In this paper, the mixture of dimethyl carbonate, ethyl methyl carbonate and diethyl carbonate was separated by middle-vessel batch distillation with feeding in middle-vessel and process control characteristics were r...In this paper, the mixture of dimethyl carbonate, ethyl methyl carbonate and diethyl carbonate was separated by middle-vessel batch distillation with feeding in middle-vessel and process control characteristics were researched. The steady state simulation results in Aspen Plus were exported to Aspen Dynamics. Then control effect of liquid level control with HighSelector, composition control(structure1, structure2) and temperature control(proportional action, proportional integration action) were proposed. Composition control structure 2 and temperature control with PI action were investigated to achieve a good control effect.展开更多
Dividing wall batch distillation with middle vessel(DWBDM)is a new type of batch distillation column,with outstanding advantages of low capital cost,energy saving and flexible operation.However,temperature control of ...Dividing wall batch distillation with middle vessel(DWBDM)is a new type of batch distillation column,with outstanding advantages of low capital cost,energy saving and flexible operation.However,temperature control of DWBDM process is challenging,since inherently dynamic and highly nonlinear,which make it difficult to give the controller reasonable set value or optimal temperature profile for temperature control scheme.To overcome this obstacle,this study proposes a new strategy to develop temperature control scheme for DWBDM combining neural network soft-sensor with fuzzy control.Dynamic model of DWBDM was firstly developed and numerically solved by Python,with three control schemes:composition control by PID and fuzzy control respectively,and temperature control by fuzzy control with neural network soft-sensor.For dynamic process,the neural networks with memory functions,such as RNN,LSTM and GRU,are used to handle with time-series data.The results from a case example show that the new control scheme can perform a good temperature control of DWBDM with the same or even better product purities as traditional PID or fuzzy control,and fuzzy control could reduce the effect of prediction error from neural network,indicating that it is a highly feasible and effective control approach for DWBDM,and could even be extended to other dynamic processes.展开更多
基金Supported by the National Natural Science Foundation of China(21676299,21476261,21506255)
文摘In this paper, the mixture of dimethyl carbonate, ethyl methyl carbonate and diethyl carbonate was separated by middle-vessel batch distillation with feeding in middle-vessel and process control characteristics were researched. The steady state simulation results in Aspen Plus were exported to Aspen Dynamics. Then control effect of liquid level control with HighSelector, composition control(structure1, structure2) and temperature control(proportional action, proportional integration action) were proposed. Composition control structure 2 and temperature control with PI action were investigated to achieve a good control effect.
基金supported by Beijing Natural Science Foundation(2222037)the Special Educating Project of the Talent for Carbon Peak and Carbon Neutrality of University of Chinese Academy of Sciences(Innovation of talent cultivation model for“dual carbon”in chemical engineering industry,E3E56501A2).
文摘Dividing wall batch distillation with middle vessel(DWBDM)is a new type of batch distillation column,with outstanding advantages of low capital cost,energy saving and flexible operation.However,temperature control of DWBDM process is challenging,since inherently dynamic and highly nonlinear,which make it difficult to give the controller reasonable set value or optimal temperature profile for temperature control scheme.To overcome this obstacle,this study proposes a new strategy to develop temperature control scheme for DWBDM combining neural network soft-sensor with fuzzy control.Dynamic model of DWBDM was firstly developed and numerically solved by Python,with three control schemes:composition control by PID and fuzzy control respectively,and temperature control by fuzzy control with neural network soft-sensor.For dynamic process,the neural networks with memory functions,such as RNN,LSTM and GRU,are used to handle with time-series data.The results from a case example show that the new control scheme can perform a good temperature control of DWBDM with the same or even better product purities as traditional PID or fuzzy control,and fuzzy control could reduce the effect of prediction error from neural network,indicating that it is a highly feasible and effective control approach for DWBDM,and could even be extended to other dynamic processes.