As an emerging multifunctional metal with the lowest melting point except for mercury,gallium combines a wide range of metallic and non-metallic elements to form advanced semiconductors critically important in cutting...As an emerging multifunctional metal with the lowest melting point except for mercury,gallium combines a wide range of metallic and non-metallic elements to form advanced semiconductors critically important in cutting-edge technologies.However,due to its low melting point and poor machinability,it is quite difficult to simultaneously characterize gallium’s elastic properties and damping characteristics using conventional methods,which is es-sential in designing and evaluating gallium-based structures.Therefore,developing effective methods to achieve accurate and efficient measurements of Young’s modulus and corresponding internal friction of gallium is of great significance.This letter studies simultaneous measurements of the variations in Young’s modulus and internal friction of gallium at varying temperatures by employing the modified piezoelectric ultrasonic composite oscil-lator technique.Combining the explicit theoretical formulas with the measured resonance and anti-resonance frequencies,it has been discovered that Young’s modulus undergoes an approximately linear decrease as the temperature rises,declining from 83.84 GPa at -70℃ to 79.37 GPa at 20℃.Moreover,like aluminum in the same Group ⅢA of the Periodic Table of Elements and exhibits a grain-boundary internal friction peak,gallium displays a longitudinal internal friction peak at approximately-12°C,with the peak value reaching 1.77×10^(-3).This basic research on gallium’s elastic properties and damping characteristics under low-temperature condi-tions will inspire further explorations of the mechanical properties of a diverse spectrum of low-melting-point functional materials and facilitate applications of gallium-based structures under complex conditions.展开更多
Laser 3D printing,also known as laser additive manufacturing(LAM),is favored for its ability to form bulk metallic glass(BMG)and its composite materials(BMGcs)with freeform geometries.In this work,two different kinds ...Laser 3D printing,also known as laser additive manufacturing(LAM),is favored for its ability to form bulk metallic glass(BMG)and its composite materials(BMGcs)with freeform geometries.In this work,two different kinds of Fe_(41)Co_(7)Cr_(15)Mo_(14)C_(15)B_(6)Y_(2)amorphous coatings(A and B)were prepared by using LAM technology under air-and water-cooled conditions,respectively;meanwhile,to reduce the cracks generated due to the residual thermal stresses,coating C obtained by air-sweep annealing of B with a low energy-density laser.The morphology and amorphous content and microstructure of the coatings were investigated,the results show many cracks in coating B deposited under water-cooled conditions,and its microstructure shows an amorphous-crystal-nanocrystalline mixed structure.Cracking was suppressed in coating C,obtained by air-sweep annealing based on coating B,but the amorphous content was reduced from 32.6 to 13.4%.And the hardness and corrosion resistance of the coating will increase with the increase in the amorphous content.Finally,the internal friction behavior of a BMGcs was prepared on the basis of the process of sample C is compared with that of as-cast amorphous alloys.The results show that the low temperature internal friction behavior of BMGcs is affected by the defects produced during printing,and the high temperature internal friction behavior is affected by the precipitated hard phase.展开更多
The 304 stainless steel with nanostructured surface layer was successfully obtained by using the high-energy shot peening (HESP) method. The internal friction and Young's modulus of this kind of surface nanocrysta...The 304 stainless steel with nanostructured surface layer was successfully obtained by using the high-energy shot peening (HESP) method. The internal friction and Young's modulus of this kind of surface nanocrystallized material were dynamically measured by means of the vibrating reed apparatus. The results implied that different treatment time could induce different microstructure and distribution characteristic of defects in this kind of materials. It is also demonstrated that there is a transition layer between the nano-layer on surface and the coarse grain region inside. The transition layer obviously has certain influence on the overall mechanical properties.展开更多
An investigation on strain amplitude-dependent internal friction （IF） of an as-cast high damping Mg-7 wt% Ni alloy was carried out. In the range of our tested strain amplitudes, whether the strain amplitude is incre...An investigation on strain amplitude-dependent internal friction （IF） of an as-cast high damping Mg-7 wt% Ni alloy was carried out. In the range of our tested strain amplitudes, whether the strain amplitude is increasing or decreasing, the strain amplitude-dependent IF curve can be divided into two stages： one is the strain amplitude weakly dependent part and the other is the strain amplitude strongly dependent part. However, after several cyclic vibrations, the IF values measured during the strain amplitude increasing are smaller than those obtained during the strain amplitude decreasing. The phenomenon is also observed at 100 C. Partial dislocations generate a short-range slip under the cyclic stress to be responsible for it.展开更多
In order to investigate the effect of internal friction of umbilical cable on its vortex-induced vibration(VIV)responses,the experimental study on VIV of bond umbilical cable(BUC)and un-bond umbilical cable(UBUC)was c...In order to investigate the effect of internal friction of umbilical cable on its vortex-induced vibration(VIV)responses,the experimental study on VIV of bond umbilical cable(BUC)and un-bond umbilical cable(UBUC)was carried out in an experimental tank.A current generator in the laboratory simulated the uniform current,and the current velocities were observed in real time by using a Doppler Velocimeter.In addition,different sizes of top tension were applied to the umbilical cable model.The VIV responses of the umbilical cable model were measured by using Fiber Bragg grating(FBG)strain sensors.The displacement responses of umbilical cable model were reconstructed based on the experimental strain data processed by modal superposition method.In this paper,the traveling wave characteristics,the spatial-temporal distribution characteristics of frequency and fatigue damage of the BUC and UBUC under VIV are studied.The experimental results show that there are obvious differences between BUC and UBUC in the response characteristics of VIV.The UBUC appears the traveling wave sooner than BUC,but its standing wave characteristics are more obvious than those of BUC at high velocities.Compared with BUC,the spatial-temporal distribution of UBUC frequencies appears wide-band distribution sooner,but has narrower bandwidth in the"lock-in"state.The level of fatigue damage of BUC was approximately the same as that of UBUC.展开更多
The effect of precipitation on the internal friction(IF)of AZ91 magnesium alloy was investigated by using X-ray diffraction(XRD)analysis,scanning electron microscope(SEM)observation,and dynamic mechanical analysis(DMA...The effect of precipitation on the internal friction(IF)of AZ91 magnesium alloy was investigated by using X-ray diffraction(XRD)analysis,scanning electron microscope(SEM)observation,and dynamic mechanical analysis(DMA).Six different states of alloy were prepared by applying different heat treatment processes:as-cast,in-complete solid solution,complete solid solution,micro-precipitation,continuous precipitation and continuous-discontinuous precipitation.It was found that the internal friction of in-completely solid-solutionized,completely solid-solutionized and micro-precipitated specimens showed a similar characteristic,and the grain boundary relaxation is completed depressed due to the Al atoms supersaturated in theα-Mg solution.However,a thermal relaxation internal friction peak was observed for continuously precipitated and continuously-discontinuously precipitated specimens at around 438 K and frequency of about 1 Hz,which was attributed to the grain boundaries relaxation.Furthermore,it was found that the relaxation of theβ-Mg17Al12/α-Mg phase interfaces should give its contribution to the background internal friction in the as-cast,continuously precipitated and continuously-discontinuously precipitated specimens.展开更多
Internal friction and elastic modulus of ternary Mn-Cu-Al alloys containing 56—60 wt-% Mn,0-3.59 wt-% Al were measured with acoustic frequency,1 kHz,in the tempera- ture range of-150 to 150℃.It was found that when t...Internal friction and elastic modulus of ternary Mn-Cu-Al alloys containing 56—60 wt-% Mn,0-3.59 wt-% Al were measured with acoustic frequency,1 kHz,in the tempera- ture range of-150 to 150℃.It was found that when the specimen was aged in the temperature range under the spinodal curve within the miscibility gap(400—500℃),the internal fric- tion increases with an increase of the aging time and reaches a maximum value at a certain ag- ing time which is shorter with a higher aging temperature.Two internal friction peaks which did not appear before the aging were observed above room temperature after a definite aging time.These are respectively the martensitic tranformation peak and the relaxation peak orig- inating from the stress-induced movement of the twin boundaries.The former peak shifts to- ward higher temperatures with an increase of the aging time,whereas the relaxation peak ap- pearing at 15℃,is independent of the aging time and temperature.The activation energy as- sociated with the relaxation peak was found to be 0.56 eV which is about the same as that of the relaxation peak in binary alloy containing 90 wt-% Mn.It was also found that the hardness,strength and the brittleness of the specimen increase when aged below the spinodal curve within the miscibility gap.The addition or Al enhances the strength but reduces the in- ternal friction of the specimen.A choice of suitable aging time and temperature can give an optimum compromise of high strength and high internal friction.Analysis of experimental re- sults suggests that spinodal decomposition leads to Mn-rich zones in the specimen and thus causes the phase transformation and the change of mechanical properties of the specimen.展开更多
The internal frictions of the specimens in the waist centre of the commercial BNb and BNbRE rails, which were left in air for two years, were measured. It is found that there is an obvious Snoek-Kê-Koester （SKK...The internal frictions of the specimens in the waist centre of the commercial BNb and BNbRE rails, which were left in air for two years, were measured. It is found that there is an obvious Snoek-Kê-Koester （SKK） peak in both steels, and still exists a measurable deformation-enhanced Shock peak（DESP） in the specimens of the BNbRE steel. The internal frictions in the deformed specimens of the both steel rails were also measured. Unlike the case of the tread specimens showing a decrease of SKK damping due to deformation, the SKK damping of the rail waist specimens increases after deformation; and the specimens containing rare earth（RE） show more noticeable damping increase than those without RE. The results of the internal friction measured during ascending and descending temperature under 700℃ show that there is a high temperature damping which can be completely disappeared during descending temperature for both steels.展开更多
Internal friction （IF） spectra during reverse martensitic transformation from 35 to 135°C at different temperature rates of 0.5,0.75,and 1°C/min for Ti50Ni27Cu23 shape memory alloy （SMA） samples were mea...Internal friction （IF） spectra during reverse martensitic transformation from 35 to 135°C at different temperature rates of 0.5,0.75,and 1°C/min for Ti50Ni27Cu23 shape memory alloy （SMA） samples were measured with a dynamic mechanical analyzer,respectively.The IF spectra were characterized by IF peak increasing progressively and peak shifting toward high temperature with an increase in temperature rate.An iterative approach was used to calculate the precise intrinsic and approximate transitory IF contributions to the normal IF spectrum.The quantitatively analyzed results indicate that the transitory IF of this alloy is nonlinearly dependent on the temperature rate and obeys a power law with a power coefficient of 0.55.The predicted and experimental IF spectra at different temperature rates of 0.75 and 1°C/min agree well with each other,respectively.展开更多
The characteristics of the low frequency internal friction and the modulus effect associated with the non-equilibrium spinodal pretransformation and the following discontinuous trans- formation was investigated in an ...The characteristics of the low frequency internal friction and the modulus effect associated with the non-equilibrium spinodal pretransformation and the following discontinuous trans- formation was investigated in an as-quenched eutectiod Al-Zn alloy.It was observed that the loss of the stability in the lattice,which corresponded to the large-amplitude long-wavelength static concentration wave in the non-equilibrium spinodal pretransformation,did not induce any effect of localized soft modulus.Although there are two aging internal friction peaks in phase transformation which correspond to the appearance and disappearance of the coherency in spinodal pretransformation and the maximum of the interface area in the discontinuous transformation respectively,the effect of localized soft modulus did not take place yet.展开更多
The internal friction and precipitate phases of the deformed Fe-P-N alloys have been investigated. It has been found that the ratio of depends on the content of P and the relation holds if the content of N is lower th...The internal friction and precipitate phases of the deformed Fe-P-N alloys have been investigated. It has been found that the ratio of depends on the content of P and the relation holds if the content of N is lower than 30wt.ppm and the content of P is lower than 640wt.ppm. It shows that the intercept K2 is related to the presence of the atomic pairs and clusters of P in the alloy matrix.展开更多
The variation of cyclic stress,internal friction and ultrasonic attenuation during cyclic deformation and relations among them have been investigated with different slip orientation Al single crystals.The results indi...The variation of cyclic stress,internal friction and ultrasonic attenuation during cyclic deformation and relations among them have been investigated with different slip orientation Al single crystals.The results indicate that the value of cyclic stress σ,internal friction Q^(-1)and ultrasonic attenuation △α depend obviously on the slip orientation.There are large differences in above three parameters for different slip orientation Al crystals.In early stage of fatigue life,σ and △α increase and Q^(-1)decreases with cycles N,and △α reached maxi- mum before σ,while Q^(-1)and σ get the valley and the peak,respectively,at same cycles.展开更多
The grain boundary internal friction(GBIF)in Fe-P and Fe-P-La alloys containing trace Cu has been studied.It is found that an addition of 0.584—0.722 wt-% La obviously reduces the IF,shifts grain boundary peaks towar...The grain boundary internal friction(GBIF)in Fe-P and Fe-P-La alloys containing trace Cu has been studied.It is found that an addition of 0.584—0.722 wt-% La obviously reduces the IF,shifts grain boundary peaks towards higher temperatures,and produces a small addi- tional peak at even higher temperature.The mechanism of GBIF is explained as the movement of defects of atomic size,namely point defects,at gram boundaries and/or their clusters un- der stress.展开更多
The influence of longitudinal and torsional bias stresses on anomalous amplitude-dependent internal friction was studied.The longitudinal bias stress may always weaken the anomalous amplitude-dependent effect,while th...The influence of longitudinal and torsional bias stresses on anomalous amplitude-dependent internal friction was studied.The longitudinal bias stress may always weaken the anomalous amplitude-dependent effect,while the torsional one may induce different effects from differ- ent directions applied.Bias stress effect exhibits only in properly heat treated and cold worked ahoy specimens.The anomalous amplitude-dependent internal friction peaks,P_3,P_2 and P_1, are found to be related closely to slant dislocation kink chains.Thus,the application of bias stress to internal friction would be contributed to the study on dislocation structure.展开更多
The behavior of rare earth element Ce in 2090 Al Li alloys was studied by the method of low frequency internal friction.The results showed that rare earth element Ce can increase the activation energy of grain bounda...The behavior of rare earth element Ce in 2090 Al Li alloys was studied by the method of low frequency internal friction.The results showed that rare earth element Ce can increase the activation energy of grain boundary and improve the grain boundary strength of alloys.Rare earth element Ce can decrease the tendency of softening of elastic modulus of 2090 Al Li alloys after heat cycle and keep high elastic modulus of initial state.展开更多
The internal friction （IF） of Mg-0.6%Zr alloy is measured in the present study and two IF peaks of （PI （97 ℃, 1 Hz） and P2 （230 ℃, 1Hz）） are found, respectively. It is shown that the novel P1 peak is frequen...The internal friction （IF） of Mg-0.6%Zr alloy is measured in the present study and two IF peaks of （PI （97 ℃, 1 Hz） and P2 （230 ℃, 1Hz）） are found, respectively. It is shown that the novel P1 peak is frequency independent and the peak temperature increased with the increase of strain amplitude or heating rate. P1 peak could be repressed by the reheating-up measurements and represented by heat treatment. The mechanism of PI peak is clarified by optical microscope （OM） and transmission electron microscope （TEM） observation, and considered to be caused by the creation and expansion of dislocations during plastic deformation. The P2 peak is a thermally activated relaxation IF peak, and activation energy is 1.46 eV, which is caused by the relaxation of the grain boundaries in Mg-0.6%Zr alloy.展开更多
Ni_(50.5)Mn_(25)Ga_(24.5)alloy with cellular microstructure was fabricated.The effect of the cellular microstructure on the internal friction(IF)behavior associated with martensitic transformation(MT),premartensitic t...Ni_(50.5)Mn_(25)Ga_(24.5)alloy with cellular microstructure was fabricated.The effect of the cellular microstructure on the internal friction(IF)behavior associated with martensitic transformation(MT),premartensitic transformation(PMT)and twin boundary motion(TBM)was investigated.Compared with conventional NiMn-Ga alloys,the temperature span of the IF_(MT)peak is significantly expanded,the IF_(PMT)is weakened,and no IF_(TBM)is detected.Both IF_(MT)and IF_(PMT)in the cellular microstructure exhibit unique frequency dispersion feature which has never been observed in conventional Ni-Mn-Ga alloys.The effect of point defects associated with the cellular microstructure is considered to understand the observed results.展开更多
The present investigation showed that the re- laxation peak at about 200℃ (f≈1Hz) was related to bainitic transformation in a CuZnAl alloy.The peak decreased when bainite precipitated.The activation energy of the pe...The present investigation showed that the re- laxation peak at about 200℃ (f≈1Hz) was related to bainitic transformation in a CuZnAl alloy.The peak decreased when bainite precipitated.The activation energy of the peak was the same as the apparent activation energy of bainitic transforma- tion.According to the relations between the peak and the bainitic transformation,the mechanism of the peak has been discussed.展开更多
1. Introduction CuZnAl shape memory alloys have beenextensively studied as a new type of material.Dejonghe[1]et al. firstly reported theirresults on the internal friction (IF) of CuZnAlalloys in 1975. Later, some rese...1. Introduction CuZnAl shape memory alloys have beenextensively studied as a new type of material.Dejonghe[1]et al. firstly reported theirresults on the internal friction (IF) of CuZnAlalloys in 1975. Later, some researchershave done much work on internal friction.But most of them were concerned withphase transformation internal frictionof martensite and reverse martensite andfew of them were about internal friction展开更多
Based on the relationship between parameters of grain boundary internal friction peak (GBP) and grain boundary character distribution (GBCD), and the internal friction results of Al-Mg, Al-Ga, Al-Cu and Al-Zn alloys, ...Based on the relationship between parameters of grain boundary internal friction peak (GBP) and grain boundary character distribution (GBCD), and the internal friction results of Al-Mg, Al-Ga, Al-Cu and Al-Zn alloys, the addition of different kinds of solute atoms has different effects on GBCD. Among them, Mg atoms are able to concentrate and stabilize GBCD in Al-Mg alloys. The origin of these effects of solute atoms on GBCD is also discussed.展开更多
基金financially supported by the National Key R&D Program of China(Grant No.2023YFF0716800)the National Natural Science Foundation of China(Grant No.12074160)the Natural Science Foundation of Liaoning Province of China(Grant No.2024-MS-181).
文摘As an emerging multifunctional metal with the lowest melting point except for mercury,gallium combines a wide range of metallic and non-metallic elements to form advanced semiconductors critically important in cutting-edge technologies.However,due to its low melting point and poor machinability,it is quite difficult to simultaneously characterize gallium’s elastic properties and damping characteristics using conventional methods,which is es-sential in designing and evaluating gallium-based structures.Therefore,developing effective methods to achieve accurate and efficient measurements of Young’s modulus and corresponding internal friction of gallium is of great significance.This letter studies simultaneous measurements of the variations in Young’s modulus and internal friction of gallium at varying temperatures by employing the modified piezoelectric ultrasonic composite oscil-lator technique.Combining the explicit theoretical formulas with the measured resonance and anti-resonance frequencies,it has been discovered that Young’s modulus undergoes an approximately linear decrease as the temperature rises,declining from 83.84 GPa at -70℃ to 79.37 GPa at 20℃.Moreover,like aluminum in the same Group ⅢA of the Periodic Table of Elements and exhibits a grain-boundary internal friction peak,gallium displays a longitudinal internal friction peak at approximately-12°C,with the peak value reaching 1.77×10^(-3).This basic research on gallium’s elastic properties and damping characteristics under low-temperature condi-tions will inspire further explorations of the mechanical properties of a diverse spectrum of low-melting-point functional materials and facilitate applications of gallium-based structures under complex conditions.
基金This work was supported by the National Natural Science Foundation of China(No.52161028)the Major Discipline Academic and Technical Leaders Training Program of Jiangxi Province(No.20213BCJ22017).
文摘Laser 3D printing,also known as laser additive manufacturing(LAM),is favored for its ability to form bulk metallic glass(BMG)and its composite materials(BMGcs)with freeform geometries.In this work,two different kinds of Fe_(41)Co_(7)Cr_(15)Mo_(14)C_(15)B_(6)Y_(2)amorphous coatings(A and B)were prepared by using LAM technology under air-and water-cooled conditions,respectively;meanwhile,to reduce the cracks generated due to the residual thermal stresses,coating C obtained by air-sweep annealing of B with a low energy-density laser.The morphology and amorphous content and microstructure of the coatings were investigated,the results show many cracks in coating B deposited under water-cooled conditions,and its microstructure shows an amorphous-crystal-nanocrystalline mixed structure.Cracking was suppressed in coating C,obtained by air-sweep annealing based on coating B,but the amorphous content was reduced from 32.6 to 13.4%.And the hardness and corrosion resistance of the coating will increase with the increase in the amorphous content.Finally,the internal friction behavior of a BMGcs was prepared on the basis of the process of sample C is compared with that of as-cast amorphous alloys.The results show that the low temperature internal friction behavior of BMGcs is affected by the defects produced during printing,and the high temperature internal friction behavior is affected by the precipitated hard phase.
文摘The 304 stainless steel with nanostructured surface layer was successfully obtained by using the high-energy shot peening (HESP) method. The internal friction and Young's modulus of this kind of surface nanocrystallized material were dynamically measured by means of the vibrating reed apparatus. The results implied that different treatment time could induce different microstructure and distribution characteristic of defects in this kind of materials. It is also demonstrated that there is a transition layer between the nano-layer on surface and the coarse grain region inside. The transition layer obviously has certain influence on the overall mechanical properties.
基金financially supported by the Natural Science Foundation of Jiangxi Province(No. 20114BAB216015)Natural Science Foundation of China(No. 50671083)
文摘An investigation on strain amplitude-dependent internal friction （IF） of an as-cast high damping Mg-7 wt% Ni alloy was carried out. In the range of our tested strain amplitudes, whether the strain amplitude is increasing or decreasing, the strain amplitude-dependent IF curve can be divided into two stages： one is the strain amplitude weakly dependent part and the other is the strain amplitude strongly dependent part. However, after several cyclic vibrations, the IF values measured during the strain amplitude increasing are smaller than those obtained during the strain amplitude decreasing. The phenomenon is also observed at 100 C. Partial dislocations generate a short-range slip under the cyclic stress to be responsible for it.
基金the Natural Science Foundation of Shandong Province(Grant No.2018GHY115045)the National Natural Science Foundation of China(Grant Nos.51979257 and 51709161).
文摘In order to investigate the effect of internal friction of umbilical cable on its vortex-induced vibration(VIV)responses,the experimental study on VIV of bond umbilical cable(BUC)and un-bond umbilical cable(UBUC)was carried out in an experimental tank.A current generator in the laboratory simulated the uniform current,and the current velocities were observed in real time by using a Doppler Velocimeter.In addition,different sizes of top tension were applied to the umbilical cable model.The VIV responses of the umbilical cable model were measured by using Fiber Bragg grating(FBG)strain sensors.The displacement responses of umbilical cable model were reconstructed based on the experimental strain data processed by modal superposition method.In this paper,the traveling wave characteristics,the spatial-temporal distribution characteristics of frequency and fatigue damage of the BUC and UBUC under VIV are studied.The experimental results show that there are obvious differences between BUC and UBUC in the response characteristics of VIV.The UBUC appears the traveling wave sooner than BUC,but its standing wave characteristics are more obvious than those of BUC at high velocities.Compared with BUC,the spatial-temporal distribution of UBUC frequencies appears wide-band distribution sooner,but has narrower bandwidth in the"lock-in"state.The level of fatigue damage of BUC was approximately the same as that of UBUC.
文摘The effect of precipitation on the internal friction(IF)of AZ91 magnesium alloy was investigated by using X-ray diffraction(XRD)analysis,scanning electron microscope(SEM)observation,and dynamic mechanical analysis(DMA).Six different states of alloy were prepared by applying different heat treatment processes:as-cast,in-complete solid solution,complete solid solution,micro-precipitation,continuous precipitation and continuous-discontinuous precipitation.It was found that the internal friction of in-completely solid-solutionized,completely solid-solutionized and micro-precipitated specimens showed a similar characteristic,and the grain boundary relaxation is completed depressed due to the Al atoms supersaturated in theα-Mg solution.However,a thermal relaxation internal friction peak was observed for continuously precipitated and continuously-discontinuously precipitated specimens at around 438 K and frequency of about 1 Hz,which was attributed to the grain boundaries relaxation.Furthermore,it was found that the relaxation of theβ-Mg17Al12/α-Mg phase interfaces should give its contribution to the background internal friction in the as-cast,continuously precipitated and continuously-discontinuously precipitated specimens.
文摘Internal friction and elastic modulus of ternary Mn-Cu-Al alloys containing 56—60 wt-% Mn,0-3.59 wt-% Al were measured with acoustic frequency,1 kHz,in the tempera- ture range of-150 to 150℃.It was found that when the specimen was aged in the temperature range under the spinodal curve within the miscibility gap(400—500℃),the internal fric- tion increases with an increase of the aging time and reaches a maximum value at a certain ag- ing time which is shorter with a higher aging temperature.Two internal friction peaks which did not appear before the aging were observed above room temperature after a definite aging time.These are respectively the martensitic tranformation peak and the relaxation peak orig- inating from the stress-induced movement of the twin boundaries.The former peak shifts to- ward higher temperatures with an increase of the aging time,whereas the relaxation peak ap- pearing at 15℃,is independent of the aging time and temperature.The activation energy as- sociated with the relaxation peak was found to be 0.56 eV which is about the same as that of the relaxation peak in binary alloy containing 90 wt-% Mn.It was also found that the hardness,strength and the brittleness of the specimen increase when aged below the spinodal curve within the miscibility gap.The addition or Al enhances the strength but reduces the in- ternal friction of the specimen.A choice of suitable aging time and temperature can give an optimum compromise of high strength and high internal friction.Analysis of experimental re- sults suggests that spinodal decomposition leads to Mn-rich zones in the specimen and thus causes the phase transformation and the change of mechanical properties of the specimen.
基金Project supported bythe Ministry of National Science and Technique (2002BA315A-5-1-2)
文摘The internal frictions of the specimens in the waist centre of the commercial BNb and BNbRE rails, which were left in air for two years, were measured. It is found that there is an obvious Snoek-Kê-Koester （SKK） peak in both steels, and still exists a measurable deformation-enhanced Shock peak（DESP） in the specimens of the BNbRE steel. The internal frictions in the deformed specimens of the both steel rails were also measured. Unlike the case of the tread specimens showing a decrease of SKK damping due to deformation, the SKK damping of the rail waist specimens increases after deformation; and the specimens containing rare earth（RE） show more noticeable damping increase than those without RE. The results of the internal friction measured during ascending and descending temperature under 700℃ show that there is a high temperature damping which can be completely disappeared during descending temperature for both steels.
文摘Internal friction （IF） spectra during reverse martensitic transformation from 35 to 135°C at different temperature rates of 0.5,0.75,and 1°C/min for Ti50Ni27Cu23 shape memory alloy （SMA） samples were measured with a dynamic mechanical analyzer,respectively.The IF spectra were characterized by IF peak increasing progressively and peak shifting toward high temperature with an increase in temperature rate.An iterative approach was used to calculate the precise intrinsic and approximate transitory IF contributions to the normal IF spectrum.The quantitatively analyzed results indicate that the transitory IF of this alloy is nonlinearly dependent on the temperature rate and obeys a power law with a power coefficient of 0.55.The predicted and experimental IF spectra at different temperature rates of 0.75 and 1°C/min agree well with each other,respectively.
文摘The characteristics of the low frequency internal friction and the modulus effect associated with the non-equilibrium spinodal pretransformation and the following discontinuous trans- formation was investigated in an as-quenched eutectiod Al-Zn alloy.It was observed that the loss of the stability in the lattice,which corresponded to the large-amplitude long-wavelength static concentration wave in the non-equilibrium spinodal pretransformation,did not induce any effect of localized soft modulus.Although there are two aging internal friction peaks in phase transformation which correspond to the appearance and disappearance of the coherency in spinodal pretransformation and the maximum of the interface area in the discontinuous transformation respectively,the effect of localized soft modulus did not take place yet.
文摘The internal friction and precipitate phases of the deformed Fe-P-N alloys have been investigated. It has been found that the ratio of depends on the content of P and the relation holds if the content of N is lower than 30wt.ppm and the content of P is lower than 640wt.ppm. It shows that the intercept K2 is related to the presence of the atomic pairs and clusters of P in the alloy matrix.
文摘The variation of cyclic stress,internal friction and ultrasonic attenuation during cyclic deformation and relations among them have been investigated with different slip orientation Al single crystals.The results indicate that the value of cyclic stress σ,internal friction Q^(-1)and ultrasonic attenuation △α depend obviously on the slip orientation.There are large differences in above three parameters for different slip orientation Al crystals.In early stage of fatigue life,σ and △α increase and Q^(-1)decreases with cycles N,and △α reached maxi- mum before σ,while Q^(-1)and σ get the valley and the peak,respectively,at same cycles.
文摘The grain boundary internal friction(GBIF)in Fe-P and Fe-P-La alloys containing trace Cu has been studied.It is found that an addition of 0.584—0.722 wt-% La obviously reduces the IF,shifts grain boundary peaks towards higher temperatures,and produces a small addi- tional peak at even higher temperature.The mechanism of GBIF is explained as the movement of defects of atomic size,namely point defects,at gram boundaries and/or their clusters un- der stress.
文摘The influence of longitudinal and torsional bias stresses on anomalous amplitude-dependent internal friction was studied.The longitudinal bias stress may always weaken the anomalous amplitude-dependent effect,while the torsional one may induce different effects from differ- ent directions applied.Bias stress effect exhibits only in properly heat treated and cold worked ahoy specimens.The anomalous amplitude-dependent internal friction peaks,P_3,P_2 and P_1, are found to be related closely to slant dislocation kink chains.Thus,the application of bias stress to internal friction would be contributed to the study on dislocation structure.
文摘The behavior of rare earth element Ce in 2090 Al Li alloys was studied by the method of low frequency internal friction.The results showed that rare earth element Ce can increase the activation energy of grain boundary and improve the grain boundary strength of alloys.Rare earth element Ce can decrease the tendency of softening of elastic modulus of 2090 Al Li alloys after heat cycle and keep high elastic modulus of initial state.
文摘The internal friction （IF） of Mg-0.6%Zr alloy is measured in the present study and two IF peaks of （PI （97 ℃, 1 Hz） and P2 （230 ℃, 1Hz）） are found, respectively. It is shown that the novel P1 peak is frequency independent and the peak temperature increased with the increase of strain amplitude or heating rate. P1 peak could be repressed by the reheating-up measurements and represented by heat treatment. The mechanism of PI peak is clarified by optical microscope （OM） and transmission electron microscope （TEM） observation, and considered to be caused by the creation and expansion of dislocations during plastic deformation. The P2 peak is a thermally activated relaxation IF peak, and activation energy is 1.46 eV, which is caused by the relaxation of the grain boundaries in Mg-0.6%Zr alloy.
基金financially supported by the National Natural Science Foundations of China(No.51601008)。
文摘Ni_(50.5)Mn_(25)Ga_(24.5)alloy with cellular microstructure was fabricated.The effect of the cellular microstructure on the internal friction(IF)behavior associated with martensitic transformation(MT),premartensitic transformation(PMT)and twin boundary motion(TBM)was investigated.Compared with conventional NiMn-Ga alloys,the temperature span of the IF_(MT)peak is significantly expanded,the IF_(PMT)is weakened,and no IF_(TBM)is detected.Both IF_(MT)and IF_(PMT)in the cellular microstructure exhibit unique frequency dispersion feature which has never been observed in conventional Ni-Mn-Ga alloys.The effect of point defects associated with the cellular microstructure is considered to understand the observed results.
文摘The present investigation showed that the re- laxation peak at about 200℃ (f≈1Hz) was related to bainitic transformation in a CuZnAl alloy.The peak decreased when bainite precipitated.The activation energy of the peak was the same as the apparent activation energy of bainitic transforma- tion.According to the relations between the peak and the bainitic transformation,the mechanism of the peak has been discussed.
文摘1. Introduction CuZnAl shape memory alloys have beenextensively studied as a new type of material.Dejonghe[1]et al. firstly reported theirresults on the internal friction (IF) of CuZnAlalloys in 1975. Later, some researchershave done much work on internal friction.But most of them were concerned withphase transformation internal frictionof martensite and reverse martensite andfew of them were about internal friction
文摘Based on the relationship between parameters of grain boundary internal friction peak (GBP) and grain boundary character distribution (GBCD), and the internal friction results of Al-Mg, Al-Ga, Al-Cu and Al-Zn alloys, the addition of different kinds of solute atoms has different effects on GBCD. Among them, Mg atoms are able to concentrate and stabilize GBCD in Al-Mg alloys. The origin of these effects of solute atoms on GBCD is also discussed.
