The benefits of using cryogenic liquid nitrogen shock to enhance coal permeability have been confirmed from experimental perspectives.In this paper,we develop a fully coupled thermo-elastic model in combination with t...The benefits of using cryogenic liquid nitrogen shock to enhance coal permeability have been confirmed from experimental perspectives.In this paper,we develop a fully coupled thermo-elastic model in combination with the strain-based isotropic damage theory to uncover the cooling-dominated cracking behaviors through three typical cases,i.e.coal reservoirs containing a wellbore,a primary fracture,and a natural fracture network,respectively.The progressive cracking processes,from thermal fracture initiation,propagation or cessation,deflection,bifurcation to multi-fracture interactions,can be well captured by the numerical model.It is observed that two hierarchical levels of thermal fractures are formed,in which the number of shorter thermal fractures consistently exceeds that of the longer ones.The effects of coal properties related to thermal stress levels and thermal diffusivity on the fracture morphology are quantified by the fracture fractal dimension and the statistical fracture number.The induced fracture morphology is most sensitive to changes in the elastic modulus and thermal expansion coefficient,both of which dominate the complexity of the fracture networks.Coal reservoir candidates with preferred thermal-mechanical properties are also recommended for improving the stimulation effect.Further findings are that there exists a critical injection temperature and a critical in-situ stress difference,above which no thermal fractures would be formed.Preexisting natural fractures with higher density and preferred orientations are also essential for the formation of complex fracture networks.The obtained results can provide some theoretical support for cryogenic fracturing design in coal reservoirs.展开更多
Selective laser melting(SLM)technology based on atomized powder was used to fabricate Al-8.5Fe-1.3V-1.7Si(wt%)alloy parts.The microstructure and crack characterization of SLM samples fabricated at various conditions w...Selective laser melting(SLM)technology based on atomized powder was used to fabricate Al-8.5Fe-1.3V-1.7Si(wt%)alloy parts.The microstructure and crack characterization of SLM samples fabricated at various conditions were presented.Results show that the cracks appear periodically along the building direction,initiate preferably at the outer edges of the as-built samples and propagated along the remelting border zone(RBZ)into deposited layers.Solid-phase cracking is proposed according to the fracture morphology.The thermal-induced residual stress during SLM combined with the precipitation of relatively large-sized Al_mFe phase in the RBZ results in the formation of cracks.Enhancing scanning speed and hatch distance enable to reduce the cracking sensitivity.The crack-free Al-8.5Fe-1.3V-1.7Si parts can be fabricated at optimized parameters of laser power of 320 W,scanning speed of 1000 mm·s^(-1)and hatch distance of0.10 mm along with proper laser pre-heating procedure.The samples built horizontally show good ultimate tensile properties of 454 MPa in average with the elongation of7.2%.展开更多
The effects of quality and content of fly ash on the early-age cracking behavior of high-flowing concrete （HFC） were investigated. The early-age cracking behavior of the HFC was analyzed by combining the tests of ev...The effects of quality and content of fly ash on the early-age cracking behavior of high-flowing concrete （HFC） were investigated. The early-age cracking behavior of the HFC was analyzed by combining the tests of evaporation capacity and electrical resistivity of the HFC. In these tests, a modified flat-type specimen was adopted. The results show that the HFC will have a lower evaporation capacity when it is mixed with fine fly ash, while it will have a higher evaporation capacity when grade II! fly ash is used as mineral admixture. And the electrical resistivity rate of HFC reduces with the increase of the content of fly ash. A nonlinear relationship exists between the cracking time of HFC and the minimum electrical resistivity. The early-age cracking behavior of HFC with fly ash can be enhanced by appropriately increasing the fine particle content and MgO, K2O, and SO3 contents of fly ash. The optimal content of fly ash, which makes a satisfied early-age cracking behavior of HFC, is obtained. And when the content of fly ash exceeds a critical value, the early-age cracking behavior of HFC will rapidly decrease.展开更多
Tests of the candidate plasma facing materials（PFMs） used in experimental fusion devices are essential due to the direct influence of in-situ plasma loading.A type of ultrafine grained（UFG） tungsten sintered by re...Tests of the candidate plasma facing materials（PFMs） used in experimental fusion devices are essential due to the direct influence of in-situ plasma loading.A type of ultrafine grained（UFG） tungsten sintered by resistance sintering under ultra-high pressure（RSUHP） method has been exposed in the edge plasma of the HT-7 tokamak to investigate its performance under plasma loading.Under cychc edge plasma loading,the UFG tungsten develops both macro and micro cracks.The macro cracks are attributed to the low temperature brittleness of the tungsten material itself,while the micro cracks are generated from local intense power flux deposition.展开更多
X90 pipeline steel is a new generation of pipeline steel developed after X80 and X100 pipeline steels,and it is now a new research hotspot at home.In order to thoroughly study the effect of applied potential on the so...X90 pipeline steel is a new generation of pipeline steel developed after X80 and X100 pipeline steels,and it is now a new research hotspot at home.In order to thoroughly study the effect of applied potential on the soil stress corrosion cracking(SCC)behavior of X90 pipeline steel,we investigated the SCC behaviors of base metal and weld joint samples in the straight-weld pipe of X90 pipeline steel at different applied potentials in near-neutral solution using electrochemical measurements methods and slow strain rate testing(SSRT).Besides,the fracture surfaces were observed through scanning electron microscope(SEM)and the mechanisms of the corrosion cracking behaviors were analyzed.And the following research results were obtained.First,the polarization curves of the base metal and weld joint samples in the NS4 solution present the typical characteristics of anodic dissolution but no activation–passivation phenomenon happens.Second,in the NS4 solution,the base metal and weld joint samples present SCC sensitivity.The SCC sensitivity indicator which is expressed by yield loss percentage elongation and yield loss percentage elongation area decreases firstly and then increases with the negative increase of the applied potential,and the SCC sensitivity of weld joint is higher than that of base metal.Third,there are three mechanisms on the SCC behaviors of base metal and weld joint samples,i.e.,anodic dissolution mechanism when the applied potential is open circuit potential(EOCP),anodic dissolution and hydrogen embrittlement mechanism when the applied potential is−850 mV,and hydrogen embrittlement mechanism when the applied potential is−1000 mV and−1200 mV.It is concluded that the research results can provide a technical support and theoretical basis for the large-scale application of X90 pipeline steel.展开更多
In the present work,uniaxial compressive tests were carried out on limestone-like samples containing two parallel open fissures or cement-infilled fissures with different geometries.Mechanical property and crack behav...In the present work,uniaxial compressive tests were carried out on limestone-like samples containing two parallel open fissures or cement-infilled fissures with different geometries.Mechanical property and crack behavior of limestone-like samples with two parallel open fissures or cement-infilled fissures were affected by bridge inclination angle and fissure inclination angle.Four types of coalescence of rock bridge for samples containing open fissures or cement-infilled fissures were summarized and classified.The closure of tensile crack was observed in the samples with small fissure inclination angle.This is a new phenomenon which is not mentioned in previous studies.Test results show that the peak strength,crack initiation stress,and coalescence type are different between open fissures and cement infilled fissures.The reason for this phenomenon is that grouting of cement can transfer stress and reduce stress concentration at the flaw tip and rock bridge area.展开更多
Steps are distinctive features for estimating the movement of the upper and lower block of faults.However,studies about the influence of steps as a special type of discontinuity on cracking behaviors and strength of r...Steps are distinctive features for estimating the movement of the upper and lower block of faults.However,studies about the influence of steps as a special type of discontinuity on cracking behaviors and strength of rock masses are limited.In this research,rock-like samples with steps and preexisting flaws were fabricated.Step height h and the inclination angle of gentle slope of the stepαwere set to different values.Direct shear tests were conducted on these samples under different normal stresses.The experimental results reveal that the inclination angle of the gentle slope of the stepα,step height h,and normal stress have an influence on the strength,crack initiation,and crack propagation of the samples.The experimental results show that crack behaviors and shear strength were affected by step inclination anglesαand step height h.As the normal stress increases,the improvement of the strength of samples with a large step height is larger than that of samples with a small step height,the improvement of the strength of samples withαof 10°is larger than that of samples withαof 0°and-10°.The discrete element method was used to simulate the shear test.Numerical results show five different types of displacement vectors,which can be used to determine whether the cracks are tensile cracks or shear cracks.The above conclusions can provide help for estimating mechanical properties and failure modes of rock masses with steps of different geometries.展开更多
In recent years, many useful experimental results on the cracking behaviors of fractured rocks have been obtainedvia uniaxial, biaxial, triaxial, and Split Hopkinson Pressure Bar (SHPB) tests. In this paper, the influ...In recent years, many useful experimental results on the cracking behaviors of fractured rocks have been obtainedvia uniaxial, biaxial, triaxial, and Split Hopkinson Pressure Bar (SHPB) tests. In this paper, the influence of theinclination angle of flaws, number of flaws, and patterns of cracks on the mechanical properties during the failureprocess under static loading and dynamic loading conditions is introduced and reviewed. The results show thatthe presence of cracks can decrease the strengths of precracked specimens, and the inclination angles, numbers,and crack patterns of pre-existing flaws can change the mechanical properties and cracking behaviors of precracked specimens. Under static loading, the closer the inclination angle is to 90, the greater the strength, theelastic modulus, and the peak strain of the precracked specimen. However, under dynamic loading, the influenceof the inclination angle varies, and the strength can increase or decrease, possibly in a V-shaped manner. Thischange can be determined by multiple factors, such as the loading path, the materials of the precracked specimen,and the number of pre-existing cracks. Under dynamic loading, the precracked specimen usually exhibits an Xshaped conjugated failure. Additionally, some problems in the study of the cracking behaviors of fractured rocksand related future research are described and presented, and corresponding suggestions and solutions are given.In particular, excavation in deep rock engineering, support of the rock surrounding the tunnel, and mining engineering have important scientific and engineering significance.展开更多
Cracking affected by wetting-drying cycles is a major cause of shallow failure of soft rock slopes.Knowledge of rock tensile properties and cracking behaviors helps better assess the stability of soft rock slopes.This...Cracking affected by wetting-drying cycles is a major cause of shallow failure of soft rock slopes.Knowledge of rock tensile properties and cracking behaviors helps better assess the stability of soft rock slopes.This study aims to examine the cracking behaviors and tensile strength of silty mudstone under wetting-drying cycles.The wetting-drying cycle and Brazilian splitting tests were performed on silty mudstone considering various cycle number and amplitude.The cracking behaviors of wetting-drying cycles were analyzed by digital image correlation,three-dimensional(3D)scanning technology,and scanning electron microscopy.The results reveal a spiral-like pattern of crack ratio escalation in silty mudstone,with a higher crack ratio observed during drying than wetting.Tensile strength and fracture energy correlate negatively with cycle number or amplitude,with cycle number exerting a more pronounced effect.The variance of the maximum principal strain reflects stages of initial deformation,linear deformation,strain localization,and stable deformation.The formation of strain localization zones reveals the physical process of crack propagation.Crack tip opening displacement progresses through stages of slow growth,exponential growth,and linear growth,delineating the process from crack initiation to stable extension.Failure modes of silty mudstone primarily involve tensile and tensile-shear failure,influenced by the geometric parameters of cracks induced by wetting-drying cycles.Fracture surface roughness and fractal dimension increase with cycle number due to mineral dissolution,physical erosion,and nondirectional crack propagation.Hydration-swelling and dehydration-shrinkage of clay minerals,along with absorption-drying cracking,initiate and merge cracks,leading to degradation of the rock mechanical properties.The findings could provide insights for mitigating shallow cracking of soft rock slopes under wetting-drying cycles.展开更多
Shale reservoirs have abundant bedding structures,which deeply alter the mechanical properties of rocks,and thus affect the reservoir stimulation performance.Previous research mostly focuses on the effects of parallel...Shale reservoirs have abundant bedding structures,which deeply alter the mechanical properties of rocks,and thus affect the reservoir stimulation performance.Previous research mostly focuses on the effects of parallel bedding on fracture propagation,while the mechanical properties and mechanisms of fracture propagation remain unclear for rocks with complex wavy bedding(e.g.China’s continentalorigin Gulong shale).Herein,a mixed phase-field fracture model of the wavy-bedding shale was applied,based on the local tension-compression decomposition phase field method(PFM)and geometric structure generation algorithm for the bedding with controllable morphological features.The parametric analysis of fracture propagation behaviors in the case of abundant complex bedding structures showed that with wavy bedding,the vertical fracture propagation rate is far higher than the horizontal propagation rate.Moreover,the development of branch fractures is suppressed during the fracturing process of the wavy-bedding sample,and the stimulated volume is limited,which is different from the characteristic of parallel bedding that promotes horizontal fracture initiation and propagation.The results showed that larger amplitudes,higher frequencies,higher inclination angles,and larger strengths of wavy bedding all promote the formation of vertical penetrating fractures and suppress the growth of branch fractures.Under such circumstances,it is hard to create a well-connected fracture network after fracturing.This research may provide a theoretical basis for understanding fracture behaviors in rocks with such complex wavy bedding.展开更多
The crack initiation and early propagation are of great significance to the overall fatigue life of material.In order to investigate the anisotropic fracture behavior of laser metal deposited Ti-6Al-4V alloy(LMD Ti64)...The crack initiation and early propagation are of great significance to the overall fatigue life of material.In order to investigate the anisotropic fracture behavior of laser metal deposited Ti-6Al-4V alloy(LMD Ti64)during the early stage,the fourpoint bending fatigue test was carried out on specimens of three different directions,as well as the forged specimens.The results indicate the anisotropic crack initiation and early propagation of LMD Ti64.The direction perpendicular to the deposition direction exhibits a better fatigue resistance than the other two.The crack initiation position and propagation path are dominated by the microstructure in the vicinity of U-notch.LMD Ti64 has a typical small crack effect,and the early crack propagation velocities in three directions are similar.Affected by the slip system of LMD Ti64,secondary cracks frequently occur,which are often found to have an angle of 60°to the main crack.The electron backscatter diffraction analysis indicates that LMD Ti64 has preferred orientations,i.e.,strong 0001//Z texture and 001//Z texture.Their crystallographic orientation will change as the direction of columnarβgrains turns over,resulting in the fatigue anisotropy of LMD Ti64 in crack initiation and early crack propagation process.展开更多
Edge cracking is one of the most serious problems in the rolling process of magnesium alloy sheets,which limits its application.In this work,the edge cracking behavior of different initial AZ31 alloy sheets,including ...Edge cracking is one of the most serious problems in the rolling process of magnesium alloy sheets,which limits its application.In this work,the edge cracking behavior of different initial AZ31 alloy sheets,including as-cast(AC),as-rolled(AR)and as-extruded(AE),was systematically investigated and compared under the online heating rolling(O-LHR)process with a single-pass reduction of 50% at 250℃.The results show that both AC and AR sheets exhibit severe edge cracking behavior after the O-LHR.Among them,the AR sheet exhibits the severest edge cracking behavior on the rolling plane(RD-TD)and longitudinal section(RD-ND),which is attributed to the strong basal texture and extremely uneven microstructure with shear bands.While no visible edge crack appears in the AE rolled sheet,which is mainly related to the tilted texture and the more dynamic recrystallization during rolling process.Moreover,it is also found that the micro-cracks of the AC rolled sheet are mainly generated in the local fine-grained area and the twins where recrystallization occurs.In the AR rolled sheet,micro-cracks mainly develop inside the shear bands.Meanwhile,the micro-crack initiation mechanism of AC and AR rolled sheets was also discussed.展开更多
The fracture mechanisms of coarse-grained heat-affected zone(CGHAZ)for Mg and Mg–Ca deoxidized high-strength low-alloy(HSLA)steels after high heat input welding(HHIW)were investigated based on the microstructures,cra...The fracture mechanisms of coarse-grained heat-affected zone(CGHAZ)for Mg and Mg–Ca deoxidized high-strength low-alloy(HSLA)steels after high heat input welding(HHIW)were investigated based on the microstructures,crack behaviors and mechanical properties.Compared to Mg–Ca steel,the proportion of intergranular acicular ferrites(IAFs)and polygonal ferrites(PFs)in Mg steel increases from 59.97%to 90.16%.The high-angle grain boundaries(HAGBs)and geometrically necessary dislocations density increase from 55.5%and 4.30×10^(14) m^(-2)to 70.4%and 5.48×10^(14) m^(–2),respectively,while effective grain size decreases from 9.46 to 8.12μm.The area fraction of radial zone in Mg steel decreases from 80.8%to 37.7%and cleavage plane is smaller with more curved and finer tearing ridges.The inclusions distributed at the center of cleavage planes and along river lines can serve as crack initiation sites.The zigzag pattern of primary crack propagation path has width of 476μm and the length of secondary cracks remains below 10μm.These cracks are deflected or arrested by IAFs,PFs and HAGBs,and tend to propagate along{110}plane family.These factors contribute to superior overall mechanical properties of Mg steel,especially increasing low-temperature impact toughness from 23 to 175 J.展开更多
Four types of granite specimens were prepared and treated by chemical corrosion for 5 and 30 days,which were then used to carry out triaxial compression tests under different confining pressuresσ_(3).Type A is the in...Four types of granite specimens were prepared and treated by chemical corrosion for 5 and 30 days,which were then used to carry out triaxial compression tests under different confining pressuresσ_(3).Type A is the intact sample with no preexisting flaws.Types B and C are the samples containing two relatively low-dip flaws and two relatively high-dip flaws,respectively.Type D is the sample including both relatively low-dip and relatively high-dip flaws.The influences of pH value of chemical solutions,flaw distribution,corrosion time andσ_(3) on triaxial stress-strain curves and ultimate failure modes are analyzed and discussed.The results show that the pH value of the chemical solution,corrosion time and the arrangement of preexisting flaws play crucial roles in the cracking behaviors of granite specimens.Type A specimens have the largest peak axial deviatoric stress,followed by Type C,Type D,and Type B specimens,respectively.It is because the decrease in the inclination of preexisting flaws induces the weakening effect due to the decrease in the shadow area along the compaction direction.Under aσ_(3) of 5 MPa,the peak axial deviatoric stress drops by approximately 40.89%,29.08%,4.08%,and 23.53%for pH=2,4,7,and 12,respectively.For intact granite(Type A)specimens,the ultimate failure mode displays a typical shear mode.The connection of two secondary cracks initiated at the tips of preexisting cracks is always the ultimate failure and crack coalescence mode for Type B specimens.The ultimate failure and crack coalescence mode of Types C and D specimens are significantly affected by pH value of the chemical solution,corrosion time andσ_(3),which is different from those of Types A and B specimens due to the differences in flow distributions.展开更多
The generation of defects,such as cracks and pores,presents significant challenges for high-strength met-als and alloys fabricated by the quick-emerging additive manufacturing technology,and subsequent post-processing...The generation of defects,such as cracks and pores,presents significant challenges for high-strength met-als and alloys fabricated by the quick-emerging additive manufacturing technology,and subsequent post-processing treatments are often necessary before their practical applications.In this work,a novel heat treatment approach,involving a pre-softening treatment before hot isostatic pressing(HIP),is developed to facilitate the crack-healing in René142 superalloy produced through laser powder bed fusion.Results demonstrate that René142 alloy exhibits a propensity for severe cracking across a wide range of printing parameters,primarily in the form of solidification cracks and liquation cracks.These cracks are formed mainly due to a wide solidification range,the presence of a liquid film,and the concentration of resid-ual stress.The pre-softening solution heat treatment significantly reduces dislocation density and resid-ual stress levels,and the subsequent HIP together leads to a defect-free,dense structure for René142 superalloy.Consequently,the René142 alloy processed by the pre-softening HIP treatment achieves an excellent combination of yield strength(850 MPa),ultimate tensile strength(1227 MPa),and elongation(13.7%),with pseudo-equiaxed grains(120-150μm)and squareγ'precipitates(approximately 540 nm).These findings provide valuable insights for exploring crack elimination methods in other nickel-based superalloys fabricated through additive manufacturing.展开更多
The understanding of crack propagation characteristics and law of rocks during the loading process is of great significance for the exploitation and support of rock engineering.In this study,the crack propagation beha...The understanding of crack propagation characteristics and law of rocks during the loading process is of great significance for the exploitation and support of rock engineering.In this study,the crack propagation behavior of rocks in triaxial compression tests was investigated in detail.The main conclusions were as follows:1)According to the evolution characteristics of crack axial strain,the differential stress?strain curve of rocks under triaxial compressive condition can be divided into three phases which are linear elastic phase,crack propagation phase,post peak phase,respectively;2)The proposed models are applied to comparison with the test data of rocks under triaxial compressive condition and different temperatures.The theoretical data calculated by the models are in good agreement with the laboratory data,indicating that the proposed model can be applied to describing the crack propagation behavior and the nonlinear properties of rocks under triaxial compressive condition;3)The inelastic compliance and crack initiation strain in the proposed model have a decrease trend with the increase of confining pressure and temperature.Peak crack axial strain increases nonlinearly with the inelastic compliance and the increase rate increases gradually.Crack initiation strain has a linear relation with peak crack axial strain.展开更多
In order to investigate the real-time cracking behavior of each component of a composite with strong interfacial bonding among lamellae, Ti-18 Nb(at.%) composite was prepared by spark plasma sintering(SPS), followed b...In order to investigate the real-time cracking behavior of each component of a composite with strong interfacial bonding among lamellae, Ti-18 Nb(at.%) composite was prepared by spark plasma sintering(SPS), followed by hot-rolling, annealing, and quenching. The microstructure and mechanical properties were characterized by scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), micro-region X-ray diffractometry(MRXRD), nanoindentation, and in-situ scanning electron microscopy tensile testing. The results show that the Ti-18 Nb consists of Ti-enriched, diffusion and Nb-enriched zones, and the sharp Nb gradient across different zones leads to inhomogeneous distribution of phase and mechanical properties. A remarkable finding is that the diffusion zones not only enable the cooperative deformation between the brittle Ti-enriched zones and the ductile Nb-enriched zones but also act as the crack-arresters to prevent the local cracks in the Ti-enriched zones from further propagating across the composite.展开更多
The thermal fatigue behavior of a single crystal superalloy SRR99 was investigated. Specimens with V-type notch were tested at the peak temperatures of 900, 1000, and 1100℃. The crack growth curves as a function of t...The thermal fatigue behavior of a single crystal superalloy SRR99 was investigated. Specimens with V-type notch were tested at the peak temperatures of 900, 1000, and 1100℃. The crack growth curves as a function of the number of cycles were plotted. With the increase of peak temperature, the crack initiation life was shortened dramatically. Through optical microscopy （OM） and scanning electron microscopy （SEM） observation, it was found that multiple small cracks nucleated at the notch tip region but only one or two of them continued to develop in the following thermal cycles. The primary cracks generally propagated along a preferential direction. Microstructure changes after thermal fatigue were also discussed on the basis of SEM observation.展开更多
The growth behaviors of short through cracks (0.2 < △a < 2.2mm) and long cracks are compared using CT type specimens in aluminum-lithium alloy 8090 T651. It is found that the short cracks grow much more than lo...The growth behaviors of short through cracks (0.2 < △a < 2.2mm) and long cracks are compared using CT type specimens in aluminum-lithium alloy 8090 T651. It is found that the short cracks grow much more than long ones and are observed to grow at the stress intensity ranges far below the long crack threshold. The distinction of growth bahavior between short and long cracks is attributed to the difference of their crack closure effect. The growth behavior of short cracks can be rationalized with that of long ones in terms of effective stress intensity ranges. The upper demarcation value of short through cracks for aluminum-lithium alloy 8090 is presented.展开更多
The fatigue crack propagation behavior of TiNi50.6 shape memory alloy was studied. The ex- periment results showed that the crack propagation properties of this alloy display difference and similarity in comparison wi...The fatigue crack propagation behavior of TiNi50.6 shape memory alloy was studied. The ex- periment results showed that the crack propagation properties of this alloy display difference and similarity in comparison with common metallic materials. Because of the stress concentra- tion there was stress induced martensite transformation (SIMT) near the crack tip though the nominal stress was lower than the threshold stress of SIMT. The position and the amount of SIMT was in situ observed by a quester remote measurement system (QRMS). The observation results showed that the position of SIMT was beside the crack tip and was not in the plastic zone of common metallic materials (in front of the crack tip). The SIMT zone at an angle of about 45°to the direction of the crack propagation, like a butterfly,appeared in the loading process, disappeared in the unloading process and grew larger with the increase of K. The crack propagation rate(da/dN) followed the linear law in lg-lg plot. Observation of the crack surface showed fatigue striation clearly. The relationship between the site and the size of the plastic zone and the SIMT zone is discussed and a model is given to explain both the similarity and the difference of the crack propagation property of TiNi50.6 to common metal materials.展开更多
基金funding support from the Natural Science Foundation of Sichuan,China(Grant No.2022NSFSC1227)the National Natural Science Foundation of China(Grant Nos.U1762216 and 51574270).
文摘The benefits of using cryogenic liquid nitrogen shock to enhance coal permeability have been confirmed from experimental perspectives.In this paper,we develop a fully coupled thermo-elastic model in combination with the strain-based isotropic damage theory to uncover the cooling-dominated cracking behaviors through three typical cases,i.e.coal reservoirs containing a wellbore,a primary fracture,and a natural fracture network,respectively.The progressive cracking processes,from thermal fracture initiation,propagation or cessation,deflection,bifurcation to multi-fracture interactions,can be well captured by the numerical model.It is observed that two hierarchical levels of thermal fractures are formed,in which the number of shorter thermal fractures consistently exceeds that of the longer ones.The effects of coal properties related to thermal stress levels and thermal diffusivity on the fracture morphology are quantified by the fracture fractal dimension and the statistical fracture number.The induced fracture morphology is most sensitive to changes in the elastic modulus and thermal expansion coefficient,both of which dominate the complexity of the fracture networks.Coal reservoir candidates with preferred thermal-mechanical properties are also recommended for improving the stimulation effect.Further findings are that there exists a critical injection temperature and a critical in-situ stress difference,above which no thermal fractures would be formed.Preexisting natural fractures with higher density and preferred orientations are also essential for the formation of complex fracture networks.The obtained results can provide some theoretical support for cryogenic fracturing design in coal reservoirs.
基金financially supported by the National High-Tech Program of China(No.21100002013101006)。
文摘Selective laser melting(SLM)technology based on atomized powder was used to fabricate Al-8.5Fe-1.3V-1.7Si(wt%)alloy parts.The microstructure and crack characterization of SLM samples fabricated at various conditions were presented.Results show that the cracks appear periodically along the building direction,initiate preferably at the outer edges of the as-built samples and propagated along the remelting border zone(RBZ)into deposited layers.Solid-phase cracking is proposed according to the fracture morphology.The thermal-induced residual stress during SLM combined with the precipitation of relatively large-sized Al_mFe phase in the RBZ results in the formation of cracks.Enhancing scanning speed and hatch distance enable to reduce the cracking sensitivity.The crack-free Al-8.5Fe-1.3V-1.7Si parts can be fabricated at optimized parameters of laser power of 320 W,scanning speed of 1000 mm·s^(-1)and hatch distance of0.10 mm along with proper laser pre-heating procedure.The samples built horizontally show good ultimate tensile properties of 454 MPa in average with the elongation of7.2%.
基金Project(50478003)supported by the National Natural Science Foundation of ChinaProject(2002F007)supported by the Natural Science Foundation of Fujian Province,China
文摘The effects of quality and content of fly ash on the early-age cracking behavior of high-flowing concrete （HFC） were investigated. The early-age cracking behavior of the HFC was analyzed by combining the tests of evaporation capacity and electrical resistivity of the HFC. In these tests, a modified flat-type specimen was adopted. The results show that the HFC will have a lower evaporation capacity when it is mixed with fine fly ash, while it will have a higher evaporation capacity when grade II! fly ash is used as mineral admixture. And the electrical resistivity rate of HFC reduces with the increase of the content of fly ash. A nonlinear relationship exists between the cracking time of HFC and the minimum electrical resistivity. The early-age cracking behavior of HFC with fly ash can be enhanced by appropriately increasing the fine particle content and MgO, K2O, and SO3 contents of fly ash. The optimal content of fly ash, which makes a satisfied early-age cracking behavior of HFC, is obtained. And when the content of fly ash exceeds a critical value, the early-age cracking behavior of HFC will rapidly decrease.
基金supported by the Key Project of Chinese Academy of Sciences(No.KJCX2-YW-N35)National Natural Science Foundation of China(No.11175205)
文摘Tests of the candidate plasma facing materials（PFMs） used in experimental fusion devices are essential due to the direct influence of in-situ plasma loading.A type of ultrafine grained（UFG） tungsten sintered by resistance sintering under ultra-high pressure（RSUHP） method has been exposed in the edge plasma of the HT-7 tokamak to investigate its performance under plasma loading.Under cychc edge plasma loading,the UFG tungsten develops both macro and micro cracks.The macro cracks are attributed to the low temperature brittleness of the tungsten material itself,while the micro cracks are generated from local intense power flux deposition.
基金supported by the National Key R&D Program of China with Project No.2016YFC0801200.
文摘X90 pipeline steel is a new generation of pipeline steel developed after X80 and X100 pipeline steels,and it is now a new research hotspot at home.In order to thoroughly study the effect of applied potential on the soil stress corrosion cracking(SCC)behavior of X90 pipeline steel,we investigated the SCC behaviors of base metal and weld joint samples in the straight-weld pipe of X90 pipeline steel at different applied potentials in near-neutral solution using electrochemical measurements methods and slow strain rate testing(SSRT).Besides,the fracture surfaces were observed through scanning electron microscope(SEM)and the mechanisms of the corrosion cracking behaviors were analyzed.And the following research results were obtained.First,the polarization curves of the base metal and weld joint samples in the NS4 solution present the typical characteristics of anodic dissolution but no activation–passivation phenomenon happens.Second,in the NS4 solution,the base metal and weld joint samples present SCC sensitivity.The SCC sensitivity indicator which is expressed by yield loss percentage elongation and yield loss percentage elongation area decreases firstly and then increases with the negative increase of the applied potential,and the SCC sensitivity of weld joint is higher than that of base metal.Third,there are three mechanisms on the SCC behaviors of base metal and weld joint samples,i.e.,anodic dissolution mechanism when the applied potential is open circuit potential(EOCP),anodic dissolution and hydrogen embrittlement mechanism when the applied potential is−850 mV,and hydrogen embrittlement mechanism when the applied potential is−1000 mV and−1200 mV.It is concluded that the research results can provide a technical support and theoretical basis for the large-scale application of X90 pipeline steel.
基金Projects(42007256, 41672258) supported by the National Natural Science Foundation of ChinaProject(B210201002)supported by the Fundamental Research Funds for the Central Universities,China。
文摘In the present work,uniaxial compressive tests were carried out on limestone-like samples containing two parallel open fissures or cement-infilled fissures with different geometries.Mechanical property and crack behavior of limestone-like samples with two parallel open fissures or cement-infilled fissures were affected by bridge inclination angle and fissure inclination angle.Four types of coalescence of rock bridge for samples containing open fissures or cement-infilled fissures were summarized and classified.The closure of tensile crack was observed in the samples with small fissure inclination angle.This is a new phenomenon which is not mentioned in previous studies.Test results show that the peak strength,crack initiation stress,and coalescence type are different between open fissures and cement infilled fissures.The reason for this phenomenon is that grouting of cement can transfer stress and reduce stress concentration at the flaw tip and rock bridge area.
基金National Natural Science Foundation of China(No.42007256 and 41672258)the Fundamental Research Funds for the Central Universities(B210201002)。
文摘Steps are distinctive features for estimating the movement of the upper and lower block of faults.However,studies about the influence of steps as a special type of discontinuity on cracking behaviors and strength of rock masses are limited.In this research,rock-like samples with steps and preexisting flaws were fabricated.Step height h and the inclination angle of gentle slope of the stepαwere set to different values.Direct shear tests were conducted on these samples under different normal stresses.The experimental results reveal that the inclination angle of the gentle slope of the stepα,step height h,and normal stress have an influence on the strength,crack initiation,and crack propagation of the samples.The experimental results show that crack behaviors and shear strength were affected by step inclination anglesαand step height h.As the normal stress increases,the improvement of the strength of samples with a large step height is larger than that of samples with a small step height,the improvement of the strength of samples withαof 10°is larger than that of samples withαof 0°and-10°.The discrete element method was used to simulate the shear test.Numerical results show five different types of displacement vectors,which can be used to determine whether the cracks are tensile cracks or shear cracks.The above conclusions can provide help for estimating mechanical properties and failure modes of rock masses with steps of different geometries.
文摘In recent years, many useful experimental results on the cracking behaviors of fractured rocks have been obtainedvia uniaxial, biaxial, triaxial, and Split Hopkinson Pressure Bar (SHPB) tests. In this paper, the influence of theinclination angle of flaws, number of flaws, and patterns of cracks on the mechanical properties during the failureprocess under static loading and dynamic loading conditions is introduced and reviewed. The results show thatthe presence of cracks can decrease the strengths of precracked specimens, and the inclination angles, numbers,and crack patterns of pre-existing flaws can change the mechanical properties and cracking behaviors of precracked specimens. Under static loading, the closer the inclination angle is to 90, the greater the strength, theelastic modulus, and the peak strain of the precracked specimen. However, under dynamic loading, the influenceof the inclination angle varies, and the strength can increase or decrease, possibly in a V-shaped manner. Thischange can be determined by multiple factors, such as the loading path, the materials of the precracked specimen,and the number of pre-existing cracks. Under dynamic loading, the precracked specimen usually exhibits an Xshaped conjugated failure. Additionally, some problems in the study of the cracking behaviors of fractured rocksand related future research are described and presented, and corresponding suggestions and solutions are given.In particular, excavation in deep rock engineering, support of the rock surrounding the tunnel, and mining engineering have important scientific and engineering significance.
基金the financial support by the National Natural Science Foundation of China(Grant No.52108397)“Xiaohe”Science and Technology Talent Special Project(Grant No.2024 TJ-X06)Water Resources Science and Technology Project of Hunan Province(Grant No.XSKJ2023059-41).
文摘Cracking affected by wetting-drying cycles is a major cause of shallow failure of soft rock slopes.Knowledge of rock tensile properties and cracking behaviors helps better assess the stability of soft rock slopes.This study aims to examine the cracking behaviors and tensile strength of silty mudstone under wetting-drying cycles.The wetting-drying cycle and Brazilian splitting tests were performed on silty mudstone considering various cycle number and amplitude.The cracking behaviors of wetting-drying cycles were analyzed by digital image correlation,three-dimensional(3D)scanning technology,and scanning electron microscopy.The results reveal a spiral-like pattern of crack ratio escalation in silty mudstone,with a higher crack ratio observed during drying than wetting.Tensile strength and fracture energy correlate negatively with cycle number or amplitude,with cycle number exerting a more pronounced effect.The variance of the maximum principal strain reflects stages of initial deformation,linear deformation,strain localization,and stable deformation.The formation of strain localization zones reveals the physical process of crack propagation.Crack tip opening displacement progresses through stages of slow growth,exponential growth,and linear growth,delineating the process from crack initiation to stable extension.Failure modes of silty mudstone primarily involve tensile and tensile-shear failure,influenced by the geometric parameters of cracks induced by wetting-drying cycles.Fracture surface roughness and fractal dimension increase with cycle number due to mineral dissolution,physical erosion,and nondirectional crack propagation.Hydration-swelling and dehydration-shrinkage of clay minerals,along with absorption-drying cracking,initiate and merge cracks,leading to degradation of the rock mechanical properties.The findings could provide insights for mitigating shallow cracking of soft rock slopes under wetting-drying cycles.
基金supported by the Technology Project of CNPC(Grant No.2023ZZ08)the National Natural Science Foundation of China(Grant No.52274058)the USTC Research Funds of the Double First-Class Initiative(Grant No.YD2090002025).
文摘Shale reservoirs have abundant bedding structures,which deeply alter the mechanical properties of rocks,and thus affect the reservoir stimulation performance.Previous research mostly focuses on the effects of parallel bedding on fracture propagation,while the mechanical properties and mechanisms of fracture propagation remain unclear for rocks with complex wavy bedding(e.g.China’s continentalorigin Gulong shale).Herein,a mixed phase-field fracture model of the wavy-bedding shale was applied,based on the local tension-compression decomposition phase field method(PFM)and geometric structure generation algorithm for the bedding with controllable morphological features.The parametric analysis of fracture propagation behaviors in the case of abundant complex bedding structures showed that with wavy bedding,the vertical fracture propagation rate is far higher than the horizontal propagation rate.Moreover,the development of branch fractures is suppressed during the fracturing process of the wavy-bedding sample,and the stimulated volume is limited,which is different from the characteristic of parallel bedding that promotes horizontal fracture initiation and propagation.The results showed that larger amplitudes,higher frequencies,higher inclination angles,and larger strengths of wavy bedding all promote the formation of vertical penetrating fractures and suppress the growth of branch fractures.Under such circumstances,it is hard to create a well-connected fracture network after fracturing.This research may provide a theoretical basis for understanding fracture behaviors in rocks with such complex wavy bedding.
基金National Natural Science Foundation of China(12172292,12072287)。
文摘The crack initiation and early propagation are of great significance to the overall fatigue life of material.In order to investigate the anisotropic fracture behavior of laser metal deposited Ti-6Al-4V alloy(LMD Ti64)during the early stage,the fourpoint bending fatigue test was carried out on specimens of three different directions,as well as the forged specimens.The results indicate the anisotropic crack initiation and early propagation of LMD Ti64.The direction perpendicular to the deposition direction exhibits a better fatigue resistance than the other two.The crack initiation position and propagation path are dominated by the microstructure in the vicinity of U-notch.LMD Ti64 has a typical small crack effect,and the early crack propagation velocities in three directions are similar.Affected by the slip system of LMD Ti64,secondary cracks frequently occur,which are often found to have an angle of 60°to the main crack.The electron backscatter diffraction analysis indicates that LMD Ti64 has preferred orientations,i.e.,strong 0001//Z texture and 001//Z texture.Their crystallographic orientation will change as the direction of columnarβgrains turns over,resulting in the fatigue anisotropy of LMD Ti64 in crack initiation and early crack propagation process.
基金financially supported by the National Natural Science Foundation of China(Nos.52071036,U2037601)the Guangdong Major Project of Basic and Applied Basic Research,China(No.2020B0301030006)+1 种基金the Independent Research Project of State Key Laboratory of Mechanical Transmissions,China(Nos.SKLMT-ZZKT-2022Z01,SKLMT-ZZKT-2022M12)the Chongqing Science and Technology Commission,China(No.CSTB2022TIAD-KPX0021)。
文摘Edge cracking is one of the most serious problems in the rolling process of magnesium alloy sheets,which limits its application.In this work,the edge cracking behavior of different initial AZ31 alloy sheets,including as-cast(AC),as-rolled(AR)and as-extruded(AE),was systematically investigated and compared under the online heating rolling(O-LHR)process with a single-pass reduction of 50% at 250℃.The results show that both AC and AR sheets exhibit severe edge cracking behavior after the O-LHR.Among them,the AR sheet exhibits the severest edge cracking behavior on the rolling plane(RD-TD)and longitudinal section(RD-ND),which is attributed to the strong basal texture and extremely uneven microstructure with shear bands.While no visible edge crack appears in the AE rolled sheet,which is mainly related to the tilted texture and the more dynamic recrystallization during rolling process.Moreover,it is also found that the micro-cracks of the AC rolled sheet are mainly generated in the local fine-grained area and the twins where recrystallization occurs.In the AR rolled sheet,micro-cracks mainly develop inside the shear bands.Meanwhile,the micro-crack initiation mechanism of AC and AR rolled sheets was also discussed.
基金financial support by the National Natural Science Foundation of China(No.52474361)the Independent Research Project of State Key Laboratory of Advanced Special Steel,Shanghai Key Laboratory of Advanced Ferrometallurgy,Shanghai University(No.SKLASS 2023-Z01)the Science and Technology Commission of Shanghai Municipality(No.19DZ2270200).
文摘The fracture mechanisms of coarse-grained heat-affected zone(CGHAZ)for Mg and Mg–Ca deoxidized high-strength low-alloy(HSLA)steels after high heat input welding(HHIW)were investigated based on the microstructures,crack behaviors and mechanical properties.Compared to Mg–Ca steel,the proportion of intergranular acicular ferrites(IAFs)and polygonal ferrites(PFs)in Mg steel increases from 59.97%to 90.16%.The high-angle grain boundaries(HAGBs)and geometrically necessary dislocations density increase from 55.5%and 4.30×10^(14) m^(-2)to 70.4%and 5.48×10^(14) m^(–2),respectively,while effective grain size decreases from 9.46 to 8.12μm.The area fraction of radial zone in Mg steel decreases from 80.8%to 37.7%and cleavage plane is smaller with more curved and finer tearing ridges.The inclusions distributed at the center of cleavage planes and along river lines can serve as crack initiation sites.The zigzag pattern of primary crack propagation path has width of 476μm and the length of secondary cracks remains below 10μm.These cracks are deflected or arrested by IAFs,PFs and HAGBs,and tend to propagate along{110}plane family.These factors contribute to superior overall mechanical properties of Mg steel,especially increasing low-temperature impact toughness from 23 to 175 J.
基金This study has been partially funded by the National Key Research and Development Program of China,China(Grant No.2020YFA0711800)the National Natural Science Foundation of China(Grant Nos.51734009,51979272,and 52179118)Natural Science Foundation of Jiangsu Province,China(No.BK20211584).These supports are gratefully acknowledged.
文摘Four types of granite specimens were prepared and treated by chemical corrosion for 5 and 30 days,which were then used to carry out triaxial compression tests under different confining pressuresσ_(3).Type A is the intact sample with no preexisting flaws.Types B and C are the samples containing two relatively low-dip flaws and two relatively high-dip flaws,respectively.Type D is the sample including both relatively low-dip and relatively high-dip flaws.The influences of pH value of chemical solutions,flaw distribution,corrosion time andσ_(3) on triaxial stress-strain curves and ultimate failure modes are analyzed and discussed.The results show that the pH value of the chemical solution,corrosion time and the arrangement of preexisting flaws play crucial roles in the cracking behaviors of granite specimens.Type A specimens have the largest peak axial deviatoric stress,followed by Type C,Type D,and Type B specimens,respectively.It is because the decrease in the inclination of preexisting flaws induces the weakening effect due to the decrease in the shadow area along the compaction direction.Under aσ_(3) of 5 MPa,the peak axial deviatoric stress drops by approximately 40.89%,29.08%,4.08%,and 23.53%for pH=2,4,7,and 12,respectively.For intact granite(Type A)specimens,the ultimate failure mode displays a typical shear mode.The connection of two secondary cracks initiated at the tips of preexisting cracks is always the ultimate failure and crack coalescence mode for Type B specimens.The ultimate failure and crack coalescence mode of Types C and D specimens are significantly affected by pH value of the chemical solution,corrosion time andσ_(3),which is different from those of Types A and B specimens due to the differences in flow distributions.
基金support of the National Natural Science Foundation of China(Project Nos.52371012 and 52301060).
文摘The generation of defects,such as cracks and pores,presents significant challenges for high-strength met-als and alloys fabricated by the quick-emerging additive manufacturing technology,and subsequent post-processing treatments are often necessary before their practical applications.In this work,a novel heat treatment approach,involving a pre-softening treatment before hot isostatic pressing(HIP),is developed to facilitate the crack-healing in René142 superalloy produced through laser powder bed fusion.Results demonstrate that René142 alloy exhibits a propensity for severe cracking across a wide range of printing parameters,primarily in the form of solidification cracks and liquation cracks.These cracks are formed mainly due to a wide solidification range,the presence of a liquid film,and the concentration of resid-ual stress.The pre-softening solution heat treatment significantly reduces dislocation density and resid-ual stress levels,and the subsequent HIP together leads to a defect-free,dense structure for René142 superalloy.Consequently,the René142 alloy processed by the pre-softening HIP treatment achieves an excellent combination of yield strength(850 MPa),ultimate tensile strength(1227 MPa),and elongation(13.7%),with pseudo-equiaxed grains(120-150μm)and squareγ'precipitates(approximately 540 nm).These findings provide valuable insights for exploring crack elimination methods in other nickel-based superalloys fabricated through additive manufacturing.
基金Project(51622404)supported by Outstanding Youth Science Foundation of the National Natural Science Foundation of ChinaProjects(51374215,11572343,51904092)supported by the National Natural Science Foundation of China+2 种基金Project(2016YFC0801404)supported by the State Key Research Development Program of ChinaProject(KCF201803)supported by Henan Key Laboratory for Green and Efficient Mining&Comprehensive Utilization of Mineral Resources,Henan Polytechnic University,ChinaProject supported by Beijing Excellent Young Scientists,China
文摘The understanding of crack propagation characteristics and law of rocks during the loading process is of great significance for the exploitation and support of rock engineering.In this study,the crack propagation behavior of rocks in triaxial compression tests was investigated in detail.The main conclusions were as follows:1)According to the evolution characteristics of crack axial strain,the differential stress?strain curve of rocks under triaxial compressive condition can be divided into three phases which are linear elastic phase,crack propagation phase,post peak phase,respectively;2)The proposed models are applied to comparison with the test data of rocks under triaxial compressive condition and different temperatures.The theoretical data calculated by the models are in good agreement with the laboratory data,indicating that the proposed model can be applied to describing the crack propagation behavior and the nonlinear properties of rocks under triaxial compressive condition;3)The inelastic compliance and crack initiation strain in the proposed model have a decrease trend with the increase of confining pressure and temperature.Peak crack axial strain increases nonlinearly with the inelastic compliance and the increase rate increases gradually.Crack initiation strain has a linear relation with peak crack axial strain.
基金Project(51625404)supported by the National Natural Science Foundation for Distinguished Young Scholar of ChinaProjects(51604104,51504295)supported by the National Natural Science Foundation of China
文摘In order to investigate the real-time cracking behavior of each component of a composite with strong interfacial bonding among lamellae, Ti-18 Nb(at.%) composite was prepared by spark plasma sintering(SPS), followed by hot-rolling, annealing, and quenching. The microstructure and mechanical properties were characterized by scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), micro-region X-ray diffractometry(MRXRD), nanoindentation, and in-situ scanning electron microscopy tensile testing. The results show that the Ti-18 Nb consists of Ti-enriched, diffusion and Nb-enriched zones, and the sharp Nb gradient across different zones leads to inhomogeneous distribution of phase and mechanical properties. A remarkable finding is that the diffusion zones not only enable the cooperative deformation between the brittle Ti-enriched zones and the ductile Nb-enriched zones but also act as the crack-arresters to prevent the local cracks in the Ti-enriched zones from further propagating across the composite.
文摘The thermal fatigue behavior of a single crystal superalloy SRR99 was investigated. Specimens with V-type notch were tested at the peak temperatures of 900, 1000, and 1100℃. The crack growth curves as a function of the number of cycles were plotted. With the increase of peak temperature, the crack initiation life was shortened dramatically. Through optical microscopy （OM） and scanning electron microscopy （SEM） observation, it was found that multiple small cracks nucleated at the notch tip region but only one or two of them continued to develop in the following thermal cycles. The primary cracks generally propagated along a preferential direction. Microstructure changes after thermal fatigue were also discussed on the basis of SEM observation.
文摘The growth behaviors of short through cracks (0.2 < △a < 2.2mm) and long cracks are compared using CT type specimens in aluminum-lithium alloy 8090 T651. It is found that the short cracks grow much more than long ones and are observed to grow at the stress intensity ranges far below the long crack threshold. The distinction of growth bahavior between short and long cracks is attributed to the difference of their crack closure effect. The growth behavior of short cracks can be rationalized with that of long ones in terms of effective stress intensity ranges. The upper demarcation value of short through cracks for aluminum-lithium alloy 8090 is presented.
文摘The fatigue crack propagation behavior of TiNi50.6 shape memory alloy was studied. The ex- periment results showed that the crack propagation properties of this alloy display difference and similarity in comparison with common metallic materials. Because of the stress concentra- tion there was stress induced martensite transformation (SIMT) near the crack tip though the nominal stress was lower than the threshold stress of SIMT. The position and the amount of SIMT was in situ observed by a quester remote measurement system (QRMS). The observation results showed that the position of SIMT was beside the crack tip and was not in the plastic zone of common metallic materials (in front of the crack tip). The SIMT zone at an angle of about 45°to the direction of the crack propagation, like a butterfly,appeared in the loading process, disappeared in the unloading process and grew larger with the increase of K. The crack propagation rate(da/dN) followed the linear law in lg-lg plot. Observation of the crack surface showed fatigue striation clearly. The relationship between the site and the size of the plastic zone and the SIMT zone is discussed and a model is given to explain both the similarity and the difference of the crack propagation property of TiNi50.6 to common metal materials.
