Powder segregation induced by mold filling is an important phenomenon that affects the final quality of metal injection molding （MIM）. The prediction of segregation in MIM requires a bi-phase flow model to describe ...Powder segregation induced by mold filling is an important phenomenon that affects the final quality of metal injection molding （MIM）. The prediction of segregation in MIM requires a bi-phase flow model to describe distinctly the flows of metallic powder and polymer binder. Viscous behaviors for the flows of each phase should hence be determined. The coefficient of interaction between the flows of two phases should also be evaluated. However, only viscosity of the mixed feedstock is measurable by capillary tests. Wall sticking is supposed in the traditional model for capillary tests, while the wall slip is important to be taken into account in MIM injection. Objective of the present paper is to introduce the slip effect in bi-phase simulation, and search the suitable way to determine the viscous behaviors for each phase with the consideration of wall slip in capillary tests. Analytical and numerical methods were proposed to realize such a specific purpose. The proposed method is based on the mass conservation between the capillary flows in mono-phase model for the mixed feedstock and in bi-phase model for the flows of two phases. Examples of the bi-phase simulation in MIM were realized with the software developed by research team. The results show evident segregation, which is valuable for improving the mould designs.展开更多
Magnetic absorbers with high permeability have significant advantages in lowfrequency and broadband electromagnetic wave(EMW)absorption.However,the insufficient magnetic loss and inherent high conductivity of existing...Magnetic absorbers with high permeability have significant advantages in lowfrequency and broadband electromagnetic wave(EMW)absorption.However,the insufficient magnetic loss and inherent high conductivity of existing magnetic absorbers limit the further expansion of EMW absorption bandwidth.Herein,the spinel(FeCoNiCrCu)_(3)O_(4) high-entropy oxides(HEO)are successfully constructed on the surface of FeCoNiCr_(0.4)Cu_(0.2) high-entropy alloys(HEA)through low-temperature oxygen bath treatment.On the one hand,HEO and HEA have different magnetocrystalline anisotropies,which is conducive to achieving continuous natural resonance to improve magnetic loss.On the other hand,HEO with low conductivity can serve as an impedance matching layer,achieving magneto-electric co-modulation.When the thickness is 5 mm,the minimum reflection loss(RL)value and absorption bandwidth(RL<−5 dB)of bi-phase high-entropy composites(BPHEC)can reach−12.8 dB and 633 MHz,respectively.The RCS reduction value of multilayer sample with impedance gradient characteristic can reach 18.34 dB m^(2).In addition,the BPHEC also exhibits temperaturestable EMW absorption performance,high Curie temperature,and oxidation resistance.The absorption bandwidth maintains between 593 and 691 MHz from−50 to 150℃.This work offers a new and tunable strategy toward modulating the electromagnetic genes for temperature-stable ultra-broadband megahertz EMW absorption.展开更多
To predict the segregation effect in metal injection moulding (MIM) injection, a bi-phasic model based on mixture theory is adopted in simulation. An explicit algorithm is developed and realized by the authors, which ...To predict the segregation effect in metal injection moulding (MIM) injection, a bi-phasic model based on mixture theory is adopted in simulation. An explicit algorithm is developed and realized by the authors, which conducts the simulation to be a cost-effective tool in MIM technology. In case of the bi-phasic simulation, the viscosity behaviours are necessary to be determined for the flows of each phase while only the viscosity of mixture is measurable by tests. It is a crucial problem for application of the bi-phasic simulation of MIM injection. A reasonable method is hence analysed and proposed to determine the viscosity behaviours of each phase. Even though this method may be furthermore modified in the future, it results in the practical simulation of segregation effects with reasonable parameters. The simulation results are compared with the measurements on injected specimens.展开更多
Metal injection moulding (MIM) is a new technology to manufacture small intricate parts in large quantity. Numerical simulation plays an important role in its development. To predict the specific segregation effect in...Metal injection moulding (MIM) is a new technology to manufacture small intricate parts in large quantity. Numerical simulation plays an important role in its development. To predict the specific segregation effect in MIM injection, mixture theory is adopted to model the injection flow by a bi-phasic model. This model conducts to the solution of two-coupled Stokes equations. It is an extremely computational consuming solution in the scope of the traditional algorithms, which induce a serious challenge to cost-effectivity of the MIM simulation. Referred to some methods proposed by Lewis in mono-phasic simulation and the implicit algorithms in MIM simulation, a new explicit algorithm is proposed and realized to perform efficiently this type of bi-phasic flow. Numerically this algorithm is devised to perform the simulation in a fully uncoupled manner except for a global solution of the pressure field in each time step. The physical coupling is taken into account in a sequential pattern by fractional steps.展开更多
A bi-phasic scaffold consisting of a columnar formaldehyde-acetalized polyvinyl alcohol (PVF) sponge and a cylindrical porous hydroxyapatite (HA) with a hollow center was devised. Rat bone marrow cells (rBMCs) were se...A bi-phasic scaffold consisting of a columnar formaldehyde-acetalized polyvinyl alcohol (PVF) sponge and a cylindrical porous hydroxyapatite (HA) with a hollow center was devised. Rat bone marrow cells (rBMCs) were seeded into the sponge placed in the hollow center of the cylindrical porous HA. The bi-phasic scaffold, a cylindrical porous HA and a PVF sponge separated from a bi-phasic scaffold after rBMC seeding, and a PVF sponge without rBMCs as a negative control, were implanted for 6 weeks into rat dorsal subcutaneous tissue. In each construct, bone formation was examined histologically and osteocalcin was measured immunochemically. Bone formation was observed in the bi-phasic scaffold and also in the cylindrical porous HA isolated from the bi-phasic scaffold. A significant difference in the quantity of osteocalcin was observed between the bi-phasic scaffold and the isolated cylindrical porous HA. No bone formation was found in the isolated PVF sponge. The bi-phasic scaffold as an outer layer of the scaffold seemed to inhibit the outflow of rBMCs from the PVF sponge. This type of bi-phasic scaffold may have two specific characteristics: Attachment of cells both in PVF sponge and cylindrical porous HA.展开更多
为解决双向DC-DC变换器(dual active bridge,DAB)采用单移相(single-phase-shift,SPS)控制产生的回流功率较高及动态性能较差的问题,提出一种采用双重移相(dual-phase-shift,DPS)控制下的最小回流功率算法与直接功率控制相结合的方法。...为解决双向DC-DC变换器(dual active bridge,DAB)采用单移相(single-phase-shift,SPS)控制产生的回流功率较高及动态性能较差的问题,提出一种采用双重移相(dual-phase-shift,DPS)控制下的最小回流功率算法与直接功率控制相结合的方法。首先对DPS控制下的基本原理及回流功率特性进行分析,并建立回流功率与移相比之间的数学关系,从而推导出各分段条件下回流功率在各阶段最小化的方案。其次在保证对变换器回流功率最小化的同时提出结合直接功率法来显著提高变换器的动态性能。最后通过MATLAB/Simulink中建立的仿真验证了上述控制策略的有效性。展开更多
基金Specialized Research Fund for the Doc-toral Program of Higher Education (No.20020613005)
文摘Powder segregation induced by mold filling is an important phenomenon that affects the final quality of metal injection molding （MIM）. The prediction of segregation in MIM requires a bi-phase flow model to describe distinctly the flows of metallic powder and polymer binder. Viscous behaviors for the flows of each phase should hence be determined. The coefficient of interaction between the flows of two phases should also be evaluated. However, only viscosity of the mixed feedstock is measurable by capillary tests. Wall sticking is supposed in the traditional model for capillary tests, while the wall slip is important to be taken into account in MIM injection. Objective of the present paper is to introduce the slip effect in bi-phase simulation, and search the suitable way to determine the viscous behaviors for each phase with the consideration of wall slip in capillary tests. Analytical and numerical methods were proposed to realize such a specific purpose. The proposed method is based on the mass conservation between the capillary flows in mono-phase model for the mixed feedstock and in bi-phase model for the flows of two phases. Examples of the bi-phase simulation in MIM were realized with the software developed by research team. The results show evident segregation, which is valuable for improving the mould designs.
基金Supported by Program for the National Natural Science Foundation of China(No.52071053,U1704253,52103334)the Fundamental Research Funds for the Central Universities(DUT24GF102)the Shandong Province Natural Science Youth Fund(ZR2024QA134)。
文摘Magnetic absorbers with high permeability have significant advantages in lowfrequency and broadband electromagnetic wave(EMW)absorption.However,the insufficient magnetic loss and inherent high conductivity of existing magnetic absorbers limit the further expansion of EMW absorption bandwidth.Herein,the spinel(FeCoNiCrCu)_(3)O_(4) high-entropy oxides(HEO)are successfully constructed on the surface of FeCoNiCr_(0.4)Cu_(0.2) high-entropy alloys(HEA)through low-temperature oxygen bath treatment.On the one hand,HEO and HEA have different magnetocrystalline anisotropies,which is conducive to achieving continuous natural resonance to improve magnetic loss.On the other hand,HEO with low conductivity can serve as an impedance matching layer,achieving magneto-electric co-modulation.When the thickness is 5 mm,the minimum reflection loss(RL)value and absorption bandwidth(RL<−5 dB)of bi-phase high-entropy composites(BPHEC)can reach−12.8 dB and 633 MHz,respectively.The RCS reduction value of multilayer sample with impedance gradient characteristic can reach 18.34 dB m^(2).In addition,the BPHEC also exhibits temperaturestable EMW absorption performance,high Curie temperature,and oxidation resistance.The absorption bandwidth maintains between 593 and 691 MHz from−50 to 150℃.This work offers a new and tunable strategy toward modulating the electromagnetic genes for temperature-stable ultra-broadband megahertz EMW absorption.
文摘To predict the segregation effect in metal injection moulding (MIM) injection, a bi-phasic model based on mixture theory is adopted in simulation. An explicit algorithm is developed and realized by the authors, which conducts the simulation to be a cost-effective tool in MIM technology. In case of the bi-phasic simulation, the viscosity behaviours are necessary to be determined for the flows of each phase while only the viscosity of mixture is measurable by tests. It is a crucial problem for application of the bi-phasic simulation of MIM injection. A reasonable method is hence analysed and proposed to determine the viscosity behaviours of each phase. Even though this method may be furthermore modified in the future, it results in the practical simulation of segregation effects with reasonable parameters. The simulation results are compared with the measurements on injected specimens.
基金Supported by the Invited Professor Program of French Ministry of Education (No. 9808588) , the French-Chinese Advanced Research Program (M98-04)the Foundation for University Key Teacher by the Chinese Ministry of Education (GG-460-10613-2770).
文摘Metal injection moulding (MIM) is a new technology to manufacture small intricate parts in large quantity. Numerical simulation plays an important role in its development. To predict the specific segregation effect in MIM injection, mixture theory is adopted to model the injection flow by a bi-phasic model. This model conducts to the solution of two-coupled Stokes equations. It is an extremely computational consuming solution in the scope of the traditional algorithms, which induce a serious challenge to cost-effectivity of the MIM simulation. Referred to some methods proposed by Lewis in mono-phasic simulation and the implicit algorithms in MIM simulation, a new explicit algorithm is proposed and realized to perform efficiently this type of bi-phasic flow. Numerically this algorithm is devised to perform the simulation in a fully uncoupled manner except for a global solution of the pressure field in each time step. The physical coupling is taken into account in a sequential pattern by fractional steps.
文摘A bi-phasic scaffold consisting of a columnar formaldehyde-acetalized polyvinyl alcohol (PVF) sponge and a cylindrical porous hydroxyapatite (HA) with a hollow center was devised. Rat bone marrow cells (rBMCs) were seeded into the sponge placed in the hollow center of the cylindrical porous HA. The bi-phasic scaffold, a cylindrical porous HA and a PVF sponge separated from a bi-phasic scaffold after rBMC seeding, and a PVF sponge without rBMCs as a negative control, were implanted for 6 weeks into rat dorsal subcutaneous tissue. In each construct, bone formation was examined histologically and osteocalcin was measured immunochemically. Bone formation was observed in the bi-phasic scaffold and also in the cylindrical porous HA isolated from the bi-phasic scaffold. A significant difference in the quantity of osteocalcin was observed between the bi-phasic scaffold and the isolated cylindrical porous HA. No bone formation was found in the isolated PVF sponge. The bi-phasic scaffold as an outer layer of the scaffold seemed to inhibit the outflow of rBMCs from the PVF sponge. This type of bi-phasic scaffold may have two specific characteristics: Attachment of cells both in PVF sponge and cylindrical porous HA.
文摘为解决双向DC-DC变换器(dual active bridge,DAB)采用单移相(single-phase-shift,SPS)控制产生的回流功率较高及动态性能较差的问题,提出一种采用双重移相(dual-phase-shift,DPS)控制下的最小回流功率算法与直接功率控制相结合的方法。首先对DPS控制下的基本原理及回流功率特性进行分析,并建立回流功率与移相比之间的数学关系,从而推导出各分段条件下回流功率在各阶段最小化的方案。其次在保证对变换器回流功率最小化的同时提出结合直接功率法来显著提高变换器的动态性能。最后通过MATLAB/Simulink中建立的仿真验证了上述控制策略的有效性。
