The precipitation of secondary Laves phases and its effect on notch sensitivity are systematically studied in Thermo-Span alloy. The results show that the precipitation peak temperature of secondary Laves phases is 9...The precipitation of secondary Laves phases and its effect on notch sensitivity are systematically studied in Thermo-Span alloy. The results show that the precipitation peak temperature of secondary Laves phases is 925 ℃. Below 925 ℃, the volume fraction of secondary Laves phases increases with the rise of the temperature, and its morphology changes from granular to thin-film;above 925 ℃, the volume fraction of secondary Laves phases shows an opposite trend to temperature, and its morphology changes from thin-film to granular. A detailed explanation through linear density (ρ) is provided that the influence of secondary Laves phases at the grain boundaries (GBs) on notch sensitivity depends on the coupling competition effect of their size, quantity, and morphology. Notably, the granular Laves phases are more beneficial to improving the notch sensitivity of the alloy compared with thin-film Laves phases. Granular secondary Laves phases can promote the formation of γ′ phases depletion zone to improve the ability of GBs to accommodate high strain localization, and effectively inhibit the crack initiation and propagation.展开更多
Inconel 718 superalloys deposited by laser solid forming （LSF） were heat treated with solution treatment,intermediate heat treatment （IHT） and two-stage aging treatment in sequence （SITA heat treatment）.The effe...Inconel 718 superalloys deposited by laser solid forming （LSF） were heat treated with solution treatment,intermediate heat treatment （IHT） and two-stage aging treatment in sequence （SITA heat treatment）.The effect of IHT temperature on microstructure,tensile property and notch sensitivity of LSFed Inconel 718 superalloy at 500 ℃ were investigated.As-deposited columnar grains have transformed to equiaxed grains and the grains were refined due to the recrystallization during the SITA heat treatment.It is found that the size and amount of δ phase dispersed at grain boundaries decreased with the increasing of IHT temperature,and δ phase disappeared when the IHT temperature reached 1 020 ℃.The ultimate tensile strength （UTS） and yield strength （YS） of smooth samples increased to a maximum when the IHT temperature reached 980 ℃ and then decreased slightly to a minimum when the IHT temperature was 1 000 ℃,and followed by slight increasing again till the IHT temperature reached 1 020 ℃,resulted from the competition of precipitation strengthening effect of γ″ and γ＇ phase and the grain boundary weakening effect caused by the gradual disappearance of δ phase with increasing the IHT temperature.The notch sensitivity factor （qe） decreased but still greater than 1 as the IHT temperature increased,which is attributed to the decrease of the size and amount of δ precipitation.展开更多
It is well known that metallic materials exhibit worse fatigue damage tolerance as they behave stronger in strength and softer in modulus. This raises concern on the long term safety of the recently developed biomecha...It is well known that metallic materials exhibit worse fatigue damage tolerance as they behave stronger in strength and softer in modulus. This raises concern on the long term safety of the recently developed biomechanical compatible titanium alloys with high strength and low modulus. Here we demonstrate via a model alloy, Ti-24 Nb-4 Zr-8 Sn in weight percent, that this group of multifunctional titanium alloys possessing nonlinear elastic deformation behavior is tolerant in fatigue notch damage. The results reveal that the alloy has a high strength-to-modulus（σ/E） ratio reaching2% but its fatigue notch sensitivity（q） is low, which decreases linearly from 0.45 to 0.25 as stress concentration factor increases from 2 to 4. This exceeds significantly the typical relationship between σ/E and q of other metallic materials exhibiting linear elasticity. Furthermore, fatigue damage is characterized by an extremely deflected mountain-shape fracture surface, resulting in much longer and more tortuous crack growth path as compared to these linear elastic materials. The above phenomena can be explained by the nonlinear elasticity and its induced stress relief at the notch root in an adaptive manner of higher stress stronger relief. This finding provides a new strategy to balance high strength and good damage tolerance property of metallic materials.展开更多
The optimized stress rupture properties of IN718 are of great interest to the aerospace industry,particularly in the presence of a notch.The deformation mechanisms for the stress rupture properties of IN718 after diff...The optimized stress rupture properties of IN718 are of great interest to the aerospace industry,particularly in the presence of a notch.The deformation mechanisms for the stress rupture properties of IN718 after different heat treatments,using electron back-scattered diffraction(EBSD)as an important tool,were investigated.The notch sensitivity of IN718 was closely associated with the distribution of theδphase.When the area fraction(A(f))of theδphase was less than 0.56%,the sample failed at the notch;while when A(f)≥2.98%,the notch sensitivity disappeared,and failure occurred on the smooth gauge.Heterogeneous deformation with strain concentrated at the grain boundaries was observed for the notch-and smooth-gauge-failed samples through EBSD analysis.Although intergranular cracking was detected in both cases,the failure mechanisms were different.Grain boundary sliding was the dominant failure mechanism for the notch-failed samples,whereas microvoid coalescence was the dominant failure mechanism for the smooth-gauge-failed samples.展开更多
Effects of surface condition on fatigue properties of a medium-strength γ-TiAl alloy Ti-45Al-5Nb-lW（at%） were investigated.It is found that the maximum stresses of fatigue samples are lower than the yield stresses ...Effects of surface condition on fatigue properties of a medium-strength γ-TiAl alloy Ti-45Al-5Nb-lW（at%） were investigated.It is found that the maximum stresses of fatigue samples are lower than the yield stresses of the medium-strength γ-TiAl alloy.Meanwhile,the local plastic deformation is unconspicuous to occur at the crack tip.In this case,the fatigue strength is mainly decided by surface conditions of maximum-stressed surface,but compressive stress and deformation especially resulted from shot peening play an important role in the improvement of the condition fatigue strength.The affecting depth of shot peening is about 250 μm.As a result,the relatively weak microstructures and phases become the preferential initiation sites and propagation routes.They are observed to be equiaxed γ grains,B2 ＋ ω grains,and α_2-γ lamellar interface in soft orientations.The existence of V-notch can significantly reduce the fatigue properties of the samples.展开更多
文摘The precipitation of secondary Laves phases and its effect on notch sensitivity are systematically studied in Thermo-Span alloy. The results show that the precipitation peak temperature of secondary Laves phases is 925 ℃. Below 925 ℃, the volume fraction of secondary Laves phases increases with the rise of the temperature, and its morphology changes from granular to thin-film;above 925 ℃, the volume fraction of secondary Laves phases shows an opposite trend to temperature, and its morphology changes from thin-film to granular. A detailed explanation through linear density (ρ) is provided that the influence of secondary Laves phases at the grain boundaries (GBs) on notch sensitivity depends on the coupling competition effect of their size, quantity, and morphology. Notably, the granular Laves phases are more beneficial to improving the notch sensitivity of the alloy compared with thin-film Laves phases. Granular secondary Laves phases can promote the formation of γ′ phases depletion zone to improve the ability of GBs to accommodate high strain localization, and effectively inhibit the crack initiation and propagation.
基金Funded by the Program for New Century Excellent Talents in University of China (No.NCET-06-0879)the National Natural Science Foundation of China (NSFC) (No.50971102)+2 种基金NPU Foundation for Fundamental Research(No.NPU-FFR-JC200808)the Fund of the State Key Laboratory of Solidification Processing (NPU) (Nos.16-TZ-2007 and 39-QZ-2009)supported by the Program of Introducing Talents of Discipline to Universities (No.08040)
文摘Inconel 718 superalloys deposited by laser solid forming （LSF） were heat treated with solution treatment,intermediate heat treatment （IHT） and two-stage aging treatment in sequence （SITA heat treatment）.The effect of IHT temperature on microstructure,tensile property and notch sensitivity of LSFed Inconel 718 superalloy at 500 ℃ were investigated.As-deposited columnar grains have transformed to equiaxed grains and the grains were refined due to the recrystallization during the SITA heat treatment.It is found that the size and amount of δ phase dispersed at grain boundaries decreased with the increasing of IHT temperature,and δ phase disappeared when the IHT temperature reached 1 020 ℃.The ultimate tensile strength （UTS） and yield strength （YS） of smooth samples increased to a maximum when the IHT temperature reached 980 ℃ and then decreased slightly to a minimum when the IHT temperature was 1 000 ℃,and followed by slight increasing again till the IHT temperature reached 1 020 ℃,resulted from the competition of precipitation strengthening effect of γ″ and γ＇ phase and the grain boundary weakening effect caused by the gradual disappearance of δ phase with increasing the IHT temperature.The notch sensitivity factor （qe） decreased but still greater than 1 as the IHT temperature increased,which is attributed to the decrease of the size and amount of δ precipitation.
基金supported by the National Key Research and Development Program of China (2016YFC1102601 and 2017YFC1104901)the National Natural Science Foundation of China (51571190 and 51631007)the Key Research Program of Frontier Sciences of Chinese Academy of Sciences (QYZDJ-SSW-JSC031)
文摘It is well known that metallic materials exhibit worse fatigue damage tolerance as they behave stronger in strength and softer in modulus. This raises concern on the long term safety of the recently developed biomechanical compatible titanium alloys with high strength and low modulus. Here we demonstrate via a model alloy, Ti-24 Nb-4 Zr-8 Sn in weight percent, that this group of multifunctional titanium alloys possessing nonlinear elastic deformation behavior is tolerant in fatigue notch damage. The results reveal that the alloy has a high strength-to-modulus（σ/E） ratio reaching2% but its fatigue notch sensitivity（q） is low, which decreases linearly from 0.45 to 0.25 as stress concentration factor increases from 2 to 4. This exceeds significantly the typical relationship between σ/E and q of other metallic materials exhibiting linear elasticity. Furthermore, fatigue damage is characterized by an extremely deflected mountain-shape fracture surface, resulting in much longer and more tortuous crack growth path as compared to these linear elastic materials. The above phenomena can be explained by the nonlinear elasticity and its induced stress relief at the notch root in an adaptive manner of higher stress stronger relief. This finding provides a new strategy to balance high strength and good damage tolerance property of metallic materials.
基金financial support from Taiyuan Iron&Steel(Group)Co.,Ltd.(TISCO,Grant No.KA22TAEC035)Baoshan Iron&Steel Co.,Ltd.(Baosteel,Grant No.BGTAECX0).
文摘The optimized stress rupture properties of IN718 are of great interest to the aerospace industry,particularly in the presence of a notch.The deformation mechanisms for the stress rupture properties of IN718 after different heat treatments,using electron back-scattered diffraction(EBSD)as an important tool,were investigated.The notch sensitivity of IN718 was closely associated with the distribution of theδphase.When the area fraction(A(f))of theδphase was less than 0.56%,the sample failed at the notch;while when A(f)≥2.98%,the notch sensitivity disappeared,and failure occurred on the smooth gauge.Heterogeneous deformation with strain concentrated at the grain boundaries was observed for the notch-and smooth-gauge-failed samples through EBSD analysis.Although intergranular cracking was detected in both cases,the failure mechanisms were different.Grain boundary sliding was the dominant failure mechanism for the notch-failed samples,whereas microvoid coalescence was the dominant failure mechanism for the smooth-gauge-failed samples.
基金financially supported by the National Natural Science Foundation of China(Nos.50971106 and 50211141)the National Higher-Education Institution General Research and Development Fund(No.2682014CX005)
文摘Effects of surface condition on fatigue properties of a medium-strength γ-TiAl alloy Ti-45Al-5Nb-lW（at%） were investigated.It is found that the maximum stresses of fatigue samples are lower than the yield stresses of the medium-strength γ-TiAl alloy.Meanwhile,the local plastic deformation is unconspicuous to occur at the crack tip.In this case,the fatigue strength is mainly decided by surface conditions of maximum-stressed surface,but compressive stress and deformation especially resulted from shot peening play an important role in the improvement of the condition fatigue strength.The affecting depth of shot peening is about 250 μm.As a result,the relatively weak microstructures and phases become the preferential initiation sites and propagation routes.They are observed to be equiaxed γ grains,B2 ＋ ω grains,and α_2-γ lamellar interface in soft orientations.The existence of V-notch can significantly reduce the fatigue properties of the samples.
