The microprecipitates in the as-grown undoped and In-doped semi-insulating GaAs single crystals have been ex- amined by JEM 200 CX transmission electron microscope.The microprecipitates consist of GaAs polycrystalline...The microprecipitates in the as-grown undoped and In-doped semi-insulating GaAs single crystals have been ex- amined by JEM 200 CX transmission electron microscope.The microprecipitates consist of GaAs polycrystalline grains of 5~100nm in size have been evidenced in dislocated crystals.Energy dispersive X-ray analysis shows that the mieropreeipitates are predominately arsenic-rich GaAs.The As/Ga atomic ratio of the microprecipitates in In-doped crystal is higher than that of undoped crystal.It is suggested that the formation of the microprecipitates may be induced by the local fluctuation of compositional undercooling during crystal growth.展开更多
文摘The microprecipitates in the as-grown undoped and In-doped semi-insulating GaAs single crystals have been ex- amined by JEM 200 CX transmission electron microscope.The microprecipitates consist of GaAs polycrystalline grains of 5~100nm in size have been evidenced in dislocated crystals.Energy dispersive X-ray analysis shows that the mieropreeipitates are predominately arsenic-rich GaAs.The As/Ga atomic ratio of the microprecipitates in In-doped crystal is higher than that of undoped crystal.It is suggested that the formation of the microprecipitates may be induced by the local fluctuation of compositional undercooling during crystal growth.