The flotation ofniobite, fersmite, and ilmenorutile was studied using 3 collectors with various concentration and pulp pH. The collecting property of different representative collectors was investigated. Experimental ...The flotation ofniobite, fersmite, and ilmenorutile was studied using 3 collectors with various concentration and pulp pH. The collecting property of different representative collectors was investigated. Experimental results show that diphosphonic acid is an effective collector for valuable niobium-containing minerals. A flotation recovery of 90.87%-91.7% is obtained with 75 mg/L diphosphonic acid at pH 2-4. The chemical adsorption of diphosphonic acid on these 3 minerals＇ surface might lead to the high recovery efficiency of the minerals, which is proved by IR and X-ray photoelectron spectroscopy spectra.展开更多
The effect of several collectors on the niobite synthetized under the condition of varying pH values and dosages were studied. The collecting property of several representative collectors was also investigated. The e...The effect of several collectors on the niobite synthetized under the condition of varying pH values and dosages were studied. The collecting property of several representative collectors was also investigated. The experimental result shows that di- phosphonic acid is a good collector for niobite. Its recovery is about 84.24%-91.17% when the pH value of the pulp is less than 5.0 and the dosage of diphosphonic acid is 140 mg/L. The sequences of the selectivity and collecting capacity of the collectors were compared. Infrared absorption spectrum (IAS) and X-ray photoelectron spectroscopy (XPS) were used to detect and analyze the ad- sorption mechanism of diphosphonic acid on the surface of niobite. The IAS result indicates that diphosphonic acid is indeed ad- sorbed on the surface of niobite, and the XPS result shows that the binding energy of P2p peak of niobite treated by diphosphonic acid has changed 2.85 eV. It confirms that the adsorption belongs to a chemisorption type.展开更多
A new process is proposed for refining niobite ore that is found in Jiangxi province of China. Niobite, also known as columbite or niobite-tantalite, is a mineral that contains tantalum and niobium. The separation pro...A new process is proposed for refining niobite ore that is found in Jiangxi province of China. Niobite, also known as columbite or niobite-tantalite, is a mineral that contains tantalum and niobium. The separation process includes two-stage grinding, gravity concentration, magnetic separation, and flotation. The tan- talum/niobium concentrate obtained had a grade of Ta2O5 18.28%, Nb2O5 41.62% at a recovery rate of Ta2O5 49.08%, Nb205 70.77%. Other minerals occurring along with the niobite, such as zinnwaldite, feld- spar, and quartz, were also recovered to comprehensively utilize this ore.展开更多
Lithium niobate on insulator(LNOI) provides a platform for the fundamental physics investigations and practical applications of integrated photonics. However, as an indispensable building block of integrated photonics...Lithium niobate on insulator(LNOI) provides a platform for the fundamental physics investigations and practical applications of integrated photonics. However, as an indispensable building block of integrated photonics, lasers are in short supply. In this paper, erbium-doped LNOI laser in the 1550-nm band was demonstrated in microdisk cavities with high quality factors fabricated in batches by UV exposure, inductively coupled plasma reactive ion etching, and chemomechanical polishing. The threshold and conversion efficiency of the erbium-doped LNOI microdisk laser were measured to be lower than 1 m W and 6.5×10^(-5)%, respectively. This work will benefit the development of integrated photonics based on LNOI.展开更多
文摘The flotation ofniobite, fersmite, and ilmenorutile was studied using 3 collectors with various concentration and pulp pH. The collecting property of different representative collectors was investigated. Experimental results show that diphosphonic acid is an effective collector for valuable niobium-containing minerals. A flotation recovery of 90.87%-91.7% is obtained with 75 mg/L diphosphonic acid at pH 2-4. The chemical adsorption of diphosphonic acid on these 3 minerals＇ surface might lead to the high recovery efficiency of the minerals, which is proved by IR and X-ray photoelectron spectroscopy spectra.
文摘The effect of several collectors on the niobite synthetized under the condition of varying pH values and dosages were studied. The collecting property of several representative collectors was also investigated. The experimental result shows that di- phosphonic acid is a good collector for niobite. Its recovery is about 84.24%-91.17% when the pH value of the pulp is less than 5.0 and the dosage of diphosphonic acid is 140 mg/L. The sequences of the selectivity and collecting capacity of the collectors were compared. Infrared absorption spectrum (IAS) and X-ray photoelectron spectroscopy (XPS) were used to detect and analyze the ad- sorption mechanism of diphosphonic acid on the surface of niobite. The IAS result indicates that diphosphonic acid is indeed ad- sorbed on the surface of niobite, and the XPS result shows that the binding energy of P2p peak of niobite treated by diphosphonic acid has changed 2.85 eV. It confirms that the adsorption belongs to a chemisorption type.
基金the Geological Survey Program fromthe Ministry of Land and Resources of China (No. 1212010816036)and the National Department Public Benefit Research Foundation from Ministry of Land and Resources of China (No. 201011031)Zhengzhou Institute of Multipurpose Utilization of Mineral Resources CAGS,for financial support and approval of this paper for publication
文摘A new process is proposed for refining niobite ore that is found in Jiangxi province of China. Niobite, also known as columbite or niobite-tantalite, is a mineral that contains tantalum and niobium. The separation process includes two-stage grinding, gravity concentration, magnetic separation, and flotation. The tan- talum/niobium concentrate obtained had a grade of Ta2O5 18.28%, Nb2O5 41.62% at a recovery rate of Ta2O5 49.08%, Nb205 70.77%. Other minerals occurring along with the niobite, such as zinnwaldite, feld- spar, and quartz, were also recovered to comprehensively utilize this ore.
基金supported by the National Key Research and Development Program of China (Grant No. 2019YFA0705000)the National Natural Science Foundation of China (Grant Nos. 12034010, 11734009, 11674181,11674184, and 11774182)+2 种基金the Higher Education Discipline Innovation Project (Grant No. B07013)the National Science Fund for Talent Training in the Basic Sciences (Grant No. J1103208)the Program for Changjiang Scholars and Innovative Research Team in University (PCSIRT)(Grant No. IRT_13R29)。
文摘Lithium niobate on insulator(LNOI) provides a platform for the fundamental physics investigations and practical applications of integrated photonics. However, as an indispensable building block of integrated photonics, lasers are in short supply. In this paper, erbium-doped LNOI laser in the 1550-nm band was demonstrated in microdisk cavities with high quality factors fabricated in batches by UV exposure, inductively coupled plasma reactive ion etching, and chemomechanical polishing. The threshold and conversion efficiency of the erbium-doped LNOI microdisk laser were measured to be lower than 1 m W and 6.5×10^(-5)%, respectively. This work will benefit the development of integrated photonics based on LNOI.
