In-situ TiB_(2)/Al–Cu composite was processed by multidirectional forging(MDF)for six passes.The microstructure evolution of the forged workpiece was examined across various regions.The mechanical properties of the a...In-situ TiB_(2)/Al–Cu composite was processed by multidirectional forging(MDF)for six passes.The microstructure evolution of the forged workpiece was examined across various regions.The mechanical properties of the as-cast and MDFed composites were compared,and their strengthening mechanisms were analyzed.Results indicate that the grain refinement achieved through the MDF process is mainly due to the subdivision of the original grains through mechanical geometric fragmentation and the occurrence of dynamic recrystallization(DRX).DRX grains are formed through discontinuous DRX,continuous DRX,and recrystallization induced by particle-stimulated nucleation.A rise in accumulated equivalent strain(Σ?ε)results in finerα-Al grains and a more uniform distribution of TiB_(2)particles,which enhance the Vickers hardness of the composite.In addition,the tensile properties of the MDFed composite significantly improve compared with those of the as-cast composites,with ultimate tensile strength and yield strength increasing by 51.2%and 54%,respectively.This enhancement is primarily due to grain refinement strengthening and dislocation strengthening achieved by the MDF process.展开更多
The effects of sub-transus(α+β)annealing treatment(ST),followed by single aging(SA)or duplex aging(DA)on the microstructural evolution and mechanical properties of near-βTi-4Al-1Sn-2Zr-5Mo-8V-2.5Cr(mass fraction,%)...The effects of sub-transus(α+β)annealing treatment(ST),followed by single aging(SA)or duplex aging(DA)on the microstructural evolution and mechanical properties of near-βTi-4Al-1Sn-2Zr-5Mo-8V-2.5Cr(mass fraction,%)alloy were investigated using optical microscopy,scanning electron microscopy,and transmission electron microscopy.The results show that the finer secondaryαphase precipitates in the alloy after DA than SA(e.g.,149 nm for SA and 69 nm for DA,both after ST at 720℃).The main reason is that the pre-aging step(300℃)in the DA process leads to the formation of intermediateωphase nanoparticles,which assist in the nucleation of the acicular secondaryαphase precipitates.In addition,the strength of the alloy after DA is higher than that of SA at the specific ST temperature.A good combination is achieved in the alloy subjected to ST at 750℃,followed by DA(UTS:1450 MPa,EL:3.87%),which is due to the precipitation of nanoscale secondaryαphase by DA.In conclusion,DA is a feasible process for this new near-βtitanium alloy.展开更多
TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging(MDF)and extrusion(EX).The grain size of the nanocomposite after MDF+EX multi-step deformation was sig...TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging(MDF)and extrusion(EX).The grain size of the nanocomposite after MDF+EX multi-step deformation was significantly decreased compared with that processed only by MDF.The average size of the recrystallized grains gradually increased after EX with increasing the number of MDF passes at 270℃.However,the grain size significantly decreased by MDF processing at 310℃.Both fine and coarse MgZn2 phases appeared in the(MDF+EX)-processed nanocomposites,and their volume fractions gradually increased with increasing the number of MDF passes before EX.Ultrahigh tensile properties(yield strength of^404 MPa,ultimate tensile strength of^450.3 MPa and elongation of^5.2%)were obtained in the nanocomposite after three MDF passes at 310℃ followed by EX.This was attributed to the refinement of the recrystallized grains,together with the improved Orowan strengthening provided by the precipitated MgZn2 particles that were generated by MDF+EX multi-step deformation.展开更多
The multidirectional forging （MDF） process was conducted at temperature of 753 K to optimize the mechanical properties of as-homogenized Mg-13Gd-4Y-2Zn-0.6Zr alloy containing long-period stacking ordered phase. The ...The multidirectional forging （MDF） process was conducted at temperature of 753 K to optimize the mechanical properties of as-homogenized Mg-13Gd-4Y-2Zn-0.6Zr alloy containing long-period stacking ordered phase. The effects of MDF passes on microstructure evolution and mechanical properties were also investigated. The results show that both the volume fraction of dynamic recrystallization （DRX） grains and mechanical properties of the deformed alloy enhanced with MDF passes increasing till seven passes. The average grain size decreased from 76 to 2.24 μm after seven passes, while the average grain size increased to 7.12 μm after nine passes. The microstructure after seven passes demonstrated randomly oriented fine DRX grains and larger basal （0001）〈1120〉 Schmid factor of 0.31. The superior mechanical properties at room temperature （RT） with ultimate tensile strength （UTS） of 416 MPa and fracture elongation of 4.12% can be obtained after seven passes. The mechanical properties at RT after nine passes are inferior to those after seven passes due to the coarsening of DRX grains, which can be ascribed to the static recovery resulting from the repeated heating at the interval of MDF passes. The elevated temperature mechanical properties of the deformed alloy after seven passes and nine passes were investigated. When test temperature was below 523 K, the elevated temperature tensile yield strength and UTS after seven passes are superior to those after nine passes, while they are inferior to that after nine passes as temperature exceeds 523 K.展开更多
Grain refinement is one of the successful and low-cost methods to develop metals having excellent combination of strength and ductility. Low carbon steel was deformed by using multidirectional forging (MDF) technique ...Grain refinement is one of the successful and low-cost methods to develop metals having excellent combination of strength and ductility. Low carbon steel was deformed by using multidirectional forging (MDF) technique at room temperature. The influence of strain amount and annealing process on the microstructure and mechanical properties of investigated steel was studied. The grain refinement mechanism was studied by the microstructure observation. The results showed that the grain refinement was attained by multidirectional forging technique. The initial coarser grains of average 38 μm size fragmented into very fine ferrite with grain sizes of about 1.2 μm. After MDF, the strength properties improved significantly, although uniform elongation and elongation decreased with increasing strain.展开更多
To explore ambient strengthening and high temperature ductility,a combined forming approach of multidirectional forging and asymmetric rolling was proposed.A novel multicomponent ultralight Mg-3.11Li-2.31Al-1.95Sn-0.9...To explore ambient strengthening and high temperature ductility,a combined forming approach of multidirectional forging and asymmetric rolling was proposed.A novel multicomponent ultralight Mg-3.11Li-2.31Al-1.95Sn-0.94Y-0.45Er alloy was fabricated.The microstructural evolution and mechanical properties were investigated by microstructural characterization and tensile test.The combined forming results in remarkable grain refinement.The ultimate tensile strength and elongation of(255±7)MPa and 24.9%,respectively,were obtained at room temperature.The contribution of various strengthening mechanisms of the rolled alloy was obtained.Microstructural examination revealed the occurrence of dynamic recrystallization at 473-573 K and dynamic grain growth at 573-623 K.The maximum elongation of 293.9%was demonstrated at 623 K and 5×10^(-4)s^(-1).The dominate deformation mechanism at elevated temperatures is dislocation viscous glide.展开更多
The deformation mechanism,microstructure evolution,and precipitation behavior of a Mg-8.9Gd-1.8Y-0.5Zr-0.2Ag(wt.%)alloy multi-directionally forged at three different temperatures were investigated.As the forging tempe...The deformation mechanism,microstructure evolution,and precipitation behavior of a Mg-8.9Gd-1.8Y-0.5Zr-0.2Ag(wt.%)alloy multi-directionally forged at three different temperatures were investigated.As the forging temperature increases,the particle-stimulated nucleation(PSN)effect diminishes as the num-ber of dynamic precipitates decreases,pyramidal slip is activated,grain boundary migration accelerates,and continuous dynamic recrystallization(CDRX)dominates.The microstructures varied greatly,although fine-grained structures were formed at all different forging temperatures.Competitive precipitation be-tween dynamic precipitate growth,dislocation-induced precipitation,and homogeneous precipitation was observed after aging treatment.Among them,the medium temperature(748 K)forged and aged alloy ex-hibits the best mechanical performance,with an ultimate tensile strength of 436 MPa,and elongation of 16.3%.The calculation indicates that the mixed precipitation structure containing theβprecipitate band provides a 35%higher strengthening contribution than the typical homogeneously distributed precipi-tates.The formation of precipitation-free zones(PFZs)ensures that aging will not cause a dramatic de-crease in ductility,which provides a reference for the industrial preparation of high-performance wrought Mg-Gd series alloys.展开更多
Al7075 sheets are widely used in aerospace industry and their higher strength-plasticity collaborative improvement requirement is urgent.In this study,the microstructure inheriting the evolution and me-chanical proper...Al7075 sheets are widely used in aerospace industry and their higher strength-plasticity collaborative improvement requirement is urgent.In this study,the microstructure inheriting the evolution and me-chanical properties of Al7075 sheets during multidirectional rotary forging(MRF)and T6 heat treatment are analyzed.The results show that the average grain size exhibits near-parabolic evolution with increas-ing MRF deformation amount.MRF20%+T6(20%MRF deformation amount+T6)condition possesses the largest grain size of 72.6μm,and its abnormal grain growth mechanism is that the medium deformation energy and high deformation heterogeneity in MRF20%deformed grains could cause asynchronous re-crystallization behavior during T6 heat treatment,and the grains with comparatively higher deformation energy get recrystallized firstly and devour adjacent grains along preferred011or223misorientation axis.MRF70%+T6 condition possesses the finest grain size of 14.2μm,and its fine grain inheriting mech-anism is that the uniformly high deformation energy in MRF70%deformed grains causes uniformly rapid recrystallization,and rapidly recrystallized grains effectively suppress grain boundary motion from adja-cent grains.With increasing MRF deformation amount,tensile strength and elongation values both exhibit near-antiparabolic evolution.MRF70%+T6 condition possesses the largest tensile strength(563 MPa)and elongation(17.73%),which increases by 8.27%and 80.55%compared to as-annealed+T6(MRF0%+T6)condition(tensile strength is 520 MPa and elongation is 9.82%),respectively.The strength-plasticity col-laborative improvement is mainly because the combination of effectively inherited fine grains,refined inclusion particles,and uniformly distributed fineη’particles after T6 heat treatment could promote smooth dislocation movement and coordinated slip behavior in most matrix grains,which contributes to the delay of stress localization and strength-plasticity collaborative improvement.展开更多
Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged...Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged alloy were analyzed.Results show that dynamic recrystallization(DRX)occurs and second phase particles precipitate along the grain boundary during the MDF process.After annealing treatment(T4),the volume fraction and size of dynamic precipitates slightly increase at a lower temperature(430℃)compared with those of MDFed sample,while they are dissolved into theα-Mg matrix at a higher temperature(450℃).At the meantime,short plate-shaped long-period stacking ordered(LPSO)phases are observed in the DRX grains of the MDFed sample and then dissolved into theα-Mg matrix during annealing at both temperatures.Typical basal texture is identified in the MDFed sample,but the basal pole tilts away from final forging direction and rare-earth texture component with<1121>orientation parallel to penultimate forging direction becomes visible after annealing.The T6 sample annealing at 430℃for 4 h and ageing at 200℃for 34 h exhibits the superior strength and ductility in this study.The ultimate tensile strength,tensile yield strength and elongation to failure,which is 455 MPa,308 MPa and 7.7%,respectively,are overall improved compared with the directly-aged(T5)sample.This paper provides a superior heat treatment schedule to manufacture high-performance large-scale Mg-Gd-Y-Zn-Zr-Ag components for industrial production.展开更多
基金supported by the Key Program for International Cooperation of the Ministry of Science and Technology,China(No.ZCGX2022001L)。
文摘In-situ TiB_(2)/Al–Cu composite was processed by multidirectional forging(MDF)for six passes.The microstructure evolution of the forged workpiece was examined across various regions.The mechanical properties of the as-cast and MDFed composites were compared,and their strengthening mechanisms were analyzed.Results indicate that the grain refinement achieved through the MDF process is mainly due to the subdivision of the original grains through mechanical geometric fragmentation and the occurrence of dynamic recrystallization(DRX).DRX grains are formed through discontinuous DRX,continuous DRX,and recrystallization induced by particle-stimulated nucleation.A rise in accumulated equivalent strain(Σ?ε)results in finerα-Al grains and a more uniform distribution of TiB_(2)particles,which enhance the Vickers hardness of the composite.In addition,the tensile properties of the MDFed composite significantly improve compared with those of the as-cast composites,with ultimate tensile strength and yield strength increasing by 51.2%and 54%,respectively.This enhancement is primarily due to grain refinement strengthening and dislocation strengthening achieved by the MDF process.
基金the financial supports from the Key Research and Development Program of Shanxi Province,China(Nos.201903D421084,201903D121056)the National Natural Science Foundation of China(Nos.52171122,52071228,51901151)。
文摘The effects of sub-transus(α+β)annealing treatment(ST),followed by single aging(SA)or duplex aging(DA)on the microstructural evolution and mechanical properties of near-βTi-4Al-1Sn-2Zr-5Mo-8V-2.5Cr(mass fraction,%)alloy were investigated using optical microscopy,scanning electron microscopy,and transmission electron microscopy.The results show that the finer secondaryαphase precipitates in the alloy after DA than SA(e.g.,149 nm for SA and 69 nm for DA,both after ST at 720℃).The main reason is that the pre-aging step(300℃)in the DA process leads to the formation of intermediateωphase nanoparticles,which assist in the nucleation of the acicular secondaryαphase precipitates.In addition,the strength of the alloy after DA is higher than that of SA at the specific ST temperature.A good combination is achieved in the alloy subjected to ST at 750℃,followed by DA(UTS:1450 MPa,EL:3.87%),which is due to the precipitation of nanoscale secondaryαphase by DA.In conclusion,DA is a feasible process for this new near-βtitanium alloy.
基金Projects(51771129,51401144,51771128)supported by the National Natural Science Foundation of China,Project supported by the Outstanding Innovative Teams of Higher Learning Institutions of Shanxi,ChinaProjects(2015021067,201601D011034)supported by the Natural Science Foundation of Shanxi Province,China+1 种基金Project(201703D421039)supported by the International Cooperation in Shanxi,ChinaProject supported by the China Scholarship Council。
文摘TiC nanoparticle-reinforced Mg−4Zn−0.5Ca matrix nanocomposites were processed by combining multidirectional forging(MDF)and extrusion(EX).The grain size of the nanocomposite after MDF+EX multi-step deformation was significantly decreased compared with that processed only by MDF.The average size of the recrystallized grains gradually increased after EX with increasing the number of MDF passes at 270℃.However,the grain size significantly decreased by MDF processing at 310℃.Both fine and coarse MgZn2 phases appeared in the(MDF+EX)-processed nanocomposites,and their volume fractions gradually increased with increasing the number of MDF passes before EX.Ultrahigh tensile properties(yield strength of^404 MPa,ultimate tensile strength of^450.3 MPa and elongation of^5.2%)were obtained in the nanocomposite after three MDF passes at 310℃ followed by EX.This was attributed to the refinement of the recrystallized grains,together with the improved Orowan strengthening provided by the precipitated MgZn2 particles that were generated by MDF+EX multi-step deformation.
基金sponsored by the Scientific Research Foundation for the Returned Overseas Chinese Scholars,State Education Ministry
文摘The multidirectional forging （MDF） process was conducted at temperature of 753 K to optimize the mechanical properties of as-homogenized Mg-13Gd-4Y-2Zn-0.6Zr alloy containing long-period stacking ordered phase. The effects of MDF passes on microstructure evolution and mechanical properties were also investigated. The results show that both the volume fraction of dynamic recrystallization （DRX） grains and mechanical properties of the deformed alloy enhanced with MDF passes increasing till seven passes. The average grain size decreased from 76 to 2.24 μm after seven passes, while the average grain size increased to 7.12 μm after nine passes. The microstructure after seven passes demonstrated randomly oriented fine DRX grains and larger basal （0001）〈1120〉 Schmid factor of 0.31. The superior mechanical properties at room temperature （RT） with ultimate tensile strength （UTS） of 416 MPa and fracture elongation of 4.12% can be obtained after seven passes. The mechanical properties at RT after nine passes are inferior to those after seven passes due to the coarsening of DRX grains, which can be ascribed to the static recovery resulting from the repeated heating at the interval of MDF passes. The elevated temperature mechanical properties of the deformed alloy after seven passes and nine passes were investigated. When test temperature was below 523 K, the elevated temperature tensile yield strength and UTS after seven passes are superior to those after nine passes, while they are inferior to that after nine passes as temperature exceeds 523 K.
文摘Grain refinement is one of the successful and low-cost methods to develop metals having excellent combination of strength and ductility. Low carbon steel was deformed by using multidirectional forging (MDF) technique at room temperature. The influence of strain amount and annealing process on the microstructure and mechanical properties of investigated steel was studied. The grain refinement mechanism was studied by the microstructure observation. The results showed that the grain refinement was attained by multidirectional forging technique. The initial coarser grains of average 38 μm size fragmented into very fine ferrite with grain sizes of about 1.2 μm. After MDF, the strength properties improved significantly, although uniform elongation and elongation decreased with increasing strain.
基金supported by the National Natural Science Foundation of China(No.51334006)。
文摘To explore ambient strengthening and high temperature ductility,a combined forming approach of multidirectional forging and asymmetric rolling was proposed.A novel multicomponent ultralight Mg-3.11Li-2.31Al-1.95Sn-0.94Y-0.45Er alloy was fabricated.The microstructural evolution and mechanical properties were investigated by microstructural characterization and tensile test.The combined forming results in remarkable grain refinement.The ultimate tensile strength and elongation of(255±7)MPa and 24.9%,respectively,were obtained at room temperature.The contribution of various strengthening mechanisms of the rolled alloy was obtained.Microstructural examination revealed the occurrence of dynamic recrystallization at 473-573 K and dynamic grain growth at 573-623 K.The maximum elongation of 293.9%was demonstrated at 623 K and 5×10^(-4)s^(-1).The dominate deformation mechanism at elevated temperatures is dislocation viscous glide.
基金supported by the National Key R&D Program of China(No.2021YFB3701100).
文摘The deformation mechanism,microstructure evolution,and precipitation behavior of a Mg-8.9Gd-1.8Y-0.5Zr-0.2Ag(wt.%)alloy multi-directionally forged at three different temperatures were investigated.As the forging temperature increases,the particle-stimulated nucleation(PSN)effect diminishes as the num-ber of dynamic precipitates decreases,pyramidal slip is activated,grain boundary migration accelerates,and continuous dynamic recrystallization(CDRX)dominates.The microstructures varied greatly,although fine-grained structures were formed at all different forging temperatures.Competitive precipitation be-tween dynamic precipitate growth,dislocation-induced precipitation,and homogeneous precipitation was observed after aging treatment.Among them,the medium temperature(748 K)forged and aged alloy ex-hibits the best mechanical performance,with an ultimate tensile strength of 436 MPa,and elongation of 16.3%.The calculation indicates that the mixed precipitation structure containing theβprecipitate band provides a 35%higher strengthening contribution than the typical homogeneously distributed precipi-tates.The formation of precipitation-free zones(PFZs)ensures that aging will not cause a dramatic de-crease in ductility,which provides a reference for the industrial preparation of high-performance wrought Mg-Gd series alloys.
基金supported by the National Natural Science Foundation of China(No.U21A20131)the Technical Development Project of COMAC Shanghai Aircraft Manufacturing Co.,Ltd.(No.COMAC-SFGS-2023-631)the 111 Project(No.B17034),andthe In-novative Research Team Development Program of Ministry of Edu-cation of China(No.IRT17R83).
文摘Al7075 sheets are widely used in aerospace industry and their higher strength-plasticity collaborative improvement requirement is urgent.In this study,the microstructure inheriting the evolution and me-chanical properties of Al7075 sheets during multidirectional rotary forging(MRF)and T6 heat treatment are analyzed.The results show that the average grain size exhibits near-parabolic evolution with increas-ing MRF deformation amount.MRF20%+T6(20%MRF deformation amount+T6)condition possesses the largest grain size of 72.6μm,and its abnormal grain growth mechanism is that the medium deformation energy and high deformation heterogeneity in MRF20%deformed grains could cause asynchronous re-crystallization behavior during T6 heat treatment,and the grains with comparatively higher deformation energy get recrystallized firstly and devour adjacent grains along preferred011or223misorientation axis.MRF70%+T6 condition possesses the finest grain size of 14.2μm,and its fine grain inheriting mech-anism is that the uniformly high deformation energy in MRF70%deformed grains causes uniformly rapid recrystallization,and rapidly recrystallized grains effectively suppress grain boundary motion from adja-cent grains.With increasing MRF deformation amount,tensile strength and elongation values both exhibit near-antiparabolic evolution.MRF70%+T6 condition possesses the largest tensile strength(563 MPa)and elongation(17.73%),which increases by 8.27%and 80.55%compared to as-annealed+T6(MRF0%+T6)condition(tensile strength is 520 MPa and elongation is 9.82%),respectively.The strength-plasticity col-laborative improvement is mainly because the combination of effectively inherited fine grains,refined inclusion particles,and uniformly distributed fineη’particles after T6 heat treatment could promote smooth dislocation movement and coordinated slip behavior in most matrix grains,which contributes to the delay of stress localization and strength-plasticity collaborative improvement.
基金supported by National Natural Science Foundation of China(Grant No.51874367 and 51574291)。
文摘Multidirectional forging(MDF)was successfully applied to fabricate large-size Mg-Gd-Y-Zn-Zr-Ag alloy in this work and effects of T4,T5 and T6 treatments on the microstructure and mechanical properties of the as-forged alloy were analyzed.Results show that dynamic recrystallization(DRX)occurs and second phase particles precipitate along the grain boundary during the MDF process.After annealing treatment(T4),the volume fraction and size of dynamic precipitates slightly increase at a lower temperature(430℃)compared with those of MDFed sample,while they are dissolved into theα-Mg matrix at a higher temperature(450℃).At the meantime,short plate-shaped long-period stacking ordered(LPSO)phases are observed in the DRX grains of the MDFed sample and then dissolved into theα-Mg matrix during annealing at both temperatures.Typical basal texture is identified in the MDFed sample,but the basal pole tilts away from final forging direction and rare-earth texture component with<1121>orientation parallel to penultimate forging direction becomes visible after annealing.The T6 sample annealing at 430℃for 4 h and ageing at 200℃for 34 h exhibits the superior strength and ductility in this study.The ultimate tensile strength,tensile yield strength and elongation to failure,which is 455 MPa,308 MPa and 7.7%,respectively,are overall improved compared with the directly-aged(T5)sample.This paper provides a superior heat treatment schedule to manufacture high-performance large-scale Mg-Gd-Y-Zn-Zr-Ag components for industrial production.
