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ZrO_2-10% Dy_2O_3纳米晶的碱性水热法合成及其烧结体的电性能研究 被引量:4
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作者 陶为华 马桂林 《中国稀土学报》 CAS CSCD 北大核心 2005年第3期328-333,共6页
以湿化学法制得Zr(OH)4和Dy(OH)3的共沉淀为前驱体, 在碱性介质(pH=7.60~13.89)中用水热法合成了ZrO2-10% Dy2O3(摩尔分数)立方相纳米晶. 研究发现, 纳米晶粒径随着反应介质pH值的增大而增大;同时纳米晶粒径随着水热反应介质温度的升... 以湿化学法制得Zr(OH)4和Dy(OH)3的共沉淀为前驱体, 在碱性介质(pH=7.60~13.89)中用水热法合成了ZrO2-10% Dy2O3(摩尔分数)立方相纳米晶. 研究发现, 纳米晶粒径随着反应介质pH值的增大而增大;同时纳米晶粒径随着水热反应介质温度的升高而增大. 将ZrO2-10% Dy2O3纳米晶在1400 ℃下烧结制得了致密的固体电解质陶瓷样品, 比通常高温固相反应法采用的烧结温度(>1550 ℃)降低了150 ℃以上. 还用交流阻抗谱法及氧浓差电池法研究了ZrO2-10% Dy2O3陶瓷样品在600~1000 ℃下的离子导电特性. 结果表明, 该陶瓷样品在600~1000 ℃下氧离子迁移数为1, 氧离子电导率的最大值为2.2×10-2 S·cm-1, 是一个优良的氧离子导体. 展开更多
关键词 zro2-10% Dy2o3 纳米晶 固体电解质 水热合成 稀土
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Fabrication and Studying the Mechanical Properties of A356 Alloy Reinforced with Al<sub>2</sub>O<sub>3</sub>-10% Vol. ZrO<sub>2</sub>Nano-particles through Stir Casting 被引量:1
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作者 Mohsen Hajizamani Hamidreza Baharvandi 《Advances in Materials Physics and Chemistry》 2011年第2期26-30,共5页
Al2O3-ZrO2 with a high level of hardness and toughness is known as ceramic steel. Due to its unique properties it can be used as a reinforcement in fabrication of metal matrix composites. In this study, nanoparticles ... Al2O3-ZrO2 with a high level of hardness and toughness is known as ceramic steel. Due to its unique properties it can be used as a reinforcement in fabrication of metal matrix composites. In this study, nanoparticles of Al2O3-10% ZrO2 with an average size of 80 nm were used to fabricate Al matrix composites containing 0.5, 1, 1.5 and 2 wt.% of the reinforcement. The fabrication route was stir casting at 850?C. There is no report about usage of this reinforcement in fabrication of composites in the literature. The microstructures of the as-cast composites were studied by scanning electron microscope (SEM). Density measurement, hardness and tensile properties were carried out to identify the mechanical properties of the composites. The results revealed that with increasing the reinforcement content, density decreased while yield, ultimate tensile strength and compressive strength increased. Also, hardness increased by increasing the reinforcement content up to 1 wt.% Al2O3-10% ZrO2 but it decreased in the samples containing higher amounts of reinforcement. 展开更多
关键词 STIR Casting al Matrix Composite al2o3-10% zro2 nanoparticles
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