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树脂催化草酸二乙酯水解动力学 被引量:1
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作者 徐艳 杨广存 +2 位作者 李振花 赵玉军 马新宾 《化学工业与工程》 CAS CSCD 2017年第1期19-24,共6页
针对Amberlyst-15树脂为催化剂的草酸二乙酯水解过程进行了研究,考察了催化剂用量、水酯比及温度对反应的影响。结果表明Amberlyst-15的加入能明显提高水解速率。草酸二乙酯水解反应为连串反应,草酸单乙酯为中间产物。基于树脂催化反应... 针对Amberlyst-15树脂为催化剂的草酸二乙酯水解过程进行了研究,考察了催化剂用量、水酯比及温度对反应的影响。结果表明Amberlyst-15的加入能明显提高水解速率。草酸二乙酯水解反应为连串反应,草酸单乙酯为中间产物。基于树脂催化反应特点提出了包含离子交换树脂催化作用和水解产生的草酸的催化作用在内的动力学模型。通过实验数据的回归获得动力学参数,模型计算与实验数据的平均相对偏差<0.06,表明该模型适用于草酸二乙酯树脂催化水解动力学规律的描述。 展开更多
关键词 水解动力学 草酸二乙酯 草酸 草酸单乙酯 离子交换树脂
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剖宫产术后产妇早期下床活动情况及影响因素 被引量:15
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作者 黄海燕 赵雨君 +2 位作者 顾宏梅 李婷婷 徐旭娟 《循证护理》 2017年第6期625-627,共3页
[目的]分析剖宫产术后产妇早期下床活动情况及其影响因素。[方法]自制调查量表,调查分析2015年3月—2016年3月行剖宫产手术的100例产妇的相关资料。[结果]早期下床活动时,71%的产妇最担心疼痛,28%产妇最担心切口裂开;28%的产妇最希望得... [目的]分析剖宫产术后产妇早期下床活动情况及其影响因素。[方法]自制调查量表,调查分析2015年3月—2016年3月行剖宫产手术的100例产妇的相关资料。[结果]早期下床活动时,71%的产妇最担心疼痛,28%产妇最担心切口裂开;28%的产妇最希望得到有关下床活动的健康教育,56%的产妇最希望护理人员能协助其下床活动。躯体疲劳是剖宫产术后早期下床活动的主要影响因素。[结论]产科医护人员应重视产后躯体疲劳的管理,合理安排剖宫产术后产妇的活动计划,加强与产妇的沟通,提供书面材料及必要的示范和协助,促进其康复。 展开更多
关键词 剖宫产 早日下床活动 影响因素 疲劳
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Technology for Coking of Heavy Crude Oil with High Acid Number 被引量:4
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作者 JiangWen zhaoyujun +3 位作者 ChengGang LiChao ShenHaiping CuiLong 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2005年第1期29-35,共7页
Sudan Khartoum Refinery Co. has selected a unique route featuring delayed coking of crude in connection with the highly sour and high-calcium heavy crude extracted from Sudanese oil block No. 6.The crude oil after pre... Sudan Khartoum Refinery Co. has selected a unique route featuring delayed coking of crude in connection with the highly sour and high-calcium heavy crude extracted from Sudanese oil block No. 6.The crude oil after pretreatment for calcium removal is subjected to coking for removal of acids and metals with the coker products being further processed. The crude oil extracted from Sudanese oil block No. 6contains as high as 13 mg KOH/g of crude in addition to a calcium content of 1600 ppm. This article makes an analysis on problems related with the operation of commercial delayed coking unit for processing of highly sour crude and bring forth measures to solve these problems. The liquid yield resulted from coking of crude oil can reach 82m%, and the petroleum coke can meet the quality requirement for class 3B petroleum coke. 展开更多
关键词 sour crude high calcium content COKING technical analysis PROCESS
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Cloning and enzymology analysis of farnesyl pyrophosphate synthase gene from a superior strain of Artemisia annua L. 被引量:6
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作者 zhaoyujun YEHechun 《Chinese Science Bulletin》 SCIE EI CAS 2003年第1期63-67,共5页
A cDNA(af1) encoding farnesyl pyrophosphate synthase AaFPS1 (FPS, EC2.5.1.1/EC2.5.1.10) from a high yield Artemisia annua strain 025 has been cloned from its cDNA library. Sequence analysis showed that the cDNA en-cod... A cDNA(af1) encoding farnesyl pyrophosphate synthase AaFPS1 (FPS, EC2.5.1.1/EC2.5.1.10) from a high yield Artemisia annua strain 025 has been cloned from its cDNA library. Sequence analysis showed that the cDNA en-coded a protein of 343 amino acid (aa) residues with mo-lecular weight of 39 kD. Deduced aa sequence of the cDNA was similar to FPS from other plants, yeast and mammals, containing 5 conserved domains found in both prenyl trans-ferase and polyprenyl synthase. The expression of the cDNA in Escherichia coli showed measurable specific activity of FPS in vitro. The enzyme was purified by ion exchange chromatography and its kinetics was measured. These re-sults would further promote the molecular regulation of ar-temisinin biosynthesis. 展开更多
关键词 黄花蒿 法尼基焦磷酸合成酶 基因克隆 酶学分析 青蒿素
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