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Multiphysics modeling of coupling compressed-air energy storage-thermal storage in salt caverns:An approach to insoluble sediment as heat reservoir feasibility analysis
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作者 Tsunming Wong Yingjie Wei +2 位作者 Yuxin Jie Xiangyang Zhao Jiamin Zhang 《Deep Underground Science and Engineering》 2025年第4期777-791,共15页
A significant number of salt caverns have high proportions of insoluble sediments,but the thermal storage utilization potential of insoluble sediments remains understudied within current research.Therefore,this study ... A significant number of salt caverns have high proportions of insoluble sediments,but the thermal storage utilization potential of insoluble sediments remains understudied within current research.Therefore,this study aims to explore the feasibility of an integrated compressed-air energy storage(CAES)coupled with insoluble sediment as the thermal storage media for salt caverns.In order to fulfill this objective,this study presents two steps to analyze the insoluble sediment's thermo-mechanical behavior under ordinary CAES conditions and coupled thermal energy storage(TES)conditions separately.A multiphysics-coupled numerical model was developed to investigate the thermal behavior of insoluble sediments at different heights.Then,a dual-cavity model with a sediment-filled channel was constructed to study the heat storage process in long-and short-term modes.Results demonstrated that sediment effectively protected cavern walls from thermal shocks caused by compressed air,maintaining temperature differentials within 1 K.Dual-cavity simulations revealed the sediment's capability to mitigate the temperature fluctuation of compressed air in caverns,achieving a 66% temperature reduction in the outflow interface during operation.The findings confirmed the feasibility of utilizing insoluble sediments for long-term thermal storage applications involving thermal cycles with ΔT=150 K,attaining a heat storage density of 50 kW·h/m^(3).The results show that the heat capacity of the sediment contributes to the cavern wall's stability and provide references for developing integrated CAES-TES systems in sediment-filled salt caverns. 展开更多
关键词 compressed-air energy storage insoluble sediment salt cavern thermal storage
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An insoluble polysaccharide from the sclerotium of Poria cocos improves hyperglycemia, hyperlipidemia and hepatic steatosis in ob/ob mice via modulation of gut microbiota 被引量:93
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作者 SUN Shan-Shan WANG Kai +2 位作者 MA Ke BAO Li LIU Hong-Wei 《Chinese Journal of Natural Medicines》 SCIE CAS CSCD 2019年第1期3-14,共12页
Metabolic syndrome characterized by obesity, hyperglycemia and liver steatosis is becoming prevalent all over the world. Herein, a water insoluble polysaccharide(WIP) was isolated and identified from the sclerotium of... Metabolic syndrome characterized by obesity, hyperglycemia and liver steatosis is becoming prevalent all over the world. Herein, a water insoluble polysaccharide(WIP) was isolated and identified from the sclerotium of Poria cocos, a widely used Traditional Chinese Medicine. WIP was confirmed to be a(1-3)-β-D-glucan with an average Mw of 4.486 × 10~6 Da by NMR and SEC-RI-MALLS analyses. Furthermore, oral treatment with WIP from P. cocos significantly improved glucose and lipid metabolism and alleviated hepatic steatosis in ob/ob mice. 16 S DNA sequencing analysis of cecum content from WIP-treated mice indicated the increase of butyrate-producing bacteria Lachnospiracea, Clostridium. It was also observed that WIP treatment elevated the level of butyrate in gut, improved the gut mucosal integrity and activated the intestinal PPAR-γ pathway. Fecal transplantation experiments definitely confirmed the causative role of gut microbiota in mediating the benefits of WIP. It is the first report that the water insoluble polysaccharide from the sclerotium of P. cocos modulates gut microbiota to improve hyperglycemia and hyperlipidemia. Thereby, WIP from P. cocos, as a prebiotic, has the potential for the prevention or cure of metabolic diseases and may elucidate new mechanism for the efficacies of this traditional herbal medicine on the regulation of lipid and glucose metabolism. 展开更多
关键词 Poria COCOS Water insoluble polysaccharide Metabolic syndrome PREBIOTICS Gut microbiota
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Modifi cation of wheat bran insoluble and soluble dietary fibers with snail enzyme 被引量:21
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作者 Xin Liu Keke Suo +7 位作者 Pei Wang Xue Li Limin Hao Jiaqing Zhu Juanjuan Yi Qiaozhen Kang Jinyong Huang Jike Lu 《Food Science and Human Wellness》 SCIE 2021年第3期356-361,共6页
Insoluble dietary fiber(IDF)and soluble dietary fiber(SDF)extracted from wheat bran were modifi ed by snail enzyme and their physicochemical properties(water retention capacity and oil retention capacity),functional p... Insoluble dietary fiber(IDF)and soluble dietary fiber(SDF)extracted from wheat bran were modifi ed by snail enzyme and their physicochemical properties(water retention capacity and oil retention capacity),functional properties(cholesterol adsorption capacity,glucose adsorption capacity and antioxidant activity)and structural characterizations were evaluated.The results showed that snail enzyme modification led to the significant increase in oil retention capacity of IDF,glucose adsorption capacity and cholesterol adsorption capacity of IDF and SDF.Enzymatic modification also markedly improved the DPPH radical scavenging capacity and reducing power of IDF and SDF.Meanwhile,scanning electron microscopy(SEM)analysis indicated the microstructures of IDF and SDF powders were signifi cantly changed.Fourier transfer-infrared spectrometry(FT-IR)showed that snail enzyme modifi cation could degrade the part of cellulose and hemicellulose of IDF and SDF.All these improved physicochemical and functional properties of IDF and SDF might depend on their structural changes.It suggested that snail enzyme modifi cation could effectively improve physicochemical and functional properties of IDF and SDF from wheat bran. 展开更多
关键词 Snail enzyme insoluble dietary fiber Soluble dietary fiber Physicochemical properties Functional properties
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Cytotoxicity of the soluble and insoluble fractions of atmospheric fine particulate matter 被引量:6
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作者 Ling Liu Qiuhua Zhou +4 位作者 Xuezhi Yang Gang Li Jingzhu Zhang Xuehua Zhou Wei Jiang 《Journal of Environmental Sciences》 SCIE EI CAS CSCD 2020年第5期105-116,共12页
Inhaled atmospheric fine particulate matter(PM2.5)includes soluble and insoluble fractions,and each fraction can interact with cells and cause adverse effects.PM2.5 samples were collected in Jinan,China,and the solubl... Inhaled atmospheric fine particulate matter(PM2.5)includes soluble and insoluble fractions,and each fraction can interact with cells and cause adverse effects.PM2.5 samples were collected in Jinan,China,and the soluble and insoluble fractions were separated.According to physiochemical characterization,the soluble fraction mainly contains watersoluble ions and organic acids,and the insoluble fraction mainly contains kaolinite,calcium carbonate and some organic carbon.The interaction between PM2.5 and model cell membranes was examined with a quartz crystal microbalance with dissipation(QCM-D)to quantify PM2.5 attachment on membranes and membrane disruption.The cytotoxicity of the total PM2.5 and the soluble and insoluble fractions,was investigated.Negatively charged PM2.5 can adhere to the positively charged membranes and disrupt them.PM2.5also adheres to negatively charged membranes but does not cause membrane rupture.Therefore,electrostatic repulsion does not prevent PM2.5 attachment,but electrostatic attraction induces remarkable membrane rupture.The human lung epithelial cell line A549 was used for cytotoxicity assessment.The detected membrane leakage,cellular swelling and blebbing indicated a cell necrosis process.Moreover,the insoluble PM2.5 fraction caused a higher cell mortality and more serious cell membrane damage than the soluble fraction.The levels of reactive oxygen species(ROS)enhanced by the two fractions were not significantly different.The findings provide more information to better understand the mechanism of PM2.5 cytotoxicity and the effect of PM2.5 solubility on cytotoxicity. 展开更多
关键词 PM2.5 Soluble fraction insoluble fraction Membrane rupture Reactive oxygen species
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Genetic Analysis of Chromosomal Loci Affecting the Content of Insoluble Glutenin in Common Wheat 被引量:4
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作者 Huaibing Jin Zhaojun Wang +8 位作者 Da Li Peipei Wu Zhengying Dong Chaowu Rong Xin Liu Huanju Qin Huili Li Daowen Wang Kunpu Zhang 《Journal of Genetics and Genomics》 SCIE CAS CSCD 2015年第9期495-505,共11页
In common wheat, insoluble glutenin (IG) is an important fraction of flour glutenin macropolymers, and insoluble glutenin content (IGC) is positively associated with key end-use quality parameters. Here, we presen... In common wheat, insoluble glutenin (IG) is an important fraction of flour glutenin macropolymers, and insoluble glutenin content (IGC) is positively associated with key end-use quality parameters. Here, we present a genetic analysis of the chromosomal loci affecting IGC with the data collected from 90 common wheat varieties cultivated in four environments. Statistical analysis showed that IGC was controlled mainly genetically and influenced by the environment. Among the major genetic components known to affect end-use quality, 1BL/1RS translocation had a significantly negative effect on IGC across all four environments. As to the different alleles of Glu-A1, -B1 and -D1 loci, Glu-Ala, Glu-Blb and Glu-Dld exhibited relatively strong positive effects on IGC in all environments. To identify new loci affecting IGC, association mapping with 1355 DArT markers was conducted. A total of 133 markers were found associated with IGC in two or more environments (P 〈 0.05), ten of which consistently affected IGC in all four environments. The phenotypic variance explained by the ten markers varied from 4.66% to 8.03%, and their elite alleles performed significantly better than the inferior counterparts in enhancing IGC. Among the ten markers, wPt-3743 and wPt-733835 reflected the action of Glu-D1, and wPt-664972 probably indicated the effect of GIu-A1. The other seven markers, forming three clusters on 2AL. 3BL or 7BL chromosome arms, represented newly identified genetic determinants of IGC. Our work provided novel insights into the genetic control of IGC, which may facilitate wheat end- use quality improvement through molecular breeding in the future. 展开更多
关键词 Common wheat insoluble glutenin GLU-1 1BL/1RS transtocation Association mapping DART
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phytoestrogens/insoluble fibers and colonic estrogen receptor β: randomized, double-blind, placebo-controlled study 被引量:3
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作者 Mariabeatrice Principi Alfredo Di Leo +8 位作者 Maria Pricci Maria Principia Scavo Raffaella Guido Sabina Tanzi Domenico Piscitelli Antonio Pisani Enzo Ierardi Maria Cristina Comelli Michele Barone 《World Journal of Gastroenterology》 SCIE CAS 2013年第27期4325-4333,共9页
AIM:To assess the safety and effect of the supplementation of a patented blend of dietary phytoestrogens and insoluble fibers on estrogen receptor (ER)-β and biological parameters in sporadic colonic adenomas. METHOD... AIM:To assess the safety and effect of the supplementation of a patented blend of dietary phytoestrogens and insoluble fibers on estrogen receptor (ER)-β and biological parameters in sporadic colonic adenomas. METHODS:A randomized, double-blind placebo-controlled trial was performed. Patients scheduled to undergo surveillance colonoscopy for previous sporadic colonic adenomas were identified, and 60 eligible patients were randomized to placebo or active dietary intervention (ADI) twice a day, for 60 d before surveillance colonoscopy. ADI was a mixture of 175 mg milk thistle extract, 20 mg secoisolariciresinol and 750 mg oat fiber extract. ER-β and ER-α expression, apoptosis and proliferation (Ki-67 LI) were assessed in colon samples. RESULTS:No adverse event related to ADI was recorded. ADI administration showed a significant increases in ER-β protein (0.822 ± 0.08 vs 0.768 ± 0.10, P = 0.04) and a general trend to an increase in ER-β LI (39.222 ± 2.69vs 37.708 ± 5.31,P = 0.06), ER-β/ER-α LI ratio (6.564 ± 10.04 vs 2.437 ± 1.53, P = 0.06), terminal deoxynucleotidyl transferase-mediated dUTP nick end labeling (35.592 ± 14.97 vs 31.541 ± 11.54, P = 0.07) and Ki-67 (53.923 ± 20.91 vs 44.833 ± 10.38, P = 0.07) approximating statistical significance. A significant increase of ER-β protein (0.805 ± 0.13 vs 0.773 ± 0.13,P = 0.04), mRNA (2.278 ± 1.19vs 1.105 ± 1.07, P < 0.02) and LI (47.533 ± 15.47 vs 34.875 ± 16.67,P < 0.05) and a decrease of ER-α protein (0.423 ± 0.06vs 0.532 ± 0.11,P < 0.02) as well as a trend to increase of ER-β/ER-α protein in ADI vs placebo group were observed in patients without polyps (1.734 ± 0.20 vs 1.571 ± 0.42, P = 0.07). CONCLUSION:The role of ER-β on the control of apoptosis, and its amenability to dietary intervention, are supported in our study. 展开更多
关键词 ESTROGEN receptor-β ESTROGEN receptor-α Terminal deoxynucleotidyl transferase-mediated dUTP NICK end labeling Sporadic adenomatous POLYPOSIS PHYTOESTROGENS insoluble fibers
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Production and characterization of insoluble α-1,3-linked glucan and soluble α-1,6-linked dextran from Leuconostoc pseudomesenteroides G29 被引量:3
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作者 Yiya Wang Tao Sun +4 位作者 Yinzhu Wang Hao Wu Yan Fang Jiangfeng Ma Min Jiang 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2021年第11期211-218,共8页
Exopolysaccharides can be produced by various bacteria and have important biological roles in bacterial survival depend on molecular weight,linkage,and conformation.In this study,Leuconostoc pseudomesenteroides G29 wa... Exopolysaccharides can be produced by various bacteria and have important biological roles in bacterial survival depend on molecular weight,linkage,and conformation.In this study,Leuconostoc pseudomesenteroides G29 was identified and found to produce two types of exopolysaccharides from sucrose including soluble and insoluble a-glucans.By regulation of pH above 5.5,soluble a-glucan production was increased to 38.4 g∙L^(-1) from 101.4 g∙L^(-1) sucrose with fewer accumulation of lactic acid and acetic acid.Simultaneously,the quantity of thick white precipitate,that is insoluble a-glucan,was also increased.Then,a-glucans were prepared by enzymatic reaction with crude glucansucrases from the supernatant of G29 fermentation broth and purified for structure analysis.Based on the integration analysis of FT-IR and NMR,it was observed that soluble a-glucan is a highly linear dextran with α-1,6 glycosidic bonds while the insoluble a-glucan has 93%of α-1,3 and 7%of α-1,6 glycosidic bond.The results extend our understanding of exopolysaccharides production by L.pseudomesenteroides,and this water insoluble α-1,3-glucan might have potential application as biomaterials and/or biochemicals. 展开更多
关键词 EXOPOLYSACCHARIDE Glucansucrase Leuconostoc pseudomesenteroides insolubleα-glucan a-1 3 glycosidic bond
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Effect of wheat bran insoluble dietary fiber with different particle size on the texture properties, protein secondary structure, and microstructure of noodles 被引量:35
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作者 Jian Zhang Mengqin Li +1 位作者 Chaoran Li Yanqi Liu 《Grain & Oil Science and Technology》 2019年第4期97-102,共6页
This study was conducted to explore how the insoluble dietary fiber(IDF)of wheat bran with different particle size affects the texture properties,water distribution,protein secondary structure and microstructure of no... This study was conducted to explore how the insoluble dietary fiber(IDF)of wheat bran with different particle size affects the texture properties,water distribution,protein secondary structure and microstructure of noodles.The results suggested that IDF addition increased the cooking loss and decreased the sensory evaluation because of the damage on dough structure,while as the IDF particle size decreased,the sensory score increased from 78.8 to 82.3 and cooking loss decreased from 8.65%to 7.65%,which could be attributed to that small particle-sized IDF limited the damage on protein network structure,decreased the T22 and t-structure,and increased the β1-structure.Moreover,IDF particle size had a significant correlation with protein secondary structures,texture properties and evaluation score of noodles.In conclusion,adding appropriate particle sizewould be an effectiveway of enhancing the nutritional and textural properties of noodles. 展开更多
关键词 Wheat bran insoluble dietary fiber Water distribution MICROSTRUCTURE Noodle quality
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A Double-Blind, Randomized, Placebo-Controlled Nutritional Study Using an Insoluble Yeast Beta-Glucan to Improve the Immune Defense System 被引量:4
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作者 Hans-Joachim Graubaum Regina Busch +1 位作者 Heike Stier Joerg Gruenwald 《Food and Nutrition Sciences》 2012年第6期738-746,共9页
Purpose: In a placebo-controlled, double-blind, randomized clinical trial, the effect of an insoluble yeast beta-glucan preparation on the incidences of common colds and its effect on common cold symptoms were compare... Purpose: In a placebo-controlled, double-blind, randomized clinical trial, the effect of an insoluble yeast beta-glucan preparation on the incidences of common colds and its effect on common cold symptoms were compared to placebo. Methods: 100 healthy participants with recurring infections were randomly assigned to receive either placebo or yeast beta-glucan (Yestimun?;n = 50 each group) over a period of 26 weeks. The subjects had to document each common cold episode in a diary, and rate 6 predefined infections symptoms on a 3-point rating scale during an infection period, resulting in an infection score. The common cold episodes were confirmed by the investigators. Results: A total of 171 common cold episodes were documented. Of these, 76 were experienced by 38 subjects in the beta-glucan group and 96 were experienced by 48 subjects in the placebo group (p = 0.406). The beta-glucan group had significantly more subjects without incidences of common cold than the placebo group (15.6% vs 2.0%;p = 0.019). During the most intense infection season (first 13 weeks of the study), the beta-glucan group had significantly less infections compared to placebo (p = 0.02). Beta-glucan significantly reduced the typical cold symptoms (“sore throat and/or difficulty swallowing”, “hoarseness and/or cough” and “runny nose”) as opposed to placebo. Conclusion: The present study demonstrates a prophylactic effect of yeast beta-glucan on the occurrence of common colds as opposed to placebo. In addition, when these episodes occurred, they were from the beginning less pronounced and subsided faster. 展开更多
关键词 RANDOMIZED PLACEBO-CONTROLLED Study insoluble YEAST BETA-GLUCAN Common Cold IMMUNE System
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Comparison of acid-detergent lignin,alkaline-peroxide lignin,and acid-detergent insoluble ash as internal markers for predicting fecal output and digestibility by cattle offered bermudagrass hays of varying nutrient composition 被引量:1
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作者 Juvenal Kanani Dirk Philipp +6 位作者 Kenneth P Coffey Elizabeth B Kegley Charles P West Shane Gadberry John Jennings Ashley N Young Robert T Rhein 《Journal of Animal Science and Biotechnology》 SCIE CAS 2014年第3期310-317,共8页
Background: The potential for acid-detergent insoluble ash (ADIA), alkaline-peroxide lignin (APL), and acid-detergent lignin (ADL) to predict fecal output (FO) and dry matter digestibility (DMD) by cattle o... Background: The potential for acid-detergent insoluble ash (ADIA), alkaline-peroxide lignin (APL), and acid-detergent lignin (ADL) to predict fecal output (FO) and dry matter digestibility (DMD) by cattle offered bermudagrass [Cynodon doctylon (L) Pers.] hays of different qualities was evaluated. Eight ruminally cannulated cows (594 ± 35.5 kg) were allocated randomly to 4 hay diets: low (L), medium low (ML), medium high (MH), and high (H) crude protein (CP) concentration (79, 111,131, and 164 g CP/kg on a DM basis, respectively). Diets were offered in 3 periods with 2 diet replicates per period and were rotated across cows between periods. Cows were individually fed 20 g DM/kg of body weight in equal feedings at 08:00 and 16:00 h for a 10-d adaptation followed by a 5-d total fecal collection. Actual DM intake (DMI), DMD, and FO were determined based on hay offered, ort, and feces excreted. These components were then analyzed for ADL, APL, and ADIA concentration to determine marker recovery and marker-based estimates of FO and DMD. Results: Forage DMI was affected by diet (P = 0.02), and DMI from MH and H was greater (P 〈 0.05) than from L. Apparent DMD tended (P = 0.08) to differ among diets while FO (P = 0.20) was not affected by diet treatments. Average ADL recovery (1.16) was greater (P 〈 0.05) than that of ADIA (1.03) and APL (1.06), but ADIA and APL did not differ (P = 0.42). Estimates of FO and DMD derived using APL and ADIA were not different (P≥0.05) from total fecal collection while those using ADL differed (P 〈 0.05). There was no diet by marker interaction (P≥ 0.22) for either FO or DMD. Conclusion: Acid-detergent insoluble ash and APL accurately predicted FO and DMD of cattle fed bermudagrass hay of varying nutrient composition. These internal markers may facilitate studies involving large numbers of animals and forages. Results from such studies may be used to develop improved equations to predict energy values of forages based on the relationship of dietary components to digestibility across a wide range of forages. 展开更多
关键词 Acid-detergent insoluble ash Alkaline-peroxide lignin BERMUDAGRASS Cattle DIGESTIBILITY Marker
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Ion-beam-assisted characterization of quinoline-insoluble particles in nuclear graphite 被引量:1
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作者 Qing Huang Xin-Qing Han +3 位作者 Peng Liu Jian-Jian Li Guan-Hong Lei Cheng Li 《Nuclear Science and Techniques》 SCIE CAS CSCD 2020年第10期23-32,共10页
The irradiation behavior of graphite is essential for its applications in the nuclear industry.However,the behavioral differences of graphite remain obscure because of the very limited comprehension of its microstruct... The irradiation behavior of graphite is essential for its applications in the nuclear industry.However,the behavioral differences of graphite remain obscure because of the very limited comprehension of its microstructural differences.One typical structure,the quinoline-insoluble(QI)particle,was investigated using IG-110 and NBG-18 graphite.After irradiation,the QI particles on the polished surface were proven to become hillocks,which were easily identifiable via scanning electron microscopy(SEM).Thus,a method that combined ion irradiation and SEM characterization was proposed to study the distribution and concentration of QI particles in graphite.During irradiation,the QI particles were found to evolve into densified spheres,which were weakly bonded with the surrounding graphite structures,thereby indicating that the densification of QI particles did not evidently contribute to graphite dimensional shrinkage.A much higher concentration of QI particles in NBG-18 than IG-110,which was suggested to be responsible for the smaller maximum dimensional shrinkage of former over the latter during irradiation,was characterized. 展开更多
关键词 Heavy ion irradiation Nuclear graphite Quinoline insoluble MICROSTRUCTURE
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Separation of Toluene Insoluble Matter from Syncrude Coker Heavy Gas Oil 被引量:1
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作者 许志明 王宗贤 +1 位作者 L.S.Kotlyar K.H.Chung 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2003年第6期747-750,共4页
Toluene insoluble matter (TIM) in coker heavy gas oil (CHGO) from oil sands bitumen is harmful to the downstream hydrotreating, and it may be difficult to be removed by conventional filtration. In order to determine i... Toluene insoluble matter (TIM) in coker heavy gas oil (CHGO) from oil sands bitumen is harmful to the downstream hydrotreating, and it may be difficult to be removed by conventional filtration. In order to determine its origin, the TIM must first be separated from CHGO for characterization. Two techniques are described to accomplish this goal. In the ultra-centrifugation approach used in this work, CHGO is blended with a miscible liquid and centrifuged under 366000 G (gravity) force. Through this procedure toluene and hexane diluents yielded TIM contents of 24μg·g-1 and 88μg·g-1 respectively. In an alternative simplified procedure, the initial ultra-centrifugation step is omitted. Several different solvents are evaluated for use as diluents but, in each case, toluene is still used in the subsequent washing steps. TIM contents determined by this method range from 23 to about 200μg·g-1. The amount of TIM separated by means of this method depends primarily on the initial diluent used. Other conditions, such as diluent-oil ratio, water-oil ratio, mixing time, temperature and water pH value, are also studied. 展开更多
关键词 SEPARATION toluene insoluble matter coker heavy gas oil
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Determination of the Insoluble Aluminum Content in Steel Samples by Using Laser-Induced Breakdown Spectroscopy 被引量:1
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作者 刘佳 贾云海 +1 位作者 张勇 孙念 《Plasma Science and Technology》 SCIE EI CAS CSCD 2015年第8期644-648,共5页
The insoluble aluminum content in steel samples has a significant influence on the quality of the steel. In this paper, laser-induced breakdown spectroscopy (LIBS) is used to analyze the insoluble aluminum content i... The insoluble aluminum content in steel samples has a significant influence on the quality of the steel. In this paper, laser-induced breakdown spectroscopy (LIBS) is used to analyze the insoluble aluminum content in steel samples using a scanning mode. The average intensity plus 2.5 standard deviations was iterated and the final iteration value was taken as the threshold that distinguishes soluble and insoluble aluminum, and thus total and soluble aluminum content calibration curves were generated. Using the relevant total and soluble aluminum content calibration curves, the total and soluble aluminum contents in steel samples could be determined. The insoluble aluminum content could be determined by subtracting the soluble aluminum content from the total aluminum content. The insoluble aluminum content of standard samples and process product samples were determined using the present mathematical model; the results agreed well with the certified reference values. This method could be used to rapidly characterize the insoluble aluminum content in steel samples. 展开更多
关键词 laser-induced breakdown spectroscopy insoluble aluminum content thresholdintensity
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Preparation of insoluble β-CD polymer and its application to enantiomers and isomers separation 被引量:1
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作者 YI Jian ming 1,TANG Kuo wen 2 (1.College of Chemistry and Chemical Engineering, Central South University, Changsha 410083, China 2.Department of Chemical Engineering, Yueyang Normal University, Yueyang 414000, China) 《Journal of Central South University of Technology》 EI 2001年第1期57-59,共3页
An insoluble β-cyclodextrin polymer cross-linked with epichlorohydrin was prepared, and its structure was identified with infrared spectrum. Colloid stationary phase was prepared by dissolving the polymer in the mixe... An insoluble β-cyclodextrin polymer cross-linked with epichlorohydrin was prepared, and its structure was identified with infrared spectrum. Colloid stationary phase was prepared by dissolving the polymer in the mixed solvent of diisopropyl ether, methylene dichloride and benzene and treated for 0.5 h by ultrasonication, and then was coated on a fused silica capillary column. The optimun reaction conditions are as follows: the mole ratio of epichlohydrin to β-cyclodextrin is 12.1:1, reacting at 65 °C for 24 h. The Chromatographic performance such as column efficiency, thermal stabilities and polarity were studied, two kinds of disubstituted benzene isomers and eight pairs of enantiomers were separated on the capillary column. The results show that the β-cyclodextrin polymer is suitable for use as a capillary gas chromatographic stationary phase, and possess excellent chromatographic properties in separating enantiomers and position isomers. 展开更多
关键词 insoluble β cyclodextrin polymer capillary gas chromatography ENANTIOMER position isomer SEPARATION
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Microscopic Analyses of Insoluble Particles in an Ice Core of ürümqi Glacier No. 1: Quantification of Mineral and Organic Particles
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作者 Nozomu Takeuchi Yoriko Ishida 李忠勤 《Journal of Earth Science》 SCIE CAS CSCD 2011年第4期431-440,共10页
Insoluble particle concentration in ice cores is commonly analyzed as a proxy for varia- tions in atmospheric mineral dust (aerosol concentration). However, recent studies have revealed that the mineral dust is not ... Insoluble particle concentration in ice cores is commonly analyzed as a proxy for varia- tions in atmospheric mineral dust (aerosol concentration). However, recent studies have revealed that the mineral dust is not only a constituent of the particles but that biogenic organic particles are also contained. We microscopically analyzed insoluble particles in a shallow ice core drilled on a mountain glacier, the Urumqi Glacier No. 1, in eastern Tienshan, China. We distinguished different morphological particles in the ice core and quantified them separately. Results showed that the insoluble particles in this ice core consisted mainly of mineral particles, amorphous organic particles, pollen, and micro- organisms. Mineral particles were the most dominant, accounting for approximately 67% of total par- ticles, and amorphous organic particles were the second most dominant, accounting for approximately 33% of the total. The annual variation in the particles for the last 11 years differed between mineral and amorphous organic particles. The results suggest that the total insoluble particle concentration in the ice core reflects not only the atmospheric mineral dust but also the organic particles blown from ground soil or produced by microbes on the glacial surface. 展开更多
关键词 ice core insoluble particle mineral dust microbes organic particles.
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Extraction, Purification, and Characterization of Insoluble Dietary Fiber from Oat Bran 被引量:1
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作者 Yun Guo Khorolgarav Byambasuren +4 位作者 Xiaoxue Liu Xueping Wang Shuang Qiu Yujie Gao Zhanzhong Wang 《Transactions of Tianjin University》 2021年第5期385-393,共9页
The dietary fiber in oats is mainly concentrated in the bran;however,the oat bran is mostly used for livestock and poultry feed and thus has a low utilization rate and low added value.In this study,insoluble dietary f... The dietary fiber in oats is mainly concentrated in the bran;however,the oat bran is mostly used for livestock and poultry feed and thus has a low utilization rate and low added value.In this study,insoluble dietary fiber(IDF)was extracted by a combination ofα-amylase and neutral protease.The optimal extraction conditions of the IDF were obtained by response surface methodology.The material-to-water ratio was 1:12.1,the concentration ofα-amylase was 1.85%,and the hydrolysis time was 39.14 min.After purifying the crude fiber with 4%sodium oxide(Na OH),70°C hot water,and anhydrous ethanol,the purity of dietary fiber exceeded 95%.X-ray diffraction analysis indicated that the IDF was predominantly amorphous.Scanning electron microscopy showed that the IDF surface exhibited a loose porous network structure.Fourier-transform infrared spectroscopy of the crude IDF showed characteristic absorption peaks at 3626,2929,1667,1538,1455,1242,and1048 cm^(-1),while the infrared spectrum of the purified IDF showed characteristic absorption peaks at 3401,2924,1744,1643,1418,and 1040 cm^(-1),which is consistent with the structure of cellulose polysaccharide.Differential scanning calorimetry analysis showed that there were three exothermic peaks at 270–310°C,320–350°C,and 440–460°C,which may represent the pyrolysis peaks of hemicellulose,cellulose,and lignin,respectively,indicating that the oat bran IDF had good thermal stability.The results indicate that the oat bran IDF can be used for the production of dietary fiber products and health-care products. 展开更多
关键词 Oat bran insoluble dietary fiber Structure characterization
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Mathematical analysis of physicochemical phenomena in the catalyst during hydrogenating depolymerization of coal extract benzene insoluble fraction
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作者 Jerzy Szczygie Marek Stolarski 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2015年第6期962-973,共12页
Efficiency and selectivity of hydrogenating depolymerization of the coal extract benzene-insoluble part over the heterogeneous Co–Mo/Al2O3 catalyst were assessed using a mathematical model. The analytical equations o... Efficiency and selectivity of hydrogenating depolymerization of the coal extract benzene-insoluble part over the heterogeneous Co–Mo/Al2O3 catalyst were assessed using a mathematical model. The analytical equations of the mathematical model were generated based on material balance incorporating the physico-chemical phenomena(reaction and diffusion) both in the autoclave and the catalyst grain. The equations offer the possibility for predicting changes of the reactants in the autoclave during the process and for determining the distribution of reactant concentrations in the grain as a function of its radius. The analytical equations of the model serve as the basis of the algorithm for assessing the influence of restrictive diffusion on the effectiveness and selectivity of the catalyst, and also for defining the optimal radii of the catalyst's pores to enable free transport of reactants in the grain interior. 展开更多
关键词 Coal extract Benzene insolubles CATALYST DEPOLYMERIZATION Kinetics
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Simulation calculation of solubility of insoluble compound M_mA_a in complex system
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作者 杨天足 张杜超 吴江华 《Journal of Central South University》 SCIE EI CAS 2012年第4期892-896,共5页
A simulation calculation model for the solubility of insoluble compound MmAa in complex system was established.According to coordination equilibrium principle,relevant dissociation reaction,complexation reaction,self-... A simulation calculation model for the solubility of insoluble compound MmAa in complex system was established.According to coordination equilibrium principle,relevant dissociation reaction,complexation reaction,self-complexation reaction and protonation reaction during insoluble compound dissolving were considered and then the mass balance equations about solubility calculation were obtained.In the case analysis,the solubility of silver chloride in ammonia system was obtained by simulation calculation,and curved surface charts of thermodynamic equilibrium about the total concentration of silver ions,pH and concentration of ammonia ions were drawn correspondingly.The results show that under the conditions of room temperature and 6 mol/L ammonia concentration,the calculated solubility value of silver chloride(34 g/L) is close to the actual value(31 g/L),demonstrating that this model is suitable for solubility calculation of insoluble compound MmAa in the complex system. 展开更多
关键词 complex system insoluble compound SOLUBILITY calculation model
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Effect of Inoculation Rhizobium and Response of Soybean-Rhizobium System to Insoluble Phosphate
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作者 Li Xiu-ping Chen Shu-zhen +2 位作者 Zhang Yan-lai Cheng Yan-bo Nian Hai 《Journal of Northeast Agricultural University(English Edition)》 CAS 2018年第1期1-8,共8页
In order to produce efficiently symbiotic system in acid soils which could be used for the recovery of insoluble phosphate soil and improvement of the fertility, etc., host range of Rhizobium was isolated from the roo... In order to produce efficiently symbiotic system in acid soils which could be used for the recovery of insoluble phosphate soil and improvement of the fertility, etc., host range of Rhizobium was isolated from the root nodules of wild and cultivated soybean varieties growing in south China, evaluated the effects of Rhizobium on enhance nitrogen fixing activities, phosphorus(P), nitrogen(N) uptakes, growth and yield of soybean under pot and field conditions. The results showed that combined Rhizobium inoculation was more effective than individual Rhizobium inoculation. The combined Rhizobium of CW54 strains had the highest effect, nodule number, nodule weight and nodule nitrogenase activity were markedly stimulated as compared to those of the control U110, respectively. The nitrogen contents in the plants treated with CW54 strains were significantly increased by 43.2% as compared to those of the control U110 in Al-P soil, but statistical significance was not observed in Fe-P soil. By contrast, inoculation with CW54 significantly enhanced phosphorus uptake of plant in Fe-P soil than that in Al-P soil. The effects of inoculation of CW54 strains in a field condition were similar to those of in a pot condition. The total biomass and yield in the plants treated with CW54 strains were significantly increased by 86.4% and 51.4% as compared to those of the control at the time of soybean podding in a field condition, respectively. These results suggested that inoculation Rhizobium was beneficial for soybean nutrient uptake, growth and yield under insoluble phosphate soil conditions. 展开更多
关键词 dry weight SOYBEAN insoluble phosphate nitrogen and phosphorus content nitrogen fixation
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The Role of Soluble, Insoluble Fibers and Their Bioactive Compounds in Cancer: A Mini Review
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作者 Dimitrios Papandreou Zujaja Tul Noor Maitha Rashed 《Food and Nutrition Sciences》 2015年第1期1-11,共11页
The cancer incidence has risen dramatically over the last decades. About 8 million people died globally according to latest reports, which represented almost 40% more than it was 20 years ago. Risk factors for the dev... The cancer incidence has risen dramatically over the last decades. About 8 million people died globally according to latest reports, which represented almost 40% more than it was 20 years ago. Risk factors for the development of cancer have been found to include smoking, alcohol, drugs, obesity and diet. Fiber intake has shown to exhibit chemoprotective effects on cancer proliferation and metastasis that may seem to be very promising. This article will review the role of different types of fiber such as, cellulose, lignin, pectin and inulin in development and prevention of different types of cancers. This article would also discuss the effectiveness of both types of fiber in cancer prevention. 展开更多
关键词 FIBER CANCER insoluble SOLUBLE Bioactive COMPOUNDS
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