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加速器质谱测量用HfF_4的固相合成研究 被引量:1
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作者 姜涛 杨通在 +2 位作者 杨君 拓飞 杨亮 《核技术》 CAS CSCD 北大核心 2010年第5期354-356,共3页
HfO2样品通过分离纯化流程后,与NH4HF2进行固相反应制成HfF4,并用加速器质谱进行测量。结果表明:α-安息香肟萃取是降低182W含量的重要步骤;固相合成法制备的HfF4样品中180HfF5-的引出束流强度是同等条件下液相合成法的3-4倍;制样方法(... HfO2样品通过分离纯化流程后,与NH4HF2进行固相反应制成HfF4,并用加速器质谱进行测量。结果表明:α-安息香肟萃取是降低182W含量的重要步骤;固相合成法制备的HfF4样品中180HfF5-的引出束流强度是同等条件下液相合成法的3-4倍;制样方法(固相合成法、液相合成法)对182W/Hf值影响不大;HfF4中182W/Hf值低至10-11g·g-1量级。 展开更多
关键词 182Hf 加速器质谱 182w HfF4 固相合成 制备
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^(182)W anomalies in mantle:a brief review
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作者 Yining Zhang Yun Liu 《Acta Geochimica》 EI CAS CSCD 2022年第4期704-716,共13页
With significant advances in mass spectrometry for isotope analysis in the last decade,e.g.,negative thermal ionization mass spectrometry and multi-collector inductively coupled plasma mass spectrometry,high-precision... With significant advances in mass spectrometry for isotope analysis in the last decade,e.g.,negative thermal ionization mass spectrometry and multi-collector inductively coupled plasma mass spectrometry,high-precision(ppm-level)measurements of tungsten(W)isotopes have been widely used for early earth differentiation processes,such as metal-silicate segregation,melting and crystallization processes during the magma ocean,and putative core-mantle exchange and dynamics.Here,we give a brief review of works on ^(182)W anomalies in terrestrial samples,including methods,results,explanations,implications,and prospects.The review will be presented by including the following parts:the introduction of W isotopes and the short-lived radioactive ^(182)Hf-^(182)W system;data notations and W isotope measurement methods;^(182)W anomalies observed in terrestrial samples;a summary of models developed for interpreting origins of positive and negative ^(182)W anomalies;future prospects. 展开更多
关键词 ^(182)W anomalies Mantle samples MC-ICPMS N-TIMS NORMALIZATION
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Recent progress in AMS measurement of ^(182)Hf at the CIAE 被引量:1
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作者 李振宇 何明 +10 位作者 董克君 贺国珠 李朝历 何贤文 张伟 胡豪 郑国文 李恒 武绍勇 袁坚 姜山 《Chinese Physics C》 SCIE CAS CSCD 2012年第11期1145-1149,共5页
In order to improve the accuracy of accelerator mass spectrometry (AMS) measurement for 182Hf/180Hf, a series of measurements have been taken in the AMS laboratory at the China Institute of Atomic Energy (CIAE). T... In order to improve the accuracy of accelerator mass spectrometry (AMS) measurement for 182Hf/180Hf, a series of measurements have been taken in the AMS laboratory at the China Institute of Atomic Energy (CIAE). The major ones include the instantaneous monitoring of 180HfF5- current, testing the stability of transmission, the alternate measurements of an unknown sample and standard, and the origin identification and minimization of background 182W. The experimental details and the improvement in the measurement accuracy, as well as some useful suggestions for better satisfying the requirements of certain practical applications, are presented in this paper. 展开更多
关键词 182Hf AMS 182w alternate measurement suppression factor
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Tungsten-182 Mssbauer experiments at liquid nitrogen temperature
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作者 HUANG Runsheng, LIU Bing, ZHANG Jinrong, LIU Cong & GAO Xuekui1. Physics Department of Nanjing University, Nanjing 210093, China 2. China Institute of Atomic Energy, Beijing 102413, China 《Chinese Science Bulletin》 SCIE EI CAS 2001年第9期732-734,共3页
A good 182Ta Mossbauer source and an apparatus designed specially were made. 182W transmission Mossbauer experiments were successfully carried out, both of the source and absorber at liquid nitrogen temperature. It wa... A good 182Ta Mossbauer source and an apparatus designed specially were made. 182W transmission Mossbauer experiments were successfully carried out, both of the source and absorber at liquid nitrogen temperature. It was found that reducing background radiation is very important to observe clear resonant effect. 展开更多
关键词 MOSSBAUER EFFECT 182w MOSSBAUER effect.
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