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In-situ Characterization of Non-aqueous Nano-dispersion Systems by Freeze-etching TEM and Comparative Study with Laser Scattering Method
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作者 欧忠文 《Journal of Wuhan University of Technology(Materials Science)》 SCIE EI CAS 2010年第3期432-436,共5页
In-situ characterization of non-aqueous nano-dispersion systems(NANDS) by freeze-etching transmission electron microscope(FETEM) was reported.To improve just-for-once successive rate of specimen preparation and ge... In-situ characterization of non-aqueous nano-dispersion systems(NANDS) by freeze-etching transmission electron microscope(FETEM) was reported.To improve just-for-once successive rate of specimen preparation and get good characterization results,an improving specimen preparation method of freezing etching was developed.Size,distribution and morphology of NANDS were directly visualized.Some information of particle dispersion feature and particle density can also be obtained.Reproductivity of the FETEM characterization is excellent.Comparing with laser scattering method,which is liable to give positive error especially for small size particle anchoring disperser,FETEM characterization can give more accurate measurement of particle size.Moreover,FETEM can give dispersion feature of nanoparticle in non-aqueous medium. 展开更多
关键词 non-aqueous nano-dispersion system dispersion state in-situ characterization FREEZE-ETCHING laser scattering method
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Disulfiram thermosensitive in-situ gel based on solid dispersion for cataract 被引量:5
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作者 Chunjuan Zhang Tonghua Xu +3 位作者 Donglei Zhang Wei He Siling Wang Tongying Jiang 《Asian Journal of Pharmaceutical Sciences》 SCIE CAS 2018年第6期527-535,共9页
To improve the corneal permeability and water-solubility of disulfiram(DSF), which is an ocular drug for cataract, P188 was selected as a matrix to prepare solid dispersion of DSF(DSF SD) by hot melt method. The DSF S... To improve the corneal permeability and water-solubility of disulfiram(DSF), which is an ocular drug for cataract, P188 was selected as a matrix to prepare solid dispersion of DSF(DSF SD) by hot melt method. The DSF SD was characterized by DSC, XRD, and IR, and the results suggested that DSF was amorphous in DSF SD. The DSF SD was added to borate buffer solution(BBS) contained 20% poloxamer P407 and 1.2% poloxamer P188 to form in-situ gel. In vitro and in vivo experiments revealed that DSF SD combined with in-situ gel(DSF SD/in-situ gel) increased the residence time and the amount of DSF penetrated through the corneal. The pharmacodynamics studies exhibited DSF SD/in-situ gel delayed the development of selenium-induced cataract at some content. These results investigated that DSF SD/in-situ gel as a drug delivery system can improve DSF ocular permeability. 展开更多
关键词 DISULFIRAM Solid dispersion in-situ GEL PERMEABILITY Anti-cataract
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High-pressure phonon dispersion of copper by using the modified analytic embedded atom method 被引量:2
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作者 张晓军 陈长乐 凤飞龙 《Chinese Physics B》 SCIE EI CAS CSCD 2013年第9期520-524,共5页
By using the Born-von Kfirmfin theory of lattice dynamics and the modified analytic embedded atom method, we reproduce the experimental results of the phonon dispersion in fcc metal Cu at zero pressure along three hig... By using the Born-von Kfirmfin theory of lattice dynamics and the modified analytic embedded atom method, we reproduce the experimental results of the phonon dispersion in fcc metal Cu at zero pressure along three high symmetry directions and four oft-symmetry directions, and then simulate the phonon dispersion curves of Cu at high pressures of 50, 100, and 150 GPa. The results show that the shapes of dispersion curves at high pressures are very similar to that at zero pressure. All the vibration frequencies of Cu in all vibration branches at high pressures are larger than the results at zero pressure, and increase correspondingly as pressure reaches 50, 100, and 150 GPa sequentially. Moreover, on the basis of phonon dispersion, we calculate the values of specific heat of Cu at different pressures. The prediction of thermodynamic quantities lays a significant foundation for guiding and judging experiments of thermodynamic properties of solids under high pressures. 展开更多
关键词 phonon dispersion high pressure SIMULATION modified analytic embedded atom method
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Preparation of natural brucite nanofibers by the dispersion method 被引量:2
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作者 Li Xu Wen Ni +3 位作者 Wenping Li Xingde Liu Hailong Yang Xiaoguang Yang 《Journal of University of Science and Technology Beijing》 CSCD 2008年第4期489-494,共6页
The preparation of natural brucite nanofibers through dispersion by the wet process is described. The test results indicate that brucite fibers can be well dispersed by using sodium dioctyl sulfosuccinate (OT) as th... The preparation of natural brucite nanofibers through dispersion by the wet process is described. The test results indicate that brucite fibers can be well dispersed by using sodium dioctyl sulfosuccinate (OT) as the dispersant at a dispersant/fiber mass ratio of 0.15:1, dispersing for 30 min at a water/solid mass ratio of 20:1. The prepared nanofibers were characterized with X-ray diffraction (XRD), scanning electron microscope (SEM), and transmission electron microscope (TEM). It is shown that the prepared single brucite nanofiber is around 30 nm in diameter and the talus of the nonsingle brucite nanofibers is about 50-150 nm in diameter. Natural brucite mineral fibers were treated by the dispersion method to obtain nanomaterials. These fibers have significant advantages over artificial nanofibers both in yield and in cost. 展开更多
关键词 BRUCITE NANOFIBER sodium dioctyl sulfosuccinate (OT) ULTRASONIC dispersion method
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A Solution of the Burger’s Equation Arising in the Longitudinal Dispersion Phenomenon in Fluid Flow through Porous Media by Mixture of New Integral Transform and Homotopy Perturbation Method 被引量:1
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作者 Kunjan Shah Twinkle Singh 《Journal of Geoscience and Environment Protection》 2015年第4期24-30,共7页
The main aim of the paper is to examine the concentration of the longitudinal dispersion phenomenon arising in fluid flow through porous media. These phenomenon yields a partial differential equation namely Burger’s ... The main aim of the paper is to examine the concentration of the longitudinal dispersion phenomenon arising in fluid flow through porous media. These phenomenon yields a partial differential equation namely Burger’s equation, which is solved by mixture of the new integral transform and the homotopy perturbation method under suitable conditions and the standard assumption. This method provides an analytical approximation in a rapidly convergent sequence with in exclusive manner computed terms. Its rapid convergence shows that the method is trustworthy and introduces a significant improvement in solving nonlinear partial differential equations over existing methods. It is concluded that the behaviour of concentration in longitudinal dispersion phenomenon is decreases as distance x is increasing with fixed time t > 0 and slightly increases with time t. 展开更多
关键词 Longitudinal dispersion Phenomenon Porous Media NEW INTEGRAL Transform HOMOTOPY PERTURBATION method
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Microstructures and properties of Al_2O_3 dispersion-strengthened copper alloys prepared through different methods 被引量:6
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作者 Zhi-qiao Yan Feng Chen +2 位作者 Fu-xing Ye Dong-ping Zhang Yi-xiang Cai 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2016年第12期1437-1443,共7页
Al2O3 dispersion copper alloy powder was prepared by intemal oxidation, and three consolidation methods--high-velocity compaction (HVC), hot pressing (HP), and hot extrusion (HE)--were used to prepare Al2O3 disp... Al2O3 dispersion copper alloy powder was prepared by intemal oxidation, and three consolidation methods--high-velocity compaction (HVC), hot pressing (HP), and hot extrusion (HE)--were used to prepare Al2O3 dispersion-strengthened copper (Cu-Al2O3) alloys. The microstructures and properties of these alloys were investigated and compared. The results show that the alloys prepared by the HP and HE methods exhibited the coarsest and finest grain sizes, respectively. The alloy prepared by the HVC method exhibited the lowest relative density (98.3% vs. 99.5% for HP and 100% for HE), which resulted in the lowest electrical conductivity (81% IACS vs. 86% IACS for HP and 87% IACS for HE). However, this alloy also exhibited the highest hardness (77 HRB vs. 69 HRB for HP and 70 HRB for HE), the highest compressive strength (443 MPa vs. 386 MPa for I/P and 378 MPa for HE), and the best hardness retention among the investigated alloys. The results illustrate that the alloy prepared by the HVC method exhibits high softening temperature and good mechanical properties at high temperatures, which imply long service life when used as spot-welding electrodes. 展开更多
关键词 dispersion-strengthened alloys copper alloys ALUMINA preparation methods microstructure properties
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The Acoustic Attenuation Prediction for Seafloor Sediment Based on in-situ Data and Machine Learning Methods
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作者 WANG Jingqiang HOU Zhengyu +6 位作者 CHEN Yinglin LI Guanbao KAN Guangming XIAO Peng LI Zhenglin MO Dinghao HUANG Jingyi 《Journal of Ocean University of China》 2025年第1期95-102,共8页
Accurate acquisition and prediction of acoustic parameters of seabed sediments are crucial in marine sound propagation research.While the relationship between sound velocity and physical properties of sediment has bee... Accurate acquisition and prediction of acoustic parameters of seabed sediments are crucial in marine sound propagation research.While the relationship between sound velocity and physical properties of sediment has been extensively studied,there is still no consensus on the correlation between acoustic attenuation coefficient and sediment physical properties.Predicting the acoustic attenuation coefficient remains a challenging issue in sedimentary acoustic research.In this study,we propose a prediction method for the acoustic attenuation coefficient using machine learning algorithms,specifically the random forest(RF),support vector machine(SVR),and convolutional neural network(CNN)algorithms.We utilized the acoustic attenuation coefficient and sediment particle size data from 52 stations as training parameters,with the particle size parameters as the input feature matrix,and measured acoustic attenuation as the training label to validate the attenuation prediction model.Our results indicate that the error of the attenuation prediction model is small.Among the three models,the RF model exhibited the lowest prediction error,with a mean squared error of 0.8232,mean absolute error of 0.6613,and root mean squared error of 0.9073.Additionally,when we applied the models to predict the data collected at different times in the same region,we found that the models developed in this study also demonstrated a certain level of reliability in real prediction scenarios.Our approach demonstrates that constructing a sediment acoustic characteristics model based on machine learning is feasible to a certain extent and offers a novel perspective for studying sediment acoustic properties. 展开更多
关键词 in-situ measurement ATTENUATION seafloor sediment machine learning methods
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Preparation of Thermosensitive Microcapsules Containing Water Soluble Powder by Melting Dispersion Cooling Method 被引量:1
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作者 Yoshinari Taguchi Natsukaze Saito +1 位作者 Atsunori Uchida Masato Tanaka 《Journal of Encapsulation and Adsorption Sciences》 2016年第3期57-69,共14页
It was tried to prepare the thermosensitive microcapsules containing the water soluble solid powder by the melting dispersion cooling method and to establish the optimum preparation conditions. As a model water solubl... It was tried to prepare the thermosensitive microcapsules containing the water soluble solid powder by the melting dispersion cooling method and to establish the optimum preparation conditions. As a model water soluble solid powder, sodium hydrogen carbonate was adopted in order to generate carbon dioxide gas and as a thermosensitive shell material, olefin resin with the melting point of ca. 40°C was used. In the experiment, the concentration of olefin resin in the shell material solution was mainly changed together with the concentrations of the oil soluble surfactant species and the α-tocopherol as a modifier of shell. Addition of α-tocopherol into the shell material solution could prevent the core from breaking away during the microencapsulation process and result in the higher microencapsulation efficiency, because the dispersion stability of solid powder in the shell material solution could be increased due to the increase in affinity between the shell material solution and solid powder. Also, the microencapsulation efficiency increased with the concentration of olefin resin, became maximum at 50 wt% and then, decreased. The microcapsules were found to begin melting at 36°C and to generate carbon dioxide gas. 展开更多
关键词 Thermosensitive Microcapsules MICROENCAPSULATION Sodium Hydrogen Carbonate Melting dispersion Cooling method Olefin Resin
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GALERKIN METHOD FOR COMPRESSIBLE FLOW OF CONTAMINATION FROM NUCLEAR WASTE WITH MOLECULAR DIFFUSION AND DISPERSION
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作者 程爱杰 王高洪 《Numerical Mathematics A Journal of Chinese Universities(English Series)》 SCIE 1999年第1期39-52,共14页
Abstract A system of quasilinear coupled equations which arise from simulation of contamination of geologic nulear waste in porous media is studied. We’ll discuss Galerkin method for the model of compressible flow wi... Abstract A system of quasilinear coupled equations which arise from simulation of contamination of geologic nulear waste in porous media is studied. We’ll discuss Galerkin method for the model of compressible flow with molecular diffusion and dispersion. Some new techniques are introcued to error analysis. Only one dimensional case is considered. The optimal error estimate in both L^2 and H^1 is proved. A contribution of this paper is how the dispersion term can be handled, 展开更多
关键词 COMPRESSIBLE flow CONTAMINATION of nuclear waste molecular diffusion and dispersion GALERKIN finite element method optimal error estimate.
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LOCAL DISCONTINUOUS GALERKIN METHOD FOR RADIAL POROUS FLOW WITH DISPERSION AND ADSORPTION
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作者 汪继文 刘慈群 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI 2004年第9期977-982,共6页
Based on the local discontinuous Galerkin methods for time-dependent convection-diffusion systems newly developed by Corkburn and Shu,according to the form of the generalized convection-diffusion equations which model... Based on the local discontinuous Galerkin methods for time-dependent convection-diffusion systems newly developed by Corkburn and Shu,according to the form of the generalized convection-diffusion equations which model the radial porous flow with dispersion and adsorption,a local discontinuous Galerkin method for radial porous flow with dispersion and adsorption was developed,a high order accurary new scheme for radial porous flow is obtained.The presented method was applied to the numerical tests of two cases of radial porous,i.e., the convection-dispersion flow and the convection-dispersion-adsorption flow,the corresponding parts of the numerical results are in good agreement with the published solutions,so the presented method is reliable.Reckoning of the computational cost also shows that the method is practicable. 展开更多
关键词 dispersion ADSORPTION radial porous flow local discontinuous Galerkin method
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ADAPTIVE FINITE ELEMENT METHOD FOR ANALYSIS OF POLLUTANT DISPERSION IN SHALLOW WATER
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作者 Somboon Otarawanna Pramote Dechaumphai 《Applied Mathematics and Mechanics(English Edition)》 SCIE EI 2005年第12期1574-1584,共11页
A finite element method for analysis of pollutant dispersion in shallow water is presented. The analysis is divided into two parts : ( 1 ) computation of the velocity flow field and water surface elevation, and (2... A finite element method for analysis of pollutant dispersion in shallow water is presented. The analysis is divided into two parts : ( 1 ) computation of the velocity flow field and water surface elevation, and (2) computation of the pollutant concentration field from the dispersion model. The method was combined with an adaptive meshing technique to increase the solution accuracy, as well as to reduce the computational time and computer memory. The finite element formulation and the computer programs were validated by several examples that have known solutions. In addition, the capability of the combined method was demonstrated by analyzing pollutant dispersion in Chao Phraya River near the gulf of Thailand. 展开更多
关键词 shallow water pollutant dispersion adaptive meshing technique finite element method
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Formation of In-Situ Dispersion Strengthening Particles in Cast FeCrAl Alloy
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作者 FENG Shuo HAN Wei +2 位作者 LUO He-li Karin G LI Chang-hai 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2010年第2期74-78,共5页
In order to fabricate dispersion strengthened alloys strengthened by submicron-sized or nano-sized stable particles through casting routes, understanding of the formation process of dispersion strengthening particles ... In order to fabricate dispersion strengthened alloys strengthened by submicron-sized or nano-sized stable particles through casting routes, understanding of the formation process of dispersion strengthening particles in metal melt is of significance. Thus, nano NiO and TiO2 particles were selected as reactant to form in-situ dispersion strengthening oxide particles in Fe20Cr5Al alloy. Nano NiO and TiO2 particle powder was separately dispersed into nano Ni powder first. The loose mixed nano powder was added in Fe20CrSAl alloy melt when pouring the melt into mold. The study shows that nano NiO particles were not as effective as nano TiO2 particles in forming dispersion strengthening Al2O3 particles. The final diameters of dispersion strengthening oxide particles arose from nano TiO2 particles were of submicron. The Brownian collision of particles had caused this coarsening. 展开更多
关键词 in-situ particle dispersion strengthening particle formation east FeCrAl alloy
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Chebyshev Pseudo-Spectral Method for Solving Fractional Advection-Dispersion Equation 被引量:2
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作者 N. H. Sweilam M. M. Khader M. Adel 《Applied Mathematics》 2014年第19期3240-3248,共9页
Fractional differential equations have recently been applied in various areas of engineering, science, finance, applied mathematics, bio-engineering and others. However, many researchers remain unaware of this field. ... Fractional differential equations have recently been applied in various areas of engineering, science, finance, applied mathematics, bio-engineering and others. However, many researchers remain unaware of this field. In this paper, an efficient numerical method for solving the fractional Advection-dispersion equation (ADE) is considered. The fractional derivative is described in the Caputo sense. The method is based on Chebyshev approximations. The properties of Chebyshev polynomials are used to reduce ADE to a system of ordinary differential equations, which are solved using the finite difference method (FDM). Moreover, the convergence analysis and an upper bound of the error for the derived formula are given. Numerical solutions of ADE are presented and the results are compared with the exact solution. 展开更多
关键词 FRACTIONAL ADVECTION-dispersion Equation Caputo FRACTIONAL DERIVATIVE Finite DIFFERENCE method CHEBYSHEV Pseudo-Spectral method Convergence Analysis
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Mixed Method for Compressible Miscible Displacement with Dispersion in Porous Media 被引量:1
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作者 Chunguang Chen 《Numerical Mathematics A Journal of Chinese Universities(English Series)》 SCIE 2007年第1期74-82,共9页
Compressible miscible displacement of one fluid by another in porous media is modelled by a nonlinear parabolic system. A finite element procedure is introduced to approximate the concentration of one fluid and the pr... Compressible miscible displacement of one fluid by another in porous media is modelled by a nonlinear parabolic system. A finite element procedure is introduced to approximate the concentration of one fluid and the pressure of the mixture. The concentration is treated by a Galerkin method while the pressure is treated by a parabolic mixed finite element method. The effect of dispersion, which is neglected in [1], is considered. Optimal order estimates in L2 are derived for the errors in the approximate solutions. 展开更多
关键词 互溶驱替 有限元分析 流体力学 离差
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A method for determining the complex refractive index dispersion of absorbing materials without thickness information
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作者 DENG Zhichao MEI Jianchun +2 位作者 WANG Jin YE Qing TIAN Jianguo 《Optoelectronics Letters》 EI 2024年第11期676-680,共5页
The complex refractive index dispersion(CRID)of absorbing materials is very important in many fields,especially in printing industry and medical research.However,due to their strong absorbing,CRID determination is sti... The complex refractive index dispersion(CRID)of absorbing materials is very important in many fields,especially in printing industry and medical research.However,due to their strong absorbing,CRID determination is still a challenge.In this study,without diluting treatment or the thickness information,a method is proposed to calculate the CRID of absorbing materials,based merely on the reflectance and transmittance spectra measurements.The method separates the CRID into absorbing part and transparent part based on Kramers-Kronig relations,and it also uses the common Cauchy dispersion formula and Fresnel reflection formula.The CRID of methyl-red-doped poly(methyl methacrylate)(MR-PMMA)(3%mass fraction)and hemoglobin(Hb)solutions(320 g/L)are determined over the spectral range from 400 nm to 750 nm,and the result shows good stability and consistency of the method. 展开更多
关键词 method absorbing dispersion
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Adjoint Method-Based Algorithm for Calculating the Relative Dispersion Ratio in a Hydrodynamic System
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作者 JI Fei JIANG Wensheng GUO Xinyu 《Journal of Ocean University of China》 SCIE CAS CSCD 2021年第4期790-802,共13页
Relative dispersion ratio(RDR)can be used to quantify the deviation behavior of a water parcel’s trajectory caused by a disturbance in a hydrodynamic system.It can be calculated by using a standard method for determi... Relative dispersion ratio(RDR)can be used to quantify the deviation behavior of a water parcel’s trajectory caused by a disturbance in a hydrodynamic system.It can be calculated by using a standard method for determining relative dispersion(RD),which accounts for the growth of the deviation of a cluster of particles from a specific initial time.However,the standard method for computing RD is time consuming.It involves numerous computations on tracing many water parcels.In this study,a new method based on the adjoint method is proposed to acquire a series of RDR fields in one round of tracing.Through this method,the continuous variation in the RDR corresponding to a time series of the disturbance time t can be obtained.The consistency and efficiency of the new method are compared with those of the standard method by applying it to a double-gyre flow and an unsteady Arnold-Beltrami-Childress flow field.Results show that the two methods have good consistency in a finite time span.The new method has a notable speedup for evaluating the RDR at multiple t. 展开更多
关键词 relative dispersion particle tracking adjoint method computational efficiency
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Suppress numerical dispersion in reversetime migration of acoustic wave equation using optimal nearly analytic discrete method
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作者 Liu Ming-Zhu He Bing-Shoug 《Applied Geophysics》 SCIE CSCD 2020年第1期133-142,170,共11页
Using staggered-grid finite difference method to solve seismic wave equation,large spatial grid and high dominant frequency of source cause numerical dispersion,staggeredgrid finite difference method,which can reduce ... Using staggered-grid finite difference method to solve seismic wave equation,large spatial grid and high dominant frequency of source cause numerical dispersion,staggeredgrid finite difference method,which can reduce the step spatial size and increase the order of difference,will multiply the calculation amount and reduce the efficiency of solving wave equation.The optimal nearly analytic discrete(ONAD)method can accurately solve the wave equation by using the combination of displacement and gradient of spatial nodes to approach the spatial partial derivative under rough grid and high-frequency condition.In this study,the ONAD method is introduced into the field of reverse-time migration(RTM)for performing forward-and reverse-time extrapolation of a two-dimensional acoustic equation,and the RTM based on ONAD method is realized via normalized cross-correlation imaging condition,effectively suppressed the numerical dispersion and improved the imaging accuracy.Using ONAD method to image the groove model and SEG/EAGE salt dome model by RTM,and comparing with the migration sections obtained by staggered-grid finite difference method with the same time order 2 nd and space order 4 th,results show that the RTM based on ONAD method can effectively suppress numerical dispersion caused by the high frequency components in source and shot records,and archive accurate imaging of complex geological structures especially the fine structure,and the migration sections of the measured data show that ONAD method has practical application value. 展开更多
关键词 Acoustic wave equation RTM ONAD method numerical dispersion suppression
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A nonparametric spectrum estimation method for dispersion and attenuation analysis of borehole acoustic measurements
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作者 Bing Wang Wei Li +1 位作者 Qing Ye Kun-Yu Ma 《Petroleum Science》 SCIE EI CAS CSCD 2023年第1期241-248,共8页
Dispersion and attenuation analysis can be used to determine formation anisotropy induced by fractures,or stresses.In this paper,we propose a nonparametric spectrum estimation method to get phase dispersion characteri... Dispersion and attenuation analysis can be used to determine formation anisotropy induced by fractures,or stresses.In this paper,we propose a nonparametric spectrum estimation method to get phase dispersion characteristics and attenuation coefficient.By designing an appropriate vector filter,phase velocity,attenuation coefficient and amplitude can be inverted from the waveform recorded by the receiver array.Performance analysis of this algorithm is compared with Extended Prony Method(EPM)and Forward and Backward Matrix Pencil(FBMP)method.Based on the analysis results,the proposed method is capable of achieving high resolution and precision as the parametric spectrum estimation methods.At the meantime,it also keeps high stability as the other nonparametric spectrum estimation methods.At last,applications to synthetic waveforms modeled using finite difference method and real data show its efficiency.The real data processing results show that the P-wave attenuation log is more sensitive to oil formation compared to S-wave;and the S-wave attenuation log is more sensitive to shale formation compared to P-wave. 展开更多
关键词 dispersion analysis Attenuation factor Nonparametric spectrum estimation method Acoustic logging Fluid type evaluation
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Preparation of Microcapsules Containing Aqueous Solution of Azur B with Melting Dispersion Cooling Method and Application to DNA Amplification Detector
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作者 Yoshinari Taguchi Ryohei Yamamoto +1 位作者 Natsukaze Saito Masato Tanaka 《Journal of Encapsulation and Adsorption Sciences》 2014年第1期15-24,共10页
Microcapsules containing the aqueous solution of Azur B of a water soluble dye were prepared with the melting dispersion cooling method and applied to the amplification detector of plant DNA. Paraffin wax with melting... Microcapsules containing the aqueous solution of Azur B of a water soluble dye were prepared with the melting dispersion cooling method and applied to the amplification detector of plant DNA. Paraffin wax with melting temperature of 75°C was used as the shell material. In the experiment, the aqueous solution (W) of Azur B as the core material was dispersed in the melted paraffin wax (O) to form the (W/O) emulsion and then, the (W/O) emulsion was dispersed in the silicon oil (O’) as the continuous phase to form the (W/O)/O’ emulsion at 85°C. After formation of the (W/O)/O’ emulsion, the microcapsules were prepared by cooling the (W/O)/O’ emulsion to 50°C. The microcapsules were prepared by changing the concentration of oil soluble surfactant in the (W/O) emulsion and the volume of the (W/O) emulsion in the (W/O)/O’ emulsion. The microencapsulation efficiency increased with the concentration of oil soluble surfactant and finally became 100% under the optimum conditions. Furthermore, the microcapsules were melted down at temperature of 85°C to reveal the sharp thermal responsibility and to release the aqueous solution of Azur B. As a result, it was found that the microcapsules were able to be applied to the amplification detector of plant DNA by utilizing the reaction between DNA and Azur B. 展开更多
关键词 MICROCAPSULES AZUR B DNA Amplification DETECTOR MELTING dispersion Cooling method Multiple EMULSION
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Gap States of ZnO Thin Films by New Methods:Optical Spectroscopy,Optical Conductivity and Optical Dispersion Energy
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作者 Vali Dalouji Shahram Solaymani +3 位作者 Laya Dejam Seyed Mohammad Elahi TSahar Rezaee Dariush Mehrparvar 《Chinese Physics Letters》 SCIE CAS CSCD 2018年第2期107-110,共4页
The optical reflectance and transmittance spectra in the wavelength range of 300-2500 nm are used to compute the absorption coefficient of zinc oxide films annealed at different post-annealing temperatures 400, 500 an... The optical reflectance and transmittance spectra in the wavelength range of 300-2500 nm are used to compute the absorption coefficient of zinc oxide films annealed at different post-annealing temperatures 400, 500 and 600°C.The values of the cross point between the curves of the real and imaginary parts of the optical conductivity ɑ_1 and ɑ_1 with energy axis of films exhibit values that correspond to optical gaps and are about 3.25-3.3 eV. The maxima of peaks in plots dR/dλ and dT/dλ versus wavelength of films exhibit optical gaps at about 3.12-3.25 eV.The values of the fundamental indirect band gap obtained from the Tauc model are at about 3.14-3.2 eV. It can be seen that films annealed at 600°C have the minimum indirect optical band gap at about 3.15 eV. The films annealed at 600°C have Urbach's energy minimum of 1.38 eV and hence have minimum disorder. The dispersion energy d of films annealed at 500°C has the minimum value of 43 eV. 展开更多
关键词 ZN Gap States of ZnO Thin Films by New methods:Optical Spectroscopy Optical Conductivity and Optical dispersion Energy OC
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