The supersaturated solution of MgO· 3B2O3 18% MgSO4 H2O was prepared and then reacted under hydrothermal condition at 120℃ . The solid phases of the different time were identified by means of chemical analysis, ...The supersaturated solution of MgO· 3B2O3 18% MgSO4 H2O was prepared and then reacted under hydrothermal condition at 120℃ . The solid phases of the different time were identified by means of chemical analysis, XRD, FT IR, SEM. The results show that the solid phases are spherical and sheet szaibelyite, which is different from those of non hydrothermal condition. On these grounds we suggested the crystallization mechanism of szaibelyite under the hydrothermal condition and then discussed the effects of hydrothermal properties on the crystallization mechanism.展开更多
The oxidative coupling of methane over Li2SO4/BaCe0.93La0.07O3 irradiated by microwave is reported. Compared with conventional heating mode. under the microwave radiation the temperature of catalytic bed is lower and ...The oxidative coupling of methane over Li2SO4/BaCe0.93La0.07O3 irradiated by microwave is reported. Compared with conventional heating mode. under the microwave radiation the temperature of catalytic bed is lower and the products were changed in selectivity favouring the production of C2 compounds.展开更多
文摘The supersaturated solution of MgO· 3B2O3 18% MgSO4 H2O was prepared and then reacted under hydrothermal condition at 120℃ . The solid phases of the different time were identified by means of chemical analysis, XRD, FT IR, SEM. The results show that the solid phases are spherical and sheet szaibelyite, which is different from those of non hydrothermal condition. On these grounds we suggested the crystallization mechanism of szaibelyite under the hydrothermal condition and then discussed the effects of hydrothermal properties on the crystallization mechanism.
文摘The oxidative coupling of methane over Li2SO4/BaCe0.93La0.07O3 irradiated by microwave is reported. Compared with conventional heating mode. under the microwave radiation the temperature of catalytic bed is lower and the products were changed in selectivity favouring the production of C2 compounds.