Texture and grain structure evolution during annealing and their effects on tensile strength and anisotropy were studied using XRD,DSC,SEM,EBSD and TEM.The results indicate that elevated rolling temperatures reduce th...Texture and grain structure evolution during annealing and their effects on tensile strength and anisotropy were studied using XRD,DSC,SEM,EBSD and TEM.The results indicate that elevated rolling temperatures reduce the f(g)_(max(Copper))/f(g)_(max(Brass))ratio,increase S-Brass fine bands,and promote S-dispersoid precipitation,leading to finer recrystallized grains.Dominant recrystallization textures transform from Goss+P to Goss and then to Goss+Cube with increasing rolling temperature.Annealing at 350℃shows four tensile strength response stages:fast softening I,rapid strengthening II,slow strengthening III,and slow softening IV.The transition from Stages I to II is driven by the formation of strong Goss and P textures,and Stage IV is linked to enhanced Cube texture.Plates with Goss+Cube textures and fine equiaxed grains exhibit the lowest YS/UTS ratio and minimal anisotropy.展开更多
Al-Cu-Mn-Mg合金因其优异的综合性能,被广泛应用于航空航天和轨道交通等领域。然而,该合金在铸造过程中容易出现热裂缺陷,严重影响铸件的质量和可靠性。因此,提高合金的晶粒细化效果,对于改善合金的铸造性能具有重要意义。Al-Ti-B细化...Al-Cu-Mn-Mg合金因其优异的综合性能,被广泛应用于航空航天和轨道交通等领域。然而,该合金在铸造过程中容易出现热裂缺陷,严重影响铸件的质量和可靠性。因此,提高合金的晶粒细化效果,对于改善合金的铸造性能具有重要意义。Al-Ti-B细化剂是铝合金铸造中最常用的晶粒细化剂,但不同Ti/B质量比的Al-Ti-B细化剂对晶粒细化效果及热裂机制尚未系统研究。采用X射线衍射仪(XRD)、光学显微镜(OM)、扫描电镜(SEM)和CRC(constrained rod cast)金属型约束热裂棒模具等,分析了不同Ti/B质量比的Al-Ti-B细化剂对铸造Al-Cu-Mn-Mg合金微观组织和热裂倾向性的影响。实验结果表明,4种Ti/B比的Al-Ti-B细化剂中Al_3Ti和TiB_2相的含量存在显著差异。在B含量均为0.3%(质量分数)的条件下,添加Al-3Ti-1B、Al-4Ti-1B、Al-5Ti-1B和Al-5Ti-2B的Al-5Cu-0.7Mn-0.55Mg合金的平均晶粒尺寸分别为162.07、113.73、107.81和88.00μm,对应的热裂纹倾向性指数依次为112、136、96和24。微观机制分析表明,Ti B_(2)相的含量对晶粒细化效果和热裂倾向性具有显著影响。特别是Al-5Ti-2B细化剂,在晶粒细化的同时,显著降低了合金的热裂倾向性,展现出优异的性能。展开更多
基金financial support from the National Key Research and Development Program of China(No.2016YFB0300900)the National Key Fundamental Research Project of China(No.2012CB619506-3)the National Natural Science Foundation of China(No.51171209)。
文摘Texture and grain structure evolution during annealing and their effects on tensile strength and anisotropy were studied using XRD,DSC,SEM,EBSD and TEM.The results indicate that elevated rolling temperatures reduce the f(g)_(max(Copper))/f(g)_(max(Brass))ratio,increase S-Brass fine bands,and promote S-dispersoid precipitation,leading to finer recrystallized grains.Dominant recrystallization textures transform from Goss+P to Goss and then to Goss+Cube with increasing rolling temperature.Annealing at 350℃shows four tensile strength response stages:fast softening I,rapid strengthening II,slow strengthening III,and slow softening IV.The transition from Stages I to II is driven by the formation of strong Goss and P textures,and Stage IV is linked to enhanced Cube texture.Plates with Goss+Cube textures and fine equiaxed grains exhibit the lowest YS/UTS ratio and minimal anisotropy.
文摘Al-Cu-Mn-Mg合金因其优异的综合性能,被广泛应用于航空航天和轨道交通等领域。然而,该合金在铸造过程中容易出现热裂缺陷,严重影响铸件的质量和可靠性。因此,提高合金的晶粒细化效果,对于改善合金的铸造性能具有重要意义。Al-Ti-B细化剂是铝合金铸造中最常用的晶粒细化剂,但不同Ti/B质量比的Al-Ti-B细化剂对晶粒细化效果及热裂机制尚未系统研究。采用X射线衍射仪(XRD)、光学显微镜(OM)、扫描电镜(SEM)和CRC(constrained rod cast)金属型约束热裂棒模具等,分析了不同Ti/B质量比的Al-Ti-B细化剂对铸造Al-Cu-Mn-Mg合金微观组织和热裂倾向性的影响。实验结果表明,4种Ti/B比的Al-Ti-B细化剂中Al_3Ti和TiB_2相的含量存在显著差异。在B含量均为0.3%(质量分数)的条件下,添加Al-3Ti-1B、Al-4Ti-1B、Al-5Ti-1B和Al-5Ti-2B的Al-5Cu-0.7Mn-0.55Mg合金的平均晶粒尺寸分别为162.07、113.73、107.81和88.00μm,对应的热裂纹倾向性指数依次为112、136、96和24。微观机制分析表明,Ti B_(2)相的含量对晶粒细化效果和热裂倾向性具有显著影响。特别是Al-5Ti-2B细化剂,在晶粒细化的同时,显著降低了合金的热裂倾向性,展现出优异的性能。
