One improved mixing-extruding machine was introduced as the second-generation product of the mixing-molding integrated technology. In the extruding system,the conventional single screw extruder was substituted by a sp...One improved mixing-extruding machine was introduced as the second-generation product of the mixing-molding integrated technology. In the extruding system,the conventional single screw extruder was substituted by a special conical twin-screw extruder,resulting in stronger feeding ability,more stable extrusion pressure,and better quality of products. The integrated mathematical model of mixing-extruding process was also established by theoretical derivation and optimization according to the experimental results.Then its accuracy was verified by the influences of the pressure of floating weight and the cooling water temperature of extruder on the mixing-extruding integrated process. The results showed that the changes of both parameters could give rise to the fluctuation of the temperature and apparent viscosity of polyblends, thus further influencing the screw rotation speed.展开更多
Continuous extruding/ extending formiug process for A2017 alloy in semi-solid state was proposed through installing extending die at the outlet of shearing- cooling- rolling （SCR） machine. A series of experiments to...Continuous extruding/ extending formiug process for A2017 alloy in semi-solid state was proposed through installing extending die at the outlet of shearing- cooling- rolling （SCR） machine. A series of experiments to produce fiat bar of A2017 alloy were carried oat. The forming process, metal flow behavior in die and microstructure and mechanical property of prodacts were investigated. It is shown that if the pouring temperature of melt was higher, the die was filled with semi-solid slurry with low solid fraction and periodical cracks would occur on the product surface ; If its pouring temperature was lower or the preheating temperature of die was lower, semisolid slurry would solidify rapidly and block the die after entering the cavity. The analysis of mass flow trace shows that the semi-solid slurry move forward layer by layer and fills the die extending cavity in radiation manner and the velocity of mass flow in the central area of extending cavity and exit of mould is the maximum, and then decreases gradually from the center to both sides of die wall. By inereasiug the die extending angle, the velocity of mass flow becomes more homogeneous. Under rational process control and die design, the A2017 fiat bar with transverse section of 10 × 50 mm and with good surface and fine equiaxed grains can be obtained by continuous extruding/extending forming process. The product＇s tensile strength and elongation are 420.5 MPa and 14.2% , respectively.展开更多
In this paper, the kinematically admissible velocity field with surface crack on forward extruding bar is put forward during the axisymmetric cup-bar combined extrusion process, in accordance with the results of model...In this paper, the kinematically admissible velocity field with surface crack on forward extruding bar is put forward during the axisymmetric cup-bar combined extrusion process, in accordance with the results of model experiments.On the basis of velocity field, the necessary condition for surface crack formation on the forward extruding bar is derived, with the help of upper bound theorem and the minimum energy principle. Meanwhile, the relationships between surface crack formation and combination of reduction in area for the part of forward and backward extursions relative residual thickness of billet (T/R0),frictional factor (m) or relative land length of ram and chamber are calculated during the extrusion process. Therefore, whether the surface crack on forward exturding bar occurs can be predicted before extruding the lower-plasticity metals for axisymmetric cup-bar combined extrusion process.The analytical results agree very well with experimental results of aluminium alloy LY12 (ASTM 2024) and LC4 (ASTM 7075).展开更多
In the paper a self-adjusting hydraulic machine for combination forming of upsetting and extruding is systematacially presented in terms of mechanical principle, design principle, machine construction, design of the k...In the paper a self-adjusting hydraulic machine for combination forming of upsetting and extruding is systematacially presented in terms of mechanical principle, design principle, machine construction, design of the key components and working routine. The machine is designed with the following features: The lower movable beam is adjusted by the ejecting cylinder, the upper upsetting beam is reset by the backstroke slide rods, and the upsetting cylinders communicate with the gas-liquid accumulators. These features make the machine conformation compact, save both the backstroke cylinder of the upper upsetting beam and the upsetting cylinder of the lower movable beam, and simplify the hydraulic system. Furthermore, the machine can resolve such problems as incomplete filling at the addendum position, microcracks at the dedendum position, greater force and lower die life during precision forging of spur gears.展开更多
The high-strength Mg-7Sn alloys(wt.%)with a heterogeneous grain structure were prepared by low-temperature extrusion(230°C)with the extrusion ratio of 9:1(9E230)and 17:1(17E230).The two extruded alloys contained ...The high-strength Mg-7Sn alloys(wt.%)with a heterogeneous grain structure were prepared by low-temperature extrusion(230°C)with the extrusion ratio of 9:1(9E230)and 17:1(17E230).The two extruded alloys contained fine dynamic recrystallization(DRX)grains(FG)and coarse un DRX grains(CG).The difference in deformability between CG and FG leads to the formation of heterogeneous grain structure.The average grain size and basal texture intensities increased while the volume fraction of CG decreased with increasing extrusion ratio.Tensile testing results indicated that the extruded 17E230 alloy exhibited higher tensile strengths than 9E230 alloy,whose tensile yield strength(σ_(0.2)),ultimate tensile strengths(σ_(b)),and elongation to failure(ε_(f))were 231.1 MPa,319.5MPa,and 12.54%respectively.The high tensile strengths of the extruded alloy mainly originated from grain refinement,texture strengthening,precipitation strengthening from a great number of nano-scale Mg_(2)Sn phases,solid solution strengthening and hetero-deformation induced(HDI)strengthening,while the good ductility of the alloy was also mainly attributed to grain refinement,activation of the non-basal slip systems and HDI hardening.展开更多
The effects of the co-addition of Ni and Zn on the microstructure and mechanical properties of the extruded Mg-6.84Y2.45Cu(MYC,wt%)alloy were researched.Results show that the as-cast Mg-6.79Y-1.21Cu-1.12Ni-1.25Zn(MYCN...The effects of the co-addition of Ni and Zn on the microstructure and mechanical properties of the extruded Mg-6.84Y2.45Cu(MYC,wt%)alloy were researched.Results show that the as-cast Mg-6.79Y-1.21Cu-1.12Ni-1.25Zn(MYCNZ,wt%)alloy consists of theα-Mg,a few Y-rich phases,lamellar 18R-long period stacking ordered(LPSO)phase,and granular Mg_(2)(Cu,Ni,Zn)phase.After the homogenization process,phase transformation occurs in MYCNZ alloy.Some 18R-LPSO phases at the grain boundary are transformed into the thin striped 14H-LPSO phase in the grains.After extrusion,the amount,morphology,and distribution of the second phase are changed,and the grain size of the extruded MYCNZ alloy is significantly reduced to approximately 2.62µm.Additionally,a weaker basal texture is formed in the extruded MYCNZ alloy.The tensile results indicate that the co-addition of Ni and Zn significantly enhances the tensile strength of the extruded MYC alloy while maintaining good ductility.The tensile yield strength(σ_(0.2)),ultimate tensile strength(σ_(b)),and elongation to failure(ε_(L))of the extruded MYCNZ alloy are 266.9 MPa,299.8 MPa,and 20.1%,respectively.This alloy has a good strength-plastic synergistic effect.The excellent tensile strength of the extruded MYCNZ alloy at room temperature is mainly due to grain refinement and the second phase strengthening effect,and its outstanding ductility is ascribed to the texture weakening and activation of non-basal slips.展开更多
This paper reviews the existing testing techniques for high voltage direct current(HVDC)cable systems,following as a backbone the structure of CIGRE Technical Brochure(TB)852:2021‘Recommendations for testing DC extru...This paper reviews the existing testing techniques for high voltage direct current(HVDC)cable systems,following as a backbone the structure of CIGRE Technical Brochure(TB)852:2021‘Recommendations for testing DC extruded cable systems for power transmission at a rated voltage up to 800 kV’because it has a fairly similar structure to CIGRE TB 853:2021 for lapped DC cables,and especially because of the impressive spread of HVDC extruded cables experienced worldwide in the last 25 years.The review considers development tests,pre-qualification tests,extension of qualification test,type tests(with hints at IEEE 1732-2017 for space charge measurements in the qualification of HVDC extruded cables),routine tests(with hints at IEEE 2862-2020 for routine tests of HVDC extruded cable system joints),sample tests and after installation tests.The review also analyses CIGRE TB 853 for lapped HVDC cable systems,as these cables remain unbeaten for submarine applications at the highest sea depths.The main novelties of CIGRE TB 852 and 853 with respect to previous standards for HVDC cable systems(mainly CIGRE TB 496 and IEC 62895 for extruded cables and CIGRE Electra 189:2000 for lapped cables)are put under the spotlight-with focus on the so-called temporary over-voltage tests-together with the limits and gaps of CIGRE TB 852.The main HVDC cable system testing equipment that is usually employed for electro-thermal tests is also treated.Emphasis is given to CIGRE TB 490 to treat the peculiarities of submarine cable systems,as well as to mechanical tests,having CIGRE TB 623 as a reference,with particular focus on the special sea trial tests.An example of an innovative sea trial testing procedure is shown,which is the outcome of a fruitful partnership between a cable manufacturer and the national Transmission System Operator in Italy.展开更多
In this work,AZ31B extruded sheets with mixed-grain microstructures were prepared through extrusion.Samples of mixed-grain microstructure with different morphologies were selected from the AZ31B extruded sheets(referr...In this work,AZ31B extruded sheets with mixed-grain microstructures were prepared through extrusion.Samples of mixed-grain microstructure with different morphologies were selected from the AZ31B extruded sheets(referred to as M1 and M2 samples,respectively).The creep tests were performed on these samples at the temperature range of 150-200℃,and the stress level range of 50-100 MPa.The creep properties and fracture behavior of AZ31 extruded sheets with mixed-grain microstructures were studied.Results showed that the creep properties of the M2 sample always outperformed that of the M1 sample and M1 and M2 samples’creep was dominated by dislocation movement.The creep rate of M2 samples(1.5×10^(-7)±1.1×10^(-10) s^(-1))is an order of magnitude lower than that of M1 samples(4.8×10^(-6)±8.1×10^(-10) s^(-1))at 200℃under 50 MPa The high activity of basal slip and softening mechanism in the M1 sample significantly accelerated creep,resulting in a relatively high creep rate.Moreover,the stress concentration within the M1 sample caused by deformation incompatibility,increased the initiation and propagation of voids,ultimately leading to fracture and poorer creep performance.However,the numerous<10µm fine grains surrounding deformed coarse grains in the M2 sample facilitated better coordination of deformation through dislocation slip,effectively slowing down the initiation of voids during the creep process.Meanwhile,the strain was uniformly distributed within each grain,mitigating stress concentration,inhibiting voids propagation,and contributing to the superior creep resistance of the M2 sample.展开更多
The use of single and twin-screw extruders for solid-phase reactions is a promising method to intensify a process in a more sustainable manner.In this manuscript,we report a detailed analysis of the residence time dis...The use of single and twin-screw extruders for solid-phase reactions is a promising method to intensify a process in a more sustainable manner.In this manuscript,we report a detailed analysis of the residence time distribution(RTD)in vertical single-screw reactors.The results will help in the selection of the right screw design that would help achieve the desired residence time,which is necessary for a reaction to happen.Experiments were conducted in three vertical screw reactors(having fixed shaft diameter)with varying dimensions using granular free-flowing powders of sodium chloride and silica with a mean particle size of∼25μm.RTD behavior was modeled using the radial particle velocities in the screw reactor's centrifugal field.Further,a method is proposed for estimating the axial dispersion coefficient of dry powders in such sheared flows using true and bulk densities of the powder and the screw shear rate.This dispersion coefficient is used in the axially dispersed plug flow model to describe the RTD behavior of screw reactors with acceptable accuracy.The theoretically predicted and experimentally obtained dispersion coefficients are found to be similar thereby confirming the suitability of the model.展开更多
The 3 D non isothermal flow of non Newtonian viscous polymer melt in a co rotating twin screw extruder is modeled. The distributions of the velocity, temperature, pressure and the viscous dissipation in the fl...The 3 D non isothermal flow of non Newtonian viscous polymer melt in a co rotating twin screw extruder is modeled. The distributions of the velocity, temperature, pressure and the viscous dissipation in the flow domain are presented by using a fluid dynamics analysis package (Polyflow). The numerical results show that the temperatures are high in the intermeshing region and on the screw surface, the maximum pressure and the minimum pressure occur in the intermeshing region, and the flow rate is almost proportional to the screw speed.展开更多
An experimental study on degeneration of the coldworking residual strainduring different cyclic loadings is presented. The expenmental results obtained showthat the residual strain of squcezing dislributes under power...An experimental study on degeneration of the coldworking residual strainduring different cyclic loadings is presented. The expenmental results obtained showthat the residual strain of squcezing dislributes under power series law ε= axb overthe horizontal line of the stress on both sides of the cenual hole. and that when the max-imum real stress at the hole is lower than the yield stress of the material. the degeneration of residual strain has a sudden change during cyclic loading, and the closer to thehole side, the more serious the degcneration.展开更多
In this paper, a theory of thick-walled shells is established by means of Hellinger-Reissner's variational principle, with displacement and stress assumptions. The displacements are expanded into power series of t...In this paper, a theory of thick-walled shells is established by means of Hellinger-Reissner's variational principle, with displacement and stress assumptions. The displacements are expanded into power series of the thickness coordinate. Only the first four and the first three terms are used for the displacements parallel and normal to the middle surface respectively. The normal extruding and transverse shear stresses are assumed to be cubic polynomials and to satisfy the boundary stress conditions on the outer and inner surfaces of the shell. The governing equations and boundary conditions are derived by means of variational principle. As an example, a thick-walled cylindrical shell is disscussed with the theory proposed. Furthermore, a photoelastic experiment has been carried out, and the results are in fair agreement with the computations.展开更多
AIM:To investigate glue extrusion after endoscopic N-butyl-2-cyanoacrylate injection on gastric variceal bleeding and to evaluate the long-term efficacy and safety of this therapy.METHODS:A total of 148 cirrhotic pati...AIM:To investigate glue extrusion after endoscopic N-butyl-2-cyanoacrylate injection on gastric variceal bleeding and to evaluate the long-term efficacy and safety of this therapy.METHODS:A total of 148 cirrhotic patients in our hospital with esophagogastric variceal bleeding(EGVB) were included in this study.N-butyl-2-cyanoacrylate was mixed with lipiodol in a 1:1 ratio and injected as a bolus of 1-3 mL according to variceal size.Patients underwent endoscopic follow-up the next week,fourth week,second month,fourth month,and seventh month after injection and then every 6 mo to determine the cast shape.An abdominal X-ray fi lm and ultrasound or computed tomographic scan were also carried out in order to evaluate the time of variceal disappearance and complete extrusion of the cast.The average follow-up time was 13.1 mo.RESULTS:The instantaneous hemostatic rate was 96.2%.Early re-bleeding after injection in 9 cases(6.2%) was estimated from rejection of adhesive.Late re-bleeding occurred in 12 patients(8.1%) at 2-18 mo.The glue cast was extruded into the lumen within one month in 86.1% of patients and eliminated within one year.Light erosion was seen at the injection position and mucosa edema in the second week.The glue casts were extruded in 18 patients(12.1%) after one week and in 64 patients(42.8%) after two weeks.All kinds of glue clumping shapes and colors on endoscopic examination were observed in 127 patients(86.1%) within one month,including punctiform,globular,pillar and variform.Forty one patients(27.9%) had glue extrusion after 3 mo and 28 patients(28.9%) after six months.The extrusion time was not related to the injection volume of histoacryl.Obliteration was seen in 70.2%(104 cases) endoscopically.The main complication was re-bleeding resulting from extrusion.The prognosis of the patients depended on the severity of the underlying liver disease.CONCLUSION:Endoscopic injection of cyanoacrylate is highly effective for gastric varices bleeding.The glue clump shape is correlated with anatomic structure of vessels.The time of extrusion was not related to dosage of the glue.展开更多
A yield phenomenon was firstly reported in an extruded Mg-6.8Y-2.5Cu alloy and the corresponding microstructure was also investigated in this work,The cast alloy is mainly composed ofα-Mg,18R long period stacking ord...A yield phenomenon was firstly reported in an extruded Mg-6.8Y-2.5Cu alloy and the corresponding microstructure was also investigated in this work,The cast alloy is mainly composed ofα-Mg,18R long period stacking order(LPSO)phase,eutectic phase(Mg_(20)Cu_(4)Y_(1)),and Mg_(2)Cu phase.The 18R LPSO phase at the dendritic grain boundary transforms into the 14H LPSO phase in the grain interior during homogenization.After extrusion,the grain size of the homogenized alloy is remarkably refined to-3.69μm and the second phase is significantly broken and distributed in the extrusion direction.Tensile testing curves of the extrude alloy at room temperature indicate that the yield strength and ultimate tensile strength increase while the elongation of the alloy decreases with increasing strain rate.Interestingly,a yield plateau fo rms and gradually decreases with increasing strain rate.The yield phenomenon is related to the dislocation multiplication and the interaction between the movable dislocations and solute atoms.展开更多
The effects of single-stage solution treatment(SST),enhanced solution treatment(EST),high-temperature pre-precipitation(HTPP)and multi-stage solution treatment(MST)on the microstructure,mechanical properties and corro...The effects of single-stage solution treatment(SST),enhanced solution treatment(EST),high-temperature pre-precipitation(HTPP)and multi-stage solution treatment(MST)on the microstructure,mechanical properties and corrosion resistance of the as-extruded 7055 aluminium alloy(AA7055)helical profile were investigated using differential scanning calorimetry(DSC),optical microscopy(OM),scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscopy(TEM).It was observed that EST and MST could promote the dissolution of the second-phase particles compared with the traditional SST,and the intergranular phases were distinctly discontinuously distributed after HTPP and MST.There was obvious difference in the main texture type and texture strength for the alloy after different solid solution treatments.HTPP could improve the corrosion resistance of the alloy by regulating the intergranular phases,but the mechanical properties were severely weakened.While the good corrosion resistance of the alloy could be obtained by MST without obvious strength loss.As a result,the MST is an ideal solid solution treatment scheme for AA7055.展开更多
The influences of binder and molding method on the catalytic performance of methane aromatization in the absence of O2 over MoO3/ZSM-5 catalysts were investigated.SEM,NH3-TPD,FT-IR of adsorbed pyridine,N2 adsorption-d...The influences of binder and molding method on the catalytic performance of methane aromatization in the absence of O2 over MoO3/ZSM-5 catalysts were investigated.SEM,NH3-TPD,FT-IR of adsorbed pyridine,N2 adsorption-desorption,cyclohexane adsorption and XPS were employed to characterize the physical and chemical properties of the catalysts.It was found that SiO2 was a suitable binder for the catalyst due to its appropriate weak acidity.The laminar catalyst comprising of an inert spherical core and a MoO3/ZSM-5 laminar shell with 0.1 0.2 mm in thickness showed a better catalytic performance than the extruded catalyst.The improved activity of the laminar catalyst could be attributed to the easy carbonization of Mo species and the quick removal of reaction products from the catalyst surface.展开更多
For the purpose of investigating the dynamic deformational behavior and failure mechanisms of magnesium under high strain rates,the Split Hopkinson Pressure Bar(SHPB)was used for investigating dynamic mechanical prope...For the purpose of investigating the dynamic deformational behavior and failure mechanisms of magnesium under high strain rates,the Split Hopkinson Pressure Bar(SHPB)was used for investigating dynamic mechanical properties of extruded Mg-Gd-Y Magnesium alloy at ambient temperature(300 K),200℃(473 K)and 300℃(573 K)temperature.The samples after compression were analyzed by scanning electron microscope(SEM)and metallographic microscope.Dynamic mechanical properties,crack performance and plastic deformation mechanism of extruded Mg-Gd-Y Magnesium alloy along the extrusion direction(ED)were discussed.The results show that,extruded Mg-Gd-Y Magnesium alloy has the largest dynamic compressive strength which is 535 MPa at ambient temperature(300 K)and strain rate of 2826 s^(−1).When temperature increases,dynamic compressive strength decreases,while ductility increases.The dynamic compression fracture mechanism of extruded Mg-Gd-Y Magnesium alloy is multi-crack propagation and intergranular quasi-cleavage fracture at both ambient temperature and high temperature.The dynamic compressive deformation mechanism of extruded Mg-Gd-Y Magnesium alloy is a combination of twinning,slipping and dynamic recrystallization at both ambient temperature and high temperature.展开更多
The influences of Ca and Ce/La microalloying on the microstructure evolution and bio-corrosion resistances of extruded Mg-Zn alloys have been systematically investigated in the current study.Compared with single Ca or...The influences of Ca and Ce/La microalloying on the microstructure evolution and bio-corrosion resistances of extruded Mg-Zn alloys have been systematically investigated in the current study.Compared with single Ca or Ce/La addition,the Ca-Ce/La cooperative microalloying results in an outstanding grain refinement,because the fine secondary phase particles effectively hinder the recrystallized grain growth.The coarse Ca2Mg6Zn3 phases promote the formation of Ca3(PO4)2 or hydroxyapatite particles during the immersion process and accelerate the dissolution of the corrosion product film,which destroys its integrity and results in the deterioration of anti-corrosive performance.The Ce/La elements can be dispersed within the conventional Mg7Zn3 phases,which reduce the internal galvanic corrosion between Mg matrix and the secondary phases,leading to an obvious improvement of corrosion resistance.Therefore,the Ca-Ce/La cooperative microalloying achieves a homogenous fine-grained microstructure and improves the protective ability of surface film,which will pave a new avenue for the design of biomedical Mg alloys in the coming future.展开更多
Low cycle fatigue behavior of extruded AZ80 magnesium alloy was investigated under uniaxial tension-compression at different strain amplitudes and strain rates.The results show that the extruded AZ80 magnesium alloy e...Low cycle fatigue behavior of extruded AZ80 magnesium alloy was investigated under uniaxial tension-compression at different strain amplitudes and strain rates.The results show that the extruded AZ80 magnesium alloy exhibits cyclic hardening at strain amplitudes ranging from 0.4%to 1.0%,the asymmetry of hysteresis loops becomes increasingly obvious when the strain amplitude increases.Higher strain rates correspond to higher stress amplitudes,high mean stresses and short fatigue life.{10–12}extension twins play a role in the cyclic deformation under higher strain amplitudes(0.8%,1.0%).The relationship between total strain energy density and fatigue life can be described by the modified Morrow model.The effect of strain rate on the fatigue life can also be predicted by the model.展开更多
基金National Natural Science Foundation of China(No.51345006)Specialized Research Fund for the Doctoral Program of Higher Education,China(No.20123719120004)
文摘One improved mixing-extruding machine was introduced as the second-generation product of the mixing-molding integrated technology. In the extruding system,the conventional single screw extruder was substituted by a special conical twin-screw extruder,resulting in stronger feeding ability,more stable extrusion pressure,and better quality of products. The integrated mathematical model of mixing-extruding process was also established by theoretical derivation and optimization according to the experimental results.Then its accuracy was verified by the influences of the pressure of floating weight and the cooling water temperature of extruder on the mixing-extruding integrated process. The results showed that the changes of both parameters could give rise to the fluctuation of the temperature and apparent viscosity of polyblends, thus further influencing the screw rotation speed.
基金Funded by the National Natural Science Foundation of China(No.50274020) and Baoshan Iron &Steel Corporation of Shanghai
文摘Continuous extruding/ extending formiug process for A2017 alloy in semi-solid state was proposed through installing extending die at the outlet of shearing- cooling- rolling （SCR） machine. A series of experiments to produce fiat bar of A2017 alloy were carried oat. The forming process, metal flow behavior in die and microstructure and mechanical property of prodacts were investigated. It is shown that if the pouring temperature of melt was higher, the die was filled with semi-solid slurry with low solid fraction and periodical cracks would occur on the product surface ; If its pouring temperature was lower or the preheating temperature of die was lower, semisolid slurry would solidify rapidly and block the die after entering the cavity. The analysis of mass flow trace shows that the semi-solid slurry move forward layer by layer and fills the die extending cavity in radiation manner and the velocity of mass flow in the central area of extending cavity and exit of mould is the maximum, and then decreases gradually from the center to both sides of die wall. By inereasiug the die extending angle, the velocity of mass flow becomes more homogeneous. Under rational process control and die design, the A2017 fiat bar with transverse section of 10 × 50 mm and with good surface and fine equiaxed grains can be obtained by continuous extruding/extending forming process. The product＇s tensile strength and elongation are 420.5 MPa and 14.2% , respectively.
文摘In this paper, the kinematically admissible velocity field with surface crack on forward extruding bar is put forward during the axisymmetric cup-bar combined extrusion process, in accordance with the results of model experiments.On the basis of velocity field, the necessary condition for surface crack formation on the forward extruding bar is derived, with the help of upper bound theorem and the minimum energy principle. Meanwhile, the relationships between surface crack formation and combination of reduction in area for the part of forward and backward extursions relative residual thickness of billet (T/R0),frictional factor (m) or relative land length of ram and chamber are calculated during the extrusion process. Therefore, whether the surface crack on forward exturding bar occurs can be predicted before extruding the lower-plasticity metals for axisymmetric cup-bar combined extrusion process.The analytical results agree very well with experimental results of aluminium alloy LY12 (ASTM 2024) and LC4 (ASTM 7075).
基金Supported by the Key Project of Jilin Province Science & Technology Department (Grant No. 20030311)the "985 Project" of Jilin University
文摘In the paper a self-adjusting hydraulic machine for combination forming of upsetting and extruding is systematacially presented in terms of mechanical principle, design principle, machine construction, design of the key components and working routine. The machine is designed with the following features: The lower movable beam is adjusted by the ejecting cylinder, the upper upsetting beam is reset by the backstroke slide rods, and the upsetting cylinders communicate with the gas-liquid accumulators. These features make the machine conformation compact, save both the backstroke cylinder of the upper upsetting beam and the upsetting cylinder of the lower movable beam, and simplify the hydraulic system. Furthermore, the machine can resolve such problems as incomplete filling at the addendum position, microcracks at the dedendum position, greater force and lower die life during precision forging of spur gears.
基金supported by the Major Science and Technology Project of Gansu Province(Grant No.22ZD6GA008)the National Natural Science Foundation of China(Nos.52261027,52001152 and 51961021)+2 种基金the Open Project of State Key Laboratory for Mechanical Behavior of Materials(20192102)Undergraduate Innovation and Entrepreneurship Training Program(Nos.DC20231482,DC20231188 and DC20231558)Gansu Provincial Excellent Graduate Students“Innovation Star”Program(2022CXZX-394)。
文摘The high-strength Mg-7Sn alloys(wt.%)with a heterogeneous grain structure were prepared by low-temperature extrusion(230°C)with the extrusion ratio of 9:1(9E230)and 17:1(17E230).The two extruded alloys contained fine dynamic recrystallization(DRX)grains(FG)and coarse un DRX grains(CG).The difference in deformability between CG and FG leads to the formation of heterogeneous grain structure.The average grain size and basal texture intensities increased while the volume fraction of CG decreased with increasing extrusion ratio.Tensile testing results indicated that the extruded 17E230 alloy exhibited higher tensile strengths than 9E230 alloy,whose tensile yield strength(σ_(0.2)),ultimate tensile strengths(σ_(b)),and elongation to failure(ε_(f))were 231.1 MPa,319.5MPa,and 12.54%respectively.The high tensile strengths of the extruded alloy mainly originated from grain refinement,texture strengthening,precipitation strengthening from a great number of nano-scale Mg_(2)Sn phases,solid solution strengthening and hetero-deformation induced(HDI)strengthening,while the good ductility of the alloy was also mainly attributed to grain refinement,activation of the non-basal slip systems and HDI hardening.
基金Major Science and Technology Project of Gansu Province(22ZD6GA008)National Natural Science Foundation of China(52261027,51961021,52001152)+2 种基金Open Project of State Key Laboratory for Mechanical Behavior of Materials(20192102)Undergraduate Innovation and Entrepreneurship Training Program(DC20231188,DC20231482,DC20231558,DC20231469,DC20231441)Supported by Sinoma Institute of Materials Research(Guang Zhou)Co.,Ltd(SIMR)。
文摘The effects of the co-addition of Ni and Zn on the microstructure and mechanical properties of the extruded Mg-6.84Y2.45Cu(MYC,wt%)alloy were researched.Results show that the as-cast Mg-6.79Y-1.21Cu-1.12Ni-1.25Zn(MYCNZ,wt%)alloy consists of theα-Mg,a few Y-rich phases,lamellar 18R-long period stacking ordered(LPSO)phase,and granular Mg_(2)(Cu,Ni,Zn)phase.After the homogenization process,phase transformation occurs in MYCNZ alloy.Some 18R-LPSO phases at the grain boundary are transformed into the thin striped 14H-LPSO phase in the grains.After extrusion,the amount,morphology,and distribution of the second phase are changed,and the grain size of the extruded MYCNZ alloy is significantly reduced to approximately 2.62µm.Additionally,a weaker basal texture is formed in the extruded MYCNZ alloy.The tensile results indicate that the co-addition of Ni and Zn significantly enhances the tensile strength of the extruded MYC alloy while maintaining good ductility.The tensile yield strength(σ_(0.2)),ultimate tensile strength(σ_(b)),and elongation to failure(ε_(L))of the extruded MYCNZ alloy are 266.9 MPa,299.8 MPa,and 20.1%,respectively.This alloy has a good strength-plastic synergistic effect.The excellent tensile strength of the extruded MYCNZ alloy at room temperature is mainly due to grain refinement and the second phase strengthening effect,and its outstanding ductility is ascribed to the texture weakening and activation of non-basal slips.
文摘This paper reviews the existing testing techniques for high voltage direct current(HVDC)cable systems,following as a backbone the structure of CIGRE Technical Brochure(TB)852:2021‘Recommendations for testing DC extruded cable systems for power transmission at a rated voltage up to 800 kV’because it has a fairly similar structure to CIGRE TB 853:2021 for lapped DC cables,and especially because of the impressive spread of HVDC extruded cables experienced worldwide in the last 25 years.The review considers development tests,pre-qualification tests,extension of qualification test,type tests(with hints at IEEE 1732-2017 for space charge measurements in the qualification of HVDC extruded cables),routine tests(with hints at IEEE 2862-2020 for routine tests of HVDC extruded cable system joints),sample tests and after installation tests.The review also analyses CIGRE TB 853 for lapped HVDC cable systems,as these cables remain unbeaten for submarine applications at the highest sea depths.The main novelties of CIGRE TB 852 and 853 with respect to previous standards for HVDC cable systems(mainly CIGRE TB 496 and IEC 62895 for extruded cables and CIGRE Electra 189:2000 for lapped cables)are put under the spotlight-with focus on the so-called temporary over-voltage tests-together with the limits and gaps of CIGRE TB 852.The main HVDC cable system testing equipment that is usually employed for electro-thermal tests is also treated.Emphasis is given to CIGRE TB 490 to treat the peculiarities of submarine cable systems,as well as to mechanical tests,having CIGRE TB 623 as a reference,with particular focus on the special sea trial tests.An example of an innovative sea trial testing procedure is shown,which is the outcome of a fruitful partnership between a cable manufacturer and the national Transmission System Operator in Italy.
基金supported by the National Natural Science Foundation of China(52474419,52374395)Natural Science Foundation of Shanxi Province(20210302123135,202303021221143)+3 种基金Scientific and Technological Achievements Transformation Guidance Special Project of Shanxi Province(202104021301022,202204021301009)Central Government Guided Local Science and Technology development projects(YDZJSX20231B003,YDZJSX2021A010)The Ministry of Science and Higher Education of the Russian Federation for financial support under the Megagrant(No.075-15-2022-1133)the National Research Foundation(NRF)grant funded by the Ministry of Science and ICT(2015R1A2A1A01006795)of Korea through the Research Institute of Advanced.
文摘In this work,AZ31B extruded sheets with mixed-grain microstructures were prepared through extrusion.Samples of mixed-grain microstructure with different morphologies were selected from the AZ31B extruded sheets(referred to as M1 and M2 samples,respectively).The creep tests were performed on these samples at the temperature range of 150-200℃,and the stress level range of 50-100 MPa.The creep properties and fracture behavior of AZ31 extruded sheets with mixed-grain microstructures were studied.Results showed that the creep properties of the M2 sample always outperformed that of the M1 sample and M1 and M2 samples’creep was dominated by dislocation movement.The creep rate of M2 samples(1.5×10^(-7)±1.1×10^(-10) s^(-1))is an order of magnitude lower than that of M1 samples(4.8×10^(-6)±8.1×10^(-10) s^(-1))at 200℃under 50 MPa The high activity of basal slip and softening mechanism in the M1 sample significantly accelerated creep,resulting in a relatively high creep rate.Moreover,the stress concentration within the M1 sample caused by deformation incompatibility,increased the initiation and propagation of voids,ultimately leading to fracture and poorer creep performance.However,the numerous<10µm fine grains surrounding deformed coarse grains in the M2 sample facilitated better coordination of deformation through dislocation slip,effectively slowing down the initiation of voids during the creep process.Meanwhile,the strain was uniformly distributed within each grain,mitigating stress concentration,inhibiting voids propagation,and contributing to the superior creep resistance of the M2 sample.
基金funding from CSIR(MLP100926)and SERB(DST,Govt.of India)(CRG//2023/001897-G)for this work.
文摘The use of single and twin-screw extruders for solid-phase reactions is a promising method to intensify a process in a more sustainable manner.In this manuscript,we report a detailed analysis of the residence time distribution(RTD)in vertical single-screw reactors.The results will help in the selection of the right screw design that would help achieve the desired residence time,which is necessary for a reaction to happen.Experiments were conducted in three vertical screw reactors(having fixed shaft diameter)with varying dimensions using granular free-flowing powders of sodium chloride and silica with a mean particle size of∼25μm.RTD behavior was modeled using the radial particle velocities in the screw reactor's centrifugal field.Further,a method is proposed for estimating the axial dispersion coefficient of dry powders in such sheared flows using true and bulk densities of the powder and the screw shear rate.This dispersion coefficient is used in the axially dispersed plug flow model to describe the RTD behavior of screw reactors with acceptable accuracy.The theoretically predicted and experimentally obtained dispersion coefficients are found to be similar thereby confirming the suitability of the model.
文摘The 3 D non isothermal flow of non Newtonian viscous polymer melt in a co rotating twin screw extruder is modeled. The distributions of the velocity, temperature, pressure and the viscous dissipation in the flow domain are presented by using a fluid dynamics analysis package (Polyflow). The numerical results show that the temperatures are high in the intermeshing region and on the screw surface, the maximum pressure and the minimum pressure occur in the intermeshing region, and the flow rate is almost proportional to the screw speed.
文摘An experimental study on degeneration of the coldworking residual strainduring different cyclic loadings is presented. The expenmental results obtained showthat the residual strain of squcezing dislributes under power series law ε= axb overthe horizontal line of the stress on both sides of the cenual hole. and that when the max-imum real stress at the hole is lower than the yield stress of the material. the degeneration of residual strain has a sudden change during cyclic loading, and the closer to thehole side, the more serious the degcneration.
文摘In this paper, a theory of thick-walled shells is established by means of Hellinger-Reissner's variational principle, with displacement and stress assumptions. The displacements are expanded into power series of the thickness coordinate. Only the first four and the first three terms are used for the displacements parallel and normal to the middle surface respectively. The normal extruding and transverse shear stresses are assumed to be cubic polynomials and to satisfy the boundary stress conditions on the outer and inner surfaces of the shell. The governing equations and boundary conditions are derived by means of variational principle. As an example, a thick-walled cylindrical shell is disscussed with the theory proposed. Furthermore, a photoelastic experiment has been carried out, and the results are in fair agreement with the computations.
文摘AIM:To investigate glue extrusion after endoscopic N-butyl-2-cyanoacrylate injection on gastric variceal bleeding and to evaluate the long-term efficacy and safety of this therapy.METHODS:A total of 148 cirrhotic patients in our hospital with esophagogastric variceal bleeding(EGVB) were included in this study.N-butyl-2-cyanoacrylate was mixed with lipiodol in a 1:1 ratio and injected as a bolus of 1-3 mL according to variceal size.Patients underwent endoscopic follow-up the next week,fourth week,second month,fourth month,and seventh month after injection and then every 6 mo to determine the cast shape.An abdominal X-ray fi lm and ultrasound or computed tomographic scan were also carried out in order to evaluate the time of variceal disappearance and complete extrusion of the cast.The average follow-up time was 13.1 mo.RESULTS:The instantaneous hemostatic rate was 96.2%.Early re-bleeding after injection in 9 cases(6.2%) was estimated from rejection of adhesive.Late re-bleeding occurred in 12 patients(8.1%) at 2-18 mo.The glue cast was extruded into the lumen within one month in 86.1% of patients and eliminated within one year.Light erosion was seen at the injection position and mucosa edema in the second week.The glue casts were extruded in 18 patients(12.1%) after one week and in 64 patients(42.8%) after two weeks.All kinds of glue clumping shapes and colors on endoscopic examination were observed in 127 patients(86.1%) within one month,including punctiform,globular,pillar and variform.Forty one patients(27.9%) had glue extrusion after 3 mo and 28 patients(28.9%) after six months.The extrusion time was not related to the injection volume of histoacryl.Obliteration was seen in 70.2%(104 cases) endoscopically.The main complication was re-bleeding resulting from extrusion.The prognosis of the patients depended on the severity of the underlying liver disease.CONCLUSION:Endoscopic injection of cyanoacrylate is highly effective for gastric varices bleeding.The glue clump shape is correlated with anatomic structure of vessels.The time of extrusion was not related to dosage of the glue.
基金Project supported by the National Natural Science Foundation of China(51961021,52001152 and 51901174)China Postdoctoral Science Foundation(2020M673383)。
文摘A yield phenomenon was firstly reported in an extruded Mg-6.8Y-2.5Cu alloy and the corresponding microstructure was also investigated in this work,The cast alloy is mainly composed ofα-Mg,18R long period stacking order(LPSO)phase,eutectic phase(Mg_(20)Cu_(4)Y_(1)),and Mg_(2)Cu phase.The 18R LPSO phase at the dendritic grain boundary transforms into the 14H LPSO phase in the grain interior during homogenization.After extrusion,the grain size of the homogenized alloy is remarkably refined to-3.69μm and the second phase is significantly broken and distributed in the extrusion direction.Tensile testing curves of the extrude alloy at room temperature indicate that the yield strength and ultimate tensile strength increase while the elongation of the alloy decreases with increasing strain rate.Interestingly,a yield plateau fo rms and gradually decreases with increasing strain rate.The yield phenomenon is related to the dislocation multiplication and the interaction between the movable dislocations and solute atoms.
基金the financial supports from the National Natural Science Foundation of China(No.51975330)Science Fund for Distinguished Young Scholars of Shandong Province,China(No.JQ201810)the Key Research and Development Program of Shandong Province,China(No.2019JZZY010360).
文摘The effects of single-stage solution treatment(SST),enhanced solution treatment(EST),high-temperature pre-precipitation(HTPP)and multi-stage solution treatment(MST)on the microstructure,mechanical properties and corrosion resistance of the as-extruded 7055 aluminium alloy(AA7055)helical profile were investigated using differential scanning calorimetry(DSC),optical microscopy(OM),scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD)and transmission electron microscopy(TEM).It was observed that EST and MST could promote the dissolution of the second-phase particles compared with the traditional SST,and the intergranular phases were distinctly discontinuously distributed after HTPP and MST.There was obvious difference in the main texture type and texture strength for the alloy after different solid solution treatments.HTPP could improve the corrosion resistance of the alloy by regulating the intergranular phases,but the mechanical properties were severely weakened.While the good corrosion resistance of the alloy could be obtained by MST without obvious strength loss.As a result,the MST is an ideal solid solution treatment scheme for AA7055.
基金supported by the National Basic Research Program of China(Grant 2005CB 221405)
文摘The influences of binder and molding method on the catalytic performance of methane aromatization in the absence of O2 over MoO3/ZSM-5 catalysts were investigated.SEM,NH3-TPD,FT-IR of adsorbed pyridine,N2 adsorption-desorption,cyclohexane adsorption and XPS were employed to characterize the physical and chemical properties of the catalysts.It was found that SiO2 was a suitable binder for the catalyst due to its appropriate weak acidity.The laminar catalyst comprising of an inert spherical core and a MoO3/ZSM-5 laminar shell with 0.1 0.2 mm in thickness showed a better catalytic performance than the extruded catalyst.The improved activity of the laminar catalyst could be attributed to the easy carbonization of Mo species and the quick removal of reaction products from the catalyst surface.
基金The authors would like to acknowledge the financial support from the National Key Basic Research Program(973 Program),Project(2013CB632205).
文摘For the purpose of investigating the dynamic deformational behavior and failure mechanisms of magnesium under high strain rates,the Split Hopkinson Pressure Bar(SHPB)was used for investigating dynamic mechanical properties of extruded Mg-Gd-Y Magnesium alloy at ambient temperature(300 K),200℃(473 K)and 300℃(573 K)temperature.The samples after compression were analyzed by scanning electron microscope(SEM)and metallographic microscope.Dynamic mechanical properties,crack performance and plastic deformation mechanism of extruded Mg-Gd-Y Magnesium alloy along the extrusion direction(ED)were discussed.The results show that,extruded Mg-Gd-Y Magnesium alloy has the largest dynamic compressive strength which is 535 MPa at ambient temperature(300 K)and strain rate of 2826 s^(−1).When temperature increases,dynamic compressive strength decreases,while ductility increases.The dynamic compression fracture mechanism of extruded Mg-Gd-Y Magnesium alloy is multi-crack propagation and intergranular quasi-cleavage fracture at both ambient temperature and high temperature.The dynamic compressive deformation mechanism of extruded Mg-Gd-Y Magnesium alloy is a combination of twinning,slipping and dynamic recrystallization at both ambient temperature and high temperature.
基金the National Natural Science Foundation(Grant nos.5177117&51671152 and 51874225)the Key Research and Development Program of Shanxi Province(Grant nos.2020KWZ-007 and 2018ZDXMGY-149)the Youth Innovation Team of Shanxi Universities and the Natural Science Foundation of Jilin Province(Grant no.20180414016GH).
文摘The influences of Ca and Ce/La microalloying on the microstructure evolution and bio-corrosion resistances of extruded Mg-Zn alloys have been systematically investigated in the current study.Compared with single Ca or Ce/La addition,the Ca-Ce/La cooperative microalloying results in an outstanding grain refinement,because the fine secondary phase particles effectively hinder the recrystallized grain growth.The coarse Ca2Mg6Zn3 phases promote the formation of Ca3(PO4)2 or hydroxyapatite particles during the immersion process and accelerate the dissolution of the corrosion product film,which destroys its integrity and results in the deterioration of anti-corrosive performance.The Ce/La elements can be dispersed within the conventional Mg7Zn3 phases,which reduce the internal galvanic corrosion between Mg matrix and the secondary phases,leading to an obvious improvement of corrosion resistance.Therefore,the Ca-Ce/La cooperative microalloying achieves a homogenous fine-grained microstructure and improves the protective ability of surface film,which will pave a new avenue for the design of biomedical Mg alloys in the coming future.
基金the National Basic Research Program of China(No.2013CB632205).
文摘Low cycle fatigue behavior of extruded AZ80 magnesium alloy was investigated under uniaxial tension-compression at different strain amplitudes and strain rates.The results show that the extruded AZ80 magnesium alloy exhibits cyclic hardening at strain amplitudes ranging from 0.4%to 1.0%,the asymmetry of hysteresis loops becomes increasingly obvious when the strain amplitude increases.Higher strain rates correspond to higher stress amplitudes,high mean stresses and short fatigue life.{10–12}extension twins play a role in the cyclic deformation under higher strain amplitudes(0.8%,1.0%).The relationship between total strain energy density and fatigue life can be described by the modified Morrow model.The effect of strain rate on the fatigue life can also be predicted by the model.
