Yielding support is often used in the squeezing tunnel to prevent damage to the lining induced by large deformation of the surrounding rock.Highly Deformable Elements(HDE)which is often installed along the circumferen...Yielding support is often used in the squeezing tunnel to prevent damage to the lining induced by large deformation of the surrounding rock.Highly Deformable Elements(HDE)which is often installed along the circumferential direction of the shotcrete lining is a common type of yielding support.To determine the yield parameters of HDE,the support characteristic of the lining using HDE and the ground pressure considering strain-softening of soft rock were analyzed by an analytical method.The analytical solution showed that when considering the strain-softening of squeezing ground,the ground pressure has a non-zero minimum value.The minimum value of ground stress can be used to determine the constant yield stress of the HDE,and the corresponding deformation of the minimum ground pressure can be used to determine the deformation capacity of the HDE.Based on the variation in the design constant yield stress and yield displacement of HDE with the in-situ stress and the mechanical parameters of the soft rock,equations were proposed for determining of the yield parameters of the HDE.展开更多
The high temperature deformation behaviors of α＋β type titanium alloy TC11 （Ti-6.5Al-3.5Mo-1.5Zr-0.3Si） with coarse lamellar starting microstructure were investigated based on the hot compression tests in the tem...The high temperature deformation behaviors of α＋β type titanium alloy TC11 （Ti-6.5Al-3.5Mo-1.5Zr-0.3Si） with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a＋fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α＋β phase field. The peak of efficiency of power dissipation in α＋β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α＋β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a＋β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.展开更多
The hot deformation behavior of homogenized zinc alloy was investigated through uniaxial compression test on a Gleeble-1500 thermal-mechanical simulator within a temperature range of 230-380°C and a strain rate r...The hot deformation behavior of homogenized zinc alloy was investigated through uniaxial compression test on a Gleeble-1500 thermal-mechanical simulator within a temperature range of 230-380°C and a strain rate range of 0.01-10 s -1 ,the corresponding flow curves and their characters were determined and analyzed,and microstructures were studied by optical,SEM and TEM microscopy.The results indicated that the microstructure evolution of zinc alloy during hot deformation involves the spheroidization of the phase of TiZn15,coarsening of the precipitated phase and dynamic recrystallization（DRX）of the phase of matrix,leading to the formation of the polyphase（η＋ε＋TiZn15）structure.The spheroidization of the phase of TiZn15 during hot deformation was beneficial to the particle nucleation stimulated and then promoted to DRX of matrix.The dynamic recrystallization grain size of the matrix phase decreased firstly and then increased with elevating the temperature,and the degree of DRX became more complete when the strain rate and strain became larger.Hot deformation accelerated the diffusion of Cu atom,which resulted in the coarsening of the precipitated phase.Thus,the microstructure was refined owing to the pinning effect of the precipitated phase.展开更多
Circumferential yielding lining is able to tolerate controlled displacements without failure,which has been proven to be an effective solution to large deformation problem in squeezing tunnels.However,up to now,there ...Circumferential yielding lining is able to tolerate controlled displacements without failure,which has been proven to be an effective solution to large deformation problem in squeezing tunnels.However,up to now,there has not been a well-established design method for it.This paper aims to present a detailed analytical computation of support characteristic curve(SCC)for circumferential yielding lining,which is a significant aspect of the implementation of convergence-confinement method(CCM)in tunnel support design.Circumferential yielding lining consists of segmental shotcrete linings and highly deformable elements,and its superior performance mainly depends on the mechanical characteristic of highly deformable element.The deformation behavior of highly deformable element is firstly investigated.Its whole deforming process can be divided into three stages including elastic,yielding and compaction stages.Especially in the compaction stage of highly deformable element,a nonlinear stress-strain relationship can be observed.For mathematical convenience,the stress-strain curve in this period is processed as several linear sub-curves.Then,the reasons for closure of circumferential yielding lining in different stages are explained,and the corresponding accurate equations required for constructing the SCC are provided.Furthermore,this paper carries out two case studies illustrating the application of all equations needed to construct the SCC for circumferential yielding lining,where the reliability and feasibility of theoretical derivation are also well verified.Finally,this paper discusses the sensitivity of sub-division in element compaction stage and the influence of element length on SCC.The outcome of this paper could be used in the design of proper circumferential yielding lining.展开更多
The hydrogen induced cracking （HIC） behavior of a high deformability pipeline steel was investigated with three different dual-phase microstructures, ferrite and bainite （F＋B）, ferrite and martensite/austenite is...The hydrogen induced cracking （HIC） behavior of a high deformability pipeline steel was investigated with three different dual-phase microstructures, ferrite and bainite （F＋B）, ferrite and martensite/austenite islands （F＋M/A） and ferrite and martensite （F＋M）, respectively. The HIC test was conducted in hydrogen sulfide （H2S）-saturated solution. The results showed that the steels with F＋B and F＋M/A dual-phase microstructures had both higher deformability and better HIC resistance, whereas the harder martensite phase in F＋M microstructure was responsible for the worst HIC resistance. The band-like hard phase in dual-phase mi- crostructure was believed to lead to increasing susceptibility to HIC.展开更多
The Ailaoshan-Red River（ASRR） shear zone is one of the major Southeast Asian tectonic discontinuities that have figured the present tectonic framework of the eastern Tibet.Several metamorphic massifs are distributed...The Ailaoshan-Red River（ASRR） shear zone is one of the major Southeast Asian tectonic discontinuities that have figured the present tectonic framework of the eastern Tibet.Several metamorphic massifs are distributed linearly along the shear zone,e.g.Xuelongshan,Diancangshan, Ailaoshan and Day Nui Con Voi from north to south.They bear a lot of lines of evidence for the tectonic evolution of the eastern Tibetan at different crustal levels in different tectonic stages.Controversy still exists on the deformation structures,microstructures and their relationship with metamorphisms along the ASRR.In this paper detailed microstructural and EBSD（Electron Backscattered Diffraction） fabric analysis of some highly sheared granitic rocks from different massifs along the ASRR are conducted.High temperature structures and microstructures are preserved in unsheared gneisses,in weakly sheared xenoliths or in some parts of the highly sheared rocks（mylonites）.Several types of high temperature quartz c-axis fabrics show symmetrical patterns or transitions from symmetrical to asymmetrical patterns.The former are attributed to coaxial deformation during regional shortening in an early stage of the Indian-Eurasian tectonic interaction and the latter are related to the transitions from coaxial compression to noncoaxial shearing during the post-collisional ASRR left lateral shearing.展开更多
The effect of cooling （laminar cooling） start temperature on the phase constitution was analyzed by quanti- tative metallography. The martensite/austenite （M/A） island distribution was fixed by colour metallograph...The effect of cooling （laminar cooling） start temperature on the phase constitution was analyzed by quanti- tative metallography. The martensite/austenite （M/A） island distribution was fixed by colour metallography. The strength and uniform elongation of the steels were tested with quasi-static tensile testing machine. The in-coordinate deformation of the soft and hard phases was analyzed using FEM. The results indicate that when the cooling start temperature is 690 ℃, the mechanical properties are the best, meeting the requirements of X80 high deformability pipeline steel.展开更多
The serrated phenomena of the quasicrystalline phase reinforced Mg-4%Li-6%Zn-1.2%Y alloy after the extrusion,solid solution treatment and aged treatment have been investigated at different temperatures.The result show...The serrated phenomena of the quasicrystalline phase reinforced Mg-4%Li-6%Zn-1.2%Y alloy after the extrusion,solid solution treatment and aged treatment have been investigated at different temperatures.The result shows that when the temperature is above 100℃,the serrated phenomenon becomes weak and all the serrated amplitudes are lower than 1 MPa.Among them,the serrated amplitude of samples in aged condition is the lowest and the value is only 0.1-0.2 MPa.The underneath mechanism for the lower plastic instability at higher temperature(≥100℃)can be ascribed to the weak pining effect of solute atoms on the movement of dislocation and release of the pile-up dislocations.展开更多
Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures(1200,1250 and 1300℃) and semi-solid temperatures(1340,1350,1360,1370 and 1380℃) with different strain rates of 0.01,0.1 and 1 s-1.Hi...Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures(1200,1250 and 1300℃) and semi-solid temperatures(1340,1350,1360,1370 and 1380℃) with different strain rates of 0.01,0.1 and 1 s-1.High temperature deformation behavior and microstructure evolution of GH4037 alloy were investigated.The results indicated that flow stress decreased rapidly at semi-solid temperatures compared to that at solid temperatures.Besides,the flow stress continued to increase after reaching the initial peak stress at semi-solid temperatures when the strain rate was 1 s-1.With increasing the deformation temperature,the size of initial solid grains and recrystallized grains increased.At semi-solid temperatures,the grains were equiaxed,and liquid phase existed at the grain boundaries and inside the grains.Discontinuous dynamic recrystallization(DDRX) characterized by grain boundary bulging was the main nucleation mechanism for GH4037 alloy.展开更多
The effect of the grain size on the tensile properties and deformation mechanisms of a nonequiatomic Fe(41)Mn(25)Ni(24)Co8 Cr2 high-entropy alloy was studied in the temperature range between 298 and 1173 K by preparin...The effect of the grain size on the tensile properties and deformation mechanisms of a nonequiatomic Fe(41)Mn(25)Ni(24)Co8 Cr2 high-entropy alloy was studied in the temperature range between 298 and 1173 K by preparing the samples with three different grain sizes through severe plastic deformation and subsequent annealing:ultrafine(sub)grain size(≤0.5μm),8.1μm and 590.2μm.In the temperature between 298 and773 K,the material with the large grain size of 590.2μm exhibited the largest tensile ductility(57%-82%)due to its high strain hardening associated with mechanical twinning,but it exhibited the lowest strength due to its large grain size.The material with the ultrafine(sub)grain size exhibited the lowest tensile ductility(3%-7%)due to a greatly reduced strain hardening ability after severe plastic deformation,but it exhibited the highest strength due to the dislocation strengthening and grain refinement strengthening.At tensile testing at temperatures above 973 K,recrystallization occurred in the material with the ultrafine(sub)grains during the sample heating and holding stage,leading to the formation of fine and equiaxed grains with the sizes of 6.8-13.5μm.The deformation behavior of the Fe(41)Mn(25)Ni(24)Co8 Cr2 with different grain sizes in the high temperature range between 973 and 1173 K,where pseudosteady-state flow was attained in the stress-strain curves,could be explained by considering the simultaneous contribution of grain boundary sliding and dislocation-climb creep to total plastic flow.The activation energies for plastic flow for the materials with different grain sizes were similar as^199 kJ/mol.In predicting the deformation mechanism,it was important to consider the change in grain size by rapid grain growth or recrystallization during the sample heating and holding stage because grain boundary sliding is a grain-size-dependent deformation mechanism.The sample with the ultrafine(sub)grains exhibited the large tensile elongations of 30%-85%due to its high strain rate sensitivity,m(0.1-0.5)at temperatures of973-1173 K.The material with the large grain size of 590.2μm exhibited the very small elongations of0.2%-8%due to its small m values(0.1-0.2)and occurrence of brittle intergranular fracture at the early stage of plastic deformation.展开更多
To control the superplastic flow and fracture and examine the variation in deformation energy,the stress and grain size of Mg-7.28Li-2.19Al-0.091Y alloy were obtained using tensile testing and microstructure quantific...To control the superplastic flow and fracture and examine the variation in deformation energy,the stress and grain size of Mg-7.28Li-2.19Al-0.091Y alloy were obtained using tensile testing and microstructure quantification,and new high temperature deformation energy models were established.Results show that the grain interior deformation energy increases with increasing the strain rate and decreases with increasing the temperature.The variation in the grain boundary deformation energy is opposite to that in the grain interior deformation energy.At a given temperature,critical cavity nucleation energy decreases with increasing strain rate and cavity nucleation becomes easy,whereas at a given strain rate,critical cavity nucleation energy increases with increasing temperature and cavity nucleation becomes difficult.The newly established models of the critical cavity nucleation radius and energy provide a way for predicting the initiation of microcrack and improving the service life of the forming parts.展开更多
A low carbon Nb-microalloyed high deformability pipeline steel with X100 grade has been processed by TMCP and followed two-stage cooling process.The microstructure is characterized by ferrite/bainite multiphase.The ef...A low carbon Nb-microalloyed high deformability pipeline steel with X100 grade has been processed by TMCP and followed two-stage cooling process.The microstructure is characterized by ferrite/bainite multiphase.The effective grain size is 1.85μm in average.The volume of ferrite is about 10-15%and the grains sizes are mostly less than 5μm.The bainite consists of granular-bainite and lath-bainite,with M/A islands finely dispersed.The longitudinal tensile yield strength,uniform elongation,yield ratio are 647MPa,7.6%and 0.78,respectively.Ferrite/bainite multiphase have large strain hardenability that resulting high strength and high deformability combination.Precipitation of Nb also improves the strength and uniform deformability by precipitation strengthening and grain refinement.展开更多
In theory, land subsidence measurement results with high accuracy can be obtained by using the Differential Interferometry Synthetic Aperture Radar(D-InSAR) at X-band. In practice, however, the measuring accuracy of D...In theory, land subsidence measurement results with high accuracy can be obtained by using the Differential Interferometry Synthetic Aperture Radar(D-InSAR) at X-band. In practice, however, the measuring accuracy of D-InSAR at X-band has been seriously affected by some factors, e.g., decorrelation and high deformation gradient. In this work, the monitoring capability of D-InSAR for coal-mining subsidence is evaluated by using SAR data acquired by TerrraSAR-X system. The SAR image registration method for low coherence image pairs, the denoising phase filter for high noise level interferogram and atmospheric effects mitigation method are the key technical aspects which directly influence the measurement results of D-InSAR at X-band. Thus, a robust image registration method, an improved phase filter method and an atmospheric effects mitigation method are proposed in this paper. The proposed image registration method successfully achieves InSAR coregistration, while the amplitude cross-correlation cannot properly coregister low coherence SAR image pairs. Moreover, the time complexity of the proposed image registration method is obviously slighter than that of the Singular Value Decomposition(SVD) method. The comparing experiment results and the unwrapping phase results show that the improved Goldstein filter is more effective than the original Goldstein filter in noise elimination. The atmospheric influence correction experiment results show that the land subsidence areas with atmospheric influence correction are more clarified than that of without atmospheric influence correction. In summary, the presented methods directly improved the measurement results of D-InSAR at X-band.展开更多
Static recrystallization of a high strain rate compressed Mg-1 Zn(wt.%)alloy was investigated using electron backscattered diffraction(EBSD).A novel 53°1010 structure was observed in the as-deformed alloy,which s...Static recrystallization of a high strain rate compressed Mg-1 Zn(wt.%)alloy was investigated using electron backscattered diffraction(EBSD).A novel 53°1010 structure was observed in the as-deformed alloy,which showed a{1012}-{1012}double twin relationship with the matrix.When the as-deformed alloy was annealed at 200°C,the{1011}compression twins and{1011}-{1012}double twins showed a higher priority to recrystallize.In addition,the coarse{1012}tension twins and their inner double twins were preferentially to recrystallize,while the lenticular tension twins had little impact on the recrystallization.Therefore,obtaining more compression twins or coarse twins instead of lenticular tension twins can be an effective approach to manipulate recrystallization process in deformed Mg alloys.展开更多
Previous investigations indicate that the creep resistance of magnesium alloys is proportional to the stability of precipitated intermetallic phases at grain boundaries.These stable intermetallic phases were considere...Previous investigations indicate that the creep resistance of magnesium alloys is proportional to the stability of precipitated intermetallic phases at grain boundaries.These stable intermetallic phases were considered to be effective to suppress the deformation by grain boundary sliding,leading to the improvement of creep properties.Based on this point,adding the alloying elements to form the stable intermetallics with high melting point became a popular way to develop the new creep resistant magnesium alloys.The present investigation,however,shows that the creep properties of binary Mg-Sn alloy are still poor even though the addition of Sn possibly results in the precipitation of thermal stable Mg_(2)Sn at grain boundaries.That means other possible mechanisms function to affect the creep response.It is finally found that the poor creep resistance is attributed to the segregation of Sn at dendritic and grain boundaries.Based on this observation,new approaches to improve the creep resistance are suggested for magnesium alloys because most currently magnesium alloys have the commonality with the Mg-Sn alloys.展开更多
A series of trial tests for high deformation(HD)X70 pipeline steel plates were performed in NISCO,and the technical routes as thermal mechanical controlled rolling process(TMCP),TMCP+Quenching(Q)and TMCP+Q&temperi...A series of trial tests for high deformation(HD)X70 pipeline steel plates were performed in NISCO,and the technical routes as thermal mechanical controlled rolling process(TMCP),TMCP+Quenching(Q)and TMCP+Q&tempering(T)were studied systematically through the plate shape quality,properties and microstructure characters.The results show that problems as plate shape and inhomogeneous microstructures are for finish rolling at low temperature and high cooling rate after the rolling by the route of TMCP.By the route of TMCP+Q,the yield strength(YS)of the trial steels is not sufficient.By the route of TMCP+QT,the YS is enhanced,as well as good toughness and plasticity due to the martensite decomposition at low temperature tempering process,and 4 sheets of HD X70 pipeline steel plates by the route TMCP+QT with superior plate shape quality,microstructure and comprehensive properties were successfully developed in NISCO.展开更多
The high temperature deformation behavior of the 9Ni steel has been studied by the Gleeble-3500 tester. The relationship between deformation resistance and deformation degree, deformation temperature and deformation r...The high temperature deformation behavior of the 9Ni steel has been studied by the Gleeble-3500 tester. The relationship between deformation resistance and deformation degree, deformation temperature and deformation rate was revealed. The results show that when the deformation degree is less than 0.2, the deformation resistance increases by about 70 to 200 MPa, while the deformation degree varied between 0.2 and 0.4, the deformation resist- ance increases by about 30--40 MPa, when the deformation degree is larger than 0.4, the deformation resistance in- creases slowly, some become stable gradually. The influence of deformation temperature on deformation resistance is larger, and deformation resistance at higher temperature is about 160 MPa smaller than at lower temperature. Higher deformation rate leads to larger deformation resistance. The deformation resistance increases about 70 to 110 MPa with the increase of the deformation rate. A new and highly accurate mathematical model of the steel was established to describe the deformation behavior during rolling.展开更多
Recrystallized grains, less than 200 nm in diameter were observed in heavily shear zones of a high strength low alloy steel and a Ni-based alloy, and Also grain refinement, less than 3 μm in diameter was made in high...Recrystallized grains, less than 200 nm in diameter were observed in heavily shear zones of a high strength low alloy steel and a Ni-based alloy, and Also grain refinement, less than 3 μm in diameter was made in high purity aluminum by ECAE at ambient temperature. The experimental results showed that high strain rate and large deformation could induce dynamic recrystallization.Based on dislocation dynamics and grain orientation change enhanced by plastic deformation,a model for the recrystallization process is developed. The model is used to explain the ultra fine grains which are formed at a temperature still much lower than that for the conventional recrystallization展开更多
With TEM、SEM, various high temperature deformed structures in W9Mo3Cr4V steel were investigated. The sub structures,recrystallized nuclei, as well as the dynamic precipitation were also studied and analyzed. The r...With TEM、SEM, various high temperature deformed structures in W9Mo3Cr4V steel were investigated. The sub structures,recrystallized nuclei, as well as the dynamic precipitation were also studied and analyzed. The relationship between recrystallized structures and dynamic precipitation was discussed. The results showed that the deformed structures in W9Mo3Cr4V steel are more complicated than those in low alloy steels. Because W9Mo3Cr4V steel is a high speed steel, there are a large number of residual carbides on the matrix. Also, much dynamic precipitating carbides will precipitate during deformation at high temperature.展开更多
This paper presents an experimental investigation on an AISI 316L stainless steel regarding mechanical properties and short uniaxial creep tests at elevated temperatures. The short time creep tests were carried out un...This paper presents an experimental investigation on an AISI 316L stainless steel regarding mechanical properties and short uniaxial creep tests at elevated temperatures. The short time creep tests were carried out under different but constant stresses. The obtained data of ultimate tensile strength, yield strength, creep curves and effects of elevated temperatures on mechanical properties were presented. For a selected rheological model, material parameters were obtained. As a justification, such rheological model is implemented in the finite element procedure for an uniaxially stressed specimen in selected environmental conditions.展开更多
基金the support of the National Natural Science Foundation of China(Grant Nos.52179113,51991392 and 52279119)the Second Comprehensive Scientific Expedition on the Tibetan Plateau(No.2019QZKK0904)。
文摘Yielding support is often used in the squeezing tunnel to prevent damage to the lining induced by large deformation of the surrounding rock.Highly Deformable Elements(HDE)which is often installed along the circumferential direction of the shotcrete lining is a common type of yielding support.To determine the yield parameters of HDE,the support characteristic of the lining using HDE and the ground pressure considering strain-softening of soft rock were analyzed by an analytical method.The analytical solution showed that when considering the strain-softening of squeezing ground,the ground pressure has a non-zero minimum value.The minimum value of ground stress can be used to determine the constant yield stress of the HDE,and the corresponding deformation of the minimum ground pressure can be used to determine the deformation capacity of the HDE.Based on the variation in the design constant yield stress and yield displacement of HDE with the in-situ stress and the mechanical parameters of the soft rock,equations were proposed for determining of the yield parameters of the HDE.
基金Project (51005112) supported by the National Natural Science Foundation of ChinaProject (2010ZF56019) supported by the Aviation Science Foundation of China+1 种基金Project (GJJ11156) supported by the Education Commission of Jiangxi Province, ChinaProject(GF200901008) supported by the Open Fund of National Defense Key Disciplines Laboratory of Light Alloy Processing Science and Technology, China
文摘The high temperature deformation behaviors of α＋β type titanium alloy TC11 （Ti-6.5Al-3.5Mo-1.5Zr-0.3Si） with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a＋fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α＋β phase field. The peak of efficiency of power dissipation in α＋β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α＋β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a＋β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.
基金Project(2009BAE71B03)supported by the National Key Technology Support Program of China During the 11th Five-year Plan Period
文摘The hot deformation behavior of homogenized zinc alloy was investigated through uniaxial compression test on a Gleeble-1500 thermal-mechanical simulator within a temperature range of 230-380°C and a strain rate range of 0.01-10 s -1 ,the corresponding flow curves and their characters were determined and analyzed,and microstructures were studied by optical,SEM and TEM microscopy.The results indicated that the microstructure evolution of zinc alloy during hot deformation involves the spheroidization of the phase of TiZn15,coarsening of the precipitated phase and dynamic recrystallization（DRX）of the phase of matrix,leading to the formation of the polyphase（η＋ε＋TiZn15）structure.The spheroidization of the phase of TiZn15 during hot deformation was beneficial to the particle nucleation stimulated and then promoted to DRX of matrix.The dynamic recrystallization grain size of the matrix phase decreased firstly and then increased with elevating the temperature,and the degree of DRX became more complete when the strain rate and strain became larger.Hot deformation accelerated the diffusion of Cu atom,which resulted in the coarsening of the precipitated phase.Thus,the microstructure was refined owing to the pinning effect of the precipitated phase.
基金supported by National Natural Science Foundation of China(Grant Nos.11872287 and 51908431)Fund of Shaanxi Key Research and Development Program(Grant No.2019ZDLGY01-10)。
文摘Circumferential yielding lining is able to tolerate controlled displacements without failure,which has been proven to be an effective solution to large deformation problem in squeezing tunnels.However,up to now,there has not been a well-established design method for it.This paper aims to present a detailed analytical computation of support characteristic curve(SCC)for circumferential yielding lining,which is a significant aspect of the implementation of convergence-confinement method(CCM)in tunnel support design.Circumferential yielding lining consists of segmental shotcrete linings and highly deformable elements,and its superior performance mainly depends on the mechanical characteristic of highly deformable element.The deformation behavior of highly deformable element is firstly investigated.Its whole deforming process can be divided into three stages including elastic,yielding and compaction stages.Especially in the compaction stage of highly deformable element,a nonlinear stress-strain relationship can be observed.For mathematical convenience,the stress-strain curve in this period is processed as several linear sub-curves.Then,the reasons for closure of circumferential yielding lining in different stages are explained,and the corresponding accurate equations required for constructing the SCC are provided.Furthermore,this paper carries out two case studies illustrating the application of all equations needed to construct the SCC for circumferential yielding lining,where the reliability and feasibility of theoretical derivation are also well verified.Finally,this paper discusses the sensitivity of sub-division in element compaction stage and the influence of element length on SCC.The outcome of this paper could be used in the design of proper circumferential yielding lining.
基金Item Sponsored by National Key Technology Research and Development Program of China(2011BAE25B03)
文摘The hydrogen induced cracking （HIC） behavior of a high deformability pipeline steel was investigated with three different dual-phase microstructures, ferrite and bainite （F＋B）, ferrite and martensite/austenite islands （F＋M/A） and ferrite and martensite （F＋M）, respectively. The HIC test was conducted in hydrogen sulfide （H2S）-saturated solution. The results showed that the steels with F＋B and F＋M/A dual-phase microstructures had both higher deformability and better HIC resistance, whereas the harder martensite phase in F＋M microstructure was responsible for the worst HIC resistance. The band-like hard phase in dual-phase mi- crostructure was believed to lead to increasing susceptibility to HIC.
基金supported by the National Key Basic Research and Development(973) Project (2009CB421001)National Natural Science Foundation of China(40872139)+2 种基金China Geological Survey (1212010661311)Ministry of Land and Resources (200811008)the Ministry of Education,Proiect 111 (B07011)
文摘The Ailaoshan-Red River（ASRR） shear zone is one of the major Southeast Asian tectonic discontinuities that have figured the present tectonic framework of the eastern Tibet.Several metamorphic massifs are distributed linearly along the shear zone,e.g.Xuelongshan,Diancangshan, Ailaoshan and Day Nui Con Voi from north to south.They bear a lot of lines of evidence for the tectonic evolution of the eastern Tibetan at different crustal levels in different tectonic stages.Controversy still exists on the deformation structures,microstructures and their relationship with metamorphisms along the ASRR.In this paper detailed microstructural and EBSD（Electron Backscattered Diffraction） fabric analysis of some highly sheared granitic rocks from different massifs along the ASRR are conducted.High temperature structures and microstructures are preserved in unsheared gneisses,in weakly sheared xenoliths or in some parts of the highly sheared rocks（mylonites）.Several types of high temperature quartz c-axis fabrics show symmetrical patterns or transitions from symmetrical to asymmetrical patterns.The former are attributed to coaxial deformation during regional shortening in an early stage of the Indian-Eurasian tectonic interaction and the latter are related to the transitions from coaxial compression to noncoaxial shearing during the post-collisional ASRR left lateral shearing.
文摘The effect of cooling （laminar cooling） start temperature on the phase constitution was analyzed by quanti- tative metallography. The martensite/austenite （M/A） island distribution was fixed by colour metallography. The strength and uniform elongation of the steels were tested with quasi-static tensile testing machine. The in-coordinate deformation of the soft and hard phases was analyzed using FEM. The results indicate that when the cooling start temperature is 690 ℃, the mechanical properties are the best, meeting the requirements of X80 high deformability pipeline steel.
基金This work was supported by the National Natural Science Foundation of China projects under Grant Nos.51171192,51271183 and 51301172the National Basic Research Program of China(973 Program)project under Grant No.2013CB632205 and the Innovation Fund of Institute of Metal Research(IMR),Chinese Academy of Sciences.
文摘The serrated phenomena of the quasicrystalline phase reinforced Mg-4%Li-6%Zn-1.2%Y alloy after the extrusion,solid solution treatment and aged treatment have been investigated at different temperatures.The result shows that when the temperature is above 100℃,the serrated phenomenon becomes weak and all the serrated amplitudes are lower than 1 MPa.Among them,the serrated amplitude of samples in aged condition is the lowest and the value is only 0.1-0.2 MPa.The underneath mechanism for the lower plastic instability at higher temperature(≥100℃)can be ascribed to the weak pining effect of solute atoms on the movement of dislocation and release of the pile-up dislocations.
基金Project(51575127)supported by the National Natural Science Foundation of China
文摘Cylindrical samples of Ni-based GH4037 alloy were compressed at solid temperatures(1200,1250 and 1300℃) and semi-solid temperatures(1340,1350,1360,1370 and 1380℃) with different strain rates of 0.01,0.1 and 1 s-1.High temperature deformation behavior and microstructure evolution of GH4037 alloy were investigated.The results indicated that flow stress decreased rapidly at semi-solid temperatures compared to that at solid temperatures.Besides,the flow stress continued to increase after reaching the initial peak stress at semi-solid temperatures when the strain rate was 1 s-1.With increasing the deformation temperature,the size of initial solid grains and recrystallized grains increased.At semi-solid temperatures,the grains were equiaxed,and liquid phase existed at the grain boundaries and inside the grains.Discontinuous dynamic recrystallization(DDRX) characterized by grain boundary bulging was the main nucleation mechanism for GH4037 alloy.
基金This research was financially supported by the Basic Research Laboratory Program through the National Research Foundation of Korea funded by the Ministry of Education,Science and Technology(Project No.NRF 2015-041523).
文摘The effect of the grain size on the tensile properties and deformation mechanisms of a nonequiatomic Fe(41)Mn(25)Ni(24)Co8 Cr2 high-entropy alloy was studied in the temperature range between 298 and 1173 K by preparing the samples with three different grain sizes through severe plastic deformation and subsequent annealing:ultrafine(sub)grain size(≤0.5μm),8.1μm and 590.2μm.In the temperature between 298 and773 K,the material with the large grain size of 590.2μm exhibited the largest tensile ductility(57%-82%)due to its high strain hardening associated with mechanical twinning,but it exhibited the lowest strength due to its large grain size.The material with the ultrafine(sub)grain size exhibited the lowest tensile ductility(3%-7%)due to a greatly reduced strain hardening ability after severe plastic deformation,but it exhibited the highest strength due to the dislocation strengthening and grain refinement strengthening.At tensile testing at temperatures above 973 K,recrystallization occurred in the material with the ultrafine(sub)grains during the sample heating and holding stage,leading to the formation of fine and equiaxed grains with the sizes of 6.8-13.5μm.The deformation behavior of the Fe(41)Mn(25)Ni(24)Co8 Cr2 with different grain sizes in the high temperature range between 973 and 1173 K,where pseudosteady-state flow was attained in the stress-strain curves,could be explained by considering the simultaneous contribution of grain boundary sliding and dislocation-climb creep to total plastic flow.The activation energies for plastic flow for the materials with different grain sizes were similar as^199 kJ/mol.In predicting the deformation mechanism,it was important to consider the change in grain size by rapid grain growth or recrystallization during the sample heating and holding stage because grain boundary sliding is a grain-size-dependent deformation mechanism.The sample with the ultrafine(sub)grains exhibited the large tensile elongations of 30%-85%due to its high strain rate sensitivity,m(0.1-0.5)at temperatures of973-1173 K.The material with the large grain size of 590.2μm exhibited the very small elongations of0.2%-8%due to its small m values(0.1-0.2)and occurrence of brittle intergranular fracture at the early stage of plastic deformation.
基金Project(51334006)supported by the National Natural Science Foundation of China
文摘To control the superplastic flow and fracture and examine the variation in deformation energy,the stress and grain size of Mg-7.28Li-2.19Al-0.091Y alloy were obtained using tensile testing and microstructure quantification,and new high temperature deformation energy models were established.Results show that the grain interior deformation energy increases with increasing the strain rate and decreases with increasing the temperature.The variation in the grain boundary deformation energy is opposite to that in the grain interior deformation energy.At a given temperature,critical cavity nucleation energy decreases with increasing strain rate and cavity nucleation becomes easy,whereas at a given strain rate,critical cavity nucleation energy increases with increasing temperature and cavity nucleation becomes difficult.The newly established models of the critical cavity nucleation radius and energy provide a way for predicting the initiation of microcrack and improving the service life of the forming parts.
文摘A low carbon Nb-microalloyed high deformability pipeline steel with X100 grade has been processed by TMCP and followed two-stage cooling process.The microstructure is characterized by ferrite/bainite multiphase.The effective grain size is 1.85μm in average.The volume of ferrite is about 10-15%and the grains sizes are mostly less than 5μm.The bainite consists of granular-bainite and lath-bainite,with M/A islands finely dispersed.The longitudinal tensile yield strength,uniform elongation,yield ratio are 647MPa,7.6%and 0.78,respectively.Ferrite/bainite multiphase have large strain hardenability that resulting high strength and high deformability combination.Precipitation of Nb also improves the strength and uniform deformability by precipitation strengthening and grain refinement.
文摘In theory, land subsidence measurement results with high accuracy can be obtained by using the Differential Interferometry Synthetic Aperture Radar(D-InSAR) at X-band. In practice, however, the measuring accuracy of D-InSAR at X-band has been seriously affected by some factors, e.g., decorrelation and high deformation gradient. In this work, the monitoring capability of D-InSAR for coal-mining subsidence is evaluated by using SAR data acquired by TerrraSAR-X system. The SAR image registration method for low coherence image pairs, the denoising phase filter for high noise level interferogram and atmospheric effects mitigation method are the key technical aspects which directly influence the measurement results of D-InSAR at X-band. Thus, a robust image registration method, an improved phase filter method and an atmospheric effects mitigation method are proposed in this paper. The proposed image registration method successfully achieves InSAR coregistration, while the amplitude cross-correlation cannot properly coregister low coherence SAR image pairs. Moreover, the time complexity of the proposed image registration method is obviously slighter than that of the Singular Value Decomposition(SVD) method. The comparing experiment results and the unwrapping phase results show that the improved Goldstein filter is more effective than the original Goldstein filter in noise elimination. The atmospheric influence correction experiment results show that the land subsidence areas with atmospheric influence correction are more clarified than that of without atmospheric influence correction. In summary, the presented methods directly improved the measurement results of D-InSAR at X-band.
基金financially supported by National Natural Science Foundation of China(No.51701121,No.51825101)Shanghai Sailing Program(17YF1408800)+2 种基金Science and Technology Commission of Shanghai Municipality(No.18511109302)Qinghai Provincial Science and Technology Key Program(No.2018-GX-A1)Startup Fund for Youngman Research at SJTU(No.18X100040022)
文摘Static recrystallization of a high strain rate compressed Mg-1 Zn(wt.%)alloy was investigated using electron backscattered diffraction(EBSD).A novel 53°1010 structure was observed in the as-deformed alloy,which showed a{1012}-{1012}double twin relationship with the matrix.When the as-deformed alloy was annealed at 200°C,the{1011}compression twins and{1011}-{1012}double twins showed a higher priority to recrystallize.In addition,the coarse{1012}tension twins and their inner double twins were preferentially to recrystallize,while the lenticular tension twins had little impact on the recrystallization.Therefore,obtaining more compression twins or coarse twins instead of lenticular tension twins can be an effective approach to manipulate recrystallization process in deformed Mg alloys.
文摘Previous investigations indicate that the creep resistance of magnesium alloys is proportional to the stability of precipitated intermetallic phases at grain boundaries.These stable intermetallic phases were considered to be effective to suppress the deformation by grain boundary sliding,leading to the improvement of creep properties.Based on this point,adding the alloying elements to form the stable intermetallics with high melting point became a popular way to develop the new creep resistant magnesium alloys.The present investigation,however,shows that the creep properties of binary Mg-Sn alloy are still poor even though the addition of Sn possibly results in the precipitation of thermal stable Mg_(2)Sn at grain boundaries.That means other possible mechanisms function to affect the creep response.It is finally found that the poor creep resistance is attributed to the segregation of Sn at dendritic and grain boundaries.Based on this observation,new approaches to improve the creep resistance are suggested for magnesium alloys because most currently magnesium alloys have the commonality with the Mg-Sn alloys.
文摘A series of trial tests for high deformation(HD)X70 pipeline steel plates were performed in NISCO,and the technical routes as thermal mechanical controlled rolling process(TMCP),TMCP+Quenching(Q)and TMCP+Q&tempering(T)were studied systematically through the plate shape quality,properties and microstructure characters.The results show that problems as plate shape and inhomogeneous microstructures are for finish rolling at low temperature and high cooling rate after the rolling by the route of TMCP.By the route of TMCP+Q,the yield strength(YS)of the trial steels is not sufficient.By the route of TMCP+QT,the YS is enhanced,as well as good toughness and plasticity due to the martensite decomposition at low temperature tempering process,and 4 sheets of HD X70 pipeline steel plates by the route TMCP+QT with superior plate shape quality,microstructure and comprehensive properties were successfully developed in NISCO.
基金Item Sponsored by National Key Technology Research and Development Program in 11th Five-Years Plan of China(2006BAE03A06)
文摘The high temperature deformation behavior of the 9Ni steel has been studied by the Gleeble-3500 tester. The relationship between deformation resistance and deformation degree, deformation temperature and deformation rate was revealed. The results show that when the deformation degree is less than 0.2, the deformation resistance increases by about 70 to 200 MPa, while the deformation degree varied between 0.2 and 0.4, the deformation resist- ance increases by about 30--40 MPa, when the deformation degree is larger than 0.4, the deformation resistance in- creases slowly, some become stable gradually. The influence of deformation temperature on deformation resistance is larger, and deformation resistance at higher temperature is about 160 MPa smaller than at lower temperature. Higher deformation rate leads to larger deformation resistance. The deformation resistance increases about 70 to 110 MPa with the increase of the deformation rate. A new and highly accurate mathematical model of the steel was established to describe the deformation behavior during rolling.
文摘Recrystallized grains, less than 200 nm in diameter were observed in heavily shear zones of a high strength low alloy steel and a Ni-based alloy, and Also grain refinement, less than 3 μm in diameter was made in high purity aluminum by ECAE at ambient temperature. The experimental results showed that high strain rate and large deformation could induce dynamic recrystallization.Based on dislocation dynamics and grain orientation change enhanced by plastic deformation,a model for the recrystallization process is developed. The model is used to explain the ultra fine grains which are formed at a temperature still much lower than that for the conventional recrystallization
基金Project Sponsored by Ministry of Science and Technology of China(G1998061513)
文摘With TEM、SEM, various high temperature deformed structures in W9Mo3Cr4V steel were investigated. The sub structures,recrystallized nuclei, as well as the dynamic precipitation were also studied and analyzed. The relationship between recrystallized structures and dynamic precipitation was discussed. The results showed that the deformed structures in W9Mo3Cr4V steel are more complicated than those in low alloy steels. Because W9Mo3Cr4V steel is a high speed steel, there are a large number of residual carbides on the matrix. Also, much dynamic precipitating carbides will precipitate during deformation at high temperature.
基金This work was conducted within the scientific project069-0691736-1737 titled "Numerical Analysis of Structural Response for Specific Service Conditions" financially sup-ported by the Ministry of Science and Technology of the Republic of Croatia.
文摘This paper presents an experimental investigation on an AISI 316L stainless steel regarding mechanical properties and short uniaxial creep tests at elevated temperatures. The short time creep tests were carried out under different but constant stresses. The obtained data of ultimate tensile strength, yield strength, creep curves and effects of elevated temperatures on mechanical properties were presented. For a selected rheological model, material parameters were obtained. As a justification, such rheological model is implemented in the finite element procedure for an uniaxially stressed specimen in selected environmental conditions.
