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Propagation criterion of hydraulic fracture in rock based on the rock micro-cracking mechanism
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作者 Qingwang Cai Bingxiang Huang +1 位作者 Xinglong Zhao Yuekun Xing 《International Journal of Mining Science and Technology》 2025年第3期433-449,共17页
Hydraulic fracture(HF)formed in rock significantly helps with the development of geo-energy and georesources.The HF formation condition was challenging to understand,with obscure rock micro-cracking mechanisms being a... Hydraulic fracture(HF)formed in rock significantly helps with the development of geo-energy and georesources.The HF formation condition was challenging to understand,with obscure rock micro-cracking mechanisms being a key factor.The rock micro-cracking mechanism under gradient pore water pressure was analyzed on the scale of mineral particles and it was combined with macroscopic boundary conditions of rock hydraulic fracturing,obtaining the propagation criterion of HF in rock based on the rock micro-cracking mechanism which was verified by experiment.The results show that the disturbed skeleton stress induced by the disturbance of gradient pore water pressure in rock equals the pore water pressure difference.The overall range of the defined mechanical shape factor a/b is around 1,but greater than0.5.Under the combined influence of pore water pressure differences and macroscopic boundary stresses on the rock micro-cracking,micro-cracks form among rock mineral particles,micro-cracks connect to form micro-hydraulic fracture surfaces,and micro-hydraulic fracture surfaces open to form macrohydraulic fractures.HF begins to form at the micro-cracking initiation pressure(MCIP),which was tested by keeping the HF tip near the initiation point.The theoretical value of MCIP calculated by the proposed propagation criterion is close to MCIP tested. 展开更多
关键词 Hydraulic fracture Propagation criterion micro-cracking mechanism Pore pressure Stress singularity
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Evolution mechanism and quantitative characterization of initial micro-cracks in marble under triaxial compression
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作者 Zhiliang WANG Songyu LI +4 位作者 Jianguo WANG Ao LI Weixiang WANG Chenchen FENG Jingjing FU 《Journal of Zhejiang University-Science A(Applied Physics & Engineering)》 SCIE EI CAS CSCD 2024年第7期586-595,共10页
The initial micro-cracks affect the evolution characteristics of macroscopic deformation and failure of rock but are often ignored in theoretical calculation,numerical simulation,and mechanical experiments.In this stu... The initial micro-cracks affect the evolution characteristics of macroscopic deformation and failure of rock but are often ignored in theoretical calculation,numerical simulation,and mechanical experiments.In this study,we propose a quantitative analysis model to investigate the effects of initial micro-cracks on the evolution of marble deformation and failure.The relationship between the micro-crack propagation and the marble failure characteristics was comprehensively studied by combining theoretical analysis with a micro-computed tomography(micro-CT)scanning technique.We found that with the increase of confining pressure,the matrix elastic modulus of the marble first increased and then tended to be stable,while the micro-cracks increased exponentially.The sensitivity ranges of the marble sample matrix elastic modulus and micro-cracks to confining pressure were 0–30 MPa and 30–50 MPa,respectively.The porosity and Poisson’s ratio decreased exponentially.The increasing proportion of internal micro-cracks led to an increase in the sample non-uniformity.The samples presented mainly shear failure under triaxial compression,and the failure angle decreased linearly with the increase of confining pressure.The convergence direction of cracks decreased gradually.This quantitative analysis model could accurately portray the relationship between the overall macroscopic deformation and the deviatoric stress of the samples at the compaction and the linear elastic stages,thus deepening the understanding of the stress–strain behavior of rocks. 展开更多
关键词 MARBLE Initial micro-cracks Triaxial compression Constitutive relationship Crack evolution
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Displacive transformation as pathway to prevent micro-cracks induced by thermal stress in additively manufactured strong and ductile high-entropy alloys 被引量:11
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作者 Rui-di LI Peng-da NIU +1 位作者 Tie-chui YUAN Zhi-ming LI 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2021年第4期1059-1073,共15页
The micro-cracking behaviors of two high-entropy alloys(HEAs) of the FeMnCoCrNi family prepared by selective laser melting were systematically studied. Residual stresses were also analyzed by X-ray diffraction techniq... The micro-cracking behaviors of two high-entropy alloys(HEAs) of the FeMnCoCrNi family prepared by selective laser melting were systematically studied. Residual stresses were also analyzed by X-ray diffraction technique. Results show that the equiatomic FeMnCoCrNi HEAs with a relatively stable single-phase face-centered cubic(FCC) structure suffered from micro-cracking with residual tensile stress after laser melting. In contrast, the metastable non-equiatomic Fe MnCoCr HEAs with reduced stacking fault energy are free of micro-cracks with residual compressive stress at various volumetric energy densities(VEDs). The displacive transformation from the FCC matrix to the hexagonal close-packed(HCP) phase during cooling prevents the micro-cracking via consuming thermal stress related internal energy. Further, the displacive transformation during tensile deformation contributes to the higher strength and ductility of the metastable dual-phase HEA compared to that of the stable single-phase HEA. These findings provide useful guidance for the design of strong, ductile, and crack-free alloys for additive manufacturing by tuning phase stability. 展开更多
关键词 selective laser melting high-entropy alloys phase transformation micro-crackING residual stress
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OMHT method for weak signal processing of GPR and its application in identification of concrete micro-crack 被引量:5
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作者 LING Tong-hua ZHANG Liang +3 位作者 HUANG Fu GU Dan-ping YU Bin ZHANG Sheng 《Journal of Central South University》 SCIE EI CAS CSCD 2019年第11期3057-3065,共9页
In the light of the problem of weak reflection signals shielded by strong reflections from the concrete surface,the detection and the recognition of hidden micro-cracks in the shield tunnel lining were studied using t... In the light of the problem of weak reflection signals shielded by strong reflections from the concrete surface,the detection and the recognition of hidden micro-cracks in the shield tunnel lining were studied using the orthogonal matching pursuit and the Hilbert transform(OMHT method).First,according to the matching pursuit algorithm and the strong reflection-forming mechanism,and based on the sparse representation theory,a sparse dictionary,adapted to the characteristics of the strong reflection signal,was selected,and a matching decomposition of each signal was performed so that the weak target signal submerged in the strong reflection was displayed more strongly.Second,the Hilbert transform was used to extract multiple parameters,such as the instantaneous amplitude,the instantaneous frequency,and the instantaneous phase,from the processed signal,and the ground penetrating radar(GPR)image was comprehensively analyzed and determined from multiple angles.The results show that the OMHT method can accurately weaken the effect of the strong impedance interface and effectively enhance the weak reflected signal energy of hidden micro-crack in the shield tunnel segment.The resolution of the processed GPR image is greatly improved,and the reflected signal of the hidden micro-crack is easily visible,which proves the validity and accuracy of the analysis method. 展开更多
关键词 orthogonal matching pursuit Hilbert transform shield tunnel lining structure hidden micro-crack
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Micro-crack detection of nonlinear Lamb wave propagation in three-dimensional plates with mixed-frequency excitation 被引量:4
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作者 Wei-Guang Zhu Yi-Feng Li +3 位作者 Li-Qiang Guan Xi-Li Wan Hui-Yang Yu Xiao-Zhou Liu 《Chinese Physics B》 SCIE EI CAS CSCD 2020年第1期336-345,共10页
We propose a nonlinear ultrasonic technique by using the mixed-frequency signals excited Lamb waves to conduct micro-crack detection in thin plate structures.Simulation models of three-dimensional(3D)aluminum plates a... We propose a nonlinear ultrasonic technique by using the mixed-frequency signals excited Lamb waves to conduct micro-crack detection in thin plate structures.Simulation models of three-dimensional(3D)aluminum plates and composite laminates are established by ABAQUS software,where the aluminum plate contains buried crack and composite laminates comprises cohesive element whose thickness is zero to simulate delamination damage.The interactions between the S0 mode Lamb wave and the buried micro-cracks of various dimensions are simulated by using the finite element method.Fourier frequency spectrum analysis is applied to the received time domain signal and fundamental frequency amplitudes,and sum and difference frequencies are extracted and simulated.Simulation results indicate that nonlinear Lamb waves have different sensitivities to various crack sizes.There is a positive correlation among crack length,height,and sum and difference frequency amplitudes for an aluminum plate,with both amplitudes decreasing as crack thickness increased,i.e.,nonlinear effect weakens as the micro-crack becomes thicker.The amplitudes of sum and difference frequency are positively correlated with the length and width of the zero-thickness cohesive element in the composite laminates.Furthermore,amplitude ratio change is investigated and it can be used as an effective tool to detect inner defects in thin 3D plates. 展开更多
关键词 nonlinear Lamb wave mixed-frequency micro-crackS amplitude ratio
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DIGITAL IMAGE CORRELATION STUDIES FOR FATIGUE MICRO-CRACK INITIATION AND PROPAGATION OF NI BASED SUPERALLOY 被引量:4
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作者 Dong Lei 1 Kefeng Wang Qing Zhang Pizhong Qiao (State Key Laboratory of Hydrology-Water Resources and Hydraulic Engineering, Hohai University, Nanjing 210098, China) (College of Mechanics and Materials, Hohai University, Nanjing 210098, China) 《Acta Mechanica Solida Sinica》 SCIE EI 2011年第S1期79-84,共6页
An experimental investigation on the mechanical mechanisms of fatigue micro-crack initiation and propagation of a nickel-based superalloy is presented. By coupling digital image correlation method and scanning electro... An experimental investigation on the mechanical mechanisms of fatigue micro-crack initiation and propagation of a nickel-based superalloy is presented. By coupling digital image correlation method and scanning electron microscope, the fatigue residual strain distribution at the grain scale has been obtained. The results showed that there is a trend of accumulation for the residual strain. Micro-cracks are more likely to initiate in or near the areas with particularly large residual strain, and propagate along the large-strain paths. 展开更多
关键词 nickel alloy digital image correlation fatigue residual strain micro-crack
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ffect of a Micro-crack on the Edge Macro-crack Propagation Rate and Path Under Mixed Loads 被引量:2
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作者 Xiaotao Li Xiaoyu Jiang 《Acta Mechanica Solida Sinica》 SCIE EI CSCD 2019年第4期517-532,共16页
The solution of a half-plane containing a micro-crack and an edge macro-crack under mixed loads is presented based on the distributed dislocation technique. The complete stress field and stress intensity factors are o... The solution of a half-plane containing a micro-crack and an edge macro-crack under mixed loads is presented based on the distributed dislocation technique. The complete stress field and stress intensity factors are obtained. The finite element model is established to simulate the macro-crack propagation path. The effect of a micro-crack on the macro-crack propagation is analyzed comprehensively. The results show that the shielding effect region is like two ‘petals’ under uniaxial tensile load and rotates with the change in micro-crack angle. For mixed loads, the shielding effect region rotates clockwise with the increasing ratio of applied loads τ∞/σ∞τ∞/σ∞ It is like two tpetals, at τ∞/σ∞ 00 < 2 and divides into two parts from the macro-crack tip at τ∞/σ∞≥ 5. The micro-crack has the attraction effect on the macro-crack propagation path. These results are useful for predicting the fracture or fatigue behaviors of materials containing micro-cracks. 展开更多
关键词 micro-crack Macro-crack propagation Distributed DISLOCATION technique COMPLETE stress field
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Modeling and Experimental Analysis of Roughness Effect on Ultrasonic Nondestructive Evaluation of Micro-crack 被引量:2
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作者 Zhe Wang Zhichao Fan +3 位作者 Xuedong Chen Yihua Kang Jingwei Cheng Wei Chen 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2021年第6期126-137,共12页
A high-precision evaluation of ultrasonic detection sensitivity for a micro-crack can be restricted by a corroded rough surface when the surface microtopography is of the same order of magnitude as the crack depth.In ... A high-precision evaluation of ultrasonic detection sensitivity for a micro-crack can be restricted by a corroded rough surface when the surface microtopography is of the same order of magnitude as the crack depth.In this study,a back-surface micro-crack is considered as a research target.A roughness-modified ultrasonic testing model for micro-cracks is established based on a multi-Gaussian beam model and the principle of phase-screen approximation.The echo signals of micro-cracks and noises corresponding to different rough front surfaces and rough back surfaces are obtained based on a reference reflector signal acquired from a two-dimensional simulation model.Further compari-son between the analytical and numerical models shows that the responses of micro-cracks under the effects of dif-ferent corroded rough surfaces can be accurately predicted.The numerical and analytical results show that the echo signal amplitude of the micro-crack decreases significantly with an increase in roughness,whereas the noise ampli-tude slightly increases.Moreover,the effect of the rough front surface on the echo signal of the micro-crack is greater than that of the rough back surface.When the root-mean-square(RMS)height of the surface microtopography is less than 15μm,the two rough surfaces have less influence on the echo signals detected by a focused transducer with a frequency of 5 MHz and diameter of 6 mm.A method for predicting and evaluating the detection accuracy of micro-cracks under different rough surfaces is proposed by combining the theoretical model and a finite element simulation.Then,a series of rough surface samples containing different micro-cracks are fabricated to experimentally validate the evaluation method. 展开更多
关键词 Surface roughness micro-crack Ultrasonic testing model Detection accuracy Evaluation method
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Image Preprocessing Methods to Identify Micro-cracks of Road Pavement 被引量:1
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作者 Hui Wang Zhang Chen Lijun Sun 《Optics and Photonics Journal》 2013年第2期99-102,共4页
Standards of highway conservation and maintenance are improved gradually following the improvement of requirements of road service. Before obvious damage such as obvious cracking (block,transverse, longitudinal ) and ... Standards of highway conservation and maintenance are improved gradually following the improvement of requirements of road service. Before obvious damage such as obvious cracking (block,transverse, longitudinal ) and rutting emerge, inconspicuous distress (micro-cracks, polishing, pockmarked) is generated previously. These inconspicuous distresses may provide basis and criteria for pavement preventive maintenance. Currently most of preventive conservation measures are determined by experienced experts in maintenance and repair of road after site visits. Thus method is difficult in operation, and has a certain amount of instability as it is based on experience and personal knowledge. In this paper, camera and laser were used for automated high-speed acquisition images. Methods to preprocess pavement image are compared. The pretreatment method suitable for analyze micro-cracks picture is elected, an effective way to remove shadow is also proposed. 展开更多
关键词 PAVEMENT DISTRESS Automatic Detection Inconspicuous DISTRESS micro-crack Laser Light IMAGE Image-preprocessing
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Theoretical Model of the Probability of Fusion between Deuterons within Deformed Lattices with Micro-cracks at Room Temperature
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作者 Frisone Fulvio 《Journal of Energy and Power Engineering》 2017年第1期63-67,共5页
In this work, we wish to demonstrate that a reaction path as the following, dislocations, deformations due to thermodynamic stress and, finally, micro-crack occurrence, can enhance the process of fusion of the deutero... In this work, we wish to demonstrate that a reaction path as the following, dislocations, deformations due to thermodynamic stress and, finally, micro-crack occurrence, can enhance the process of fusion of the deuterons introduced into the lattice by deuterium loading. In fact, calculating the rate of deuteron-plasmon-deuteron fusion within a micro-crack, showed, together with an enhancement of the tunneling effect, an increase of at least 2-3 orders of magnitude compared to the probability of fusion on the no deformed lattice. In fact, strong electric fields can take place in the micro-crack and the deuterons are accelerated to the energy which are enough for the D-D tunnelling. These phenomena open the way to the theoretical hypothesis that a kind of chain reaction, catalyzed by the micro-cracks produced in the structure as a result of deuterium loading, can favour the process of deuteron-plasmon fusion. 展开更多
关键词 Condensed matter dislocations lattice deformation micro-cracks.
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Probability of Deuteron-Plasmon Fusion at Room Temperature within Micro-cracks of Crystalline Lattices with Deuterium Loading
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作者 Fulvio Frisone 《Journal of Energy and Power Engineering》 2017年第7期446-449,共4页
This communication seeks to demonstrate that, at room temperature, the deformation of the crystalline lattice can influence the process of interaction of deuterons introduced within it. Calculations of this probabilit... This communication seeks to demonstrate that, at room temperature, the deformation of the crystalline lattice can influence the process of interaction of deuterons introduced within it. Calculations of this probability, in fact, showed an increase of at least 2-3 orders of magnitude with respect to the probability of fusion on the surface of the lattice. These phenomena open the way to the theoretical hypothesis of a kind of chain reaction, as a result of the deuterium loading and catalysed by micro-cracks formed in the structure by micro-explosions, can favour the process. 展开更多
关键词 Deuteron-plasmon micro-crackS lattice defects.
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Diffusive healing of internal fatigue micro-cracks in pure titanium
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作者 杨君刚 孙军 张海龙 《中国有色金属学会会刊:英文版》 CSCD 2001年第5期675-680,共6页
The internal micro cracks with the critical length about 30?μm and thickness less than 1?μm were introduced into the pure titanium samples by uniaxial tension compression low cycle fatigue method. The experimental r... The internal micro cracks with the critical length about 30?μm and thickness less than 1?μm were introduced into the pure titanium samples by uniaxial tension compression low cycle fatigue method. The experimental results indicate that the internal fatigue micro crack clearly evolves from the original penny shaped crack into a string of spherical voids in the longitudinal section plane of the fatigue sample after the vacuum diffusive healing at the high temperature. The quantitative relationship between the radius and the spacing of spherical voids depends on the crack position (within grains, on grain boundaries or transgranular sites) and its orientations within the grain. The diffusive healing, the related thermodynamics and mechanism, and the effect of the surface tension anisotropy on the relationship between void diameter and void spacing are also discussed. 展开更多
关键词 pure titanium internal fatigue micro crack diffusive healing
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基于数字体图像相关法的砂浆内部微裂隙识别与量化 被引量:2
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作者 毛灵涛 苏方圆 +1 位作者 刘海洲 刘昱清 《工程力学》 北大核心 2025年第5期169-183,共15页
结合微CT原位加载扫描,利用数字体图像相关法实现了砂浆试件内部亚体素级微裂隙的识别与量化。利用微CT原位加载系统获得了单轴压缩条件下砂浆试件在不同阶段的体图像,对其破坏特征进行了分析;介绍了正则化全局数字体图像相关法和微裂... 结合微CT原位加载扫描,利用数字体图像相关法实现了砂浆试件内部亚体素级微裂隙的识别与量化。利用微CT原位加载系统获得了单轴压缩条件下砂浆试件在不同阶段的体图像,对其破坏特征进行了分析;介绍了正则化全局数字体图像相关法和微裂隙识别原理,分析评价了位移场测量及微裂隙识别精度;基于试件的体图像,计算得到了其内部的三维位移场,由灰度残差及最大主应变识别损伤单元,设定损伤因子,对新生微裂隙演化进行了识别与量化。结果表明:引入正则化条件及损伤因子,提高了全局数字体图像相关法的测量精度,实现了亚体素级新生微裂隙的识别与量化;试件的位移场及应变场精细化显示出内部孔隙及裂隙周边变形的局部化特征;试件局部区域在弹性阶段已出现亚体素级微裂隙,在塑性阶段及破坏初期,新生的亚体素级微裂隙占比高于体素级微裂隙。该文研究为混凝土内部微裂隙的识别与量化提供了新的思路与方法。 展开更多
关键词 混凝土 砂浆 微裂隙 数字体图像相关法 微CT
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高温灰岩单轴压缩力学特征与微观解析
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作者 黄锋 刘星辰 +2 位作者 周洋 郑艾辰 杨冬 《地下空间与工程学报》 北大核心 2025年第1期70-77,共8页
为研究高温处理后灰岩单轴压缩力学特征,对常温(25℃)与经历高温(100℃、200℃、300℃、400℃、500℃和600℃)处理后的灰岩开展了物理特征测试、单轴压缩试验、SEM电镜扫描与XRD衍射分析,基于岩石微观裂损规律解析了灰岩单轴压缩力学特... 为研究高温处理后灰岩单轴压缩力学特征,对常温(25℃)与经历高温(100℃、200℃、300℃、400℃、500℃和600℃)处理后的灰岩开展了物理特征测试、单轴压缩试验、SEM电镜扫描与XRD衍射分析,基于岩石微观裂损规律解析了灰岩单轴压缩力学特征。结果表明:随着处理温度升高,灰岩表观颜色由青灰色演变为红褐色,体积增长率、质量损失率呈非线性增大;高温处理使灰岩微观质地分层、裂隙发育、孔洞溶蚀,受压破裂断口面起伏与尖角特征显著;高温催化了灰岩矿物组分的热解与化合反应,岩石综合硬度系数与坚固性系数存在显著线性相关性;揭示灰岩热损伤的阈值温度为200℃,峰值强度与弹性模量均在此温度下达到峰值。 展开更多
关键词 高温处理 灰岩 力学特征 微观裂损 硬度系数
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Very high cycle fatigue resistance improvement of Mg-Gd-Zn-Zr alloy by introducing curved long-period stacking ordered lamellae
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作者 Min Zhan Xinglin Yang +7 位作者 Shoucheng Shi Yao Chen Lang Li Bing Xue Yongbo Li Wanshuang Yi Qingyuan Wang Chao He 《Journal of Magnesium and Alloys》 2025年第3期1218-1231,共14页
Magnesium alloys with long-period stacking ordered(LPSO)structures are known for their impressive static mechanical strength,but the consistent occurrence of slip-cracking along the LPSO lamellae,which do not effectiv... Magnesium alloys with long-period stacking ordered(LPSO)structures are known for their impressive static mechanical strength,but the consistent occurrence of slip-cracking along the LPSO lamellae,which do not effectively impede the movement of basal dislocations,has prompted concerns about their very high cycle fatigue(VHCF)performance.In this study,an extruded Mg-Gd-Zn-Zr alloy was developed,showcasing exceptional VHCF resistance due to its bimodal structure comprisingfine grains and coarse grains consisting of curved LPSO lamellae.The investigation on the crack initiation mechanism revealed that slip-induced cracking predominantly occurs infine-grained regions rather than in the interior of coarse grains.The extrusion process aligns the basal planes of most coarse grains parallel to the axial direction,and the presence of curved LPSO lamellae acts as barriers to the movement of basal dislocations,thereby effectively increasing the threshold for slip-cracking along the basal plane.Consequently,fatigue damage manifests in the form of slip bands and micro-cracks within the interior offine grains,ultimately resulting in fatigue crack initiation,propagation andfinal fracture. 展开更多
关键词 Very high cycle fatigue Mg-Gd-Zn-Zr alloy Crack initiation Curved LPSO lamellae micro-crackS
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渗透树脂联合美白技术修复微裂氟斑牙 被引量:1
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作者 张文怡 尹昭 张健 《中国组织工程研究》 CAS 北大核心 2025年第4期686-691,共6页
背景:微研磨、家庭美白联合渗透树脂治疗氟斑牙具有良好的效果,但该方法对氟斑牙微裂纹的影响尚不清楚。目的:探究微研磨、家庭美白联合渗透树脂修复微裂氟斑牙的效果。方法:①临床研究:选择2020年7月至2021年3月就诊于天津医科大学口... 背景:微研磨、家庭美白联合渗透树脂治疗氟斑牙具有良好的效果,但该方法对氟斑牙微裂纹的影响尚不清楚。目的:探究微研磨、家庭美白联合渗透树脂修复微裂氟斑牙的效果。方法:①临床研究:选择2020年7月至2021年3月就诊于天津医科大学口腔医院修复科的23例微裂氟斑牙患者,包括255颗微裂氟斑牙,均接受牙齿微研磨术、家庭美白与渗透树脂联合治疗,对比治疗前及治疗结束后1周、1个月的牙齿颜色、牙齿敏感程度和牙齿疼痛阈值。②体外实验:收集牙齿表面至少存在一条裂纹的氟斑牙60颗,随机分3组处理:对照组不进行任何处理,美白组进行微研磨与家庭美白处理,联合组进行微研磨、家庭美白和渗透树脂联合处理,每组20颗,测量处理后3组牙齿样本的显微硬度。结果与结论:①临床研究:治疗结束后6个月,255颗微裂氟斑牙中牙齿美白治疗显效207颗、有效48颗,总体治疗有效率为100%。随着治疗时间的延长,中、重度牙齿度敏感程度占比呈下降趋势,治疗结束后6个月,255颗氟斑牙中无重度敏感、15颗为中度敏感、125颗为轻度敏感、115颗无敏感,与治疗前的氟斑牙敏感程度相比差异有显著性意义(P<0.05)。治疗前与治疗结束后1周、6个月的牙齿疼痛阈值比较差异无显著性意义(P>0.05)。②体外实验:美白组牙齿显微硬度值低于对照组、联合组(P<0.05),对照组与联合组牙齿显微硬度值比较差异无显著性意义(P>0.05)。③结果表明,微研磨、家庭美白联合渗透树脂治疗微裂氟斑牙具有较好的疗效。 展开更多
关键词 氟斑牙 微裂纹 渗透树脂 牙齿美白 治疗效果 显微硬度
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油水双响应固井水泥环自修复材料制备与评价
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作者 朱志平 张春梅 +4 位作者 李锟 刘帅 程小伟 梅开元 李心雨 《过程工程学报》 北大核心 2025年第9期963-974,共12页
针对固井水泥环微裂缝破坏其完整性的问题,本工作以硅酸钠为自修复剂、硅藻土为载体、乙基纤维素为表面包覆材料,成功制备了油水双响应型包覆式自修复材料,并系统评价其对水泥石的自修复效果。结果表明,硅藻土的最佳煅烧温度为600℃,此... 针对固井水泥环微裂缝破坏其完整性的问题,本工作以硅酸钠为自修复剂、硅藻土为载体、乙基纤维素为表面包覆材料,成功制备了油水双响应型包覆式自修复材料,并系统评价其对水泥石的自修复效果。结果表明,硅藻土的最佳煅烧温度为600℃,此温度下制备的硅藻土具有最大的比表面积和孔体积,且孔洞分布均匀,对硅酸钠的吸附性能最优。乙基纤维素与硅酸钠、硅藻土均无化学反应,其中2wt%乙基纤维素溶液的包覆效果最佳,可在吸附硅酸钠的硅藻土表面形成一层平整光滑且致密的包覆膜。包覆型自修复材料在水泥中的最佳掺量为4wt%。自修复14 d后,水泥石微裂缝完全闭合,渗透率降至0.31mD,较空白水泥石降低69.31%;同时,其抗压强度达到26.6±1.3 MPa,抗压强度恢复率高达85.3%,为空白水泥石同期恢复率的2.1倍。经数据拟合发现,水泥石抗压强度恢复率随自修复材料掺量的增加呈先上升后下降趋势,4.5wt%掺量时自修复效果最佳。结合X射线衍射和热重分析结果可知,当水泥石中产生微裂缝时,自修复材料表面的乙基纤维素膜遇油溶解,随后自修复剂硅酸钠消耗水泥石中的氢氧化钙和水反应生成水化硅酸钙,进而填充裂缝实现自修复。 展开更多
关键词 固井水泥环 微裂缝 油水双响应 自修复材料 渗透率 抗压强度恢复率
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基于微流控模型的超临界CO_(2)压裂返排微观机制
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作者 谢平 王海柱 +4 位作者 王斌 张云鹏 徐润滋 麦汉 董卓鑫 《西安石油大学学报(自然科学版)》 北大核心 2025年第3期57-65,74,共10页
为揭示超临界CO_(2)压裂后压裂流体的返排机制,设计搭建了高温高压微观可视化实验平台,设计制作了含天然微裂缝的微流控模型,研究了超临界CO_(2)压裂后CO_(2)返排规律,对比了CO_(2)和常规水基压裂液返排特征及储层流体运移分布规律。结... 为揭示超临界CO_(2)压裂后压裂流体的返排机制,设计搭建了高温高压微观可视化实验平台,设计制作了含天然微裂缝的微流控模型,研究了超临界CO_(2)压裂后CO_(2)返排规律,对比了CO_(2)和常规水基压裂液返排特征及储层流体运移分布规律。结果表明,CO_(2)的可压缩性与溶解性是影响超临界CO_(2)返排的重要因素,使得CO_(2)在地层中几乎无游离态残余,同时也导致CO_(2)的返排速度更慢,返排时间更长。明确了裂缝走向与压力梯度的夹角是影响压裂液缝内返排的主要因素,夹角<45°时,压力对缝内流体的驱动效果较为明显,返排效果较好;夹角>45°时,返排效果较差。研究结果可为CO_(2)压裂返排工艺设计提供理论基础。 展开更多
关键词 压裂液返排 超临界CO_(2) 微裂缝 储层流体运移 微观可视化
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涡轮叶片热障涂层中微小缺陷的阵列超声瑞利波检测
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作者 蔡苏阳 陈振华 +4 位作者 冯萍 张浩喆 何喜 方雨婷 卢超 《电子测量与仪器学报》 北大核心 2025年第8期22-29,共8页
航空涡轮叶片的热障涂层可降低叶片表面温度、防止表面高温腐蚀,涂层缺陷严重影响叶片使用性能,复杂的叶片曲面形状及其基体结构导致涂层缺陷的无损检测困难。鉴于瑞利波对表面应力和表面微裂纹等损伤变化敏感的特性,提出了基于广义瑞... 航空涡轮叶片的热障涂层可降低叶片表面温度、防止表面高温腐蚀,涂层缺陷严重影响叶片使用性能,复杂的叶片曲面形状及其基体结构导致涂层缺陷的无损检测困难。鉴于瑞利波对表面应力和表面微裂纹等损伤变化敏感的特性,提出了基于广义瑞利波传播的涡轮叶片热障涂层表面微裂纹缺陷无损检测方法。设计了专用超声阵列换能器并搭建了瑞利波检测系统,提取沿叶片宽度方向上叶背涂层中传播的瑞利波检测信号,分析叶片幅度的分布特征与叶片内部复杂结构的关联;最后,分析叶片中人工窄槽对瑞利波传播特征的影响,并提出涂层缺陷的广义瑞利波检测方法。结果表明,涡轮叶片复杂表面轮廓、内腔导流结构导致对瑞利波幅度具有显著影响;将完好叶片涂层的瑞利波幅度分布与带窄槽(500μm×80μm×20μm)的叶片涂层瑞利波幅度分布特征相对比表明,含窄槽路径上传播的超声波幅度明显上升,平均增大了54.3 mV,该特征可用于涡轮叶片热障涂层表面微裂纹缺陷损伤的无损检测。 展开更多
关键词 涡轮叶片 热障涂层 瑞利波 微裂纹
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EVOLUTION OF IDEAL MICRO-CRACK SYSTEM 被引量:2
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作者 柯孚久 白以龙 夏蒙棼 《Science China Mathematics》 SCIE 1990年第12期1447-1459,共13页
The ideal micro-cracks are treated with the number-density function; the characteristics of their evolution are investigated; a deterministic model is applied to the discussion of their extension. It is discowred that... The ideal micro-cracks are treated with the number-density function; the characteristics of their evolution are investigated; a deterministic model is applied to the discussion of their extension. It is discowred that under certain conditions saturation may occur in the number-density. The main features of the statistical formulationare illustrated by several examples and compared with those observed in experiments. 展开更多
关键词 IDEAL micro-crackS number-density SATURATION NUCLEATION extension.
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