Textured surfaces with certain micro/nano structures have been proven to possess some advanced functions,such as reducing friction,improving wear and increasing wettability.Accurate prediction of micro/nano surface te...Textured surfaces with certain micro/nano structures have been proven to possess some advanced functions,such as reducing friction,improving wear and increasing wettability.Accurate prediction of micro/nano surface textures is of great significance for the design,fabrication and application of functional textured surfaces.In this paper,based on the kinematic analysis of cutter teeth,the discretization of ultrasonic machining process,transformation method of coordinate systems and the cubic spline data interpolation,an integrated theoretical model was established to characterize the distribution and geometric features of micro textures on the surfaces machined by different types of ultrasonic vibration-assisted milling(UVAM).Based on the theoretical model,the effect of key process parameters(vibration directions,vibration dimensions,cutting parameters and vibration parameters)on tool trajectories and microtextured surface morphology in UVAM is investigated.Besides,the effect of phase difference on the elliptical shape in 2D/3D ultrasonic elliptical vibration-assisted milling(UEVAM)was analyzed.Compared to conventional numerical models,the method of the cubic spline data interpolation is applied to the simulation of microtextured surface morphology in UVAM,which is more suitable for characterizing the morphological features of microtextured surfaces than traditional methods due to the presence of numerous micro textures.The prediction of surface roughness indicates that the magnitude of ultrasonic amplitude in z-direction should be strictly limited in 1D rotary UVAM,2D and 3D UEVAM due to the unfavorable effect of axial ultrasonic vibration on the surface quality.This study can provide theoretical guidance for the design and fabrication of microtextured surfaces in UVAM.展开更多
During the metal cutting process,especially in continuous contact conditions like turning,the challenge of lubricants failing to effectively reach the cutting point remains unresolved.Micro-textured cutting tools offe...During the metal cutting process,especially in continuous contact conditions like turning,the challenge of lubricants failing to effectively reach the cutting point remains unresolved.Micro-textured cutting tools offer a potential solution for tool-chip contact challenges.Inspired by the evolutionary achievements of the biosphere,micro-textures are expected to overcome lubrication limitations in cutting zones.Drawing on the anti-gravity water transport seen at the mouth edge of the Nepenthes plant,an innovative microchannel with Nepenthes-shaped contours was designed on the rake face to enable controlled lubricant transport.However,the dynamics of lubricant delivery on textured surfaces are not fully understood.This study first analyzed the microstructure and water transport mechanism of Nepenthes to reconstruct a micro-textured surface for controlled lubricant transport.A dynamic model was then developed to describe lubricant transport within open microchannels,with mathematical simulations predicting transport speed and flow distance.To validate this model,diffusion experiments of alumina soybean oil nanolubricant on polycrystalline diamond(PCD)cutting tool surfaces were conducted,showing an average prediction deviation of 5.01%.Compared with the classical Lucas-Washburn model,the new model improved prediction accuracy by 4.72%.Additionally,comparisons were made to examine droplet spreading and non-uniform diffusion on textured surfaces,revealing that the T2 surface exhibited the strongest unidirectional diffusion characteristics.The contact angle ratio,droplet unidirectional spreading ratio,and droplet spreading aspect ratio were 0.48,1.75,and 3.99,respectively.Finally,the anti-wear,friction-reducing,and efficiency-enhancing mechanisms of micro-textured surfaces in minimum quantity lubrication turning were analyzed.This approach may support continuous cutting of difficult-tomachine materials.展开更多
The microstructure and mechanical properties of Inconel 617 alloy rolled at room temperature with different deformation degrees(20%,50%,70%)were investigated.The grain refinement mechanism and main texture types of In...The microstructure and mechanical properties of Inconel 617 alloy rolled at room temperature with different deformation degrees(20%,50%,70%)were investigated.The grain refinement mechanism and main texture types of Inconel 617 alloy during rolling were analyzed via electron backscatter diffraction and X-ray diffraction,and the microhardness and tensile properties of Inconel 617 alloy with different deformation degrees were tested.Results reveal that the grains of Inconel 617 alloy are refined during the rolling deformation process,and the refinement mechanism is the fragmentation of original grains caused by the increase in dislocation density and strain gradient.The main microtextures of the rolled samples are Goss{011}<001>,Rotated Goss{110}<110>,Brass{011}<211>,and P{011}<112>textures,and their intensity is increased with increase in deformation degree.After rolling deformation,the strength of the Inconel 617 alloy is improved and the ductility is reduced by the combined effect of grain refinement and dislocation strengthening.Comprehensively,the yield strength and elongation of Inconel 617 alloy after 20%deformation are 772.48 MPa and 0.1962,respectively,presenting good synergy effect.展开更多
Static recrystallization(SRX)characteristics of a powder metallurgy superalloy were investigated by isothermal compression at 1080–1170℃ under strain rates of 0.01–0.1 s^(−1),strains of 0.1,0.22,or 0.5,and holding ...Static recrystallization(SRX)characteristics of a powder metallurgy superalloy were investigated by isothermal compression at 1080–1170℃ under strain rates of 0.01–0.1 s^(−1),strains of 0.1,0.22,or 0.5,and holding time of 0–300 s.The impacts of temperature,strain rate,holding time,and strain on the SRXed grain size,volume fraction,and microtexture were explored by electron backscatter diffraction technique.It was found that temperature played a key role in these processes.As SRX progressed,the<110>fiber parallel to the axis compression direction gradually weakened and was replaced by the<001>fiber because<001>was the preferred recrystallization orientation and grain growth direction for the Ni-based superalloy.Moreover,high temperatures and low strain rates promoted the formation of the<001>fiber.Three nucleation mechanisms during SRX process were found:grain boundary bulging,primary twin assistance,and subgrain coalescence.Grain boundary bulging occurred under all process conditions;however,at low temperatures and high strain rates,the latter two mechanisms could provide additional nucleation modes.In addition,SRX size and volume fraction models were established.展开更多
The microstructural evolution of banded 5A90 A1-Li alloy during superplastic deformation at 475℃ with an initial strain rate of 8× 10^-4 S^-1 was studied using EBSD technique. The results showed that, before def...The microstructural evolution of banded 5A90 A1-Li alloy during superplastic deformation at 475℃ with an initial strain rate of 8× 10^-4 S^-1 was studied using EBSD technique. The results showed that, before deformation, the grain shape appeared to be banded, the most grain boundaries belonged to low-angle boundaries, and the initial sheet had a dominate of { 110}（112） brass texture. During deformation, there were grain growth, grain shape change, misorientation increasing and textural weakening. The fraction of high-angle boundaries increased rapidly once the flow stress reached the peak value. Corresponding deformation mechanism for various stages of deformation was suggested. Dislocation activity was the dominant mechanism in the first stage, then dynamic recrystallization occurred, and grain rotation was expected as an accommodation for grain boundary sliding （GBS）. At large strains, GBS was the main mechanism.展开更多
Rapid solidification of undercooled Ni-15%Cu （mole fraction） alloy was studied using glass fluxing and cyclic superheating. To show the effect of cooling history on the microstrucyure and microtexture evolution, the...Rapid solidification of undercooled Ni-15%Cu （mole fraction） alloy was studied using glass fluxing and cyclic superheating. To show the effect of cooling history on the microstrucyure and microtexture evolution, the as-solidified samples were either cooled naturally or quenched into water after recalescence. At low undercooling, grain-refined microstructure has a random texture and a highly oriented texture without annealing twins for the case of naturally cooling and quenching, respectively. At high undercooling, a fully random texture as well as a number of annealing twins are observed, and recrystallization and grain growth independently happen on the cooling history. Fluid flow and recrystallization play an important role in the microtexture formation for grain refinement at both low and high undercooling.展开更多
In this paper, the orange peel defect in the surface range of the st14 steel sheet has been investigated using the electron backscattered diffraction (EBSD) technique. It has been found that the orange peel defect in ...In this paper, the orange peel defect in the surface range of the st14 steel sheet has been investigated using the electron backscattered diffraction (EBSD) technique. It has been found that the orange peel defect in the st14 steel sheet was resulted from the local coarse grains which were produced during hot-rolling due to the critical deformation in dual-phase zone. During deep drawing, the coarse grains with {100}<001> microtexture can slip on the {112}<111> slip system to form bulging and yields orange peel defects, while the coarse grains with {112}<110> orientation do not form the defect as the Schmid factor of {112}<111> slip system in it equals zero.展开更多
The mineral assemblage and content and surface microtextures of slipping zone soil of several landslides in the Three Gorges Reservoir District have been analyzed using the scanning electron microscope (SEM) and X-ray...The mineral assemblage and content and surface microtextures of slipping zone soil of several landslides in the Three Gorges Reservoir District have been analyzed using the scanning electron microscope (SEM) and X-ray diffractometer (XRD). All the mineral assemblages are similar in these landslides. The main minerals are montmorillonite, illite, kaolinite, chlorite, quartz and feldspar. There are two kinds of surface microtexture in the slipping zone soil, i.e., linear scratches and arcuate scratches. Based on analyses of the changes of the microtextures, one can obtain information about the number, directions and stages of landslide movements. The authors have also studied the mechanism of landslide formation, evaluated the stability of landslides and revival possibility of ancient landslides and forecasted the activity of similar landslides in different districts. The surface microtexture features of stable landslides and mobile landslides are summarized and it is concluded that the existence of filamentous bacteria may result in or increase movements of landslides.展开更多
Nickel liner of shaped charge with nano-sized grains was prepared by electroforming technique and the ultra-highstrain-rate deformation was performed by explosive detonation.The as-electroformed and post-deformed micr...Nickel liner of shaped charge with nano-sized grains was prepared by electroforming technique and the ultra-highstrain-rate deformation was performed by explosive detonation.The as-electroformed and post-deformed microstructures of electroformed nickel liner of shaped charge were observed by optical metallography(OM),scanning electron microscopy(SEM) and transmission electron microscopy(TEM) and the orientation distribution of the grains was analyzed by electron backscattering pattern(EBSP) technique.Both melting phenomenon in the jet fragment and recovery and recrystallization in the slug after ultra-high-strain-rate deformation were observed.The research evidence shows that dynamic recovery and recrystallization play an important role in ultra-high-strain-rate deformation for electroformed nickel liner of shaped charge with nano-sized grain.展开更多
Variant selection under specific applied stresses during precipitation of a plates from prior-βmatrix in Ti-6 Al-4 V was investigated by 3 D phase field simulations.The model incorporates the Burgers transformation p...Variant selection under specific applied stresses during precipitation of a plates from prior-βmatrix in Ti-6 Al-4 V was investigated by 3 D phase field simulations.The model incorporates the Burgers transformation path fromβto a phase,with consideration of interfacial energy anisotropy,externally applied stresses and elastic interactions among a variants andβmatrix.The Gibbs free energy and atomic mobility data are taken from available thermodynamic and kinetic databases.It was found that external stresses have a profound influence on variant selection,and the selection has a sensitive dependence,as evidenced by both interaction energy calculations and phase field simulations.Compared with normal stresses,shear stresses applied in certain directions were found more effective in accelerating the transformation,with a stronger preference to fewer variants.The volume fractions of various a variants and the final microstructure were determined by both the external stress and the elastic interaction among different variants.The a clusters formed by variants with Type2 misorientation([11-20]/60°)relation were found more favored than those with Type4([-1055-3]/63.26°)under certain applied tensile stress such as along<111>β.The mechanical properties of different microstructures from our phase field simulation under different conditions were calculated for different loading conditions,utilizing crystal plastic finite element simulation.The mechanical behavior of the various microstructures from phase field simulation can be evaluated well before the alloys are fabricated,and therefore it is possible to select microstructure for optimizing the mechanical properties of the alloy through thermomechanical processing based on the two types of simulations.展开更多
Constraints from P-T pseudosections （MnNCKFMASH system）, foliation intersection/ inflection axes preserved in porphyroblasts （FIAs）, mineral assemblages and textural relationships for rocks containing all three Al...Constraints from P-T pseudosections （MnNCKFMASH system）, foliation intersection/ inflection axes preserved in porphyroblasts （FIAs）, mineral assemblages and textural relationships for rocks containing all three Al2 SiO5 polymorphs indicate a kyanite→ andalusite→ sillimanite sequential formation at different times rather than stable coexistence at the Al2SiO5 triple point. All three Al2SiO5 polymorphs grew in the Chl, Bt, Ms, Grt, St, Pl and Crd bearing Ordovician Clayhole Schist in Balcooma, northeastern Australia separately along a looped P-T-t-D path that swaps from clockwise to anticlockwise in the tectono-metamorphic history of the region. Kyanite grew during crustal thickening in an Early Silurian Orogenic event followed by decompression/heating, andalusite and fibrolitic sillimanite growth during Early Devonian exhumation.展开更多
Corrosion re sistance of Zircaloy-4 alloy tube in superheated steam at 673 K/10.3 MPa is anisotropic.A part of the surface undergoes uniform corrosion while the other suffers nodular corrosion.Narrow and wide nodules ...Corrosion re sistance of Zircaloy-4 alloy tube in superheated steam at 673 K/10.3 MPa is anisotropic.A part of the surface undergoes uniform corrosion while the other suffers nodular corrosion.Narrow and wide nodules are observed after an exposure period of 3 and 30 days,respectively.A new matrix transformation method is established in order to study the formation mechanism of nodules in the cross-section(CS) of Zircaloy-4 alloy tube using the EBSD technique,while the CS perpendicular to axial direction(AD).The results reveal that the microtexture is a key factor behind the two types of corrosion.Furthermore,the oxide layers grow anisotropically over the corroded surface.A thick oxide layer forms over the nodular corrosion region on the grains with c-axis oriented in the range of 40° around tangential direction(TD),whereas a thin oxide layer over the uniform corrosion region is detected on the grains with c-axis oriented in the range of 68° around TD.In short,the anisotropic growth of oxide layer was caused by the change of microtexture of the Zr-4 alloy tube,and this anisotropic growth of oxide layer contributed to the nodules formation.展开更多
Apparent differences in sedimentation and diagenesis exist between carbonate reservoirs in different areas and affect their petrophysical and elastic properties.To elucidate the relevant mechanism,we study and analyze...Apparent differences in sedimentation and diagenesis exist between carbonate reservoirs in different areas and affect their petrophysical and elastic properties.To elucidate the relevant mechanism,we study and analyze the characteristics of rock microstructure and elastic properties of carbonates and their variation regularity using 89 carbonate samples from the different areas The results show that the overall variation regularities of the physical and elastic properties of the carbonate rocks are controlled by the microtextures of the microcrystalline calcite,whereas the traditional classification of rock-and pore-structures is no longer applicable.The micrite microtextures can be divided,with respect to their morphological features,into porous micrite,compact micrite,and tight micrite.As the micrites evolves from the first to the last type,crystal boundaries are observed with increasingly close coalescence,the micritic intercrystalline porosity and pore-throat radius gradually decrease;meanwhile,the rigidity of the calcite microcrystalline particle boundary and elastic homogeneity are enhanced.As a result,the seismic elastic characteristics,such as permeability and velocity of samples,show a general trend of decreasing with the increase of porosity.For low-porosity rock samples(φ<5%)dominated by tight micrite,the micritic pores have limited contributions to porosity and permeability and the micrite elastic properties are similar to those of the rock matrix.In such cases,the macroscopic physical and elastic properties are more susceptible to the formation of cracks and dissolution pores,but these features are controlled by the pore structure.The pore aspect ratio can be used as a good indication of pore types.The bulk modulus aspect ratio for dissolution pores is greater than 0.2,whereas that of the intergranular pores ranges from 0.1 to 0.2.The porous and compact micrites are observed to have a bulk modulus aspect ratio less than 0.1,whereas the ratio of the tight micrite approaches 0.2。展开更多
Fisher Island and Broknes Peninsula in the Larsemann Hills constitute part of a polar lowland periglacial environment between marine and glacial ecosystems. The landscape is characterized by gently rolling hills and b...Fisher Island and Broknes Peninsula in the Larsemann Hills constitute part of a polar lowland periglacial environment between marine and glacial ecosystems. The landscape is characterized by gently rolling hills and broad valleys interspersed with lakes formed in glacially scoured basins. We analyzed the physieochemical parameters and the ionic constituents of water samples from 10 lakes in each of these two locations. Our results showed considerable differences between the two regions and demon- strated the influence of lithology and processes including weathering, evaporation, and atmospheric precipitation. All major cations and anions in the lake waters showed positive correlations indicating balanced ionic concentrations. Unconsolidated sediments were sparsely distributed and scattered over glacial deposits, valley fills, and occasional moraine ridges. The type and rate of sedi- mentation was mainly controlled by surface run-off and aeolian influx. The sediment samples from lake beds and the catchment area on Fisher Island were immature and poorly to very poorly sorted, consisting of gravelly sand with negligible silt and finer fractions. Sediments had a polymodal grain size distribution with the two major populations lying between -2 and 1 phi and be- tween 0 and 1.5 phi. The sediments were lithic arenite to arkosic in composition and the microtextures imprinted over quartz grains were dominated by mechanical textures resulting from several stages of glacial crushing and grinding. The presence of deep disso- lution cavities, cryptocrystalline precipitation, and euhedral crystal growth signified the effect of chemical activity after the deposition of grains in the lacustrine environment.展开更多
Ti2 AlNb-based alloy powder metallurgy(PM)compacts were prepared via hot isostatic pressing(HIP)under relatively low temperature(920 and 980℃)and at certain pressure(130 MPa).The microstructure,composition and orient...Ti2 AlNb-based alloy powder metallurgy(PM)compacts were prepared via hot isostatic pressing(HIP)under relatively low temperature(920 and 980℃)and at certain pressure(130 MPa).The microstructure,composition and orientation of B2,α2 and O phases in the compacts were characterized and analyzed with an aim to investigate the effect of unsuitable HIPping parameters on the appearance of prior particle boundary(PPB),which seriously affects the mechanical properties of the alloy.The results show that moreα2 phase is the characteristics of the PPB in Ti2AlNb-based alloy when HIPped at relatively low temperature.Increasing HIPping temperature to the upper part of the two-phase region can effectively inhibit the formation of PPB.Electron backscatter diffraction measurements show the specific orientation relationship between phases,which helps us understand the origin of a2 and O phase and the corresponding transformation path.The HIPping at a higher temperature can weaken the micro-texture intensity of theα2 and O phase due to the increase of misorientation in B2 phase.Theα2 phase at cell wall keeps the Burgers orientation relationship(BOR)with the grain on one side,and does not satisfy the BOR with the other.It is found that some O phase variants inside the cell HIPped at 980℃can only maintainα2-O OR withα2 owing to theα2→O phase transformation forming the O phase,while these O variants deviate from B2-O OR with B2 phase.展开更多
Most of past researches on the skid resistance/road wetness relationship deal with thick water depths （〉 1 mm）. Questions remain as to the variation of skid resistance with thin water films and the transition betwe...Most of past researches on the skid resistance/road wetness relationship deal with thick water depths （〉 1 mm）. Questions remain as to the variation of skid resistance with thin water films and the transition between the dry state and the so-called ＂damp＂ or ＂humid＂ state at which the skid resistance drop can be as high as 30%-40%. This paper deals with a theoretical and experimental assessment of the friction-water depth relationship. The main objective is to estimate local water depths trapped between the tire and the road asperities and to define a so-called ＂critical＂ water depth which can be used to detect risky situations for road users. Tests are performed in laboratory. It was found that the friction-water depth curves have an inverse-S shape and present an initial constant-friction part before decreasing to a minimum value. A ＂critical＂ water depth, defined as the water depth above which the friction coefficient collapses significantly, is determined from surface texture on critical water depth is discussed. observed friction-water depth curves. Influence of test speed and展开更多
Adequate pavement skid resistance is a key requirement for safe road operations.Unfortunately,the measurement and prediction of the skid resistance property of an in-service road pavement,or pavement mixture specimens...Adequate pavement skid resistance is a key requirement for safe road operations.Unfortunately,the measurement and prediction of the skid resistance property of an in-service road pavement,or pavement mixture specimens in the laboratory,is a highly challenging process from both theoretical and practical points of view.For more than 60 years,owing to the lack of theoretical solutions to the complex tire-fluid-pavement interaction problem,the practice of pavement skid resistance determination and prediction has essentially been derived from experimental and field observed data.The rapid development of efficient numerical computational techniques and high-power computing facilities in the last two decades made it possible for researchers to numerically solve the tire-fluidpavement interaction problem.It enables the numerical evaluation and prediction of high-speed wet skid resistance,and the determination of the tire-pavement kinetic friction coefficient in the evaluation of low-speed skid resistance.This paper presents a state-of-the-art review of the research development of theoretical mechanistic approaches in the determination and prediction of pavement skid resistance.It covers the following main aspects of the subject matter:(i)mechanisms of skid resistance generation in dry,wetted(i.e.,damp),wet and flooded pavements;(ii)theoretical evaluation of pavement skid resistance in dry,wetted,wet and flooded states;(iii)theoretical approaches in pavement skid resistance prediction;and(iv)concepts of representing the skid resistance state of pavement.The capability of finite element simulation approach for wet skid resistance evaluation with good accuracy is explained.Also highlighted is the practical significance of the Concept of Skid Resistance State.Areas of practical applications of the concept,coupled with the simulation model,are introduced.They include applications in driving safety analysis,road safety design and control,design of paving mixtures,safety maintenance and management of pavements,and harmonization of skid resistance measurements and predictions.展开更多
Nickel shaped-charge liners with nano-sized grains were prepared by the electroforming technique, and the deformation at ultrahigh strain rate was performed by explosive detonation. The as-formed and post-deformed mic...Nickel shaped-charge liners with nano-sized grains were prepared by the electroforming technique, and the deformation at ultrahigh strain rate was performed by explosive detonation. The as-formed and post-deformed microstructures of electroformed nickel shaped-charge liners with nano-sized grains were observed by means of transmission electron microscopy, and the orientation distribution of the grains was analyzed by the electron backscattering pattern （EBSP） technique. The melting phenomenon in the jet fragment and the recovery and recrystallization in the slug after plastic deformation at ultrahigh-strain rate were observed in the ultrafine-grained nickel shaped-charge liners. The research evidence shows that dynamic recovery and recrystallization play an important role in plastic deformation at ultrahigh strain rate.展开更多
Carbonate rocks are common in many parts of the world, including the Eastern Mediterranean, where they host significant groundwater supplies and are widely used as building and ornamental stones. The porosity of carbo...Carbonate rocks are common in many parts of the world, including the Eastern Mediterranean, where they host significant groundwater supplies and are widely used as building and ornamental stones. The porosity of carbonate rocks plays a critical role in fluid storage and retrieval. The pore structure connectivity, in particular, controls many properties of geological formations, as well as the relationships between the properties of individual minerals and the bulk properties of the rock. To study the relationships between porosity, rock properties, pore structure, pore size, and their impact on reservoir characteristics, 46 carbonate rock samples were collected from four stratigraphic sections exposed near Sidon, South Lebanon. The studied carbonate rocks are related to marine deposits of different ages(e.g., Upper Cretaceous, Eocene, and Upper Miocene). In order to understand the pore connectivity, the MICP(mercury injection capillary pressure) technique was conducted on ten representative samples. Results from the SEM analysis indicate the dominance of very fine and fine pore sizes, with various categories ranging in diameter from 0.1 to10 μm. The MICP data revealed that the pore throat radii vary widely from 0.001 to 1.4 μm, and that all samples are dominated by micropore throats. The grain size analysis indicated that the studied rocks have significant amounts of silt-and clay-size grains with respect to the coarser ‘sand-size’ particles, suggesting a high proportion of microporosity. Obtained results, such as the poorly-sorted nature of grains, high microporosity, and the high percentage of micropore throats, justify the observed low mean hydraulic radius, the high entry pressure, and the very low permeability of the studied samples. These results suggest that the carbonate rocks near Sidon(south of Lebanon) are possibly classified as non-reservoir facies.展开更多
The natural hydrophobicity of surfaces can be enhanced if they are microtextured due to air trapped in the structure, which provides the deposited drop with a composite surface made of solid and air on which it is res...The natural hydrophobicity of surfaces can be enhanced if they are microtextured due to air trapped in the structure, which provides the deposited drop with a composite surface made of solid and air on which it is rest. Here, a series of grating microstructure surfaces with different parameters have been designed and fabricated by a novel soft lithography. The water contact angles （WCA） on these rough surfaces are measured through optical contact angle meter. The results indicate that all the WCA on the surfaces with grating microstructures are up to 150~; WCA increases and the hydrophobic performance also enhances with the decrease of the ridge width under the other fixed parameter condition; Experimental data obtained basically consists with the Cassie＇s theoretical prediction. The effects of geometric parameters of the microstructures on wettability of the grating sufaces are investigated.展开更多
基金Supported by Shandong Provincial Natural Science Foundation of China(Grant No.ZR2023QE041)China Postdoctoral Science Foundation(Grant No.2023M731862)National Natural Science Foundation of China(Grant No.51975112).
文摘Textured surfaces with certain micro/nano structures have been proven to possess some advanced functions,such as reducing friction,improving wear and increasing wettability.Accurate prediction of micro/nano surface textures is of great significance for the design,fabrication and application of functional textured surfaces.In this paper,based on the kinematic analysis of cutter teeth,the discretization of ultrasonic machining process,transformation method of coordinate systems and the cubic spline data interpolation,an integrated theoretical model was established to characterize the distribution and geometric features of micro textures on the surfaces machined by different types of ultrasonic vibration-assisted milling(UVAM).Based on the theoretical model,the effect of key process parameters(vibration directions,vibration dimensions,cutting parameters and vibration parameters)on tool trajectories and microtextured surface morphology in UVAM is investigated.Besides,the effect of phase difference on the elliptical shape in 2D/3D ultrasonic elliptical vibration-assisted milling(UEVAM)was analyzed.Compared to conventional numerical models,the method of the cubic spline data interpolation is applied to the simulation of microtextured surface morphology in UVAM,which is more suitable for characterizing the morphological features of microtextured surfaces than traditional methods due to the presence of numerous micro textures.The prediction of surface roughness indicates that the magnitude of ultrasonic amplitude in z-direction should be strictly limited in 1D rotary UVAM,2D and 3D UEVAM due to the unfavorable effect of axial ultrasonic vibration on the surface quality.This study can provide theoretical guidance for the design and fabrication of microtextured surfaces in UVAM.
基金Supported by National Natural Science Foundation of China(Grant Nos.52375447,52305477 and 52105457)Shandong Provincial Natural Science Foundation(Grant Nos.ZR2023QE057,ZR2024QE100 and ZR2024ME255)+2 种基金Qingdao Municipal Science and Technology Planning Park Cultivation Plan(Grant No.23-1-5-yqpy-17-qy)the Science and Technology SMEs Innovation Capacity Improvement Project of Shandong Province(Grant No.2022TSGC1115)the Special Fund of Taishan Scholars Project。
文摘During the metal cutting process,especially in continuous contact conditions like turning,the challenge of lubricants failing to effectively reach the cutting point remains unresolved.Micro-textured cutting tools offer a potential solution for tool-chip contact challenges.Inspired by the evolutionary achievements of the biosphere,micro-textures are expected to overcome lubrication limitations in cutting zones.Drawing on the anti-gravity water transport seen at the mouth edge of the Nepenthes plant,an innovative microchannel with Nepenthes-shaped contours was designed on the rake face to enable controlled lubricant transport.However,the dynamics of lubricant delivery on textured surfaces are not fully understood.This study first analyzed the microstructure and water transport mechanism of Nepenthes to reconstruct a micro-textured surface for controlled lubricant transport.A dynamic model was then developed to describe lubricant transport within open microchannels,with mathematical simulations predicting transport speed and flow distance.To validate this model,diffusion experiments of alumina soybean oil nanolubricant on polycrystalline diamond(PCD)cutting tool surfaces were conducted,showing an average prediction deviation of 5.01%.Compared with the classical Lucas-Washburn model,the new model improved prediction accuracy by 4.72%.Additionally,comparisons were made to examine droplet spreading and non-uniform diffusion on textured surfaces,revealing that the T2 surface exhibited the strongest unidirectional diffusion characteristics.The contact angle ratio,droplet unidirectional spreading ratio,and droplet spreading aspect ratio were 0.48,1.75,and 3.99,respectively.Finally,the anti-wear,friction-reducing,and efficiency-enhancing mechanisms of micro-textured surfaces in minimum quantity lubrication turning were analyzed.This approach may support continuous cutting of difficult-tomachine materials.
基金Natural Science Foundation of Gansu Province(23JRRA922)National Natural Science Foundation of China(52265049)+1 种基金Industrial Support Program for Colleges and Universities in Gansu Province(2022CYZC-26)Key Research and Development Plan Project of Gansu Province(23YFGA0054)。
文摘The microstructure and mechanical properties of Inconel 617 alloy rolled at room temperature with different deformation degrees(20%,50%,70%)were investigated.The grain refinement mechanism and main texture types of Inconel 617 alloy during rolling were analyzed via electron backscatter diffraction and X-ray diffraction,and the microhardness and tensile properties of Inconel 617 alloy with different deformation degrees were tested.Results reveal that the grains of Inconel 617 alloy are refined during the rolling deformation process,and the refinement mechanism is the fragmentation of original grains caused by the increase in dislocation density and strain gradient.The main microtextures of the rolled samples are Goss{011}<001>,Rotated Goss{110}<110>,Brass{011}<211>,and P{011}<112>textures,and their intensity is increased with increase in deformation degree.After rolling deformation,the strength of the Inconel 617 alloy is improved and the ductility is reduced by the combined effect of grain refinement and dislocation strengthening.Comprehensively,the yield strength and elongation of Inconel 617 alloy after 20%deformation are 772.48 MPa and 0.1962,respectively,presenting good synergy effect.
基金supported by the technology development fund of Beijing Research Institute of Mechanical&Electrical Technology Co.,Ltd.,CAM,Construction of Innovation Leading Talents and Innovation Team of China Academy of Machinery Science and Technology Group:Vacuum forming technology and equipment innovation team.
文摘Static recrystallization(SRX)characteristics of a powder metallurgy superalloy were investigated by isothermal compression at 1080–1170℃ under strain rates of 0.01–0.1 s^(−1),strains of 0.1,0.22,or 0.5,and holding time of 0–300 s.The impacts of temperature,strain rate,holding time,and strain on the SRXed grain size,volume fraction,and microtexture were explored by electron backscatter diffraction technique.It was found that temperature played a key role in these processes.As SRX progressed,the<110>fiber parallel to the axis compression direction gradually weakened and was replaced by the<001>fiber because<001>was the preferred recrystallization orientation and grain growth direction for the Ni-based superalloy.Moreover,high temperatures and low strain rates promoted the formation of the<001>fiber.Three nucleation mechanisms during SRX process were found:grain boundary bulging,primary twin assistance,and subgrain coalescence.Grain boundary bulging occurred under all process conditions;however,at low temperatures and high strain rates,the latter two mechanisms could provide additional nucleation modes.In addition,SRX size and volume fraction models were established.
基金Project(51205419)supported by the National Natural Science Foundation of China
文摘The microstructural evolution of banded 5A90 A1-Li alloy during superplastic deformation at 475℃ with an initial strain rate of 8× 10^-4 S^-1 was studied using EBSD technique. The results showed that, before deformation, the grain shape appeared to be banded, the most grain boundaries belonged to low-angle boundaries, and the initial sheet had a dominate of { 110}（112） brass texture. During deformation, there were grain growth, grain shape change, misorientation increasing and textural weakening. The fraction of high-angle boundaries increased rapidly once the flow stress reached the peak value. Corresponding deformation mechanism for various stages of deformation was suggested. Dislocation activity was the dominant mechanism in the first stage, then dynamic recrystallization occurred, and grain rotation was expected as an accommodation for grain boundary sliding （GBS）. At large strains, GBS was the main mechanism.
基金Project(2011CB610403)supported by the National Basic Research Program of ChinaProject(51125002)supported by the National Natural Science Fund for Distinguished Young Scholars of China+3 种基金Projects(51101122,51071127,50901059)supported by the National Natural Science Foundation of ChinaProject(1110502)supported by the Fok Ying Tong Education Foundation,ChinaProjects(66-QP-2010,24-TZ-2009)supported by the Free Research Fund of State Key Laboratory of Solidification Processing,ChinaProject(B08040)supported by the Program of Introducing Talents of Discipline to Universities,China
文摘Rapid solidification of undercooled Ni-15%Cu （mole fraction） alloy was studied using glass fluxing and cyclic superheating. To show the effect of cooling history on the microstrucyure and microtexture evolution, the as-solidified samples were either cooled naturally or quenched into water after recalescence. At low undercooling, grain-refined microstructure has a random texture and a highly oriented texture without annealing twins for the case of naturally cooling and quenching, respectively. At high undercooling, a fully random texture as well as a number of annealing twins are observed, and recrystallization and grain growth independently happen on the cooling history. Fluid flow and recrystallization play an important role in the microtexture formation for grain refinement at both low and high undercooling.
基金This work was supported by the National Natural Science Foundation of China under grant No.50171040.
文摘In this paper, the orange peel defect in the surface range of the st14 steel sheet has been investigated using the electron backscattered diffraction (EBSD) technique. It has been found that the orange peel defect in the st14 steel sheet was resulted from the local coarse grains which were produced during hot-rolling due to the critical deformation in dual-phase zone. During deep drawing, the coarse grains with {100}<001> microtexture can slip on the {112}<111> slip system to form bulging and yields orange peel defects, while the coarse grains with {112}<110> orientation do not form the defect as the Schmid factor of {112}<111> slip system in it equals zero.
文摘The mineral assemblage and content and surface microtextures of slipping zone soil of several landslides in the Three Gorges Reservoir District have been analyzed using the scanning electron microscope (SEM) and X-ray diffractometer (XRD). All the mineral assemblages are similar in these landslides. The main minerals are montmorillonite, illite, kaolinite, chlorite, quartz and feldspar. There are two kinds of surface microtexture in the slipping zone soil, i.e., linear scratches and arcuate scratches. Based on analyses of the changes of the microtextures, one can obtain information about the number, directions and stages of landslide movements. The authors have also studied the mechanism of landslide formation, evaluated the stability of landslides and revival possibility of ancient landslides and forecasted the activity of similar landslides in different districts. The surface microtexture features of stable landslides and mobile landslides are summarized and it is concluded that the existence of filamentous bacteria may result in or increase movements of landslides.
基金Project(50671012) supported by the National Natural Science Foundation of China
文摘Nickel liner of shaped charge with nano-sized grains was prepared by electroforming technique and the ultra-highstrain-rate deformation was performed by explosive detonation.The as-electroformed and post-deformed microstructures of electroformed nickel liner of shaped charge were observed by optical metallography(OM),scanning electron microscopy(SEM) and transmission electron microscopy(TEM) and the orientation distribution of the grains was analyzed by electron backscattering pattern(EBSP) technique.Both melting phenomenon in the jet fragment and recovery and recrystallization in the slug after ultra-high-strain-rate deformation were observed.The research evidence shows that dynamic recovery and recrystallization play an important role in ultra-high-strain-rate deformation for electroformed nickel liner of shaped charge with nano-sized grain.
基金financially supported by the National Key Research and Development Program of China(Nos.2016YFB0701304 and 2016YFC0304200)the Strategic Priority Research Program of Chinese Academy of Sciences(No.XDC01040100)+1 种基金the Special Project on Information Technology of the Chinese Academy of Sciences(No.XXH13506-304)the CAS-Shenyang Supercomputing Center and the Doctoral Scientific Research Foundation of Liaoning Province(No.20180540133)。
文摘Variant selection under specific applied stresses during precipitation of a plates from prior-βmatrix in Ti-6 Al-4 V was investigated by 3 D phase field simulations.The model incorporates the Burgers transformation path fromβto a phase,with consideration of interfacial energy anisotropy,externally applied stresses and elastic interactions among a variants andβmatrix.The Gibbs free energy and atomic mobility data are taken from available thermodynamic and kinetic databases.It was found that external stresses have a profound influence on variant selection,and the selection has a sensitive dependence,as evidenced by both interaction energy calculations and phase field simulations.Compared with normal stresses,shear stresses applied in certain directions were found more effective in accelerating the transformation,with a stronger preference to fewer variants.The volume fractions of various a variants and the final microstructure were determined by both the external stress and the elastic interaction among different variants.The a clusters formed by variants with Type2 misorientation([11-20]/60°)relation were found more favored than those with Type4([-1055-3]/63.26°)under certain applied tensile stress such as along<111>β.The mechanical properties of different microstructures from our phase field simulation under different conditions were calculated for different loading conditions,utilizing crystal plastic finite element simulation.The mechanical behavior of the various microstructures from phase field simulation can be evaluated well before the alloys are fabricated,and therefore it is possible to select microstructure for optimizing the mechanical properties of the alloy through thermomechanical processing based on the two types of simulations.
文摘Constraints from P-T pseudosections （MnNCKFMASH system）, foliation intersection/ inflection axes preserved in porphyroblasts （FIAs）, mineral assemblages and textural relationships for rocks containing all three Al2 SiO5 polymorphs indicate a kyanite→ andalusite→ sillimanite sequential formation at different times rather than stable coexistence at the Al2SiO5 triple point. All three Al2SiO5 polymorphs grew in the Chl, Bt, Ms, Grt, St, Pl and Crd bearing Ordovician Clayhole Schist in Balcooma, northeastern Australia separately along a looped P-T-t-D path that swaps from clockwise to anticlockwise in the tectono-metamorphic history of the region. Kyanite grew during crustal thickening in an Early Silurian Orogenic event followed by decompression/heating, andalusite and fibrolitic sillimanite growth during Early Devonian exhumation.
文摘Corrosion re sistance of Zircaloy-4 alloy tube in superheated steam at 673 K/10.3 MPa is anisotropic.A part of the surface undergoes uniform corrosion while the other suffers nodular corrosion.Narrow and wide nodules are observed after an exposure period of 3 and 30 days,respectively.A new matrix transformation method is established in order to study the formation mechanism of nodules in the cross-section(CS) of Zircaloy-4 alloy tube using the EBSD technique,while the CS perpendicular to axial direction(AD).The results reveal that the microtexture is a key factor behind the two types of corrosion.Furthermore,the oxide layers grow anisotropically over the corroded surface.A thick oxide layer forms over the nodular corrosion region on the grains with c-axis oriented in the range of 40° around tangential direction(TD),whereas a thin oxide layer over the uniform corrosion region is detected on the grains with c-axis oriented in the range of 68° around TD.In short,the anisotropic growth of oxide layer was caused by the change of microtexture of the Zr-4 alloy tube,and this anisotropic growth of oxide layer contributed to the nodules formation.
基金supported by the National Natural Science Foundation of China(Nos.41774136 and 41374135)the Sichuan Science and Technology Program(No.2016ZX05004-003)
文摘Apparent differences in sedimentation and diagenesis exist between carbonate reservoirs in different areas and affect their petrophysical and elastic properties.To elucidate the relevant mechanism,we study and analyze the characteristics of rock microstructure and elastic properties of carbonates and their variation regularity using 89 carbonate samples from the different areas The results show that the overall variation regularities of the physical and elastic properties of the carbonate rocks are controlled by the microtextures of the microcrystalline calcite,whereas the traditional classification of rock-and pore-structures is no longer applicable.The micrite microtextures can be divided,with respect to their morphological features,into porous micrite,compact micrite,and tight micrite.As the micrites evolves from the first to the last type,crystal boundaries are observed with increasingly close coalescence,the micritic intercrystalline porosity and pore-throat radius gradually decrease;meanwhile,the rigidity of the calcite microcrystalline particle boundary and elastic homogeneity are enhanced.As a result,the seismic elastic characteristics,such as permeability and velocity of samples,show a general trend of decreasing with the increase of porosity.For low-porosity rock samples(φ<5%)dominated by tight micrite,the micritic pores have limited contributions to porosity and permeability and the micrite elastic properties are similar to those of the rock matrix.In such cases,the macroscopic physical and elastic properties are more susceptible to the formation of cracks and dissolution pores,but these features are controlled by the pore structure.The pore aspect ratio can be used as a good indication of pore types.The bulk modulus aspect ratio for dissolution pores is greater than 0.2,whereas that of the intergranular pores ranges from 0.1 to 0.2.The porous and compact micrites are observed to have a bulk modulus aspect ratio less than 0.1,whereas the ratio of the tight micrite approaches 0.2。
文摘Fisher Island and Broknes Peninsula in the Larsemann Hills constitute part of a polar lowland periglacial environment between marine and glacial ecosystems. The landscape is characterized by gently rolling hills and broad valleys interspersed with lakes formed in glacially scoured basins. We analyzed the physieochemical parameters and the ionic constituents of water samples from 10 lakes in each of these two locations. Our results showed considerable differences between the two regions and demon- strated the influence of lithology and processes including weathering, evaporation, and atmospheric precipitation. All major cations and anions in the lake waters showed positive correlations indicating balanced ionic concentrations. Unconsolidated sediments were sparsely distributed and scattered over glacial deposits, valley fills, and occasional moraine ridges. The type and rate of sedi- mentation was mainly controlled by surface run-off and aeolian influx. The sediment samples from lake beds and the catchment area on Fisher Island were immature and poorly to very poorly sorted, consisting of gravelly sand with negligible silt and finer fractions. Sediments had a polymodal grain size distribution with the two major populations lying between -2 and 1 phi and be- tween 0 and 1.5 phi. The sediments were lithic arenite to arkosic in composition and the microtextures imprinted over quartz grains were dominated by mechanical textures resulting from several stages of glacial crushing and grinding. The presence of deep disso- lution cavities, cryptocrystalline precipitation, and euhedral crystal growth signified the effect of chemical activity after the deposition of grains in the lacustrine environment.
基金The supports from the National Key Research and Development Program of China (No.2016YFB0701304)the CAS Informatization Project (No.XXH13506-304)the Doctoral Scientific Research Foundation of Liaoning Province (No.20180540133)
文摘Ti2 AlNb-based alloy powder metallurgy(PM)compacts were prepared via hot isostatic pressing(HIP)under relatively low temperature(920 and 980℃)and at certain pressure(130 MPa).The microstructure,composition and orientation of B2,α2 and O phases in the compacts were characterized and analyzed with an aim to investigate the effect of unsuitable HIPping parameters on the appearance of prior particle boundary(PPB),which seriously affects the mechanical properties of the alloy.The results show that moreα2 phase is the characteristics of the PPB in Ti2AlNb-based alloy when HIPped at relatively low temperature.Increasing HIPping temperature to the upper part of the two-phase region can effectively inhibit the formation of PPB.Electron backscatter diffraction measurements show the specific orientation relationship between phases,which helps us understand the origin of a2 and O phase and the corresponding transformation path.The HIPping at a higher temperature can weaken the micro-texture intensity of theα2 and O phase due to the increase of misorientation in B2 phase.Theα2 phase at cell wall keeps the Burgers orientation relationship(BOR)with the grain on one side,and does not satisfy the BOR with the other.It is found that some O phase variants inside the cell HIPped at 980℃can only maintainα2-O OR withα2 owing to theα2→O phase transformation forming the O phase,while these O variants deviate from B2-O OR with B2 phase.
文摘Most of past researches on the skid resistance/road wetness relationship deal with thick water depths （〉 1 mm）. Questions remain as to the variation of skid resistance with thin water films and the transition between the dry state and the so-called ＂damp＂ or ＂humid＂ state at which the skid resistance drop can be as high as 30%-40%. This paper deals with a theoretical and experimental assessment of the friction-water depth relationship. The main objective is to estimate local water depths trapped between the tire and the road asperities and to define a so-called ＂critical＂ water depth which can be used to detect risky situations for road users. Tests are performed in laboratory. It was found that the friction-water depth curves have an inverse-S shape and present an initial constant-friction part before decreasing to a minimum value. A ＂critical＂ water depth, defined as the water depth above which the friction coefficient collapses significantly, is determined from surface texture on critical water depth is discussed. observed friction-water depth curves. Influence of test speed and
文摘Adequate pavement skid resistance is a key requirement for safe road operations.Unfortunately,the measurement and prediction of the skid resistance property of an in-service road pavement,or pavement mixture specimens in the laboratory,is a highly challenging process from both theoretical and practical points of view.For more than 60 years,owing to the lack of theoretical solutions to the complex tire-fluid-pavement interaction problem,the practice of pavement skid resistance determination and prediction has essentially been derived from experimental and field observed data.The rapid development of efficient numerical computational techniques and high-power computing facilities in the last two decades made it possible for researchers to numerically solve the tire-fluidpavement interaction problem.It enables the numerical evaluation and prediction of high-speed wet skid resistance,and the determination of the tire-pavement kinetic friction coefficient in the evaluation of low-speed skid resistance.This paper presents a state-of-the-art review of the research development of theoretical mechanistic approaches in the determination and prediction of pavement skid resistance.It covers the following main aspects of the subject matter:(i)mechanisms of skid resistance generation in dry,wetted(i.e.,damp),wet and flooded pavements;(ii)theoretical evaluation of pavement skid resistance in dry,wetted,wet and flooded states;(iii)theoretical approaches in pavement skid resistance prediction;and(iv)concepts of representing the skid resistance state of pavement.The capability of finite element simulation approach for wet skid resistance evaluation with good accuracy is explained.Also highlighted is the practical significance of the Concept of Skid Resistance State.Areas of practical applications of the concept,coupled with the simulation model,are introduced.They include applications in driving safety analysis,road safety design and control,design of paving mixtures,safety maintenance and management of pavements,and harmonization of skid resistance measurements and predictions.
基金supported by the National Natural Science Foundation of China (No.50671012)
文摘Nickel shaped-charge liners with nano-sized grains were prepared by the electroforming technique, and the deformation at ultrahigh strain rate was performed by explosive detonation. The as-formed and post-deformed microstructures of electroformed nickel shaped-charge liners with nano-sized grains were observed by means of transmission electron microscopy, and the orientation distribution of the grains was analyzed by the electron backscattering pattern （EBSP） technique. The melting phenomenon in the jet fragment and the recovery and recrystallization in the slug after plastic deformation at ultrahigh-strain rate were observed in the ultrafine-grained nickel shaped-charge liners. The research evidence shows that dynamic recovery and recrystallization play an important role in plastic deformation at ultrahigh strain rate.
基金supported by a grant from the University Research Board (URB) of the American University of Beirut (AUB) (Nos. 103603, 24687)。
文摘Carbonate rocks are common in many parts of the world, including the Eastern Mediterranean, where they host significant groundwater supplies and are widely used as building and ornamental stones. The porosity of carbonate rocks plays a critical role in fluid storage and retrieval. The pore structure connectivity, in particular, controls many properties of geological formations, as well as the relationships between the properties of individual minerals and the bulk properties of the rock. To study the relationships between porosity, rock properties, pore structure, pore size, and their impact on reservoir characteristics, 46 carbonate rock samples were collected from four stratigraphic sections exposed near Sidon, South Lebanon. The studied carbonate rocks are related to marine deposits of different ages(e.g., Upper Cretaceous, Eocene, and Upper Miocene). In order to understand the pore connectivity, the MICP(mercury injection capillary pressure) technique was conducted on ten representative samples. Results from the SEM analysis indicate the dominance of very fine and fine pore sizes, with various categories ranging in diameter from 0.1 to10 μm. The MICP data revealed that the pore throat radii vary widely from 0.001 to 1.4 μm, and that all samples are dominated by micropore throats. The grain size analysis indicated that the studied rocks have significant amounts of silt-and clay-size grains with respect to the coarser ‘sand-size’ particles, suggesting a high proportion of microporosity. Obtained results, such as the poorly-sorted nature of grains, high microporosity, and the high percentage of micropore throats, justify the observed low mean hydraulic radius, the high entry pressure, and the very low permeability of the studied samples. These results suggest that the carbonate rocks near Sidon(south of Lebanon) are possibly classified as non-reservoir facies.
基金the National Natural Science Foundation of China (No. 51065009)the Science Fund Project of Jiangxi Provincial Department of Education (No. GJJ11095)
文摘The natural hydrophobicity of surfaces can be enhanced if they are microtextured due to air trapped in the structure, which provides the deposited drop with a composite surface made of solid and air on which it is rest. Here, a series of grating microstructure surfaces with different parameters have been designed and fabricated by a novel soft lithography. The water contact angles （WCA） on these rough surfaces are measured through optical contact angle meter. The results indicate that all the WCA on the surfaces with grating microstructures are up to 150~; WCA increases and the hydrophobic performance also enhances with the decrease of the ridge width under the other fixed parameter condition; Experimental data obtained basically consists with the Cassie＇s theoretical prediction. The effects of geometric parameters of the microstructures on wettability of the grating sufaces are investigated.
