Carbon nanosheet films were deposited on A1 substrates by using plasma assisted chemical vapor deposition (PACVD) technique. And after being peeled off from A1 substrates, carbon nanosheet powders (CNSPs) were obt...Carbon nanosheet films were deposited on A1 substrates by using plasma assisted chemical vapor deposition (PACVD) technique. And after being peeled off from A1 substrates, carbon nanosheet powders (CNSPs) were obtained. In Raman spectrum of carbon film, there was a strong and broadened peak at about 1,580 cm^-1, indicating a carbon diamond-like film. Atomic force microscope image showed that the carbon diamond-like film had a grain size less than 100 nm, and its surface roughness Ra was 17.95 nm in an area of 5×5 μm^2. The CNSPs were irregular sheets with curly edges and a length of several micrometers to several hundreds of micrometers. The BET surface area of CNSPs was 6.66 m^2/g with no micro-pore present, which was confirmed by N2 adsorption-desorption characterization. In the adsorption testing, when the relative pressure p/po was higher than 0.3, the adsorption behavior did not follow the Langmuir equation. The addition of CNSPs to carbon black (catalyst support) could improve hydrodesulfurization performance of carbon supported Ni-W catalysts for diesel oil.展开更多
An experimental investigation of the saturation ion current densities (Jions) in hydrogen inductively coupled plasma (ICP) produced by a large-power (2-32 kW) radio frequency (RF) generator is reported, then s...An experimental investigation of the saturation ion current densities (Jions) in hydrogen inductively coupled plasma (ICP) produced by a large-power (2-32 kW) radio frequency (RF) generator is reported, then some reasonable explanations are given out. With the increase of RF power, the experimental results show three stages: in the first stage (2-14 kW), the electron temperature will rise with the increase of RF power in the ICP, thus, the Jions increases continually as the electron temperature rises in the ICP. In the second stage (14 20 kW), as some H- ions lead to the mutual neutralization (MN), the slope of Jio^s variation firstly decreases then increases. In the third stage (20-32 kW), both the electronic detachment (ED) and the associative detachment (AD) in the ICP result in the destruction of H- ions, therefore, the increased amplitude of the Jions in the third stage is weaker than the one in the first stage. In addition, with the equivalent transformer model, we successfully Explain that the Jions at different radial locations in ICP has the same rule. Finally, it is found that the Jions has nothing to do with the outer/inner puffing gas pressure ratio, which is attributed to the high-speed movement of hydrogen molecules.展开更多
An electron cyclotron resonance heating experiment has been performed by using a gyrotron system for the fundamental and second harmonic resonance heating on CT-6B tokamak.Obvious changes are observed in soft X-ray ra...An electron cyclotron resonance heating experiment has been performed by using a gyrotron system for the fundamental and second harmonic resonance heating on CT-6B tokamak.Obvious changes are observed in soft X-ray radiations,electron cyclotron emission,displacement of plasma column,impurity line radiations,and bremsstrahlung radiation when heating pulse is injected,indicating an increase of the plasma electron temperature.展开更多
基金the Venture Fund of PetroChina Company Limted (050511-3-4)
文摘Carbon nanosheet films were deposited on A1 substrates by using plasma assisted chemical vapor deposition (PACVD) technique. And after being peeled off from A1 substrates, carbon nanosheet powders (CNSPs) were obtained. In Raman spectrum of carbon film, there was a strong and broadened peak at about 1,580 cm^-1, indicating a carbon diamond-like film. Atomic force microscope image showed that the carbon diamond-like film had a grain size less than 100 nm, and its surface roughness Ra was 17.95 nm in an area of 5×5 μm^2. The CNSPs were irregular sheets with curly edges and a length of several micrometers to several hundreds of micrometers. The BET surface area of CNSPs was 6.66 m^2/g with no micro-pore present, which was confirmed by N2 adsorption-desorption characterization. In the adsorption testing, when the relative pressure p/po was higher than 0.3, the adsorption behavior did not follow the Langmuir equation. The addition of CNSPs to carbon black (catalyst support) could improve hydrodesulfurization performance of carbon supported Ni-W catalysts for diesel oil.
基金supported by the National Magnetic Confinement Fusion Science Program of China(Nos.2011GB108011 and 2010GB103001)the Major International(Regional)Project Cooperation and Exchanges of China(No.11320101005)the Startup Fund from Fuzhou University(No.510071)
文摘An experimental investigation of the saturation ion current densities (Jions) in hydrogen inductively coupled plasma (ICP) produced by a large-power (2-32 kW) radio frequency (RF) generator is reported, then some reasonable explanations are given out. With the increase of RF power, the experimental results show three stages: in the first stage (2-14 kW), the electron temperature will rise with the increase of RF power in the ICP, thus, the Jions increases continually as the electron temperature rises in the ICP. In the second stage (14 20 kW), as some H- ions lead to the mutual neutralization (MN), the slope of Jio^s variation firstly decreases then increases. In the third stage (20-32 kW), both the electronic detachment (ED) and the associative detachment (AD) in the ICP result in the destruction of H- ions, therefore, the increased amplitude of the Jions in the third stage is weaker than the one in the first stage. In addition, with the equivalent transformer model, we successfully Explain that the Jions at different radial locations in ICP has the same rule. Finally, it is found that the Jions has nothing to do with the outer/inner puffing gas pressure ratio, which is attributed to the high-speed movement of hydrogen molecules.
文摘An electron cyclotron resonance heating experiment has been performed by using a gyrotron system for the fundamental and second harmonic resonance heating on CT-6B tokamak.Obvious changes are observed in soft X-ray radiations,electron cyclotron emission,displacement of plasma column,impurity line radiations,and bremsstrahlung radiation when heating pulse is injected,indicating an increase of the plasma electron temperature.