期刊文献+
共找到1,387篇文章
< 1 2 70 >
每页显示 20 50 100
Design method and experimental study of three-step method for electrochemical machining of blisks
1
作者 Moqi SHEN Jia LIU +1 位作者 Wenbo WU Di ZHU 《Chinese Journal of Aeronautics》 2025年第9期559-571,共13页
To ensure the dimensional accuracy of the final blade profile,it is necessary for precision Electrochemical Machining(ECM)of blade profile to come into an equilibrium state.However,after Electrochemical Trepanning(ECT... To ensure the dimensional accuracy of the final blade profile,it is necessary for precision Electrochemical Machining(ECM)of blade profile to come into an equilibrium state.However,after Electrochemical Trepanning(ECTr),the cascade channel of the blisk is narrow,and the blank allowance distribution is uneven,making it difficult for the precision ECM to become balanced.In blisk production,the two-step method cannot make precision ECM enter equilibrium for some blisk types.A three-step processing method is proposed to overcome this problem.The threestep method adds Electrochemical Homogenizing Machining(ECHM)between the ECTr and precision ECM steps so that the blank allowance can be homogenized quickly without unduly affecting the minimum allowance.Comparative machining experiments of the two-and three-step methods were performed to verify the improvement to blade machining accuracy.The processing results show that the contour parameters of the blade after the three-step method implementation are much better.The allowance difference of the concave(convex)side decreased by 70.5%(65%).In addition,the current in the three-step method is stable at 110 A at the end of precision ECM,verifying successfully entering the equilibrium state. 展开更多
关键词 Electrochemical machining BLISK Mathematical model Processing method three-step method
原文传递
Field observation of air-sea CO_(2) and H2O flux using the eddy covariance method based on 100 Hz gas analyzer in the Bohai and Yellow Seas
2
作者 Tan Yu Yuhan Xia +8 位作者 Zhengli Qiu Bangyi Tao Yan Bai Xianqiang He Bing Chen Mingxing Li Yu Wang Qilan Zhang Chao Liang 《Acta Oceanologica Sinica》 2025年第7期161-176,共16页
Air-sea water vapor and CO_(2) flux observation experiments were carried out at the Yantai National Satellite Ocean Calibration Platform and the jetty at Monolithic Beach,Juehua Island,using a 100 Hz gas analyzer.The ... Air-sea water vapor and CO_(2) flux observation experiments were carried out at the Yantai National Satellite Ocean Calibration Platform and the jetty at Monolithic Beach,Juehua Island,using a 100 Hz gas analyzer.The observations were corrected by employing wild point rejection,linear detrending,delay correction,coordinate rotation,time matching,and Webb,Pearman,and Leuning(WPL)correction.The results of spectral analysis and a turbulence development adequacy data quality check showed that the overall observation data quality was good.The air-sea water vapor and CO_(2) flux results showed that the observation duration affected both the air-sea flux intensity and direction at different observation frequencies.At shorter observation durations,the air-sea flux values measured at 100 Hz were smaller than the 20 Hz measurements and had opposite directions.In addition,the WPL correction reduced the overall air-sea flux and partially minimized the effect of observation frequency on the air-sea flux intensity.These results showed that high-frequency observations showed more turbulence variations than low-frequency observations.This conclusion could promote an understanding of small-scale turbulence variations. 展开更多
关键词 eddy correlation method 100 Hz gas analyzer TDLAS air-sea flux observation frequency
在线阅读 下载PDF
Method of analyzing vibration characteristics of armature system of hermetically sealed electromagnetic relay
3
作者 REN Wan-bin CUI Li +1 位作者 LUO Fu-biao ZHAI Guo-fu 《Journal of Zhejiang University-Science A(Applied Physics & Engineering)》 SCIE EI CAS CSCD 2007年第3期434-438,共5页
Published research is minimal on vibration characteristics of hermetically sealed electromagnetic relay (EMR) ex- posed to mechanical environment. The vibration characteristics of armature system, link contact system ... Published research is minimal on vibration characteristics of hermetically sealed electromagnetic relay (EMR) ex- posed to mechanical environment. The vibration characteristics of armature system, link contact system with electromagnetic system will cause EMR malfunction. The nonlinear dynamics model of armature systems was studied by considering electro- magnetic attraction force and opposite mechanical force in this paper. Angular displacements of armature under different sinu- soidal vibration conditions are solved in order to obtain the failure mode result from armature system. Vibration tests showed the presented analyzing method is suitable for EMR. The conclusions are instructive for increasing vibration resistance of armature systems of EMR, and are significant for reliability design of switch apparatus. 展开更多
关键词 Hermetically sealed electromagnetic relay (EMR) Armature system Vibration characteristics analyzing method
在线阅读 下载PDF
A Comparison between Neutron Activation Analysis and X-Ray Fluorescence Methods in Analyzing the Granite Samples
4
作者 Hayder Salah Naeem Pegah Moradi Khaniabadi Eid Mahmoud Eid 《Journal of Chemistry and Chemical Engineering》 2013年第9期803-807,共5页
This study focused on the performance of where elements analysing techniques were used to detect the elements in granite stones. These techniques are NAA (neutron activation analysis) and XRF (X-ray fluorescence).... This study focused on the performance of where elements analysing techniques were used to detect the elements in granite stones. These techniques are NAA (neutron activation analysis) and XRF (X-ray fluorescence). They were applied to detect the elements in samples which had been chosen from different areas of Pulua Penang in Malaysia collected by geophysics group which helped to describe and identify the elements found in the granite stone that were used in the study procedures to control the analytical results. The integration of both methods has enabled the researcher to determine 40 elements in the samples. The numbers of elements detected by XRF analysis method are 12 elements (Ar, K, Sc, Ti, V, Cr, Mn, Fe, Co, Ni, Cu and Zn); while, the elements detected by NAA method have three folds of elements with XRF analysis method were 35 elements (Na, AI, Si, K, Ca, Sc,Ti, Mn, Fe, Co, Ga, Ce, As, Br, Rb, Zr, Sb, I, Cs, Ba, La, Nd, Sm, Eu,Tb, Dy, Yb, Lu, Hf, Ta, W, Au, Pa and Np). Seven common elements were detected in both techniques: K, Sc, Ti, V, Mn, Fe and Co. Si has a higher concentration in NAA technique which is 331.8 ppm. Sc has a lower concentration in XRF technique which is 0.25 ppm. Nd has a lower concentration in NAA technique which is 3.09 - 10-5 ppm. Finally, it is found that the NAA is better to detect the elements than XRF. 展开更多
关键词 Radiation science radiation physics NAA XRF analyzing methods.
在线阅读 下载PDF
A semi-implicit three-step method based on SUPG finite element formulation for flow in lid driven cavities with different geometries 被引量:1
5
作者 Cheng HUAN Dai ZHOU Yan BAO 《Journal of Zhejiang University-Science A(Applied Physics & Engineering)》 SCIE EI CAS CSCD 2011年第1期33-45,共13页
A numerical algorithm using a bilinear or linear finite element and semi-implicit three-step method is presented for the analysis of incompressible viscous fluid problems. The streamline upwind/Petrov-Galerkin (SUPG) ... A numerical algorithm using a bilinear or linear finite element and semi-implicit three-step method is presented for the analysis of incompressible viscous fluid problems. The streamline upwind/Petrov-Galerkin (SUPG) stabilization scheme is used for the formulation of the Navier-Stokes equations. For the spatial discretization, the convection term is treated explicitly, while the viscous term is treated implicitly, and for the temporal discretization, a three-step method is employed. The present method is applied to simulate the lid driven cavity problems with different geometries at low and high Reynolds numbers. The results compared with other numerical experiments are found to be feasible and satisfactory. 展开更多
关键词 Semi-implicit three-step method Streamline upwind/Petrov-Galerkin (SUPG) finite element method (FEM) Unsteady incompressible flows Lid driven cavity problem
原文传递
Application of Dynamic Linear Detecting Method in Data Processing of the Portable Blood Sugar Analyzer
6
作者 Xiaohao Wang Ran Liu +2 位作者 Fei Tang Yangchun Yu Zhaoying Zhou 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2006年第A03期80-82,共3页
In this paper,a dynamic linear detecting method,that the non-linear coefficient NL% was led and the non-linearity of data were estimated continuously and dynamically and determined when NL% exceeded reference value (... In this paper,a dynamic linear detecting method,that the non-linear coefficient NL% was led and the non-linearity of data were estimated continuously and dynamically and determined when NL% exceeded reference value (5%),was used for data processing and could solve the problem caused by the phenomenon of substrate depleting occurred following the redox reaction in portable blood sugar analyzer.By contrast to the conventional end-point method,the dynamic linear detecting method is based on multipoint data collecting.Experiments of measuring the calibration glucose solution with 8 various concentrations from 50 mg/dl to 400 mg/dl were carried out with the analyzer developed by our group.The linear regression curve,whose correlation for the data was 0.9995 and the residual was 2.8080,were obtained.The obtained correlation,residual, and the computation workload are all fit for the portable blood sugar analyzer. 展开更多
关键词 data processing portable blood sugar analyzer dynamic linear detecting method
在线阅读 下载PDF
ZnO micro-nano composite hydrophobic film prepared by the three-step method
7
作者 马恺 李华 +3 位作者 张晗 许小亮 公茂刚 杨周 《Chinese Physics B》 SCIE EI CAS CSCD 2009年第5期1942-1946,共5页
The hydrophobicity of the lotus leaf is mainly due to its surface micro-nano composite structure. In order to mimic the lotus structure, ZnO micro-nano composite hydrophobic films were prepared via the three-step meth... The hydrophobicity of the lotus leaf is mainly due to its surface micro-nano composite structure. In order to mimic the lotus structure, ZnO micro-nano composite hydrophobic films were prepared via the three-step method. On thin buffer films of SiO2, which were first fabricated on glass substrates by the so,gel dip-coating method, a ZnO seed layer was deposited via RF magnetron sputtering. Then two different ZnO films, micro-nano and micro-only flowerlike structures, were grown by the hydrothermal method. The prepared films have different hydrophobic properties after surface modification. The structures of the obtained ZnO films were characterized using x-ray diffraction and field-emission scanning electron microscopy. A conclusion that a micro-nano composite structure is more beneficial to hydrophobicity than a micro-only structure was obtained through research into the effect of structure on hydrophobic properties. 展开更多
关键词 three-step method ZNO micro-nano structure hydrophobic film
原文传递
General Convergence Analysis for Three-step Projection Methods and Applications to Variational Problems
8
作者 L UO Hong-lin L UO Hui-lin 《Chinese Quarterly Journal of Mathematics》 CSCD 2009年第2期239-243,共5页
First a general model for a three-step projection method is introduced, and second it has been applied to the approximation solvability of a system of nonlinear variational inequality problems in a Hilbert space setti... First a general model for a three-step projection method is introduced, and second it has been applied to the approximation solvability of a system of nonlinear variational inequality problems in a Hilbert space setting. Let H be a real Hilbert space and K be a nonempty closed convex subset of H. For arbitrarily chosen initial points x0, y0, z0 ∈ K, compute sequences xn, yn, zn such thatT : K→ H is a nonlinear mapping onto K. At last three-step models are applied to some variational inequality problems. 展开更多
关键词 two-step model general three-step model system of strongly monotonic non-linear variational inequalities projection formulas convergence of three-projection method
在线阅读 下载PDF
Accuracy verification and practice of simultaneous thermal analyzer
9
作者 LI Haixia YANG Xiuhong +2 位作者 TIAN Liyan LUO Minting GUO Yanwen 《实验技术与管理》 北大核心 2025年第11期133-139,共7页
The accuracy of thermal analysis measurements is critical to analyze material properties correctly,making the improvement of measurement precision and proper uncertainty analysis of test results absolutely essential.A... The accuracy of thermal analysis measurements is critical to analyze material properties correctly,making the improvement of measurement precision and proper uncertainty analysis of test results absolutely essential.As a primary thermal analysis instrument,the simultaneous thermal analyzer(STA)has unique advantages,which combines the functionalities of thermogravimetric(TG)analyzersand differential scanning calorimeters(DSC).However,the absence of standard quality control procedures has resulted in poor measurement reproducibility,low accuracy,and inadequate traceability of analytical results.This study utilized a multi-point temperature calibration method based on national certified reference materials to reduce instrument temperature indication errors.On this basis,we innovatively established a comprehensive quality control system encompassing laboratory environmental control,standard method selection,instrument performance verification,reference material traceability,and uncertainty analysis,thereby achieving standardized operational procedures for thermal analysis measurement.Taking the"determination of initial melting temperature of unknown substances"as a representative case study,a component resolution model for thermal analysis test uncertainty was developed.Through systematic analysis of both the reference material-introduced component and measurement repeatability component,complete traceability of test results was achieved.This approach ensures data validity and enhances the accuracy of test results.This provides crucial technical support and practical reference for the standardization of thermal analysis measurement procedure and assessment of result reliability. 展开更多
关键词 thermal analysis accuracy simultaneous thermal analyzer standardized testing procedures instrument performance qualification method selection traceability analysis uncertainty analysis
在线阅读 下载PDF
微粉化非诺贝特粒度及粒度分布研究
10
作者 付志玲 杨楠楠 +3 位作者 刘佩 白秀秀 尚斌 李霞 《中国药业》 2026年第1期83-85,共3页
目的建立测定微粉化非诺贝特粒度的方法。方法进样前用5号标准药典筛进行预分散,检测仪器为Mastersizer 3000型激光粒度仪,检测方法为干法,颗粒类型为非球形,进样量为0.20 g,折射率为1.53,颗粒吸收率为0.01,背景测试时间为10 s,样品测... 目的建立测定微粉化非诺贝特粒度的方法。方法进样前用5号标准药典筛进行预分散,检测仪器为Mastersizer 3000型激光粒度仪,检测方法为干法,颗粒类型为非球形,进样量为0.20 g,折射率为1.53,颗粒吸收率为0.01,背景测试时间为10 s,样品测试时间为8 s,测量次数为1次,遮光度为1%~5%,分散气压为1.50 bar,振动进样速率为50%,文丘里管类型为标准文丘里管,料斗间隙为1.00 mm,分析模型为通用型。结果重复性、耐用性试验结果的RSD均小于8%。3批样品的累积粒度分布达到10%,50%,90%时对应的粒径(D_(10),D_(50),D_(90))分别为2.30~2.36μm、5.33~5.35μm、10.56~10.69μm。结论所建立的方法操作简单、快捷,能满足微粉化非诺贝特生产过程中的快速检测,且重复性、耐用性均良好,适用于该产品的粒度控制。 展开更多
关键词 非诺贝特 微粉化 激光粒度仪干法 粒度分布
暂未订购
A Rapid Method for Measuring Seed Protein Content in Cowpea (<i>Vigna unguiculata</i>(L.) Walp) 被引量:1
11
作者 Yuejin Weng Ainong Shi +5 位作者 Waltram Second Ravelombola Wei Yang Jun Qin Dennis Motes David Octor Moseley Pengyin Chen 《American Journal of Plant Sciences》 2017年第10期2387-2396,共10页
Cowpea (Vigna unguiculata (L.) Walp), a legume crop that is grown in the worldwide, provides beneficial proteins for human consumption and animal feeding. In comparison, Rapid N analyzer as traditional method, has bee... Cowpea (Vigna unguiculata (L.) Walp), a legume crop that is grown in the worldwide, provides beneficial proteins for human consumption and animal feeding. In comparison, Rapid N analyzer as traditional method, has been widely used to measure protein content through the percentage of total nitrogen in the seed’s grounded powder. Near-Infrared Reflectance (NIR) has commonly been used to measure protein content in soybean seeds using whole grain without the need of seed grinding, which makes it possible to obtain fast results at a lower cost-per-analysis than the traditional combustion method. The specific objective of this study is to test a rapid method for measuring cowpea seed protein content by the NIR analyzer comparing to the traditional rapid N analyzer. A total of 240 cowpea genotypes were used in this study, including six seed coat colors, black, blackeye, browneye, cream, pinkeye, and red with 40 cowpea genotypes. The results showed that a linear relationship exists between the NIR analyzer and the Rapid N analyzer in the six different color groups. The correlation efficiency (r) between the seed protein contents from NIR and Rapid N was higher for pinkeye seed (r = 0.867), blackeye (0.771), cream (0.729), browneye (0.700), and red (0.623), respectively, but lower for black seeds, indicating that the NIR analyzer can be used to measure protein content for cowpea seeds with the five types of seed coat except black. Overview, the cowpea seed protein content measured from the NIR analyzer showed a little higher seed protein content. A series of regression models with different seed coat color have been built to adjust to protein content of colorful cowpea seeds from the NIR analyzer. But, it is not recommended to use for black color seeds due to a very low correlation efficiency (r) value with 0.184. 展开更多
关键词 COWPEA Seed PROTEIN CONTENT PROTEIN Measurement method Rapid N analyzER Near-Infrared Reflectance (NIR) Vigna unguiculata
暂未订购
A TOTAL CONTENT X—RAY FLUORESCENCE METHOD FOR COPPER PROSPECTING
12
作者 周四春 谢庭周 葛良全 《Nuclear Science and Techniques》 SCIE CAS CSCD 1992年第3期191-195,共5页
A new method is proposed to prospect copper deposits with portable XRF analyzer. The method is based on the close relation between Cu and the chalcophile elements or some other elements in the geochemical anomalies of... A new method is proposed to prospect copper deposits with portable XRF analyzer. The method is based on the close relation between Cu and the chalcophile elements or some other elements in the geochemical anomalies of a Cu deposit. Applications of the technique in Northeast China are presented. 展开更多
关键词 Portable X-RAY FLUORESCENCE analyzERS Total content X-RAY FLUORESCENCE method PROSPECTING for COPPER DEPOSITS
在线阅读 下载PDF
Study on the wind field and pollutant dispersion in street canyons using a stable numerical method
13
作者 Dennis Y.C. LEUNG 《Journal of Environmental Sciences》 SCIE EI CAS CSCD 2005年第3期488-490,共3页
A stable finite element method for the time dependent Navier-Stokes equations was used for studying the wind flow and pollutant dispersion within street canyons. A three-step fractional method was used to solve the ve... A stable finite element method for the time dependent Navier-Stokes equations was used for studying the wind flow and pollutant dispersion within street canyons. A three-step fractional method was used to solve the velocity field and the pressure field separately from the governing equations. The Streamline Upwind Petrov-Galerkin(SUPG) method was used to get stable numerical results. Numerical oscillation was minimized and satisfactory results can be obtained for flows at high Reynolds numbers. Simulating the flow over a square cylinder within a wide range of Reynolds numbers validates the wind field model. The Strouhal numbers obtained from the numerical simulation had a good agreement with those obtained from experiment. The wind field model developed in the present study is applied to simulate more complex flow phenomena in street canyons with two different building configurations. The results indicated that the flow at rooftop of buildings might not be assumed parallel to the ground as some numerical modelers did. A counter-clockwise rotating vortex may be found in street canyons with an inflow from the left to right. In addition, increasing building height can increase velocity fluctuations in the street canyon under certain circumstances, which facilitate pollutant dispersion. At high Reynolds numbers, the flow regimes in street canyons do not change with inflow velocity. 展开更多
关键词 finite element method Streamline Upwind Petrov-Galerkin method three-step fractional method
在线阅读 下载PDF
Application of CLEAR-VOF method to wave and flow simulations
14
作者 Ying-wei SUN Hai-gui KANG 《Water Science and Engineering》 EI CAS 2012年第1期67-78,共12页
A two-dimensional numerical model based on the Navier-Stokes equations and computational Lagrangian-Eulerian advection remap-volume of fluid (CLEAR-VOF) method was developed to simulate wave and flow problems. The N... A two-dimensional numerical model based on the Navier-Stokes equations and computational Lagrangian-Eulerian advection remap-volume of fluid (CLEAR-VOF) method was developed to simulate wave and flow problems. The Navier-Stokes equations were discretized with a three-step finite element method that has a third-order accuracy. In the CLEAR-VOF method, the VOF function F was calculated in the Lagrangian manner and allowed the complicated free surface to be accurately captured. The propagation of regular waves and solitary waves over a flat bottom, and shoaling and breaking of solitary waves on two different slopes were simulated with this model, and the numerical results agreed with experimental data and theoretical solutions. A benchmark test of dam-collapse flow was also simulated with an unstructured mesh, and the capability of the present model for wave and flow simulations with unstructured meshes, was verified. The results show that the model is effective for numerical simulation of wave and flow problems with both structured and unstructured meshes. 展开更多
关键词 water wave water flow numerical simulation CLEAR-VOF three-step finite element method
在线阅读 下载PDF
Assessment of the Phylogenetic Affiliation Levels of Water Mite(Acari,Hydrachnidia)Species with the Elemental Analysis Method
15
作者 Ferruh Asci Mustafa Ucar +1 位作者 Saban Kabak Muhlis Ozkan 《Advances in Bioscience and Biotechnology》 2015年第6期427-432,共6页
10 different species of water mites which are Georgella helvetica, Eylais extendens, Hydrachna globose, Hydrachna prosifera, Hydrachna skorikowi, Hydrodroma despiciens, Hydryphantes dispar, Limnesia fulgida, Eylais se... 10 different species of water mites which are Georgella helvetica, Eylais extendens, Hydrachna globose, Hydrachna prosifera, Hydrachna skorikowi, Hydrodroma despiciens, Hydryphantes dispar, Limnesia fulgida, Eylais setosa, Hydryphantes flexuosus were used in this study. The total masses of these species were measured as mg with the use of an elemental analyzer to calculate the percentage of the organic components of their structures. The achieved values were assessed separately for each species and element with the interpolation method. Out of these organic elements, the amount of C with an approximately value of 50% was the highest for all species while the amounts of S which was approximately 1% was determined as the lowest for almost all species. The observed values were discussed in terms of the systematic of water mites. 展开更多
关键词 Water Mites ACARI HYDRACHNIDIA Elemental analyzer Interpolation method
暂未订购
Application of Three Steps and Middle Column Method in Shallow Buried Tunnel with Strong Expansive Surrounding Rock
16
作者 LIMingyu 《外文科技期刊数据库(文摘版)工程技术》 2022年第6期031-038,共8页
In the Chenggong tunnel of Kunming, aiming at the engineering of shallow buried and strongly expanded surrounding rock, the construction method of three steps plus central columns is introduced. The soil of Chenggong ... In the Chenggong tunnel of Kunming, aiming at the engineering of shallow buried and strongly expanded surrounding rock, the construction method of three steps plus central columns is introduced. The soil of Chenggong Tunnel is tested in laboratory to determine its expansibility. The traditional three-step method and three-step plus center pillar method are compared and analyzed by using MIDAS-GTS. Finally, the deformation of surrounding rock after the construction of three-step plus center pillar method is obtained through on-site monitoring. The results show that: 1) The free expansion rate, montmorillonite content and cation exchange capacity of Chenggong tunnel soil are determined, and the expansive parameters are obtained. 2) Through numerical simulation, it is concluded that under the condition of strong expansive soil and weak surrounding rock, the settlement of vault and two sides caused by the traditional step method are both larger than that of the three steps plus center pillar method. This new improved method can effectively reduce the disturbance to surrounding rock and significantly reduce the settlement of vault;3) The data of vault settlement and displacement of two sides of the tunnel after the construction of the three-step plus center pillar method are obtained by on-site monitoring, and are simulated and analyzed by using MIDAS-GTS software. The relative error value of vault settlement obtained by the two methods is 1%, which indicates that MIDAS-GTS has good simulation effect on the stress state and deformation state of the tunnel, and further indicates that this method is very practical for the case of small convergence of side walls and large vault settlement. 展开更多
关键词 shallow buried tunnel with strong swelling surrounding rock three-step middle column method laboratory tests numerical simulation field monitoring
原文传递
基于频域扫描的表层土壤含水量检测算法
17
作者 宋华军 刘旭 +2 位作者 田岳 任鹏 沈美丽 《电子器件》 2025年第4期950-954,共5页
土壤水是作物生长发育直接水源,土壤含水量是监测作物旱情的最重要的指标。目前土壤含水量检测算法无法满足大规模的监测需要,存在精度较低,易受天气、地表状况等因素影响的问题。微波测量方法能解决上述问题,但是当前该方法采用时域脉... 土壤水是作物生长发育直接水源,土壤含水量是监测作物旱情的最重要的指标。目前土壤含水量检测算法无法满足大规模的监测需要,存在精度较低,易受天气、地表状况等因素影响的问题。微波测量方法能解决上述问题,但是当前该方法采用时域脉冲,具有噪声大等问题。基于去噪声能力强的矢量网络分析仪采用频域扫描方法,使用菲涅尔反射系数进行反演,建立土壤含水量和介电常数关系模型。反演结果表明,不同含水量的土壤介电常数存在明显差别,得到的含水量的精确度能够满足设计要求。 展开更多
关键词 土壤含水量 介电常数 矢量网络分析仪 自由空间法
在线阅读 下载PDF
基于临界流锐孔动态稀释的痕量氧分析仪校准装置及方法
18
作者 于瑞祥 任逸尘 +4 位作者 刘旺旺 高艳秋 董翊 姜阳 魏王慧 《化学分析计量》 2025年第7期114-119,共6页
设计了一套基于临界流锐孔的动态稀释原理的痕量氧分析仪校准装置,用于痕量氧分析仪在0~1 000nmol/mol使用范围内的校准。介绍了临界流锐孔基本原理,验证了稀释装置中纯化器的性能,对稀释装置的稀释准确性进行了研究,建立了痕量氧分析... 设计了一套基于临界流锐孔的动态稀释原理的痕量氧分析仪校准装置,用于痕量氧分析仪在0~1 000nmol/mol使用范围内的校准。介绍了临界流锐孔基本原理,验证了稀释装置中纯化器的性能,对稀释装置的稀释准确性进行了研究,建立了痕量氧分析仪的校准方法,实现了一次连接即可完成零点及量程点的校准,并对校准方法的示值误差进行了不确定度评定。结果表明,3个校准点示值误差的不确定度与被评定仪器的最大允许误差(±15%)之比不大于1/3,证明以稀释装置建立的校准方法对痕量氧分析仪在0~1 000 nmol/mol使用范围内的校准是合理的。该校准装置与方法可实现现场校准服务功能,为企业痕量氧分析仪的计量校准工作提供了重要的技术参考与实践依据。 展开更多
关键词 临界流锐孔 动态稀释 痕量氧分析仪 校准装置 校准方法 不确定度评定
在线阅读 下载PDF
天然气行业几种典型露点仪校准方法适应性分析
19
作者 李阳 《石油石化节能与计量》 2025年第4期57-62,共6页
天然气中的水含量,是衡量天然气质量的重要指标。在管道输送过程中,天然气水含量越高,越易在管道中形成水合物,在管道低洼处聚集,既影响输气效率,又易造成管道腐蚀。为防止天然气中的水分及水合物在天然气管输过程中产生的不利影响,越... 天然气中的水含量,是衡量天然气质量的重要指标。在管道输送过程中,天然气水含量越高,越易在管道中形成水合物,在管道低洼处聚集,既影响输气效率,又易造成管道腐蚀。为防止天然气中的水分及水合物在天然气管输过程中产生的不利影响,越来越多的输气场站安装了在线露点监测设备,常用的在线露点分析仪大部分采用阻容法、光纤法、电解法等工作原理。但目前针对该类型设备尚无相关的检定规程,仅能依据JJF 1272—2011《阻容法露点湿度计校准规范》开展校准工作。在现有的校准规范基础上,深入研究几种典型露点分析仪的校准方法,对不同型号、不同品牌、不同原理的露点分析仪的校准工作进行总结,并对工作中遇到的问题给出合理建议。 展开更多
关键词 水露点分析仪 阻容法 光纤法 电解法 校准规范 校准方法
在线阅读 下载PDF
BOD-Q水质测定仪的研制及其实验教学应用
20
作者 宋诚 王厦 刘鸿 《大学化学》 2025年第2期89-96,共8页
生化需氧量(BOD)是水污染控制领域科学研究中关键的数据指标。传统BOD基于溶氧耗量的检测方法,具有测试周期长、结果误差大、重现性差、操作复杂等问题,严重制约着水环境水生态领域的发展和实验教学的应用。本文提出一种BOD检测的新原... 生化需氧量(BOD)是水污染控制领域科学研究中关键的数据指标。传统BOD基于溶氧耗量的检测方法,具有测试周期长、结果误差大、重现性差、操作复杂等问题,严重制约着水环境水生态领域的发展和实验教学的应用。本文提出一种BOD检测的新原理、新方法、新仪器,阐述了一项原始创新科学仪器——“BOD-Q水质测定仪”的研制及其实验教学应用,结果表明,该仪器将BOD检测时间从传统的5天缩短至0.5–5小时,检测误差≤10%,将该仪器引入实验教学中可丰富教学内容,提高教学质量。 展开更多
关键词 BOD 微生物库伦法 BOD-Q水质测定仪 原始创新科学仪器 实验教学
在线阅读 下载PDF
上一页 1 2 70 下一页 到第
使用帮助 返回顶部