The effect of deformation resistance of AlCr_(1.3)TiNi_(2) eutectic high-entropy alloys under various current densities and strain rates was investigated during electrically-assisted compression.Results show that at c...The effect of deformation resistance of AlCr_(1.3)TiNi_(2) eutectic high-entropy alloys under various current densities and strain rates was investigated during electrically-assisted compression.Results show that at current density of 60 A/mm^(2) and strain rate of 0.1 s^(−1),the ultimate tensile stress shows a significant decrease from approximately 3000 MPa to 1900 MPa with reduction ratio of about 36.7%.However,as current density increases,elongation decreases due to intermediate temperature embrittlement.This is because the current induces Joule effect,which then leads to stress concentration and more defect formation.Moreover,the flow stress is decreased with the increase in strain rate at constant current density.展开更多
AZ31/Al/Ta composites were prepared using the vacuum hot compression bonding(VHCB)method.The effect of hot compressing temperature on the interface microstructure evolution,phase constitution,and shear strength at the...AZ31/Al/Ta composites were prepared using the vacuum hot compression bonding(VHCB)method.The effect of hot compressing temperature on the interface microstructure evolution,phase constitution,and shear strength at the interface was investigated.Moreover,the interface bonding mechanisms of the AZ31/Al/Ta composites during the VHCB process were explored.The results demonstrate that as the VHCB temperature increases,the phase composition of the interface between Mg and Al changes from the Mg-Al brittle intermetallic compounds(Al_(12)Mg_(17)and Al_(3)Mg_(2))to the Al-Mg solid solution.Meanwhile,the width of the Al/Ta interface diffusion layer at 450℃increases compared to that at 400℃.The shear strengths are 24 and 46 MPa at 400 and 450℃,respectively.The interfacial bonding mechanism of AZ31/Al/Ta composites involves the coexistence of diffusion and mechanical meshing.Avoiding the formation of brittle phases at the interface can significantly improve interfacial bonding strength.展开更多
Data compression plays a vital role in datamanagement and information theory by reducing redundancy.However,it lacks built-in security features such as secret keys or password-based access control,leaving sensitive da...Data compression plays a vital role in datamanagement and information theory by reducing redundancy.However,it lacks built-in security features such as secret keys or password-based access control,leaving sensitive data vulnerable to unauthorized access and misuse.With the exponential growth of digital data,robust security measures are essential.Data encryption,a widely used approach,ensures data confidentiality by making it unreadable and unalterable through secret key control.Despite their individual benefits,both require significant computational resources.Additionally,performing them separately for the same data increases complexity and processing time.Recognizing the need for integrated approaches that balance compression ratios and security levels,this research proposes an integrated data compression and encryption algorithm,named IDCE,for enhanced security and efficiency.Thealgorithmoperates on 128-bit block sizes and a 256-bit secret key length.It combines Huffman coding for compression and a Tent map for encryption.Additionally,an iterative Arnold cat map further enhances cryptographic confusion properties.Experimental analysis validates the effectiveness of the proposed algorithm,showcasing competitive performance in terms of compression ratio,security,and overall efficiency when compared to prior algorithms in the field.展开更多
In this study,compacted loess samples with varying compaction water content but identical dry density were prepared to investigate the evolution of their hydraulic conductivity and compression behavior.Additionally,en...In this study,compacted loess samples with varying compaction water content but identical dry density were prepared to investigate the evolution of their hydraulic conductivity and compression behavior.Additionally,environmental scanning electron microscopy(ESEM)and nuclear magnetic resonance(NMR)analyses were conducted to gain microstructural insights into loess behavior at the laboratory scale.The results indicate that the maximum saturated hydraulic conductivity is observed at the lowest compaction water content,particularly in the early stage of permeability tests.In particular,for loess compacted at water contents below the optimum(as determined by the modified Proctor compaction test),the hydraulic conductivity decreases throughout the permeability tests.Conversely,when the water content exceeds the optimum level,the hydraulic conductivity shows an increasing trend.In terms of compression behavior,when the as-compacted samples are loaded in oedometer conditions,an increase in material compressibility is observed with increasing compaction water content.Again,a different phenomenological behavior was observed when the compaction water content exceeded the optimum,i.e.an abrupt increase in loess compressibility.ESEM tests provide microstructural confirmation of this evidence,as the surface morphology of the compacted loess changes significantly with increasing compaction water content.The microstructural evolution was also quantified in terms of area ratio using image processing software.Finally,NMR was used to quantify the intra-and inter-aggregate water at different compaction water contents,once again highlighting a threshold for the presence or absence of inter-aggregate water similar to the optimum water content.展开更多
The creep deformation and mechanical properties of 2219 aluminum alloy were experimentally investigated under both tension and compression at the temperature of 165℃for different time.The results indicated that the c...The creep deformation and mechanical properties of 2219 aluminum alloy were experimentally investigated under both tension and compression at the temperature of 165℃for different time.The results indicated that the creep deformation under tensile stress was greater than that under compressive stress.As the stress level increases,the compressive creep rate showed more significant increase.The yield strength after compressive stress creep-ageing was higher than that after stress-free ageing,with the lowest strength observed in the tensile-aged sample.Overall,the average phase length after compressive stress creep-ageing was larger than after tensile stress ageing.Under tensile stress,the number and size of precipitates at small angles to the stress direction were larger than those perpendicular to the stress direction.In contrast,under compressive stress,this relationship was reversed,and the preferential orientation of phases became more pronounced with ageing time.A unified,physics-based creep-ageing constitutive model,accounting for the orientation of precipitation,was developed for both tensile and compressive stress conditions.The predicted results were in good agreement with the experimental data.These findings,along with the developed model,provide a theoretical and simulation basis for precise creep-ageing forming of components under complex stresses.展开更多
During gas extraction from deep coal,the rock endures high effective stress,with both the time-dependent deformation and anisotropic structure of the rock controlling the permeability evolution.To reveal this phenomen...During gas extraction from deep coal,the rock endures high effective stress,with both the time-dependent deformation and anisotropic structure of the rock controlling the permeability evolution.To reveal this phenomenon,a numerical simulation framework of the finite volume method and transient embedded discrete fracture model is proposed to establish a new constitutive model that links poroelastoplastic deformation,adsorption-induced swelling,and aperture compression.From this model,anisotropic permeability tensors were derived to further achieve the simulation of coevolution.Meanwhile,our permeability model was verified against the measured permeability data,and the history match of the numerical model showed better results where the mismatch was less than 5%.The results indicate that(1)the long-term permeability evolution clearly showed the competitive effects of multiple deformation mechanisms,which involves three stages:compaction-dominated decline,adsorption-dominated rebound,and creep-controlled loss.(2)The increased number of compressible cleats/fractures accelerated the initial permeability decline,while the increased desorption-induced strain promoted faster rebound and enhancement and higher viscosity coefficients enhanced the creep effect,which led to significant long-term permeability loss.(3)Massive hydraulic fracturing created a larger drainage area,accelerating methane desorption and causing sharp permeability rebound with reduced residual gas,which shows that the permeability remained higher than the initial values even after the extensive extraction via the fractured horizontal wells.The permeability evolution mechanisms displayed varying properties,such as coal rank and burial depth,and distinct characteristics.A precise understanding of multiple competitive stress effects is crucial for optimizing coalbed methane extraction techniques and improving recovery efficiency.展开更多
The asymmetric creep aging behaviors of a pre-treated Al-Zn-Mg-Cu alloy under high and low stresses have been investigated for high precision creep age forming application of aluminum integral panels.With the increase...The asymmetric creep aging behaviors of a pre-treated Al-Zn-Mg-Cu alloy under high and low stresses have been investigated for high precision creep age forming application of aluminum integral panels.With the increase of applied stress,the creep strains under the tensile stresses are higher than those of compressive stresses and the asymmetry of creep strain is more obvious.However,the mechanical properties of tensile stress creep aged samples are lower than those of compressive stress creep aged samples.Dislocation density,dislocation moving velocity and the proportion of precipitates directly lead to the asymmetry of creep strain and mechanical properties after tensile-compressive creep aging process.In addition,the tensile and compressive stresses have little effect on the width of the precipitate-free zone(PFZ).It indicates that in the high stress creep age forming process of the pretreated Al-Zn-Mg-Cu alloy,the tensile stress promotes the dislocation motion to obtain a better creep strain but weakens its mechanical properties compared with the compressive stress.In the field of civil aviation aircraft component manufacturing,the introduction of tension and compression stress asymmetry into the creep constitutive model may improve the accuracy of creep age forming components.展开更多
The electric vertical takeoff and landing(e VTOL)aircraft shows great potential for rapid military personnel deployment on the battlefield.However,its susceptibility to control loss,complex crashes,and extremely limit...The electric vertical takeoff and landing(e VTOL)aircraft shows great potential for rapid military personnel deployment on the battlefield.However,its susceptibility to control loss,complex crashes,and extremely limited bottom energy-absorbing space demands higher comprehensive crashworthiness of its subfloor thin-walled structures.This study investigated the energy absorption capacity of novel concave polygonal carbon fiber reinforced plastics(CFRP)tubes under multi-angle collisions.Quasistatic compression experiments and finite element simulations were conducted to assess the failure mode and energy absorption.The influences of cross-section shapes,loading conditions,and geometry parameters on crashworthiness metrics were further analyzed.The results revealed that,under the similar weight,concave polygonal tubes exhibited superior energy absorption under axial loads compared to regular polygonal and circular tubes,attributed to the increased number of axial splits.However,both regular and concave polygonal tubes,particularly the latter,demonstrated reduced oblique energy absorption compared to traditional square tubes with the increasing ratio of SEA value decreased from 20%-16%.Notably,this reduction in energy absorption can be compensated for by the implementation of inward and outward crusher plugs,and with them,the concave polygonal tubes demonstrated outstanding overall crashworthiness performance under multiple loading conditions.This concave cross-sectional design methods could serve as a guidance for the development of the eVTOL subfloor.展开更多
Interfacial evolution and bonding mechanism of reduced activation ferritic/martensitic(RAFM)steel were systematically investigated through a series of hot compression tests conducted at various strains(0.15-0.8),strai...Interfacial evolution and bonding mechanism of reduced activation ferritic/martensitic(RAFM)steel were systematically investigated through a series of hot compression tests conducted at various strains(0.15-0.8),strain rates(0.001-1 s^(-1)),and temperatures(950-1050℃).Interfacial microstructural analysis revealed that plastic deformation of surface asperities effectively removes interfacial voids,and the evolution of dynamic recrystallization(DRX)aids in achieving a joint characterized by homogeneously refined microstructure and adequate interfacial grain boundary(IGB)migration.Electron backscattered diffraction analysis demonstrated that the continuous dynamic recrystallization,characterized by progressive subgrain rotation,is the prevailing DRX nucleation mechanism in RAFM steel during hot compression bonding.During DRX evolution,emerging DRX grains in the interfacial region expand into adjacent areas,transforming T-type triple junction grain boundaries into equal form,and resulting in a serrated and intricate interface.Elevated temperatures and strains,coupled with reduced strain rates,augment DRX grain nucleation and IGB migration,thus enhancing RAFM joint quality with regard to the interface bonding ratio and the interface migration ratio.展开更多
An innovative method of hot compression bonding is proposed in this work for the joining of 9Cr oxide dispersion strengthened(ODS)alloy and 9Cr reduced-activation ferritic/martensitic(RAFM)alloy.The microstructural ev...An innovative method of hot compression bonding is proposed in this work for the joining of 9Cr oxide dispersion strengthened(ODS)alloy and 9Cr reduced-activation ferritic/martensitic(RAFM)alloy.The microstructural evolution of the bonding interface was investigated by scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD),and transmission electron microscopy(TEM).The results verify that the pinning effect of nano-oxides particles(NPs)in 9Cr ODS alloy significantly enhances its dynamic recrystallization(DRX)temperature and deformation resistance.Continuous DRX(CDRX)first occurred on the 9Cr RAFM alloy side,and the areas near the bonding interface were composed of recrystallized grains.With increasing strain,CDRX also showed up on the 9Cr ODS alloy side.Inevitable slight oxidation occurred at the bonding interface during the hot compression bonding(HCB)process,and the interfacial oxides transformed from initial coarse CrO to TiO and finally to Y-Ti-O nanoparticles with sizes comparable to pre-existing NPs dispersed in the 9Cr ODS alloy matrix.It is believed that interfacial oxide transformation and grain structure consistency contributed to the excellent interface healing of the two dissimilar alloy pieces.The effectiveness of the bonding was tested by tensile tests and fractography analysis,revealing that ideal metallurgical bonding could be achieved under a controlled strain level of 10%at 800℃ followed by soaking at 1000℃ for 4 h.展开更多
The microstructural evolution of Cu−19Ni−6Cr−7Mn alloy during aging treatment was investigated.After aging for 120 min at 500℃,the alloy exhibited excellent mechanical properties,including a tensile strength of 978 M...The microstructural evolution of Cu−19Ni−6Cr−7Mn alloy during aging treatment was investigated.After aging for 120 min at 500℃,the alloy exhibited excellent mechanical properties,including a tensile strength of 978 MPa and an elastic modulus of 145.8 GPa.After aging for 240 min at 500℃,the elastic modulus of the alloy reached 149.5 GPa,which was among the highest values reported for Cu alloys.It was worth mentioning that the tensile strength increased rapidly from 740 to 934 MPa after aging for 5 min at 500℃,which was close to the maximum tensile strength(978 MPa).Analysis of the underlying strengthening mechanisms and phase transformation behavior revealed that the Cu−19Ni−6Cr−7Mn alloy underwent spinodal decomposition and DO_(22) ordering during the first 5 min of aging at 500℃,and L1_(2) ordered phases and bcc-Cr precipitates appeared.Therefore,the enhanced mechanical properties of the Cu−19Ni−6Cr−7Mn alloy can be attributed to the stress field generated by spinodal decomposition and the presence of nanoscale ordered phase and Cr precipitates.展开更多
基金National Natural Science Foundation of China(52305349)Heilongjiang Touyan Team(HITTY-20190036)+2 种基金Heilongjiang Provincial Natural Science Foundation of China(LH2023E033)CGN-HIT Advanced Nuclear and New Energy Research Institute(CGN-HIT202305)Natural Science Basic Research Program of Shaanxi Province(2023-JC-QN-0518)。
文摘The effect of deformation resistance of AlCr_(1.3)TiNi_(2) eutectic high-entropy alloys under various current densities and strain rates was investigated during electrically-assisted compression.Results show that at current density of 60 A/mm^(2) and strain rate of 0.1 s^(−1),the ultimate tensile stress shows a significant decrease from approximately 3000 MPa to 1900 MPa with reduction ratio of about 36.7%.However,as current density increases,elongation decreases due to intermediate temperature embrittlement.This is because the current induces Joule effect,which then leads to stress concentration and more defect formation.Moreover,the flow stress is decreased with the increase in strain rate at constant current density.
基金National Natural Science Foundation of China(52275308,52301146)Fundamental Research Funds for the Central Universities(2023JG007)Supported by Shi Changxu Innovation Center for Advanced Materials(SCXKFJJ202207)。
文摘AZ31/Al/Ta composites were prepared using the vacuum hot compression bonding(VHCB)method.The effect of hot compressing temperature on the interface microstructure evolution,phase constitution,and shear strength at the interface was investigated.Moreover,the interface bonding mechanisms of the AZ31/Al/Ta composites during the VHCB process were explored.The results demonstrate that as the VHCB temperature increases,the phase composition of the interface between Mg and Al changes from the Mg-Al brittle intermetallic compounds(Al_(12)Mg_(17)and Al_(3)Mg_(2))to the Al-Mg solid solution.Meanwhile,the width of the Al/Ta interface diffusion layer at 450℃increases compared to that at 400℃.The shear strengths are 24 and 46 MPa at 400 and 450℃,respectively.The interfacial bonding mechanism of AZ31/Al/Ta composites involves the coexistence of diffusion and mechanical meshing.Avoiding the formation of brittle phases at the interface can significantly improve interfacial bonding strength.
基金the Deanship of Graduate Studies and Scientific Research at Qassim University for financial support(QU-APC-2025).
文摘Data compression plays a vital role in datamanagement and information theory by reducing redundancy.However,it lacks built-in security features such as secret keys or password-based access control,leaving sensitive data vulnerable to unauthorized access and misuse.With the exponential growth of digital data,robust security measures are essential.Data encryption,a widely used approach,ensures data confidentiality by making it unreadable and unalterable through secret key control.Despite their individual benefits,both require significant computational resources.Additionally,performing them separately for the same data increases complexity and processing time.Recognizing the need for integrated approaches that balance compression ratios and security levels,this research proposes an integrated data compression and encryption algorithm,named IDCE,for enhanced security and efficiency.Thealgorithmoperates on 128-bit block sizes and a 256-bit secret key length.It combines Huffman coding for compression and a Tent map for encryption.Additionally,an iterative Arnold cat map further enhances cryptographic confusion properties.Experimental analysis validates the effectiveness of the proposed algorithm,showcasing competitive performance in terms of compression ratio,security,and overall efficiency when compared to prior algorithms in the field.
基金the China Postdoctoral Science Foundation(Grant No.2024MD753992)Shaanxi Geotechnical Mechanics and Engineering Young Talent Support Program Project(Grant No.YESS2024005)the National Natural Science Foundation of China(Grant No.41931285).
文摘In this study,compacted loess samples with varying compaction water content but identical dry density were prepared to investigate the evolution of their hydraulic conductivity and compression behavior.Additionally,environmental scanning electron microscopy(ESEM)and nuclear magnetic resonance(NMR)analyses were conducted to gain microstructural insights into loess behavior at the laboratory scale.The results indicate that the maximum saturated hydraulic conductivity is observed at the lowest compaction water content,particularly in the early stage of permeability tests.In particular,for loess compacted at water contents below the optimum(as determined by the modified Proctor compaction test),the hydraulic conductivity decreases throughout the permeability tests.Conversely,when the water content exceeds the optimum level,the hydraulic conductivity shows an increasing trend.In terms of compression behavior,when the as-compacted samples are loaded in oedometer conditions,an increase in material compressibility is observed with increasing compaction water content.Again,a different phenomenological behavior was observed when the compaction water content exceeded the optimum,i.e.an abrupt increase in loess compressibility.ESEM tests provide microstructural confirmation of this evidence,as the surface morphology of the compacted loess changes significantly with increasing compaction water content.The microstructural evolution was also quantified in terms of area ratio using image processing software.Finally,NMR was used to quantify the intra-and inter-aggregate water at different compaction water contents,once again highlighting a threshold for the presence or absence of inter-aggregate water similar to the optimum water content.
基金Project(JCKY2023205B003)supported by the Defense Industrial Technology Development Program,China。
文摘The creep deformation and mechanical properties of 2219 aluminum alloy were experimentally investigated under both tension and compression at the temperature of 165℃for different time.The results indicated that the creep deformation under tensile stress was greater than that under compressive stress.As the stress level increases,the compressive creep rate showed more significant increase.The yield strength after compressive stress creep-ageing was higher than that after stress-free ageing,with the lowest strength observed in the tensile-aged sample.Overall,the average phase length after compressive stress creep-ageing was larger than after tensile stress ageing.Under tensile stress,the number and size of precipitates at small angles to the stress direction were larger than those perpendicular to the stress direction.In contrast,under compressive stress,this relationship was reversed,and the preferential orientation of phases became more pronounced with ageing time.A unified,physics-based creep-ageing constitutive model,accounting for the orientation of precipitation,was developed for both tensile and compressive stress conditions.The predicted results were in good agreement with the experimental data.These findings,along with the developed model,provide a theoretical and simulation basis for precise creep-ageing forming of components under complex stresses.
基金support of the National Natural Science Foundation of China(U23B6004 and 52404045)the CAST Young Talent Support Program,Doctoral Student Special Project.
文摘During gas extraction from deep coal,the rock endures high effective stress,with both the time-dependent deformation and anisotropic structure of the rock controlling the permeability evolution.To reveal this phenomenon,a numerical simulation framework of the finite volume method and transient embedded discrete fracture model is proposed to establish a new constitutive model that links poroelastoplastic deformation,adsorption-induced swelling,and aperture compression.From this model,anisotropic permeability tensors were derived to further achieve the simulation of coevolution.Meanwhile,our permeability model was verified against the measured permeability data,and the history match of the numerical model showed better results where the mismatch was less than 5%.The results indicate that(1)the long-term permeability evolution clearly showed the competitive effects of multiple deformation mechanisms,which involves three stages:compaction-dominated decline,adsorption-dominated rebound,and creep-controlled loss.(2)The increased number of compressible cleats/fractures accelerated the initial permeability decline,while the increased desorption-induced strain promoted faster rebound and enhancement and higher viscosity coefficients enhanced the creep effect,which led to significant long-term permeability loss.(3)Massive hydraulic fracturing created a larger drainage area,accelerating methane desorption and causing sharp permeability rebound with reduced residual gas,which shows that the permeability remained higher than the initial values even after the extensive extraction via the fractured horizontal wells.The permeability evolution mechanisms displayed varying properties,such as coal rank and burial depth,and distinct characteristics.A precise understanding of multiple competitive stress effects is crucial for optimizing coalbed methane extraction techniques and improving recovery efficiency.
基金Project(2021YFB3400900)supported by the National Key R&D Program of ChinaProjects(51905551,52205435)supported by the National Natural Science Foundation of China Youth Foundation+1 种基金Project(2022ZZTS0196)supported by the Fundamental Research Founds for the Central Universities,ChinaProject(CX20220282)supported by the Hunan Provincial Innovation Foundation for Postgraduate,China。
文摘The asymmetric creep aging behaviors of a pre-treated Al-Zn-Mg-Cu alloy under high and low stresses have been investigated for high precision creep age forming application of aluminum integral panels.With the increase of applied stress,the creep strains under the tensile stresses are higher than those of compressive stresses and the asymmetry of creep strain is more obvious.However,the mechanical properties of tensile stress creep aged samples are lower than those of compressive stress creep aged samples.Dislocation density,dislocation moving velocity and the proportion of precipitates directly lead to the asymmetry of creep strain and mechanical properties after tensile-compressive creep aging process.In addition,the tensile and compressive stresses have little effect on the width of the precipitate-free zone(PFZ).It indicates that in the high stress creep age forming process of the pretreated Al-Zn-Mg-Cu alloy,the tensile stress promotes the dislocation motion to obtain a better creep strain but weakens its mechanical properties compared with the compressive stress.In the field of civil aviation aircraft component manufacturing,the introduction of tension and compression stress asymmetry into the creep constitutive model may improve the accuracy of creep age forming components.
基金financially supported by the Fundamental Research Funds for the Central Universities,Sun Yat-sen University(Grant No.24qnpy041)the Science and Technology Innovation Key R&D Program of Chongqing(Grant No.CSTB2023TIAD-STX0030)。
文摘The electric vertical takeoff and landing(e VTOL)aircraft shows great potential for rapid military personnel deployment on the battlefield.However,its susceptibility to control loss,complex crashes,and extremely limited bottom energy-absorbing space demands higher comprehensive crashworthiness of its subfloor thin-walled structures.This study investigated the energy absorption capacity of novel concave polygonal carbon fiber reinforced plastics(CFRP)tubes under multi-angle collisions.Quasistatic compression experiments and finite element simulations were conducted to assess the failure mode and energy absorption.The influences of cross-section shapes,loading conditions,and geometry parameters on crashworthiness metrics were further analyzed.The results revealed that,under the similar weight,concave polygonal tubes exhibited superior energy absorption under axial loads compared to regular polygonal and circular tubes,attributed to the increased number of axial splits.However,both regular and concave polygonal tubes,particularly the latter,demonstrated reduced oblique energy absorption compared to traditional square tubes with the increasing ratio of SEA value decreased from 20%-16%.Notably,this reduction in energy absorption can be compensated for by the implementation of inward and outward crusher plugs,and with them,the concave polygonal tubes demonstrated outstanding overall crashworthiness performance under multiple loading conditions.This concave cross-sectional design methods could serve as a guidance for the development of the eVTOL subfloor.
基金The authors are grateful to the National Natural Science Foundation of China(Grant Nos.52034004 and 52271111)the National Key R&D Program of China(2022YFB3705300)for grant and financial support.
文摘Interfacial evolution and bonding mechanism of reduced activation ferritic/martensitic(RAFM)steel were systematically investigated through a series of hot compression tests conducted at various strains(0.15-0.8),strain rates(0.001-1 s^(-1)),and temperatures(950-1050℃).Interfacial microstructural analysis revealed that plastic deformation of surface asperities effectively removes interfacial voids,and the evolution of dynamic recrystallization(DRX)aids in achieving a joint characterized by homogeneously refined microstructure and adequate interfacial grain boundary(IGB)migration.Electron backscattered diffraction analysis demonstrated that the continuous dynamic recrystallization,characterized by progressive subgrain rotation,is the prevailing DRX nucleation mechanism in RAFM steel during hot compression bonding.During DRX evolution,emerging DRX grains in the interfacial region expand into adjacent areas,transforming T-type triple junction grain boundaries into equal form,and resulting in a serrated and intricate interface.Elevated temperatures and strains,coupled with reduced strain rates,augment DRX grain nucleation and IGB migration,thus enhancing RAFM joint quality with regard to the interface bonding ratio and the interface migration ratio.
基金supported by the National Natural Science Foundation of China(Grant Nos.52233017,51774265,52301032,and 52173305)the National Key Research and Development Program(Grant No.2018YFA0702900)+2 种基金the National Science and Technology Major Project of China(Grant No.2019ZX06004010)the Strategic Priority Research Program of the Chinese Academy of Sciences(Grant No.XDC04000000)the LingChuang Research Project of China National Nuclear Corporation,CNNC Science Fund for Talented Young Scholars,the Program of CAS Interdisciplinary Innovation Team,and the Youth Innovation Promotion Association,CAS.
文摘An innovative method of hot compression bonding is proposed in this work for the joining of 9Cr oxide dispersion strengthened(ODS)alloy and 9Cr reduced-activation ferritic/martensitic(RAFM)alloy.The microstructural evolution of the bonding interface was investigated by scanning electron microscopy(SEM),electron back-scattered diffraction(EBSD),and transmission electron microscopy(TEM).The results verify that the pinning effect of nano-oxides particles(NPs)in 9Cr ODS alloy significantly enhances its dynamic recrystallization(DRX)temperature and deformation resistance.Continuous DRX(CDRX)first occurred on the 9Cr RAFM alloy side,and the areas near the bonding interface were composed of recrystallized grains.With increasing strain,CDRX also showed up on the 9Cr ODS alloy side.Inevitable slight oxidation occurred at the bonding interface during the hot compression bonding(HCB)process,and the interfacial oxides transformed from initial coarse CrO to TiO and finally to Y-Ti-O nanoparticles with sizes comparable to pre-existing NPs dispersed in the 9Cr ODS alloy matrix.It is believed that interfacial oxide transformation and grain structure consistency contributed to the excellent interface healing of the two dissimilar alloy pieces.The effectiveness of the bonding was tested by tensile tests and fractography analysis,revealing that ideal metallurgical bonding could be achieved under a controlled strain level of 10%at 800℃ followed by soaking at 1000℃ for 4 h.
基金supported by the National Key R&D Program of China (No. 2021YFB3700700)the Henan Province Top Talent Training Program Project, China (No. 244500510020)the High-level Talent Research Start-up Project Funding of Henan Academy of Sciences, China (No. 242017001)。
文摘The microstructural evolution of Cu−19Ni−6Cr−7Mn alloy during aging treatment was investigated.After aging for 120 min at 500℃,the alloy exhibited excellent mechanical properties,including a tensile strength of 978 MPa and an elastic modulus of 145.8 GPa.After aging for 240 min at 500℃,the elastic modulus of the alloy reached 149.5 GPa,which was among the highest values reported for Cu alloys.It was worth mentioning that the tensile strength increased rapidly from 740 to 934 MPa after aging for 5 min at 500℃,which was close to the maximum tensile strength(978 MPa).Analysis of the underlying strengthening mechanisms and phase transformation behavior revealed that the Cu−19Ni−6Cr−7Mn alloy underwent spinodal decomposition and DO_(22) ordering during the first 5 min of aging at 500℃,and L1_(2) ordered phases and bcc-Cr precipitates appeared.Therefore,the enhanced mechanical properties of the Cu−19Ni−6Cr−7Mn alloy can be attributed to the stress field generated by spinodal decomposition and the presence of nanoscale ordered phase and Cr precipitates.
