects of cold rolling deformation on the microstructure, hardness, and creep behavior of high nitrogen austenitic stainless steel （HNASS） are investigated. Microstructure characterization shows that 70% cold rolling deformation results in significant refinement of the microstructure of this steel, with its average twin thickness reducing from 6.4 μm to 14 nm. Nanoindentation tests at different strain rates demonstrate that the hardness of the steel with nano-scale twins （nt-HNASS） is about 2 times as high as that of steel with micro-scale twins （mt-HNASS）. The hardness of nt-HNASS exhibits a pronounced strain rate dependence with a strain rate sensitivity （m value） of 0.0319, which is far higher than that of mt-HNASS （m = 0.0029）. nt-HNASS shows more significant load plateaus and a higher creep rate than mt-HNASS. Analysis reveals that higher hardness and larger m value of nt-HNASS arise from stronger strain hardening role, which is caused by the higher storage rate of dislocations and the interactions between dislocations and high density twins. The more significant load plateaus and higher creep rates of nt-HNASS are due to the rapid relaxation of the dislocation structures generated during loading.
基金the financial support of National Natural Science Foundation of China(Grant No.52378392)“Foal Eagle Program”Youth Top-notch Talent Project of Fujian Province(Grant No.00387088)Natural Science Foundation of Fujian Province(Grant No.2020J06013).
文摘Enzyme-induced carbonate precipitation(EICP)has emerged as an innovative soil stabilization technology to precipitate CaCO_(3)by catalyzing urea decomposition.Although extensive efforts have been made to increase the calcium carbonate content(CCC)formed in the EICP process for the better biocementation effect,the cementability and micromechanical properties of CaCO_(3)are rarely known.A study of the cementitious characteristics and micromechanical properties of CaCO_(3)precipitates with different mixing percentages of crystal morphology is essential for soil improvement.In the present study,ultrasonic oscillation tests and nanoindentation tests were performed to investigate the cementability and micromechanical properties of CaCO_(3)precipitate.The results show that the cementability and micromechanical properties of CaCO_(3)precipitate are related to the composition of the crystal morphology.A high content of calcite is beneficial to improve the adhesion of calcium carbonate precipitate.Calcite has better mechanical properties(elastic modulus,hardness and ductility)than vaterite,and the presence of vaterite can significantly affect the measured value of mechanical properties in nanoindentation tests.The ductility of CaCO_(3)precipitate induced by crude soybean urease(CSU)is higher than that of CaCO_(3)precipitate induced by commercially available pure enzyme,suggesting that commercially available pure enzyme can be replaced by CSU for cost-effective field-scale engineering applications.This work can provide insight into optimizing the properties of CaCO_(3)precipitate from the micro-scale.
