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HAFT·EDN共晶的制备、晶体结构和热分解性能 被引量:2
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作者 武碧栋 王苗 +1 位作者 刘淑杰 王晶禹 《火炸药学报》 EI CAS CSCD 北大核心 2020年第6期578-583,共6页
以3-氨基-4-(四唑-5-基)呋咱(HAFT)和硝酸乙二胺(EDN)为原料,制备得到二元共晶HAFT·EDN,采用X射线衍射仪(XRD)、红外光谱、元素分析和X-射线单晶衍射仪表征了目标物结构;采用差示扫描量热(DSC)对HAFT·EDN共晶进行了热性能测试... 以3-氨基-4-(四唑-5-基)呋咱(HAFT)和硝酸乙二胺(EDN)为原料,制备得到二元共晶HAFT·EDN,采用X射线衍射仪(XRD)、红外光谱、元素分析和X-射线单晶衍射仪表征了目标物结构;采用差示扫描量热(DSC)对HAFT·EDN共晶进行了热性能测试,并测试了其撞击感度和摩擦感度;通过Kissinger法、Ozawa法和Starink法计算分析了非等温动力学、热爆炸临界温度等性能参数。结果表明,该晶体属于单斜晶系,空间群为P21/c,晶体学参数为:a=7.515(4),b=9.823(5),c=14.828(8),β=86.152(9),V=1092.1(10)3,Dc=1.680g/cm3,其活化能为127.58kJ/mol,热爆炸临界温度为283.7℃,分解反应过程活化熵(ΔS≠)为-44.08kJ/mol,活化焓(ΔH≠)为119.68kJ/mol,吉布斯自由能(ΔG≠)为143.33kJ/mol,具有较好的稳定性,对撞击和摩擦刺激均钝感。 展开更多
关键词 有机化学 共晶 3-氨基-4-(四唑-5-基)呋咱 HAFT EDN 晶体结构 热分析
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Input series out putparallel based multi-modular boost half bridge DC-DC converter with a dynamic control scheme
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作者 SOOMRO Amir Mahmood SYED Amjad Ali +2 位作者 KHIZER Arbab Nighat 廖晓钟 MANZOOR Muhammad Farhan 《Journal of Beijing Institute of Technology》 EI CAS 2014年第4期519-526,共8页
Multi-modular system plays an important role in power system architecture because low voltage and low power converters can be connected in any combination parallel or series at input/ output side in order to obtained ... Multi-modular system plays an important role in power system architecture because low voltage and low power converters can be connected in any combination parallel or series at input/ output side in order to obtained any given power system specifications. Multi-modular boost haft bridge DC-DC converter in the configuration of input series output parallel has been investigated in this paper. The boost half bridge DC-DC converters are connected in input series output parallel con- figuration in order to achieve equal input voltage sharing and output current sharing between the con- verters. This can be achieved with the help of dynamic control scheme which consists of two loops, a voltage loop and a current loop, for each module. Dynamic behavior of multi-modular converter configuration has been observe by varying the load condition. Moreover, the results obtained through multi-modular converter describe that the system has good dynamic and steady state response. Al- though two converter modules are focused in this paper but it can be modified to any number of modules. 展开更多
关键词 boost haft bridge BHB input series output parallel ISOP input voltage sharing(IVS) multi-modular output current sharing (OCS)
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