Conducting complete energy audit (both process and utility) of a sponge iron unit is challenging as there is no laid down procedure to audit the process side. Further, the average heat to power ratio (kWth/kWe) of spo...Conducting complete energy audit (both process and utility) of a sponge iron unit is challenging as there is no laid down procedure to audit the process side. Further, the average heat to power ratio (kWth/kWe) of sponge iron plants ranges from (25:1) to (31:1). This shows that the manufacturing process mostly uses thermal energy and application of electrical energy is insignificant. The main & only source of thermal energy is coal and the entire coal is fed to the rotary kiln. Therefore we find that “Kiln” is the “Black-Box” of this industry and the success of energy efficiency is hidden in the kiln process chemistry. This article tries to establish detailed energy audit methodology of sponge iron manufacturing process or kiln operation with a view to finding out major energy saving potential of the unit. In the research work we find that it is the incomplete reaction of coal that causes the major energy inefficiency in the process. Substantial amount of un-reacted carbon comes out with the char (by-product) which has virtually zero commercial value. The article also puts a question mark on the justification of using high-grade imported coal in such energy inefficient industries.展开更多
Most outburst mines in China adopt the measures of pre drainage by drilling along the seam for gas control in the mining area, that is, drilling along the seam from the air roadway of the mining machine to the mining ...Most outburst mines in China adopt the measures of pre drainage by drilling along the seam for gas control in the mining area, that is, drilling along the seam from the air roadway of the mining machine to the mining area. The drainage effect of drilling along the seam is directly related to the gas control effect of the mining area. For many years, we have carried out the measures according to the provisions of the detailed rules for the prevention and control of coal and gas outburst. The sealing length of the bedding hole is consistently kept at 8m, and the depth of the sealing section is kept at about 10m, and the extraction concentration and pure amount have been maintained at a low level, resulting in relatively large gas emission during mining. We break the Convention and calculate the sealing depth of the hole according to the pre drainage equivalent width of the coal roadway. At the same time, the extended version of high-pressure grouting is used for two plugs and one injection seal, so that the hole sealing depth of the borehole is within the equivalent width of the roadway pre drainage gas, and the length of the hole sealing section is longer. At the same time, combined with the whole process casing running technology of bedding drilling, the contact area between the screen pipe and the coal wall is likely to be increased, and good results have been achieved in preventing the impact of hole collapse and other phenomena on the drainage effect. The concentration of single hole drainage and the net amount of main pipe drainage have been greatly improved, and the gas content and gas pressure of coal have decreased significantly.展开更多
The dynamics of the drying process of polymer solutions are important for the development of coatings and films.In the present work,digital holographic microscopy(DHM)was performed to capture the drying dynamics of po...The dynamics of the drying process of polymer solutions are important for the development of coatings and films.In the present work,digital holographic microscopy(DHM)was performed to capture the drying dynamics of poly(ethylene oxide)(PEO)droplets using a gold nanoparticle tracer,where the heterogeneous flow field in different regions was illustrated.This demonstrates that the gold nanoparticles at either the center or the edge regions of the droplet exhibit anisotropic kinematic behavior.At early stage,Marangoni backflow causes gold nanoparticles to move towards the edge firstly,and the circles back towards the droplet center after arriving the contact line with a sudden increase in z axis for 10.4μm,indicating the scale of the upward-moving microscopic flow vortices.This phenomenon does not occur in water droplets in the absence of polymers.The gold nanoparticles underwent Brownian-like motion at the center of the PEO droplet or water droplet owing to the low perturbation of the flow field.At the late stage of pinning of the PEO droplets,the motion showed multiple reverses in the direction of the gold nanoparticles,indicating the complexity of the flow field.This study enhances the understanding of the drying dynamics of polymer solution droplets and offers valuable insights into the fabrication of surface materials.展开更多
Supercapacitors are efficient and versatile energy storage devices,offering remarkable power density,fast charge/discharge rates,and exceptional cycle life.As research continues to push the boundaries of their perform...Supercapacitors are efficient and versatile energy storage devices,offering remarkable power density,fast charge/discharge rates,and exceptional cycle life.As research continues to push the boundaries of their performance,electrode fabrication techniques are critical aspects influencing the overall capabilities of supercapacitors.Herein,we aim to shed light on the advantages offered by dry electrode processing for advanced supercapacitors.Notably,our study explores the performance of these electrodes in three different types of electrolytes:organic,ionic liquids,and quasi-solid states.By examining the impact of dry electrode processing on various electrode and electrolyte systems,we show valuable insights into the versatility and efficacy of this technique.The supercapacitors employing dry electrodes demonstrated significant improvements compared with conventional wet electrodes,with a lifespan extension of+45%in organic,+192%in ionic liquids,and+84%in quasi-solid electrolytes.Moreover,the increased electrode densities achievable through the dry approach directly translate to improved volumetric outputs,enhancing energy storage capacities within compact form factors.Notably,dry electrode-prepared supercapacitors outperformed their wet electrode counterparts,exhibiting a higher energy density of 6.1 Wh cm^(-3)compared with 4.7 Wh cm^(-3)at a high power density of 195Wcm^(-3),marking a substantial 28%energy improvement in the quasi-solid electrolyte.展开更多
Biomaterial will shrink during the drying process. The characteristics of shrinkage and rehydration of fresh peas were studied. Drying curves, shrinkage and rehydration curves of peas without seed coats and whole peas...Biomaterial will shrink during the drying process. The characteristics of shrinkage and rehydration of fresh peas were studied. Drying curves, shrinkage and rehydration curves of peas without seed coats and whole peas were compared. In addition, different volumetric shrinkage coefficients were obtained and discussed. The results show that seed coats resist moisture movement not only from inside to outside but also from outside to inside during different drying conditions. During a seed’s drying process, the drying curve is similar to the shrinkage curve. The higher the heat flux is, the less drying time is needed, and in the meantime, volume would shrink more and more intensively. Dried media will break easily at high heat flux. When we create a drying regime, both drying speed and the quality of dried media should be considered.展开更多
A numerical simulation for a model of wood drying process is considered. The model is given by a couple of nonlinear differential equations. One is a nonlinear parabolic equation and the other one is a nonlinear ordin...A numerical simulation for a model of wood drying process is considered. The model is given by a couple of nonlinear differential equations. One is a nonlinear parabolic equation and the other one is a nonlinear ordinary equation. A difference scheme is derived by the method of reduction of order. First, a new variable is introduced and the original problem is rewritten into a system of the first-order differential equations. Secondly, a difference scheme is constructed for the later problem. The solvability, stability and convergence of the difference scheme are proved by the energy method. The convergence order of the difference scheme is secondorder both in time and in space. A prior error estimate is put forward. The new variable is put aside to reduce the computational cost. A numerical example testifies the theoretical result.展开更多
A particular porosity method named ＂slot method＂ is implemented in a depth-integrated shallow water flow model （DIVAST） to simulate wetting and drying processes. Discussed is the relationship between the shape fac...A particular porosity method named ＂slot method＂ is implemented in a depth-integrated shallow water flow model （DIVAST） to simulate wetting and drying processes. Discussed is the relationship between the shape factors of the ＂slot＂ and the preset depth used in ＂wetting-drying＂ algorithm. Two typical tests are conducted to examine the performance of the method with the effect of the shape factors of the ＂slot＂ being checked in detail in the first test. Numerical results demonstrate that： 1 ） no additional effort to improve the finite difference scheme is needed to implement ＂slot method＂ in DIVAST, and 2） ＂slot method＂ will simulate wetting and diying processes correctly if the shape factors of the ＂slot＂ being selected properly.展开更多
A type of antibacterial bacterial cellulose(BC) film was prepared for potential uses as wound dressing.In order to obtain a high antibacterial effect,some forms of BC films,including the wet and dried ones were utiliz...A type of antibacterial bacterial cellulose(BC) film was prepared for potential uses as wound dressing.In order to obtain a high antibacterial effect,some forms of BC films,including the wet and dried ones were utilized as the template to in situ synthesize silver nanoparticles(AgNPs).The effects of drying methods including freeze-drying,heat drying and air drying,on the microstructures and physical properties of BC,as well as the silver contents and the antibacterial performances of the BC/AgNPs composites were investigated.It was found that the AgNPs impregnated on the dried BC films were inclined to achieve a faster silver releasing rate than the wet one,which was suitable for acute traumas treatment.展开更多
Hemicellulose has a wide range of applications,including that as an emulsifier for the food industry and raw material for the synthesis of bioethanol/biochemicals and biodegradable films.Hemicellulose is usually prese...Hemicellulose has a wide range of applications,including that as an emulsifier for the food industry and raw material for the synthesis of bioethanol/biochemicals and biodegradable films.Hemicellulose is usually present as a spent liquor,such as the prehydrolysis liquor of the prehydrolysis kraft dissolving pulp production process and the alkali extraction liquor of the cold caustic extraction of pulp fibers.Due to its dilute nature,hemicellulose needs to be dried for practical utilization,and this is challenging.In this study,cellulose and hemicellulose in a bleached bamboo kraft pulp were separated using an alkali extraction process.Hemicellulose obtained from the extraction liquor was dried by an ammonium carbonate-assisted drying process.The effects of drying time and drying temperature were determined.Structure of the hemicellulose obtained by the ammonium carbonate-assisted drying process was similar to that of original hemicellulose,as revealed by detailed Fourier transform infrared and X-ray diffraction analyses.The novel drying method was more energy efficient and required a shorter drying time than the conventional freeze drying method,and the excellent solubility in alkaline solutions favored the chemical modification of hemicellulose.The dried hemicellulose can be used as a renewable raw material for the preparation of hydrogels and other substances such as bioethanol/biochemicals and biodegradable films.展开更多
针对传统鱼糕货架期短、运输条件苛刻、食用方法单一等问题,本研究通过配方优化与真空冷冻干燥技术开发新型鱼糕产品,旨在延长其保质期、提升营养均衡性并拓展即食化、多场景应用潜力,同时为水产制品的工业化加工提供工艺参考。以鲢鱼...针对传统鱼糕货架期短、运输条件苛刻、食用方法单一等问题,本研究通过配方优化与真空冷冻干燥技术开发新型鱼糕产品,旨在延长其保质期、提升营养均衡性并拓展即食化、多场景应用潜力,同时为水产制品的工业化加工提供工艺参考。以鲢鱼为主要原料,基于层次分析-熵权法构建综合评分模型,选择猪肥肉、鸡肉、玉米淀粉和蛋清添加量进行单因素实验,并在单因素实验基础上通过遗传算法结合Box-Behnken响应面法对鱼糕冻干配方进行优化。通过扫描电子显微镜(scanning electron microscopy,SEM)分析微观结构,测定蛋白质、脂肪、水分、灰分等理化指标,并基于Arrhenius方程预测货架期。确定了鱼糕冻干最优配方为:相对碎鱼肉用量,猪肥肉添加量10%(质量分数),鸡肉添加量20%,玉米淀粉添加量11%,蛋清添加量8%,综合评分达0.87±0.34。微观结构显示孔隙分布均匀,真空冷冻干燥处理前后关键理化指标无显著变化。基于Arrhenius方程的货架期模型预测25℃贮藏期为77 d,较鲜切鱼糕(4~7 d)延长11倍。本研究得到了色泽均匀、口感酥脆、货架期长以及营养均衡的鱼糕冻干制品,为鱼糕制品常温储运与即食化应用提供借鉴。展开更多
Introduction Cationic starches are a series of products of which various sorts with different properties and usages can all be produced via cationic reactions by using different types of etherification agents under di...Introduction Cationic starches are a series of products of which various sorts with different properties and usages can all be produced via cationic reactions by using different types of etherification agents under different conditions. As an additive and strengthening agent,展开更多
OBJECTIVE： To study the effects of the drying processing in terms operational parameters on the bio- active constituents of six YuanzhJ （Radix Palygalae） samples across China. METHODS： Six Yuanzhi （Radix Palygala...OBJECTIVE： To study the effects of the drying processing in terms operational parameters on the bio- active constituents of six YuanzhJ （Radix Palygalae） samples across China. METHODS： Six Yuanzhi （Radix Palygalae） samples were investigated using thermogravimetry analysis. The heating courses were set in two ways： the temperature-programmed process from room temperature to 150℃ ,and the constant-temperature course at 50℃, 70℃ and 90℃. RESULTS： The peak temperature of six Yuanzhi （Radix Palygalae） samples ranged from 78℃ to 88℃. The mass loss rate of Yuanzhi （Radix Palygalae） alcohol-soluble extract was significantly increased when heated at 90℃. Four types of bioactive ingredients were detected in volatile oils of Yuanzhi （Radix Palygalae） sample from Shanxi province by Gas Chromatography-mass spectrometry analysis. Fourier Transform Infrared Spectroscopy results showed that the drying temperature exerted a great influence on types and amount of ingredients of Yuanzhi （Radix Palygalae）. The kinetic study showed that the constant-temperature drying process of Yuanzhi Radix Palygalae） samples could be well de- scribed by the Page Model, especially for the drying process at 50~C, in which R2 and SD values were more than 0.98 and less than 0.04, respectively.The drying constant k of three Yuanzhi （Radix Palygalae） samples from Shanxi, Gansu and Shaanxi provinces in China was corresponding to the Arrhenius equation, and their activation energies were 28.07, 2.5.38 and 21.48 kJ/mol, respectively. CONCLUSION： The drying process of Yuanzhi （Radix Palygalae） was very important for bioactive ingredients improvement in Yuanzhi （Radix Palygalae）. Temperature was a thermodynamic property significantly affecting the process.展开更多
[Objectives]To determine the drying process of different functional rhubarbs.[Methods]The contents of tannins,bianthrone,free anthraquinones and combined anthraquinones in medicinal rhubarb were determined by HPLC.The...[Objectives]To determine the drying process of different functional rhubarbs.[Methods]The contents of tannins,bianthrone,free anthraquinones and combined anthraquinones in medicinal rhubarb were determined by HPLC.The results were analyzed by two-way analysis of variance.[Results]Under different drying conditions,the contents of tannins,bianthrone,free anthraquinones and combined anthraquinones in medicinal rhubarb were significantly different.Taking the tannins content as the index,the optimum drying condition of the rhizome is 1 cm thick,dried at 60℃,the root is cut 1 cm thick,and dried at 30℃;the bianthrone content is used as an indicator,the rhizome is optimally dried.The condition is to cut 1 cm thick,dry at 60℃,the root is cut to 5 cm thick,and dried at 40℃;the free anthraquinones content is used as an index,and the optimum drying condition of the rhizome is 3 cm thick and dried at 50℃.The root is cut to a thickness of 3 cm and dried at 30℃.The combine anthraquinones content is used as an indicator.The optimum drying conditions for the rhizome are 5 cm thick,dried at 40℃,and the root is cut to 5 cm thick and dried at 70℃.[Conclusions]Different functional components of rhubarb have different directional processing methods.The drying process can reduce the drying temperature or increase the thickness of the slice,and the directional processing of the diarrhea-type rhubarb can be processed.The drying process can be carried out by increasing the drying temperature or reducing the thickness of the slice directed processing of heat-clearing and purging-fire rhubarb.展开更多
Carbon aerogels were synthesized via ambient pressure drying process using resorcinolformaldehyde as precursor and P123 to strengthen their skeletons. CO2 activation technology was implemented to improve surface areas...Carbon aerogels were synthesized via ambient pressure drying process using resorcinolformaldehyde as precursor and P123 to strengthen their skeletons. CO2 activation technology was implemented to improve surface areas and adjust pore size distribution. The synthesis process was optimized, and the morphology, structure, adsorption properties and electrochemical behavior of different samples were characterized. The CO2-activated samples achieved a high specific capacitance of 129.2 F/g in 6 M KOH electrolytes at the current density of 1 m A/cm^2 within the voltage range of 0-0.8 V. The optimized activation temperature and duration were determined to be 950 ℃ and 4 h, respectively.展开更多
文摘Conducting complete energy audit (both process and utility) of a sponge iron unit is challenging as there is no laid down procedure to audit the process side. Further, the average heat to power ratio (kWth/kWe) of sponge iron plants ranges from (25:1) to (31:1). This shows that the manufacturing process mostly uses thermal energy and application of electrical energy is insignificant. The main & only source of thermal energy is coal and the entire coal is fed to the rotary kiln. Therefore we find that “Kiln” is the “Black-Box” of this industry and the success of energy efficiency is hidden in the kiln process chemistry. This article tries to establish detailed energy audit methodology of sponge iron manufacturing process or kiln operation with a view to finding out major energy saving potential of the unit. In the research work we find that it is the incomplete reaction of coal that causes the major energy inefficiency in the process. Substantial amount of un-reacted carbon comes out with the char (by-product) which has virtually zero commercial value. The article also puts a question mark on the justification of using high-grade imported coal in such energy inefficient industries.
文摘Most outburst mines in China adopt the measures of pre drainage by drilling along the seam for gas control in the mining area, that is, drilling along the seam from the air roadway of the mining machine to the mining area. The drainage effect of drilling along the seam is directly related to the gas control effect of the mining area. For many years, we have carried out the measures according to the provisions of the detailed rules for the prevention and control of coal and gas outburst. The sealing length of the bedding hole is consistently kept at 8m, and the depth of the sealing section is kept at about 10m, and the extraction concentration and pure amount have been maintained at a low level, resulting in relatively large gas emission during mining. We break the Convention and calculate the sealing depth of the hole according to the pre drainage equivalent width of the coal roadway. At the same time, the extended version of high-pressure grouting is used for two plugs and one injection seal, so that the hole sealing depth of the borehole is within the equivalent width of the roadway pre drainage gas, and the length of the hole sealing section is longer. At the same time, combined with the whole process casing running technology of bedding drilling, the contact area between the screen pipe and the coal wall is likely to be increased, and good results have been achieved in preventing the impact of hole collapse and other phenomena on the drainage effect. The concentration of single hole drainage and the net amount of main pipe drainage have been greatly improved, and the gas content and gas pressure of coal have decreased significantly.
基金supported by the Key-Area Research and Development Program of Guangdong Province(No.2023B0101200006)Guangdong Basic and Applied Basic Research Foundation(No.2024A1515011926)+1 种基金Fund of Guangdong Provincial Key Laboratory of Luminescence from Molecular Aggregates,Guangzhou 510640,China(South China University of Technology)(No.2023B1212060003)State Key Laboratory of Applied Microbiology Southern China(No.SKLAM008-2022)。
文摘The dynamics of the drying process of polymer solutions are important for the development of coatings and films.In the present work,digital holographic microscopy(DHM)was performed to capture the drying dynamics of poly(ethylene oxide)(PEO)droplets using a gold nanoparticle tracer,where the heterogeneous flow field in different regions was illustrated.This demonstrates that the gold nanoparticles at either the center or the edge regions of the droplet exhibit anisotropic kinematic behavior.At early stage,Marangoni backflow causes gold nanoparticles to move towards the edge firstly,and the circles back towards the droplet center after arriving the contact line with a sudden increase in z axis for 10.4μm,indicating the scale of the upward-moving microscopic flow vortices.This phenomenon does not occur in water droplets in the absence of polymers.The gold nanoparticles underwent Brownian-like motion at the center of the PEO droplet or water droplet owing to the low perturbation of the flow field.At the late stage of pinning of the PEO droplets,the motion showed multiple reverses in the direction of the gold nanoparticles,indicating the complexity of the flow field.This study enhances the understanding of the drying dynamics of polymer solution droplets and offers valuable insights into the fabrication of surface materials.
基金funding of the joint Polish-German project SUPILMIX(PR-1173/27)by the German Research Foundation(DFG,Deutsche Forschungsgemeinschaft)+1 种基金funding from the Alexander von Humboldt Foundation.D.L.the German Chemical Industry Fund for the financial support through a Liebig Fellowship.
文摘Supercapacitors are efficient and versatile energy storage devices,offering remarkable power density,fast charge/discharge rates,and exceptional cycle life.As research continues to push the boundaries of their performance,electrode fabrication techniques are critical aspects influencing the overall capabilities of supercapacitors.Herein,we aim to shed light on the advantages offered by dry electrode processing for advanced supercapacitors.Notably,our study explores the performance of these electrodes in three different types of electrolytes:organic,ionic liquids,and quasi-solid states.By examining the impact of dry electrode processing on various electrode and electrolyte systems,we show valuable insights into the versatility and efficacy of this technique.The supercapacitors employing dry electrodes demonstrated significant improvements compared with conventional wet electrodes,with a lifespan extension of+45%in organic,+192%in ionic liquids,and+84%in quasi-solid electrolytes.Moreover,the increased electrode densities achievable through the dry approach directly translate to improved volumetric outputs,enhancing energy storage capacities within compact form factors.Notably,dry electrode-prepared supercapacitors outperformed their wet electrode counterparts,exhibiting a higher energy density of 6.1 Wh cm^(-3)compared with 4.7 Wh cm^(-3)at a high power density of 195Wcm^(-3),marking a substantial 28%energy improvement in the quasi-solid electrolyte.
文摘Biomaterial will shrink during the drying process. The characteristics of shrinkage and rehydration of fresh peas were studied. Drying curves, shrinkage and rehydration curves of peas without seed coats and whole peas were compared. In addition, different volumetric shrinkage coefficients were obtained and discussed. The results show that seed coats resist moisture movement not only from inside to outside but also from outside to inside during different drying conditions. During a seed’s drying process, the drying curve is similar to the shrinkage curve. The higher the heat flux is, the less drying time is needed, and in the meantime, volume would shrink more and more intensively. Dried media will break easily at high heat flux. When we create a drying regime, both drying speed and the quality of dried media should be considered.
基金The National Natural Science Foundation of China (No10471023)
文摘A numerical simulation for a model of wood drying process is considered. The model is given by a couple of nonlinear differential equations. One is a nonlinear parabolic equation and the other one is a nonlinear ordinary equation. A difference scheme is derived by the method of reduction of order. First, a new variable is introduced and the original problem is rewritten into a system of the first-order differential equations. Secondly, a difference scheme is constructed for the later problem. The solvability, stability and convergence of the difference scheme are proved by the energy method. The convergence order of the difference scheme is secondorder both in time and in space. A prior error estimate is put forward. The new variable is put aside to reduce the computational cost. A numerical example testifies the theoretical result.
基金the National Natural Science Foundation of China (Grant No.10702050)the Natural Science Foundation of Tianjin (Grant No.07JCYBJC07500)the Support Plan of Science and Technology of Tianjin (Grant No.07ZCGYSH01700)
文摘A particular porosity method named ＂slot method＂ is implemented in a depth-integrated shallow water flow model （DIVAST） to simulate wetting and drying processes. Discussed is the relationship between the shape factors of the ＂slot＂ and the preset depth used in ＂wetting-drying＂ algorithm. Two typical tests are conducted to examine the performance of the method with the effect of the shape factors of the ＂slot＂ being checked in detail in the first test. Numerical results demonstrate that： 1 ） no additional effort to improve the finite difference scheme is needed to implement ＂slot method＂ in DIVAST, and 2） ＂slot method＂ will simulate wetting and diying processes correctly if the shape factors of the ＂slot＂ being selected properly.
基金“111 Project” Biomedical Textile Materials Science and Technology,China(No.B07024)Natural Science Foundation of Shanghai,China(No.15ZR1401000)the Fundamental Research Funds for the Central Universities,China
文摘A type of antibacterial bacterial cellulose(BC) film was prepared for potential uses as wound dressing.In order to obtain a high antibacterial effect,some forms of BC films,including the wet and dried ones were utilized as the template to in situ synthesize silver nanoparticles(AgNPs).The effects of drying methods including freeze-drying,heat drying and air drying,on the microstructures and physical properties of BC,as well as the silver contents and the antibacterial performances of the BC/AgNPs composites were investigated.It was found that the AgNPs impregnated on the dried BC films were inclined to achieve a faster silver releasing rate than the wet one,which was suitable for acute traumas treatment.
基金the National Key Research and Development Program of China(2017YFB0307900,2019YFC1905903)the National Natural Science Foundation of China(31700507)the Major Project on the Integration of Industry-Education-Research of Fujian Provincial Department of Science and Technology(2018H6003).
文摘Hemicellulose has a wide range of applications,including that as an emulsifier for the food industry and raw material for the synthesis of bioethanol/biochemicals and biodegradable films.Hemicellulose is usually present as a spent liquor,such as the prehydrolysis liquor of the prehydrolysis kraft dissolving pulp production process and the alkali extraction liquor of the cold caustic extraction of pulp fibers.Due to its dilute nature,hemicellulose needs to be dried for practical utilization,and this is challenging.In this study,cellulose and hemicellulose in a bleached bamboo kraft pulp were separated using an alkali extraction process.Hemicellulose obtained from the extraction liquor was dried by an ammonium carbonate-assisted drying process.The effects of drying time and drying temperature were determined.Structure of the hemicellulose obtained by the ammonium carbonate-assisted drying process was similar to that of original hemicellulose,as revealed by detailed Fourier transform infrared and X-ray diffraction analyses.The novel drying method was more energy efficient and required a shorter drying time than the conventional freeze drying method,and the excellent solubility in alkaline solutions favored the chemical modification of hemicellulose.The dried hemicellulose can be used as a renewable raw material for the preparation of hydrogels and other substances such as bioethanol/biochemicals and biodegradable films.
文摘针对传统鱼糕货架期短、运输条件苛刻、食用方法单一等问题,本研究通过配方优化与真空冷冻干燥技术开发新型鱼糕产品,旨在延长其保质期、提升营养均衡性并拓展即食化、多场景应用潜力,同时为水产制品的工业化加工提供工艺参考。以鲢鱼为主要原料,基于层次分析-熵权法构建综合评分模型,选择猪肥肉、鸡肉、玉米淀粉和蛋清添加量进行单因素实验,并在单因素实验基础上通过遗传算法结合Box-Behnken响应面法对鱼糕冻干配方进行优化。通过扫描电子显微镜(scanning electron microscopy,SEM)分析微观结构,测定蛋白质、脂肪、水分、灰分等理化指标,并基于Arrhenius方程预测货架期。确定了鱼糕冻干最优配方为:相对碎鱼肉用量,猪肥肉添加量10%(质量分数),鸡肉添加量20%,玉米淀粉添加量11%,蛋清添加量8%,综合评分达0.87±0.34。微观结构显示孔隙分布均匀,真空冷冻干燥处理前后关键理化指标无显著变化。基于Arrhenius方程的货架期模型预测25℃贮藏期为77 d,较鲜切鱼糕(4~7 d)延长11倍。本研究得到了色泽均匀、口感酥脆、货架期长以及营养均衡的鱼糕冻干制品,为鱼糕制品常温储运与即食化应用提供借鉴。
文摘Introduction Cationic starches are a series of products of which various sorts with different properties and usages can all be produced via cationic reactions by using different types of etherification agents under different conditions. As an additive and strengthening agent,
基金Supported by the National Science and Technology Support Program of the Ministry of Science and Technology of the People's Republic of China (No.2011BAI07B05)Shanxi Science and Technology Tackling Fund (No.20100311090,20130313015-2)Department of Health of Shanxi province Tackling Fund (No.200834)
文摘OBJECTIVE： To study the effects of the drying processing in terms operational parameters on the bio- active constituents of six YuanzhJ （Radix Palygalae） samples across China. METHODS： Six Yuanzhi （Radix Palygalae） samples were investigated using thermogravimetry analysis. The heating courses were set in two ways： the temperature-programmed process from room temperature to 150℃ ,and the constant-temperature course at 50℃, 70℃ and 90℃. RESULTS： The peak temperature of six Yuanzhi （Radix Palygalae） samples ranged from 78℃ to 88℃. The mass loss rate of Yuanzhi （Radix Palygalae） alcohol-soluble extract was significantly increased when heated at 90℃. Four types of bioactive ingredients were detected in volatile oils of Yuanzhi （Radix Palygalae） sample from Shanxi province by Gas Chromatography-mass spectrometry analysis. Fourier Transform Infrared Spectroscopy results showed that the drying temperature exerted a great influence on types and amount of ingredients of Yuanzhi （Radix Palygalae）. The kinetic study showed that the constant-temperature drying process of Yuanzhi Radix Palygalae） samples could be well de- scribed by the Page Model, especially for the drying process at 50~C, in which R2 and SD values were more than 0.98 and less than 0.04, respectively.The drying constant k of three Yuanzhi （Radix Palygalae） samples from Shanxi, Gansu and Shaanxi provinces in China was corresponding to the Arrhenius equation, and their activation energies were 28.07, 2.5.38 and 21.48 kJ/mol, respectively. CONCLUSION： The drying process of Yuanzhi （Radix Palygalae） was very important for bioactive ingredients improvement in Yuanzhi （Radix Palygalae）. Temperature was a thermodynamic property significantly affecting the process.
基金National Natural Science Foundation of China(31570331,31170307)National Key Research and Development Program of China(2017YFC1700702)Project of Beijing University of Chinese Medicine(2019-JYB-XS-087).
文摘[Objectives]To determine the drying process of different functional rhubarbs.[Methods]The contents of tannins,bianthrone,free anthraquinones and combined anthraquinones in medicinal rhubarb were determined by HPLC.The results were analyzed by two-way analysis of variance.[Results]Under different drying conditions,the contents of tannins,bianthrone,free anthraquinones and combined anthraquinones in medicinal rhubarb were significantly different.Taking the tannins content as the index,the optimum drying condition of the rhizome is 1 cm thick,dried at 60℃,the root is cut 1 cm thick,and dried at 30℃;the bianthrone content is used as an indicator,the rhizome is optimally dried.The condition is to cut 1 cm thick,dry at 60℃,the root is cut to 5 cm thick,and dried at 40℃;the free anthraquinones content is used as an index,and the optimum drying condition of the rhizome is 3 cm thick and dried at 50℃.The root is cut to a thickness of 3 cm and dried at 30℃.The combine anthraquinones content is used as an indicator.The optimum drying conditions for the rhizome are 5 cm thick,dried at 40℃,and the root is cut to 5 cm thick and dried at 70℃.[Conclusions]Different functional components of rhubarb have different directional processing methods.The drying process can reduce the drying temperature or increase the thickness of the slice,and the directional processing of the diarrhea-type rhubarb can be processed.The drying process can be carried out by increasing the drying temperature or reducing the thickness of the slice directed processing of heat-clearing and purging-fire rhubarb.
基金Funded by the National High Technology Research and Development Program(863 Program)(No.2013AA050905),China Academy of Engineering Physics,Mianyang,China
文摘Carbon aerogels were synthesized via ambient pressure drying process using resorcinolformaldehyde as precursor and P123 to strengthen their skeletons. CO2 activation technology was implemented to improve surface areas and adjust pore size distribution. The synthesis process was optimized, and the morphology, structure, adsorption properties and electrochemical behavior of different samples were characterized. The CO2-activated samples achieved a high specific capacitance of 129.2 F/g in 6 M KOH electrolytes at the current density of 1 m A/cm^2 within the voltage range of 0-0.8 V. The optimized activation temperature and duration were determined to be 950 ℃ and 4 h, respectively.
