MnxNi0.5-xZn0.5Fe2O4 nanorods were successfully synthesized by the thermal treatment of rod-like precursors that were fabricated by the co-precipitation of Mn2＋, Ni2＋, and Fe2＋ in the lye. The phase, morphology, an...MnxNi0.5-xZn0.5Fe2O4 nanorods were successfully synthesized by the thermal treatment of rod-like precursors that were fabricated by the co-precipitation of Mn2＋, Ni2＋, and Fe2＋ in the lye. The phase, morphology, and particle diameter were examined by the X-ray diffraction and transmission electron microscopy. The magnetic properties of the samples were studied using a vibrating sample magnetometer. nanorods with a diameter of 35 nm and an The results indicated that pure Ni0.5-xZn0.5Fe2O4 aspect ratio of 15 were prepared. It was found that the diametei of the MnxNi0.5-xZn0.5Fe2O4（0≤x≤0.5） samples increased, the length and the aspect .ratio decreased, with an increase in x value. When x=0.5, the diameter and the aspect ratio of the sample reached up to 50 nm and 7-8, respectively. The coercivity of the samples first increased and then decreased with the increase in the x value. The coercivity of the samples again increased when the x value was higher than 0.4. When x=0.5, the coercivity of the MnxNi0.5-xZn0.5Fe2O4 sample reached the maximal value （134.3 Oe） at the calcination temperature of 600 ℃. The saturation magnetization of the samples first increased and then. decreased with the increase in the x value. When x=0.2, the saturation magnetizat：ion of the sample reached the maximal value （68.5 emu/g） at the calcination temperature of 800 ℃.展开更多
Neutron diffraction measurements on Nd2(Fe0,Si0 ,)14B at room temperature and 77 K were performed. Data analysis using profile refinement was carried out. The results show that at room temperature Si atoms occupy pref...Neutron diffraction measurements on Nd2(Fe0,Si0 ,)14B at room temperature and 77 K were performed. Data analysis using profile refinement was carried out. The results show that at room temperature Si atoms occupy preferentially 4c, 8j, and I6k2 sites, and the magnetic moments of bath Nd and Fe are parallel to C-axis. At 77 K, the site occupations remain unchanged as in room temperature, while the calculated Nd magnetic moment direction has an angular deviation of 37.8 ° from C-axis.展开更多
The influences of micro alloy and heat treatment procedure on the hardening of DJ108Ti alloy, which is based on the electrolytic Al Si(2 05%) Ti(0 25%) Fe(0 30%) multi component alloy, have been investigated...The influences of micro alloy and heat treatment procedure on the hardening of DJ108Ti alloy, which is based on the electrolytic Al Si(2 05%) Ti(0 25%) Fe(0 30%) multi component alloy, have been investigated. The results indicate that the micro alloy based on the multi component alloy makes α Al dendrites in DJ108Ti alloy refined; that the improved heat treatment procedure makes the eutectic Si phases granulated , the Fe phase refined, and the strengthening phases of Mg2Si and Al2Cu fully precipitated. The micro alloy and the heat treatment procedure harden DJ108Ti alloy and benefit the abrasion resistance of the alloy展开更多
文摘MnxNi0.5-xZn0.5Fe2O4 nanorods were successfully synthesized by the thermal treatment of rod-like precursors that were fabricated by the co-precipitation of Mn2＋, Ni2＋, and Fe2＋ in the lye. The phase, morphology, and particle diameter were examined by the X-ray diffraction and transmission electron microscopy. The magnetic properties of the samples were studied using a vibrating sample magnetometer. nanorods with a diameter of 35 nm and an The results indicated that pure Ni0.5-xZn0.5Fe2O4 aspect ratio of 15 were prepared. It was found that the diametei of the MnxNi0.5-xZn0.5Fe2O4（0≤x≤0.5） samples increased, the length and the aspect .ratio decreased, with an increase in x value. When x=0.5, the diameter and the aspect ratio of the sample reached up to 50 nm and 7-8, respectively. The coercivity of the samples first increased and then decreased with the increase in the x value. The coercivity of the samples again increased when the x value was higher than 0.4. When x=0.5, the coercivity of the MnxNi0.5-xZn0.5Fe2O4 sample reached the maximal value （134.3 Oe） at the calcination temperature of 600 ℃. The saturation magnetization of the samples first increased and then. decreased with the increase in the x value. When x=0.2, the saturation magnetizat：ion of the sample reached the maximal value （68.5 emu/g） at the calcination temperature of 800 ℃.
文摘Neutron diffraction measurements on Nd2(Fe0,Si0 ,)14B at room temperature and 77 K were performed. Data analysis using profile refinement was carried out. The results show that at room temperature Si atoms occupy preferentially 4c, 8j, and I6k2 sites, and the magnetic moments of bath Nd and Fe are parallel to C-axis. At 77 K, the site occupations remain unchanged as in room temperature, while the calculated Nd magnetic moment direction has an angular deviation of 37.8 ° from C-axis.
文摘The influences of micro alloy and heat treatment procedure on the hardening of DJ108Ti alloy, which is based on the electrolytic Al Si(2 05%) Ti(0 25%) Fe(0 30%) multi component alloy, have been investigated. The results indicate that the micro alloy based on the multi component alloy makes α Al dendrites in DJ108Ti alloy refined; that the improved heat treatment procedure makes the eutectic Si phases granulated , the Fe phase refined, and the strengthening phases of Mg2Si and Al2Cu fully precipitated. The micro alloy and the heat treatment procedure harden DJ108Ti alloy and benefit the abrasion resistance of the alloy
