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Stability evaluation of the tunnel portal slope based on improved unascertained measure method
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作者 ZHANG Cengceng HUANG Shibing +1 位作者 ZHENG Luobin LI Wen 《Journal of Mountain Science》 2025年第6期2261-2275,共15页
The stability of the tunnel portal slope is crucial for ensuring safe tunnel construction.Thus,a sound stability evaluation is of significance.Given the unique geological characteristics of tunnel portal slopes,it is ... The stability of the tunnel portal slope is crucial for ensuring safe tunnel construction.Thus,a sound stability evaluation is of significance.Given the unique geological characteristics of tunnel portal slopes,it is necessary to establish a specific evaluation indicator system that differs from those used for ordinary slopes.Based on the unascertained measure method,uncertainties in the indicator are addressed by introducing the left and right half cloud asymmetric cloud model to optimize the linear membership function.The subjectivity of confidence criterion level identification is also improved by using the Euclidean distance method.Thus,a stability evaluation model for the tunnel portal slope is established based on the improved unascertained measure method.Finally,using the collected tunnel portal slope data,the results of four evaluation methods are compared with the safety factor levels.The evaluation methods include the traditional unascertained measure method,the method improved by using the left and right half cloud asymmetric cloud model,the method improved by using the Euclidean distance method,and the method improved by using both the left and right half cloud asymmetric cloud model and the Euclidean distance method.The results show that the accuracy rates of these four methods are 50%,55%,85%,and 90%,respectively.Among them,the joint improvement method has the slightest deviation,with only one level,while the other three methods had deviations of two levels.This result verifies the stability and effectiveness of the joint improvement method,providing a reference for tunnel portal slope stability evaluation. 展开更多
关键词 Tunnel portal slope Stability evaluation Improved unascertained measure method Left and right half cloud asymmetric cloud model Euclidean distance method
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Soil Bulk Density Estimation Methods: A Review 被引量:12
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作者 Ahmed Abed Gatea AL-SHAMMARY Abbas Z.KOUZANI +3 位作者 Akif KAYNAK Sui Yang KHOO Michael NORTON Will GATES 《Pedosphere》 SCIE CAS CSCD 2018年第4期581-596,共16页
Measurement of soil bulk density is important for understanding the physical, chemical, and biological properties of soil. Accurate and rapid soil bulk density measurement techniques play a significant role in agricul... Measurement of soil bulk density is important for understanding the physical, chemical, and biological properties of soil. Accurate and rapid soil bulk density measurement techniques play a significant role in agricultural experimental research. This review is a comprehensive summary of existing measurement methods and evaluates their advantages, disadvantages, potential sources of error,and directions for future development. These techniques can be broadly categorised as direct and indirect methods. Direct methods include core, clod, and excavation sampling, whereas indirect methods include the radiation and regression approaches. The core method is most widely used, but it is time consuming and difficult to use for sampling multiple soil depths. The size of the coring cylinder used, operator experience, sampling depth, and in-situ soil moisture content significantly affect its accuracy. The clod method is suitable for use with heavy clay soils, and its accuracy is dependent on equipment calibration, drying time, and operator experience, but the process is complicated and time consuming. Excavation techniques are most commonly used to evaluate the bulk density of forest soils, but have major limitations as they cannot be used in soils with large pores and their measurement accuracy is strongly influenced by soil texture and the type of analysis selected. The indirect methods appear to have greater accuracy than direct approaches, but have higher costs, are more complex, and require greater operator experience. One such approach uses gamma radiation, and its accuracy is strongly influenced by soil depth. Regression methods are economical as they can make indirect measurements, but these depend on good, quality data of soil texture and organic matter content and geographical and climatic properties. Also, like most of the other approaches, its accuracy decreases with sampling depth. 展开更多
关键词 measurement accuracy direct measurement methods gamma radiation indirect measurement methods regression methods sampling depth soil properties
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Drilling-based measuring method for the c-φ parameter of rock and its field application 被引量:8
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作者 Bei Jiang Fenglin Ma +5 位作者 Qi Wang Hongke Gao Dahu Zhai Yusong Deng Chuanjie Xu Liangdi Yao 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2024年第1期65-76,共12页
The technology of drilling tests makes it possible to obtain the strength parameter of rock accurately in situ. In this paper, a new rock cutting analysis model that considers the influence of the rock crushing zone(R... The technology of drilling tests makes it possible to obtain the strength parameter of rock accurately in situ. In this paper, a new rock cutting analysis model that considers the influence of the rock crushing zone(RCZ) is built. The formula for an ultimate cutting force is established based on the limit equilibrium principle. The relationship between digital drilling parameters(DDP) and the c-φ parameter(DDP-cφ formula, where c refers to the cohesion and φ refers to the internal friction angle) is derived, and the response of drilling parameters and cutting ratio to the strength parameters is analyzed. The drillingbased measuring method for the c-φ parameter of rock is constructed. The laboratory verification test is then completed, and the difference in results between the drilling test and the compression test is less than 6%. On this basis, in-situ rock drilling tests in a traffic tunnel and a coal mine roadway are carried out, and the strength parameters of the surrounding rock are effectively tested. The average difference ratio of the results is less than 11%, which verifies the effectiveness of the proposed method for obtaining the strength parameters based on digital drilling. This study provides methodological support for field testing of rock strength parameters. 展开更多
关键词 Digital drilling Rock crushing zone c-u parameter Measurement method Field application
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A New Method for Measurement of Local Solid Flux in Gas-Solid Two-phase Flow 被引量:8
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作者 鄂承林 卢春喜 +2 位作者 徐春明 高金森 时铭显 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2003年第6期617-621,共5页
Previous works have shown that the suction probe cannot be used to accurately measure the upward and downward particle fluxes independently. A new method using a single optical probe to measure the local solid flux is... Previous works have shown that the suction probe cannot be used to accurately measure the upward and downward particle fluxes independently. A new method using a single optical probe to measure the local solid flux is presented. The measurement of upward, downward and net solid fluxes was carried out in a cold model circulating fluidized bed (CFB) unit. The result shows that the profile of the net solid flux is in good agreement with the previous experimental data measured with a suction probe. The comparison between the average solid flux determined with the optical measuring system and the external solid flux was made, and the maximum deviationturned out to be 22%, with the average error being about 6.9%. These confirm that the optical fiber system can be successfully used to measure the upward, downward and net solid fluxes simultaneously by correctly processing the sampling signals obtained from the optical measuring system. 展开更多
关键词 fluidized bed measuring method optical fiber probe local solid flux
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A review of welding residual stress test methods 被引量:9
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作者 Gan Shiming Liu Huaying +1 位作者 Zhai Zhiping Han Yongquan 《China Welding》 CAS 2022年第2期45-55,共11页
Due to local uneven heating during the welding process,the residual stress of the structure after welding affects the reliability of it.In order to ensure the reliability,it is of great significance to test the residu... Due to local uneven heating during the welding process,the residual stress of the structure after welding affects the reliability of it.In order to ensure the reliability,it is of great significance to test the residual stress distribution of the welded joint.It has always been the focus to find a simple and feasible method for residual stress testing to quickly and accurately obtain the residual stress distribution of welded joints.The mechanical measurement method has high measurement accuracy,convenient and easy operation,but it will cause certain damage to the components.Physical measurement method can avoid damage to components,but its test cost is usually high,and its measurement accuracy can also be affected by the material microstructure characteristics of welded components.Based on the advantages and disadvantages of these two residual stress test methods,a modal test method is proposed.This method is a non-destructive measurement method.Based on the mathematical relationship between the residual stress of the welded structure and the natural frequency(mathematical model),the natural frequency is measured through the modal test to calculate the residual stress quickly.However,it is difficult to establish a mathematical model with this method,and it is not suitable for realization. 展开更多
关键词 welding residual stress mechanical measurement method physical measurement method modal test method
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An error analysis and optimization method for combined measurement with binocular vision 被引量:5
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作者 Yongkang LU Wei LIU +5 位作者 Yang ZHANG Junqing LI Weiqi LUO Yanze ZHANG Hongwen XINGb Lei ZHANG 《Chinese Journal of Aeronautics》 SCIE EI CAS CSCD 2021年第10期282-292,共11页
The accurate measurement of surfaces of large aviation components is vital for the assessment of manufacturing and assembly quality of such components.To satisfy the measurement requirement of large-size components,mo... The accurate measurement of surfaces of large aviation components is vital for the assessment of manufacturing and assembly quality of such components.To satisfy the measurement requirement of large-size components,most current researches pay more attention to combined measurement methods utilizing different measuring instruments,but the related researches on error analysis and optimization methods are not taken enough attention.This paper proposes a combined laser-assisted measurement method with feature enhancement techniques,and it also develops an error propagation model of the main factors affecting the overall measurement error in detail.Firstly,the surface of a large-size component is measured by the measurement system at multiple stations.Secondly,a control point coordinate system is established as a bridge to unify all local measurement data into the global coordinate system.To improve the overall measurement accuracy,the pixel extraction error as a key factor causing the overall measurement error is analyzed in detail.Next,the error propagation model is established,and some optimization strategies of layout for minimizing measurement error and transformation error are researched.Finally,experiments are carried out to verify the effectiveness of the proposed method.The results show that the measurement error of the proposed method reaches 0.073%and 0.14%with a 1 D standard ruler and a flat plate,respectively. 展开更多
关键词 Aviation assembly Combined measurement method Error propagation Large-size aviation component Overall optimization
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Study on Measurement Methods of Multi-Directional Waves—Wave Gauge Array Method 被引量:5
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作者 Yu Yuxiu Liu Shuxue Prof. Department of Civil Engineering, Dalian University of Technology, Dalian Assistant Researcher, Department of Civil Engineering, Dalian University of Technology, Dalian 《China Ocean Engineering》 SCIE EI 1992年第2期233-242,共10页
Measuring multi-directional waves with the wave gauge array is one of the fundamental and easily realised methods. In this paper, the wave gauge array is described and the effects of the gauge spacing, the array orien... Measuring multi-directional waves with the wave gauge array is one of the fundamental and easily realised methods. In this paper, the wave gauge array is described and the effects of the gauge spacing, the array orientations, etc. of the three array arrangements, i. e., linear array, T-type array and pentagon array, on the resolution of the directional spreading of waves, are investigated experimentally. This study can be used as a reference in the experimental study and the field measurement of directional waves. 展开更多
关键词 multi-directional waves measurement method directional spectrum wave gauge array
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Self-heating Probe Instrument and Method for Measuring High Temperature Melting Volume Change Rate of Material 被引量:2
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作者 WANG Junwei WANG Zhiping +1 位作者 LU Yang CHENG Bo 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2013年第2期371-376,共6页
The castings defects are affected by the melting volume change rate of material. The change rate has an important effect on running safety of the high temperature thermal storage chamber, too. But the characteristics ... The castings defects are affected by the melting volume change rate of material. The change rate has an important effect on running safety of the high temperature thermal storage chamber, too. But the characteristics of existing measuring installations are complex structure, troublesome operation and low precision. In order to measure the melting volume change rate of material accurately and conveniently, a self-designed measuring instrument, self-heating probe instrument, and measuring method are described. Temperature in heating cavity is controlled by PID temperature controller; melting volume change rate υ and molten density are calculated based on the melt volume which is measured by the instrument. Positive and negative υ represent expansion and shrinkage of the sample volume after melting, respectively. Taking eutectic LiF+CaF2 for example, its melting volume change rate and melting density at 1 123 K are -20.6% and 2 651 kg/m–3 measured by this instrument, which is only 0.71% smaller than literature value. Density and melting volume change rate of industry pure aluminum at 973 K and analysis pure NaCl at 1 123 K are detected by the instrument too. The measure results are agreed with report values. Measuring error sources are analyzed and several improving measures are proposed. In theory, the measuring errors of the change rate and molten density which are measured by the self-designed instrument is nearly 1/20-1/50 of that measured by the refitted mandril thermal expansion instrument. The self-designed instrument and method have the advantages of simple structure, being easy to operate, extensive applicability for material, relatively high accuracy, and most importantly, temperature and sample vapor pressure have little effect on the measurement accuracy. The presented instrument and method solve the problems of complicated structure and procedures, and large measuring errors for the samples with high vapor pressure by existing installations. 展开更多
关键词 high temperature volume expansion rate molten density measuring instrument measuring method
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Measurement methods and analysis tools for rail irregularities:a case study for urban tram track 被引量:3
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作者 Laura Chiacchiari Giuseppe Loprencipe 《Journal of Modern Transportation》 2015年第2期137-147,共11页
Rail irregularities, in particular for urban rail- way infrastructures, are one of the main causes for the generation of noise and vibrations. In addition, repetitive loading may also lead to decay of the structural e... Rail irregularities, in particular for urban rail- way infrastructures, are one of the main causes for the generation of noise and vibrations. In addition, repetitive loading may also lead to decay of the structural elements of the rolling stock. This further causes an increase in main- tenance costs and reduction of service life. Monitoring these defects on a periodic basis enables the network rail managers to apply proactive measures to limit further damage. This paper discusses the measurement methods for rail corrugation with particular regard to the analysis tools for evaluating the thresholds of acceptability in re- lation to the tramway Italian transport system. Further- more, a method of analysis has been proposed: an application of the methodology used for treating road profiles has been also utilized for the data processing of rail profilometric data. 展开更多
关键词 Rail corrugation Noise disturbance Measurement methods Continuous measurement Dataprocessing algorithm Wavebands filtering
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Scaled radar cross section measurement method for lossy targets via dynamically matching reflection coefficients in THz band 被引量:1
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作者 Shuang Pang Yang Zeng +2 位作者 Qi Yang Bin Deng Hong-Qiang Wang 《Chinese Physics B》 SCIE EI CAS CSCD 2022年第6期759-764,共6页
In the terahertz band,the dispersive characteristic of dielectric material is one of the major problems in the scaled radar cross section(RCS)measurement,which is inconsistent with the electrodynamics similitude deduc... In the terahertz band,the dispersive characteristic of dielectric material is one of the major problems in the scaled radar cross section(RCS)measurement,which is inconsistent with the electrodynamics similitude deducted according to the Maxwell’s equations.Based on the high-frequency estimation method of physical optics(PO),a scaled RCS measurement method for lossy objects is proposed through dynamically matching the reflection coefficients according to the distribution of the object facets.Simulations of the model of SLICY are conducted,and the inversed RCS of the lossy prototype is obtained using the proposed method.Comparing the inversed RCS with the calculated results,the validity of the proposed method is demonstrated.The proposed method provides an effective solution to the scaled RCS measurement for lossy objects in the THz band. 展开更多
关键词 scaled measurement method radar cross section lossy targets TERAHERTZ
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ADAPTIVE FUSION ALGORITHMS BASED ON WEIGHTED LEAST SQUARE METHOD 被引量:9
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作者 SONG Kaichen NIE Xili 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2006年第3期451-454,共4页
Weighted fusion algorithms, which can be applied in the area of multi-sensor data fusion, are advanced based on weighted least square method. A weighted fusion algorithm, in which the relationship between weight coeff... Weighted fusion algorithms, which can be applied in the area of multi-sensor data fusion, are advanced based on weighted least square method. A weighted fusion algorithm, in which the relationship between weight coefficients and measurement noise is established, is proposed by giving attention to the correlation of measurement noise. Then a simplified weighted fusion algorithm is deduced on the assumption that measurement noise is uncorrelated. In addition, an algorithm, which can adjust the weight coefficients in the simplified algorithm by making estimations of measurement noise from measurements, is presented. It is proved by emulation and experiment that the precision performance of the multi-sensor system based on these algorithms is better than that of the multi-sensor system based on other algorithms. 展开更多
关键词 Weighted least square method Data fusion Measurement noise Correlation
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An overview on observational instruments and measuring methods for dewfall 被引量:1
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作者 Qiang Zhang XiaoCui Hao +2 位作者 XiaoMei Wen Sheng Wang Jian Zeng 《Research in Cold and Arid Regions》 2011年第1期78-85,共8页
This paper systematically summarizes previous measuring methods and observational instruments for the magnitude of dewfall on land surface, analyzes the characteristics of common observational instruments for land sur... This paper systematically summarizes previous measuring methods and observational instruments for the magnitude of dewfall on land surface, analyzes the characteristics of common observational instruments for land surface dewfall, and describes several basic dewfall measurement methods. Moreover, the basic principles of these methods and instruments are interpreted, and their advantages, disadvantages, and applicability are analyzed. Recommendations for the further improvement of these observational instruments and the development of dewfall measuring methods are presented, and new technologies and scientific proposals for exploiting dewfall are elucidated. 展开更多
关键词 dewfall measuring methods observational instrument exploitation and utilization technology
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Measurement Method of the Thickness Uniformity for Polymer Films 被引量:1
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作者 YANGHong-liang RENQuan FANYun-zheng 《Semiconductor Photonics and Technology》 CAS 2003年第2期128-132,共5页
Several methods for investigating the thickness uniformity of polymer thin films are presented as well as their measurement principles. A comparison of these experimental methods is given.The cylindrical lightwave ref... Several methods for investigating the thickness uniformity of polymer thin films are presented as well as their measurement principles. A comparison of these experimental methods is given.The cylindrical lightwave reflection method is found to can obtain the thickness distribution along a certain direction.It is a simple and suitable method to evaluate the film thickness uniformity. 展开更多
关键词 Polymer complex thin films Thickness uniformity Measurement method
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A lattice measuring method based on integral imaging technology 被引量:1
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作者 ZHANG Xiao-dong LI Suo-yin +3 位作者 HAN Zhi-guo ZHAO Lin LIANG Fa-guo WU Ai-hua 《Optoelectronics Letters》 EI 2021年第5期313-316,共4页
Aiming at the problem that the lattice feature exceeds the view field of the scanning electron microscope(SEM)measuring system,a new lattice measuring method is proposed based on integral imaging technology.When the s... Aiming at the problem that the lattice feature exceeds the view field of the scanning electron microscope(SEM)measuring system,a new lattice measuring method is proposed based on integral imaging technology.When the system works,the SEM measuring system is equivalent to an integral image acquisition system.Firstly,a lattice measuring method is researched based on integral imaging theory.Secondly,the system parameters are calibrated by the VLSI lattice standard.Finally,the value of the lattice standard to be tested is determined based on the calibration parameters and the lattice measuring algorithm.The experimental results show that,compared with the traditional electron microscope measurement method,the relative error of the measured value of the algorithm is maintained within 0.2%,with the same level of measurement accuracy,but it expands the field of view of the electron microscope measurement system,which is suitable for the measurement of samples under high magnification. 展开更多
关键词 SEM IMAGE A lattice measuring method based on integral imaging technology
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TECHNOLOGY OF QUANTITATIVE ANALYSIS ON VIBRATORY STRESS RELIEF BASED ON ULTRASONIC TIME-OF-ARRIVAL METHOD 被引量:4
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作者 He Wen Ma Zhenyu Wang Xingli 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2005年第3期461-463,共3页
The effect of vibratory stress relief (VSR) is usually evaluated with the indirect method of observing the change of amplitude frequency response characteristics of structures. A new kind of evaluating method of VSR... The effect of vibratory stress relief (VSR) is usually evaluated with the indirect method of observing the change of amplitude frequency response characteristics of structures. A new kind of evaluating method of VSR based on the ultrasonic time-of-arrival method (UTM), which can obtain the residual stress directly through measuring the propagation time of ultrasonic wave in the material, is presented. At first, the principle of the measuring method of residual stress based on UTM is analyzed. Then the measuring system of the method is described, which is in virtue of ultrasonic flaw detector and high-sampling-rate digital oscillograph. And a set of calibration system that contains a piece of standard specimen is also introduced. Experimental results prove the relation between the residual stress and the propagation time of ultrasonic in workpieces. Finally, the measuring and calibration systems are applied in evaluating the effect of VSR. The final test results show that the method is effective. 展开更多
关键词 Ultrasonic time-of-arrival method Residual stress Measure Vibratory stress relief
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Research on dynamic measurement method of speckle in laser display 被引量:1
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作者 LIU Hong LIU Yaning ZHANG Xiaoyu 《Optoelectronics Letters》 EI 2024年第6期360-366,共7页
Laser display technology is the most promising display technology in the market and is widely used in many fields. However, laser speckle has been troubling the application and expansion of this technology in some fie... Laser display technology is the most promising display technology in the market and is widely used in many fields. However, laser speckle has been troubling the application and expansion of this technology in some fields. In order to better evaluate the speckle, speckle measurement methods must be studied. In this study, a dynamic measurement method for laser speckles is proposed according to the optical superposition characteristics of speckle, which can reduce the influence of non-coherent factors on the speckle measurement results. The feasibility of the dynamic speckle measurement method is verified by designing an experimental scheme. 展开更多
关键词 Research on dynamic measurement method of speckle in laser display
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Reliability of gas holdup measurements using the differential pressure method in a cyclone-static micro-bubble flotation column 被引量:1
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作者 Xia Wencheng Yang Jianguo Wang Yuling 《Mining Science and Technology》 EI CAS 2011年第6期797-801,共5页
Gas holdup is one of the key parameters in flotation process. Gas holdup as measured by a differential pressure method was investigated and the relative errors compared to the average gas holdup from the volume expans... Gas holdup is one of the key parameters in flotation process. Gas holdup as measured by a differential pressure method was investigated and the relative errors compared to the average gas holdup from the volume expansion method. The errors were used to establish optimum measurement positions. The results show that the measurement position should be in the middle of the column and in the region half way from the center to the wall (the half-radius). The gas holdup along the axial direction is lower at the bottom and higher at the top of the floatation column. The gas holdup along the radial direction is lower near the wall and higher near the center of the flotation column. The average gas holdup measure- ment can be replaced by regional gas holdup values. 展开更多
关键词 Gas holdup distribution Differential pressure method Measurement positions Axial direction Radial direction
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Establishment of a Static Model Based on Measured Heat Loss for COREX Process
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作者 Wei SHEN Sheng-li WU +2 位作者 Ming-yin KOU Kai-ping DU Ying SUN 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2015年第3期200-206,共7页
The heat loss and its,distribution are of great importance for the calculation and simulation of COREX process. Based on Baosteel COREX process, a method was applied to measure the heat loss of the furnace shell, the ... The heat loss and its,distribution are of great importance for the calculation and simulation of COREX process. Based on Baosteel COREX process, a method was applied to measure the heat loss of the furnace shell, the accessory equipments and the cooling water system. Then, a static model was established based on the measured heat loss of COREX process. The results showed that the main heat loss of furnace shells took place at the dome of the COREX melter-gasifier and the reducing gas entrance position of the shaft furnace while the main heat loss caused by cooling water occurred at the tap hole area. And the heat loss caused by cooling water accounts for about 85% of the total heat loss in COREX process. The measured total heat loss for producing every 1 t hot metal was 542. 164 MJ, which accounted for about 92 % of the theoretical total heat loss. 展开更多
关键词 COREX process heat loss heat loss distribution static model measurement method
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Analysis and Application of the Synthetic Relative Measuring Method in On-Line Monitoring for Capacitive Equipment in Power Systems
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作者 Qing Guo Li-Jun Qin Hua-Wei Jin 《Journal of Electronic Science and Technology》 CAS 2011年第3期270-277,共8页
On-line measurement for dielectric loss angle can effectively monitor the insulation condition of capacitive equipment in power systems. Synthetic relative measuring methods not only markedly overcome the shortcomings... On-line measurement for dielectric loss angle can effectively monitor the insulation condition of capacitive equipment in power systems. Synthetic relative measuring methods not only markedly overcome the shortcomings of traditional absolute measuring methods but also greatly improve the accuracy of dielectric loss angle measurement. However, synthetic relative measuring methods based on two or three pieces of capacitive equipment do not have the characteristic of generality. In this paper, a principle of synthetic relative measuring method is presented. The example of application for synthetic relative methods based on three and four pieces of capacitive equipment running in the same phase is taken to present the failure judgment matrices for N pieces of equipment. According to these matrices, the fault condition of N pieces of capacitive equipment can be watched, which is more general. Then some problems needing to be concerned along with two diagnostic methods used in diagnostic system are introduced. Finally, two programmable flow charts for the two methods are given and corresponding examples demonstrate their feasibility in practice. 展开更多
关键词 Index Terms-Capacitive equipment dielectric loss angle on-line monitoring synthetic relative measuring method failure judgment matrix.
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Measuring methods for three kinds of polyhydroxyalkanoates from activated sludge by gas chromatography
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作者 陈玮 陈志强 +2 位作者 吕炳南 温沁雪 张运海 《Journal of Harbin Institute of Technology(New Series)》 EI CAS 2011年第5期113-118,共6页
Gas chromatography determination of polyhydroxyalkanoates has been common;however,the pretreatment steps are often complex,and gas chromatography operation conditions are not given in detail.In this study,gas chromato... Gas chromatography determination of polyhydroxyalkanoates has been common;however,the pretreatment steps are often complex,and gas chromatography operation conditions are not given in detail.In this study,gas chromatography is used for analyzing PHB,PHV and PH2MV,three majors of PHAs in activated sludge.The sample was centrifuged at a speed of 4000 r/min for the separation of floc and supernatant,freezen,and dried for 12 h in vacuum freezing drier;and then transferred to the fridge for freezing to ice and drying for 12 h in vacuum freezing drier;then chloroform and a simple composition digestion solution including methanol,sulfuric acid and benzoic acid was added;digested at 105 ℃ for 6 h;cooled to room temperature,the lower solution of the result can be used for analyzing.Samples were analyzed by gas chromatography with FID detector and auto sampler;the standard curve of standard material shows an excellent linear relationship with correlation coefficients larger than 0.99;the relative standard deviation (RSD) of sludge samples is less than 1%.The recovery rates of each sample are between 95%-105%.The GC analysis time of each PHA sample is shorter than 10 minutes. 展开更多
关键词 POLYHYDROXYALKANOATES activated sludge gas chromatography measuring method
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