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Analysis of Orange Peel Defect in St14 Steel Sheet by Electron Backscattered Diffraction (EBSD) 被引量:7
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作者 ShengquanCAO JinxuZHANG +1 位作者 JianshengWU JiaguangCHEN 《Journal of Materials Science & Technology》 SCIE EI CAS CSCD 2005年第1期17-20,共4页
In this paper, the orange peel defect in the surface range of the st14 steel sheet has been investigated using the electron backscattered diffraction (EBSD) technique. It has been found that the orange peel defect in ... In this paper, the orange peel defect in the surface range of the st14 steel sheet has been investigated using the electron backscattered diffraction (EBSD) technique. It has been found that the orange peel defect in the st14 steel sheet was resulted from the local coarse grains which were produced during hot-rolling due to the critical deformation in dual-phase zone. During deep drawing, the coarse grains with {100}<001> microtexture can slip on the {112}<111> slip system to form bulging and yields orange peel defects, while the coarse grains with {112}<110> orientation do not form the defect as the Schmid factor of {112}<111> slip system in it equals zero. 展开更多
关键词 electron backscattered diffraction (EBSD) Orange peel defect Stl4 steel MICROTEXTURE
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Detection of Coaxial Backscattered Electrons in SEM 被引量:5
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作者 JIANG Chang-zhong REN Da-zhi (Department of Physics, Wuhan University, Wuhan 430072, China) 《Wuhan University Journal of Natural Sciences》 CAS 2000年第1期41-44,共4页
We present a coaxial detection of the backscattered electrons in SEM. The lens-aperture has been used to filter in energy and focus the backscattered electrons. This particular geometry allows us to eliminate the low ... We present a coaxial detection of the backscattered electrons in SEM. The lens-aperture has been used to filter in energy and focus the backscattered electrons. This particular geometry allows us to eliminate the low energy backscattered electrons and collect the backscattered electrons, which are backscattered close to the incident beam orientation. The main advantage of this geometry is adapted to topographic contrast attenuation and atomic number contrast enhancement. Thus this new SEM is very suitable to analyze the material composition. 展开更多
关键词 scanning electron microscopy backscattered electrons coaxial detection
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A MONTE CARLO SIMULATION OF SECONDARY ELECTRON AND BACKSCATTERED ELECTRON IMAGES IN SCANNING ELECTRON MICROSCOPY 被引量:1
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作者 H.M.Li Z.J.Ding 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2005年第3期351-355,共5页
A new parallel Monte Carlo simulation method of secondary electron (SE) and back scattered electron images (BSE) of scanning electron microscopy (SEM) for a com plex geometric structure has been developed. This paper ... A new parallel Monte Carlo simulation method of secondary electron (SE) and back scattered electron images (BSE) of scanning electron microscopy (SEM) for a com plex geometric structure has been developed. This paper describes briefly the si mulation method and the modification to the conventional sampling method for the step length. Example simulation results have been obtained for several artifici al structures. 展开更多
关键词 Monte Carlo SEM secondary electrons backscattered electrons
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Analysis of retained austenite in TRIP590 steel by electron backscattered diffraction method 被引量:1
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作者 Yu-cheng Zhang Yang Meng +4 位作者 Gui-bin Cui Hui-ping Jia Xin-hua Ju Zhong-hang Jiang Ze-jun Ma 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2020年第3期355-365,共11页
The retained austenite content in TRIP590 steel was first measured by X-ray diffraction(XRD)method.Then,the effect of different test parameters(indexing rate,step size,field number,etc.)on the measured results of reta... The retained austenite content in TRIP590 steel was first measured by X-ray diffraction(XRD)method.Then,the effect of different test parameters(indexing rate,step size,field number,etc.)on the measured results of retained austenite content in TRIP590 steel by electron backscattered diffraction(EBSD)method was studied.By comparing the measured results between XRD and EBSD method,the optimal test parameters for the analysis of retained austenite content using EBSD were determined.Finally,the total content of retained austenite and the retained austenite contents with different aspect ratios in TRIP590 steel were analyzed,respectively.The results showed that the test parameters have a great influence on the measured results of retained austenite content in TRIP590 steel.In order to improve the test accuracy,high indexing rates,small step sizes and more field number are necessary for the analysis of retained austenite content in TRIP590 steel by EBSD method. 展开更多
关键词 TRIP590 STEEL RETAINED AUSTENITE electron backscattered DIFFRACTION INDEXING rate Step size
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In situ backscattered electron imaging study of the effect of annealing on the deformation behaviors of Ni electroformed from additive-free and saccharin-containing sulfamate solutions
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作者 Kai Jiang Hiroaki Nakano +2 位作者 Satoshi Oue Tatsuya Morikawa Wen-huai Tian 《International Journal of Minerals,Metallurgy and Materials》 SCIE EI CAS CSCD 2019年第1期114-123,共10页
The Ni samples were electroformed from additive-free(AF) and saccharin-containing(SC) sulfamate solutions, respectively. In situ backscattered electron(BSE) imaging, electron backscatter diffraction(EBSD), and electro... The Ni samples were electroformed from additive-free(AF) and saccharin-containing(SC) sulfamate solutions, respectively. In situ backscattered electron(BSE) imaging, electron backscatter diffraction(EBSD), and electron-probe microanalysis(EPMA) were used to investigate the effect of annealing on the deformation behaviors of the AF and SC samples. The results indicate that columnar grains of the as-deposited AF sample had an approximated average width of 3 μm and an approximated aspect ratio of 8. The average width of columnar grains of the as-deposited SC sample was reduced to approximately 400 nm by the addition of saccharin to the electrolyte. A few very-large grains distributed in the matrix of the SC sample after annealing. No direct evidence indicated that S segregated at the grain boundaries before or after annealing. The average value of the total elongations of the SC samples decreased from 16% to 6% after annealing, whereas that of the AF samples increased from 18% to 50%. The dislocation recovery in grain-boundary areas of the annealed AF sample was reduced, which contributed to the appearance of microvoids at the triple junctions. The incompatibility deformation between very-large grains and fine grains contributed to the brittle fracture behavior of the annealed SC Ni. 展开更多
关键词 backscattered electron imaging ANNEALING electroformed NI SULFAMATE solution deformation BEHAVIORS
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Quasi-in situ electron backscatter diffraction analysis of twinning±detwinning behavior in AZ31 magnesium-alloy rolled plates subjected to compression loading in different directions
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作者 Le Zhou Guiyuan Ren +5 位作者 Tianqi Huang Zhi Wang Feng Wang Ziqi Wei Pingli Mao Zheng Liu 《Journal of Magnesium and Alloys》 2025年第5期2358-2373,共16页
In this study,the twinning-detwinning behavior and slip behavior of rolled AZ31 magnesium-alloy plates during a three-step intermittent dynamic compression process along the rolling direction(RD)and normal direction(N... In this study,the twinning-detwinning behavior and slip behavior of rolled AZ31 magnesium-alloy plates during a three-step intermittent dynamic compression process along the rolling direction(RD)and normal direction(ND),are investigated via quasi-in situ electron backscatter diffraction,and the causes of the twinning and detwinning behavior are explained according to Schmid law,local strain coordination,and slip trajectories.It is found that the twins are first nucleated and grow at a compressive strain of 3%along the RD.In addition to the Schmid factor(SF),the strain coordination factor(m’)also influences the selection of the twin variants during the twinning process,resulting in the nucleation of twins with a low SF.During the second and third steps of the application of continuous compressive strains with magnitudes and directions of 3%RD+3%ND and 3%RD+3%ND+2.5%ND,detwinning occurs to different extents.The observation of the detwinning behavior reveals that the order in which multiple twins within the same grain undergo complete detwinning is related to Schmid law and the strain concentration,with a low SF and a high strain concentration promoting complete detwinning.The interaction between slip dislocations and twin boundaries in the deformed grains as well as the pinning of dislocations at the tips of the {1012} tensile twins with a special structure result in incomplete detwinning.Understanding the microstructural evolution and twinning behavior of magnesium alloys under different deformation geometries is important for the development of high-strength and high-toughness magnesium alloys. 展开更多
关键词 Quasi-in situ electron backscatter diffraction Twinning and detwinning Schmid law Strain coordination
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ENERGY DISTRIBUTION OF BACKSCATTERED ELECTRONS FROM HEAVY METALS
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作者 K. Salma 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2005年第3期345-350,共6页
The full energy distribution of backscattered electrons from the elastic peak do wn to the true-secondary electron peak for heavy metals, Ta, W, Pt and Au, in Au ger electron spectroscopy in the EN(E) mode has been st... The full energy distribution of backscattered electrons from the elastic peak do wn to the true-secondary electron peak for heavy metals, Ta, W, Pt and Au, in Au ger electron spectroscopy in the EN(E) mode has been studied with a Monte Carlo simulation method, which includes cascade-secondary-electron production. The sim ulation model is based on the use of a dielectric function for describing inelas tic scattering and secondary excitation, and on the use of Mott cross sections f or elastic scattering. A systematic comparison between the calculated and experi mental spectra measured with a cylindrical mirror analyzer has been made for pri mary energies ranging from 1 to 5keV. Excellent agreement was obtained for these heavy metals on the backscattering background at primary energies in the keV re gion. A significant contribution of cascade secondary electrons to the measured spectra on the low-energy side was found. 展开更多
关键词 backscattered electrons Monte Carlo AES heavy metal
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Simulation of Secondary Electron and Backscattered Electron Emission in A6 Relativistic Magnetron Driven by Different Cathode
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作者 刘美琴 李博轮 +2 位作者 刘纯亮 Fuks MIKHAIL Edl SCHAMILOGLU 《Plasma Science and Technology》 SCIE EI CAS CSCD 2015年第1期64-70,共7页
Prticle-in-cell(PIC) simulations demonstrated that,when the relativistic magnetron with diffraction output(MDO) is applied with a 410 kV voltage pulse,or when the relativistic magnetron with radial output is appli... Prticle-in-cell(PIC) simulations demonstrated that,when the relativistic magnetron with diffraction output(MDO) is applied with a 410 kV voltage pulse,or when the relativistic magnetron with radial output is applied with a 350 kV voltage pulse,electrons emitted from the cathode with high energy will strike the anode block wall.The emitted secondary electrons and backscattered electrons affect the interaction between electrons and RF fields induced by the operating modes,which decreases the output power in the radial output relativistic magnetron by about 15%(10%for the axial output relativistic magnetron),decreases the anode current by about 5%(5%for the axial output relativistic magnetron),and leads to a decrease of electronic efficiency by 8%(6%for the axial output relativistic magnetron).The peak value of the current formed by secondary and backscattered current equals nearly half of the amplitude of the anode current,which may help the growth of parasitic modes when the applied magnetic field is near the critical magnetic field separating neighboring modes.Thus,mode competition becomes more serious. 展开更多
关键词 secondary electron and backscattered electron emission relativistic magnetron mode competition critical magnetic field output power anode current electronic efficiency transparent cathode solid cathode
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Crystallographic Characteristic of Intermetallic Compounds in Al-Si-Mg Casting Alloys Using Electron Backscatter Diffraction 被引量:2
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作者 ZOU Yongzhi XU Zhengbing +1 位作者 HE Juan ZENG Jianmin 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2010年第3期305-311,共7页
The Al-Si-Mg alloy which can be strengthened by heat treatment is widely applied to the key components of aerospace and aeronautics. Iron-rich intermetallic compounds are well known to be strongly influential on mecha... The Al-Si-Mg alloy which can be strengthened by heat treatment is widely applied to the key components of aerospace and aeronautics. Iron-rich intermetallic compounds are well known to be strongly influential on mechanical properties in Al-Si-Mg alloys. But intermetallic compounds in cast Al-Si-Mg alloy intermetallics are often misidentified in previous metallurgical studies. It was described as many different compounds, such as AlFeSi, Al8Fe2Si, Al5(Fe, Mn)3Si2 and so on. For the purpose of solving this problem, the intermetallic compounds in cast Al-Si alloys containing 0.5% Mg were investigated in this study. The iron-rich compounds in Al-Si-Mg casting alloys were characterized by optical microscope(OM), scanning electron microscope(SEM), energy dispersive X-ray spectrometer(EDS), electron backscatter diffraction(EBSD) and X-ray powder diffraction(XRD). The electron backscatter diffraction patterns were used to assess the crystallographic characteristics of intermetallic compounds. The compound which contains Fe/Mg-rich particles with coarse morphologies was Al8FeMg3Si6 in the alloy by using EBSD. The compound belongs to hexagonal system, space group P6_2m, with the lattice parameter a=0.662 nm, c=0.792 nm. The β-phase is indexed as tetragonal Al3FeSi2, space group I4/mcm, a=0.607 nm and c=0.950 nm. The XRD data indicate that Al8FeMg3Si6 and Al3FeSi2 are present in the microstructure of Al-7Si-Mg alloy, which confirms the identification result of EBSD. The present study identified the iron-rich compound in Al-Si-Mg alloy, which provides a reliable method to identify the intermetallic compounds in short time in Al-Si-Mg alloy. Study results are helpful for identification of complex compounds in alloys. 展开更多
关键词 Al-Si-Mg alloys intermetallic compound electron backscatter diffraction(EBSD) X-ray powder diffraction(XRD)
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Modelling of electron energy absorption and backscattering during EBW 被引量:1
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作者 Fang Yuchao Yang Ziyou +1 位作者 Dong Shulei He Jingshan 《China Welding》 EI CAS 2020年第1期26-36,共11页
A three-dimensional heat flux model for deep-penetrating electron beam welding(EBW)is established to mathematically describe the physical heat generation process during interaction between electrons and the dynamic mo... A three-dimensional heat flux model for deep-penetrating electron beam welding(EBW)is established to mathematically describe the physical heat generation process during interaction between electrons and the dynamic molten pool free surface.Monte Carlo method is used to determine the electron-target interaction,and random distribution of initial electrons,progressive trajectory tracing and electron backscattering models are used to describe the spatial distribution of electrons absorption.The model is verified in preset keyholes and applied in the simulation on electron beam welding process,and the calculated bead shape shows a good consistency with experimental results. 展开更多
关键词 Heat source model electron beam RANDOMNESS backscattERING KEYHOLE
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In Situ Electron Backscatter Diff raction Analysis for Microstructure Evolution and Deformation Models of Mg–Ce Alloy During Uniaxial Loading
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作者 Fang-Wei Jiao Li Jin +1 位作者 Jie Dong Feng-Hua Wang 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2019年第2期263-268,共6页
Previous studies showed that signifi cant increases in elongation in Mg–Ce alloys due to the Ce addition and the solute drag eff ect by Ce addition were ascribed to the non-basal dislocation slip activating and the t... Previous studies showed that signifi cant increases in elongation in Mg–Ce alloys due to the Ce addition and the solute drag eff ect by Ce addition were ascribed to the non-basal dislocation slip activating and the texture altering. The microstructure evolution and deformation models of extruded Mg-0.5 wt%Ce alloy rods under uniaxial tension have been studied using in situ electron backscatter diff raction. The basal and non-basal slips were characterized by using slip line trace analysis. The results provide evidence for that pyramidal slip activated during deformation, besides basal slip and extension twinning, which contributes to the texture weakening and ductility increasing in Mg-0.5 wt%Ce alloy. 展开更多
关键词 Texture Non-basal SLIP TWINNING In SITU electron backscattered diff raction(EBSD) Trace ANALYSIS
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An Algorithm to Analyze Electron Backscatter Diffraction Data for Grain Reconstruction:from Methodology to Application
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作者 Xue-Hao Zheng Hong-Wang Zhang 《Acta Metallurgica Sinica(English Letters)》 SCIE EI CAS CSCD 2016年第5期491-499,共9页
An algorithm for grain reconstruction based on electron backscatter diffraction data was proposed in this paper. This algorithm can well record the original data arrangement when an external file for the reconstructed... An algorithm for grain reconstruction based on electron backscatter diffraction data was proposed in this paper. This algorithm can well record the original data arrangement when an external file for the reconstructed grain(s) was exported for further post-processing. Assisted by an in-house MATLAB program, grain reconstruction, lattice rotations, orientation spreads, and slip system analysis can be performed. The validity of this algorithm has been successfully tested by polycrystalline Ni before and after channel die compression. 展开更多
关键词 Grain reconstruction ALGORITHM electron backscatter diffraction DEFORMATION Nickle
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Crystallographic analysis of lath martensite in a 13Cr-5Ni steel by electron backscattering diffraction
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作者 Wen-bo Liu Peng-cheng Song +3 位作者 Chi Zhang Di Yun Chun-fa Yao Zhi-gang Yang 《Journal of Iron and Steel Research International》 SCIE EI CAS CSCD 2018年第2期213-220,共8页
Morphology observation and crystallographic analysis of lath martensite in 13Cr-5Ni steel were investigated by electron backscattering diffraction (EBSD) in a scanning electron microscope. The pole figures of the mi... Morphology observation and crystallographic analysis of lath martensite in 13Cr-5Ni steel were investigated by electron backscattering diffraction (EBSD) in a scanning electron microscope. The pole figures of the microstructure measured by EBSD showed that the martensite in this steel held the Kurdjumov-Sachs (K-S) orientation relationship, and the boundary misorientations after the austenite-martensite transformation were also analyzed. However, not all the 24 possible variants in the K-S relationship were observed in a single prior austenite grain. Sub-blocks with special combinations were observed, which can be explained by the minimization of the total shape strain between the adjacent variants introduced during the martensite transformation and relatively low carbon content in the 13Cr-5Ni steel. 展开更多
关键词 electron backscattering diffraction Martensite transformation Boundary misorientation Orientationrelationship
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Monte Carlo Simulation of the Coaxial Electrons Backscattering from Thin Films
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作者 Hu Da-ping School of Management, Huazhong University of Science and Technology, Wuhan 430074, Hubei, China 《Wuhan University Journal of Natural Sciences》 CAS 2002年第2期203-206,共4页
By using the Monte Carlo method, we simulated the trajectories of coaxial backscattering electrons corresponding to a new type of scanning electron microscope. From the calculated results, we obtain a universal expres... By using the Monte Carlo method, we simulated the trajectories of coaxial backscattering electrons corresponding to a new type of scanning electron microscope. From the calculated results, we obtain a universal expression, which describes with good accuracy the backscattering coefficient versus film thickness under all conditions used. By measuring the coaxial backscattering coefficient and using this universal formula, the thickness of thin films can be determined if the composition is known. 展开更多
关键词 Monte Carlo simulation coaxial backscattered electrons thin film scanning electron microscope
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电子背散射衍射技术及其在镁合金研究中的应用
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作者 商景利 杨伟 《江西冶金》 2026年第1期36-54,共19页
电子背散射衍射(EBSD)技术能够对晶体材料进行快速、大范围的定点取向分析,已成为继电镜技术和X射线衍射技术之后的又一项重要的材料表征技术,在材料研究领域的应用日益广泛。镁及其合金具有轻质、储氢密度高、生物力学相容性好、可降... 电子背散射衍射(EBSD)技术能够对晶体材料进行快速、大范围的定点取向分析,已成为继电镜技术和X射线衍射技术之后的又一项重要的材料表征技术,在材料研究领域的应用日益广泛。镁及其合金具有轻质、储氢密度高、生物力学相容性好、可降解等特点,在结构材料和功能材料领域均展现出广阔的应用前景。金属镁具有密排六方晶体结构,镁合金产品易形成特定织构并表现为各向异性,这些特性均与多晶镁内部各晶粒取向有关。本文系统阐述了EBSD技术的工作原理和样品制备方法,重点梳理了EBSD结果呈现方式及数据深度分析方法,并总结了EBSD技术的研究进展和应用现状。同时,结合具体实例,归纳了EBSD技术在镁合金组织基础表征、孪生行为分析、再结晶行为研究等方面的应用,并探讨了其应用过程中存在的问题。最后,对EBSD技术未来的发展趋势进行了展望。 展开更多
关键词 电子背散射衍射 镁合金 取向 织构
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Design of an efficient collector for the HIAF electron cooling system 被引量:5
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作者 Mei-Tang Tang Li-Jun Mao +9 位作者 Hai-Jiao Lu Li-Xia Zhao Jie Li Xiao-Ping Sha Fu Ma Yun-Bin Zhou Kai-Min Yan Xiao-Ming Ma Xiao-Dong Yang Jian-Cheng Yang 《Nuclear Science and Techniques》 SCIE EI CAS CSCD 2021年第10期39-49,共11页
A collector with high perveance,efficient recu-peration,and low secondary emissions is required for the 450-keV electron cooler in the HIAF accelerator complex.To optimize the collection efficiency of the collector,a ... A collector with high perveance,efficient recu-peration,and low secondary emissions is required for the 450-keV electron cooler in the HIAF accelerator complex.To optimize the collection efficiency of the collector,a simulation program,based on the Monte Carlo simulations,was developed in the world’s first attempt to calculate the electron collection efficiency.In this program,the backscattering electrons and secondary electrons generated on the collector surface are calculated using a Monte Carlo approach,and all electron trajectories in the collector region are tracked by the Runge–Kutta method.In this paper,the features and structure of our program are described.The backscattering electron yields,with various collector surface materials,are calculated using our pro-gram.Moreover,the collector efficiencies for various col-lector structures and electromagnetic fields are simulated and optimized.The measurement results of the collection efficiency of the HIAF collector prototype and the CSRm synchrotron are also reported.These experimental results were in good agreement with the simulation results of our program. 展开更多
关键词 electron cooler Secondary electron backscattering electron Monte Carlo method Dielectric function
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热处理态X80钢韧性不均匀问题分析 被引量:1
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作者 牛靖 周海斌 +4 位作者 魏可嘉 程俊 王鹏 黄铎 刘迎来 《热加工工艺》 北大核心 2025年第6期38-41,47,共5页
为了解决热处理态X80管线钢韧性不均匀问题,选择典型冲击试样进行了断口分析、微观组织及背散射电子衍射分析。结果表明,微观组织不均匀性,存在大块状准多边形铁素体,导致大角度晶界含量低,有效晶粒尺寸大且均匀性差,是热处理态X80钢部... 为了解决热处理态X80管线钢韧性不均匀问题,选择典型冲击试样进行了断口分析、微观组织及背散射电子衍射分析。结果表明,微观组织不均匀性,存在大块状准多边形铁素体,导致大角度晶界含量低,有效晶粒尺寸大且均匀性差,是热处理态X80钢部分冲击试样发生解理脆断的根本原因。设法获得细小的准多边形铁素体可以提高X80中的大角度晶界含量,细化有效晶粒尺寸,可以兼顾热处理态X80钢的强韧性。 展开更多
关键词 X80管线钢 冲击韧性 背散射电子衍射 有效晶粒尺寸
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高应变率下氢对18CrNiMo7-6合金钢力学性能的影响
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作者 王刚 张明 +3 位作者 佟阳 厉灿 陈增涛 李凌霄 《钢铁》 北大核心 2025年第8期203-214,共12页
氢脆是高强钢在氢环境中服役失效的关键诱因,其作用机制与应变速率密切相关。通过分离式霍普金森压杆(split Hopkinson pressure bar,SHPB)试验结合电化学充氢技术,系统研究了在高应变速率(400~2700 s^(-1))下氢对18CrNiMo7-6合金钢动... 氢脆是高强钢在氢环境中服役失效的关键诱因,其作用机制与应变速率密切相关。通过分离式霍普金森压杆(split Hopkinson pressure bar,SHPB)试验结合电化学充氢技术,系统研究了在高应变速率(400~2700 s^(-1))下氢对18CrNiMo7-6合金钢动态力学性能与微观组织的影响,并揭示了其作用机制。试验结果表明,18CrNiMo7-6合金钢在高应变速率下表现出显著的应变率强化效应,应变速率从400 s^(-1)增至2700 s^(-1)时,屈服强度提升107.72%,塑性流动应变增加387.88%。微观分析表明,高应变速率促使小角度晶界比例上升、晶粒细化,同时几何必须位错(geometrically necessary discocation,GND)密度显著增加,小角度晶界、细晶粒、GND共同形成多尺度障碍网络,显著提高位错运动阻力,使18CrNiMo7-6合金钢表现出应变率强化效应。氢对18CrNiMo7-6合金钢力学性能的影响呈现应变速率依赖性,即在应变速率为400~1100 s^(-1)时,氢导致动态屈服强度提高,但塑性损失显著;而在应变速率为1900~2700 s^(-1)时,氢会使强度降低,塑性损失趋近于0。通过EBSD分析揭示了氢与应变速率耦合作用下18CrNiMo7-6合金钢的变形机制。氢降低了小角度晶界比例,加剧了局部应变集中,并提高了GND密度。提出在高应变速率下氢通过钉扎位错运动加重局部塑性变形,但应变速率升高会削弱氢对位错运动的钉扎效应。结果为高应变速率下氢对18CrNiMo7-6合金钢性能的影响提供了新的试验依据与理论解释,对优化其在极端工况下的应用具有重要参考价值。 展开更多
关键词 高应变率 18CrNiMo7-6合金钢 氢脆 霍普金森压杆 电子背散衍射 动态冲击 位错运动 氢与应变速率耦合作用
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中国药典2025年版扫描电子显微镜法技术解读 被引量:1
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作者 陈超 王妍 +5 位作者 訾晓伟 章蔼静 戴寿沣 张传杰 史沛 陈雪帆 《中国现代应用药学》 北大核心 2025年第20期3512-3522,共11页
目的解读中国药典2025年版中新增的“扫描电子显微镜法”(以下简称扫描电镜法),为标准的实施提供帮助,为药品检测提供科学依据。方法通过对不同国家药典标准进行比较,介绍中国药典中扫描电镜法的增订概况,系统阐述了该方法的制定背景、... 目的解读中国药典2025年版中新增的“扫描电子显微镜法”(以下简称扫描电镜法),为标准的实施提供帮助,为药品检测提供科学依据。方法通过对不同国家药典标准进行比较,介绍中国药典中扫描电镜法的增订概况,系统阐述了该方法的制定背景、技术特点和实施要点,同时结合药品检测的实际案例,探讨了方法的具体应用。结果中国药典2025年版中新增的扫描电镜法为药品检测提供了更为精确、高效的技术手段。该方法能够直观展现药品表面的微观形貌,准确分析药品的成分和元素组成,进行结晶学分析,从而有效提升了药品检测的准确性和科学性。结论中国药典2025年版新增的“扫描电子显微镜法”具有重要的应用价值,不仅为药品质量控制提供了有力的技术支撑,还为药品研发的创新发展注入了新的活力。 展开更多
关键词 扫描电子显微镜 中国药典 二次电子 背散射电子 X射线能谱 美国药典 欧洲药典
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晶体塑性变形机理及其数值模拟方法的研究进展 被引量:1
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作者 赵帅 王素娟 《制造技术与机床》 北大核心 2025年第2期99-107,共9页
对晶体塑性有限元数值模拟的应用状况进行了研究,描述了晶体塑性理论、晶体塑性变形机理、硬化机制等算法。同时关注了电子背散射衍射(electron backscatter diffraction,EBSD)技术在晶体学织构测量与分析中的应用优势,采用衍射图案准... 对晶体塑性有限元数值模拟的应用状况进行了研究,描述了晶体塑性理论、晶体塑性变形机理、硬化机制等算法。同时关注了电子背散射衍射(electron backscatter diffraction,EBSD)技术在晶体学织构测量与分析中的应用优势,采用衍射图案准确掌握晶体结构与取向等信息,为晶体塑性有限元数值模拟提供精确的数据输入。因此,对现有的晶体塑性理论、参数获取方式、衍射图像分析方法进行了总结。目前,晶体塑性有限元数值模拟经过大量的检验,证明了该方法在模拟金属塑性变形机理中的有效性,并广泛应用于探究材料塑性变形机理的研究中。依据系统的晶体塑性有限元数值模拟研究框架开展论述,以期全面了解晶体塑性有限元在加工中的研究进展,为高性能材料设计、优化和实际应用提供新的思路。 展开更多
关键词 电子背散射衍射 塑性变形机理 晶体塑性理论 晶体塑性有限元 晶体织构
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